Patents by Inventor Shiro Tsukamoto

Shiro Tsukamoto has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).

  • Patent number: 8728255
    Abstract: Provided is a pot-shaped copper sputtering target manufactured with die forging, wherein the Vickers hardness Hv at all locations of the inner surface of the pot-shaped target is 70 or greater. With this pot-shaped copper sputtering target, the average crystal grain size in the target structure is 65 ?m or less. Further, the inner surface of the pot-shaped target comprises crystalline orientations of (220), (111), (200), (311) obtained by X-ray diffraction, and the crystalline orientation of the face subject to erosion of the pot-shaped target is of a (220) primary orientation. An object of the present invention is to obtain a manufacturing method of a high quality sputtering target by improving and devising the forging process and heat treatment process to make the crystal grain size refined and uniform, and to obtain a high-quality sputtering target.
    Type: Grant
    Filed: February 8, 2006
    Date of Patent: May 20, 2014
    Assignee: JX Nippon Mining & Metals Corporation
    Inventors: Atsushi Fukushima, Shiro Tsukamoto
  • Patent number: 8663440
    Abstract: The object of this invention is to provide a high quality titanium target for sputtering capable of reducing the impurities that cause generation of particles and abnormal discharge, which is free from fractures and cracks during high power sputtering (high rate sputtering), and capable of stabilizing the sputtering properties and effectively suppressing the generation of particles upon deposition. This invention is able to solve foregoing problems using a high purity titanium target for sputtering containing, as additive components, 3 to 10 mass ppm of S and 0.5 to 3 mass ppm of Si, and in which the purity of the target excluding additive components and gas components is 99.995 mass percent or higher.
    Type: Grant
    Filed: September 28, 2010
    Date of Patent: March 4, 2014
    Assignee: JX Nippon Mining & Metals Corporation
    Inventors: Shiro Tsukamoto, Tomio Otsuki
  • Publication number: 20140027277
    Abstract: A high-purity titanium target for sputtering, which contains, as additive components, one or more elements selected from Al, Si, S, Cl, Cr, Fe, Ni, As, Zr, Sn, Sb, B, and La in a total amount of 3 to 100 mass ppm, and of which the purity excluding additive components and gas components is 99.99 mass % or higher. An object of this invention is to provide a high-quality titanium target for sputtering, which is free from fractures and cracks during high-power sputtering (high-rate sputtering) and capable of stabilizing the sputtering characteristics.
    Type: Application
    Filed: February 3, 2012
    Publication date: January 30, 2014
    Applicant: JX NIPPON MINING & METALS CORPORATION
    Inventors: Nobuhito Makino, Takeo Okabe, Shiro Tsukamoto
  • Publication number: 20130220805
    Abstract: Provided is a sputtering target-backing plate assembly wherein a Cu—Cr alloy backing plate is bonded to a Ti target via a layer of a strain absorbing material placed at an interface between the Ti target and the Cu—Cr alloy backing plate. In particular, the present invention relates to a sputtering target-backing plate assembly and a production method thereof, the assembly being capable of absorbing strain at the interface between the target and the backing plate in order to prevent deformation (displacement) during sputtering. An object of the present invention is to solve a problem inherent to Titanium (Ti) and a problem in selecting a backing plate compatible with it.
    Type: Application
    Filed: October 25, 2011
    Publication date: August 29, 2013
    Applicant: JX NIPPON MINING & METALS CORPORATION
    Inventors: Shiro Tsukamoto, Kazumasa Ohashi
  • Publication number: 20130186753
    Abstract: Provided is a titanium target for sputtering having a Shore hardness Hs of 20 or more and a basal plane orientation ratio of 70% or less. In the titanium target for sputtering, the purity of titanium is 99.995 mass % or more, excluding gas components. It is an object of the present invention to provide a high-quality titanium target for sputtering, in which impurities are reduced, and which can prevent occurrence of cracking or breaking in high-power sputtering (high-rate sputtering), stabilize sputtering characteristics, and effectively suppress occurrence of particles during formation of a film.
    Type: Application
    Filed: October 24, 2011
    Publication date: July 25, 2013
    Applicant: JX NIPPON MINING & METALS CORPORATION
    Inventors: Shiro Tsukamoto, Nobuhito Makino, Hideaki Fukuyo
  • Publication number: 20120318668
    Abstract: Provided is a tantalum coil for sputtering disposed between a substrate and a sputtering target, wherein the tantalum coil has irregularities so that the surface roughness Rz of the tantalum coil is 150 ?m or more and the number of threads is 15 to 30 TPI (Threads per inch) in a transverse direction and 10 to 30 TPI in a vertical direction. An object of the present invention is to take measures to prevent the sputtered grains accumulated on the surface of a tantalum coil from flaking so as to prevent the generation of particles and arcing that is caused by the flaking of the sputtered grains accumulated on the surface of the coil disposed between a substrate and a sputtering target, and the adhesion of the scattered flakes onto the substrate surface; and thereby to provide a technology of improving the quality and productivity of electronic components and stably providing semiconductor elements and devices.
    Type: Application
    Filed: March 14, 2011
    Publication date: December 20, 2012
    Applicant: JX NIPPON MINING & METALS CORPORATION
    Inventor: Shiro Tsukamoto
  • Publication number: 20120255859
    Abstract: An assembly of a gadolinium target and a titanium backing plate, wherein the gadolinium target-titanium backing plate assembly has a solid-phase diffusion-bonded interface at a bonding interface between the gadolinium target and the titanium backing plate. An object of the present invention is to discover a backing plate that is suitable for the gadolinium sputtering target, explore the optimal bonding conditions, improve the deposition rate, stabilize the sputtering process, and prevent the occurrence of warpage and separation of the target material and the backing plate by increasing the bonding strength between the target material and the backing plate, as well as inhibit the generation of particles during sputtering.
    Type: Application
    Filed: December 21, 2010
    Publication date: October 11, 2012
    Applicant: JX NIPPON MINING & METALS CORPORATION
    Inventor: Shiro Tsukamoto
  • Patent number: 8183073
    Abstract: The method of manufacturing the semiconductor device comprises the step of forming quantum dots 16 on a base layer 10 by self-assembled growth; the step of irradiating Sb or GaSb to the surface of the base layer 10 before or in the step of forming quantum dots 16; the step of etching the surfaces of the quantum dots 16 with an As raw material gas to thereby remove an InSb layer 18 containing Sb deposited on the surfaces of the quantum dots 16; and growing a capping layer 22 on the quantum dots 16 with the InSb layer 18 removed.
    Type: Grant
    Filed: December 16, 2010
    Date of Patent: May 22, 2012
    Assignees: Fujitsu Limited, The University of Tokyo
    Inventors: Yasuhiko Arakawa, Denis Guimard, Shiro Tsukamoto, Hiroji Ebe, Mitsuru Sugawara
  • Publication number: 20120073964
    Abstract: The object of this invention is to provide a high quality titanium target for sputtering capable of reducing the impurities that cause generation of particles and abnormal discharge, which is free from fractures and cracks during high power sputtering (high rate sputtering), and capable of stabilizing the sputtering properties and effectively suppressing the generation of particles upon deposition. This invention is able to solve foregoing problems using a high purity titanium target for sputtering containing, as additive components, 3 to 10 mass ppm of S and 0.5 to 3 mass ppm of Si, and in which the purity of the target excluding additive components and gas components is 99.995 mass percent or higher.
    Type: Application
    Filed: September 28, 2010
    Publication date: March 29, 2012
    Applicant: JX NIPPON MINING & METALS CORPORATION
    Inventors: Shiro Tsukamoto, Tomio Otsuki
  • Publication number: 20110308940
    Abstract: Provided are a lanthanum target for sputtering which has a recrystallized structure with an average crystal grain size of 100 ?m or less and has no spotty macro patterns on the surface; and a method of producing a lanthanum target for sputtering, wherein lanthanum is melted and cast to produce an ingot, the ingot is subject to knead forging at a temperature of 300 to 500° C. and subsequently subject to hot upset forging to form the shape into a rough target shape, and this is additionally subject to machining to obtain a target. This invention aims to offer technology for efficiently and stably providing a lanthanum target for sputtering which has no spotty macro patterns on the surface, and a method of producing the same.
    Type: Application
    Filed: March 17, 2010
    Publication date: December 22, 2011
    Applicant: JX NIPPON MINING & METALS CORPORATION
    Inventors: Shiro Tsukamoto, Tomio Otsuki
  • Publication number: 20110290644
    Abstract: Provided are a lanthanum target for sputtering which has a Vickers hardness of 60 or more and no spotty macro patterns on the surface, and a method of producing a lanthanum target for sputtering, wherein lanthanum is melted and cast to produce an ingot, the ingot is subject to knead forging at a temperature of 300 to 500° C. and subsequently subject to upset forging at 300 to 500° C. to form the shape into a rough target shape, and this is additionally subject to machining to obtain a target. This invention aims to offer technology for efficiently and stably providing a lanthanum target for sputtering that has no spotty macro patterns on the surface, and a method of producing the same.
    Type: Application
    Filed: March 17, 2010
    Publication date: December 1, 2011
    Applicant: JX NIPPON MINING & METALS CORPORATION
    Inventors: Shiro Tsukamoto, Tomio Otsuki
  • Publication number: 20110134950
    Abstract: The method of manufacturing the semiconductor device comprises the step of forming quantum dots 16 on a base layer 10 by self-assembled growth; the step of irradiating Sb or GaSb to the surface of the base layer 10 before or in the step of forming quantum dots 16; the step of etching the surfaces of the quantum dots 16 with an As raw material gas to thereby remove an InSb layer 18 containing Sb deposited on the surfaces of the quantum dots 16; and growing a capping layer 22 on the quantum dots 16 with the InSb layer 18 removed.
    Type: Application
    Filed: December 16, 2010
    Publication date: June 9, 2011
    Applicants: FUJITSU LIMITED, THE UNIVERSITY OF TOKYO
    Inventors: Yasuhiko Arakawa, Denis Guimard, Shiro Tsukamoto, Hiroji Ebe, Mitsuru Sugawara
  • Patent number: 7951275
    Abstract: Provided is a hollow cathode sputtering target comprising an inner bottom face having a surface roughness of Ra?1.0 ?m, and preferably Ra?0.5 ?m. This hollow cathode sputtering target has superior sputter film evenness (uniformity), generates few arcing and particles, is capable of suppressing the peeling of the redeposited film on the bottom face, and has superior deposition characteristics.
    Type: Grant
    Filed: August 24, 2004
    Date of Patent: May 31, 2011
    Assignee: JX Nippon Mining & Metals Corporation
    Inventor: Shiro Tsukamoto
  • Patent number: 7892871
    Abstract: The method of manufacturing the semiconductor device comprises the step of forming quantum dots 16 on a base layer 10 by self-assembled growth; the step of irradiating Sb or GaSb to the surface of the base layer 10 before or in the step of forming quantum dots 16; the step of etching the surfaces of the quantum dots 16 with an As raw material gas to thereby remove an InSb layer 18 containing Sb deposited on the surfaces of the quantum dots 16; and growing a capping layer 22 on the quantum dots 16 with the InSb layer 18 removed.
    Type: Grant
    Filed: May 15, 2007
    Date of Patent: February 22, 2011
    Assignees: Fujitsu Limited, The University of Tokyo
    Inventors: Yasuhiko Arakawa, Denis Guimard, Shiro Tsukamoto, Hiroji Ebe, Mitsuru Sugawara
  • Publication number: 20100044223
    Abstract: Provided is a method of producing an ytterbium sputtering target, wherein an ytterbium target material having Vickers hardness (Hv) of the material surface of 15 or more and 40 or less is prepared in advance, and a surface of the ytterbium target material having the foregoing surface hardness is subject to final finish processing by way of machining. With the ytterbium sputtering target, present invention aims to remarkably reduce the irregularities (gouges) on the target surface after the final finish processing of the target material, and to inhibit the generation of particles during sputtering.
    Type: Application
    Filed: February 5, 2009
    Publication date: February 25, 2010
    Applicant: NIPPON MINING & METALS CO., LTD.
    Inventor: Shiro Tsukamoto
  • Publication number: 20090090621
    Abstract: Technology for efficiently and stably providing an erbium sputtering target with low generation of particles during sputtering and capable of achieving favorable uniformity of the sputtered film, as well as a method for manufacturing such an erbium sputtering target is provided. More specifically, an erbium sputtering target is manufactured by forging and heat treatment, wherein the target purity is 3N5 or higher, and the average grain size of crystals observed in the target structure is 1 to 20 mm. The method of manufacturing an erbium sputtering target includes the steps of subjecting a vacuum-cast ingot having a purity of 3N5 or higher to constant temperature forging within a temperature range of 1100 to 1200° C., subsequently subjecting the forged target material to heat treatment at a temperature of 800 to 1200° C., adjusting the target purity to be 3N5 or higher and the average grain size of the target structure to be 1 to 20 mm, and cutting this out to obtain a target.
    Type: Application
    Filed: June 12, 2008
    Publication date: April 9, 2009
    Applicant: NIPPON MINING & METALS CO., LTD.
    Inventor: Shiro Tsukamoto
  • Publication number: 20090057139
    Abstract: Provided is a pot-shaped copper sputtering target manufactured with die forging, wherein the Vickers hardness Hv at all locations of the inner surface of the pot-shaped target is 70 or greater. With this pot-shaped copper sputtering target, the average crystal grain size in the target structure is 65 ?m or less. Further, the inner surface of the pot-shaped target comprises crystalline orientations of (220), (111), (200), (311) obtained by X-ray diffraction, and the crystalline orientation of the face subject to erosion of the pot-shaped target is of a (220) primary orientation. An object of the present invention is to obtain a manufacturing method of a high quality sputtering target by improving and devising the forging process and heat treatment process to make the crystal grain size refined and uniform, and to obtain a high-quality sputtering target.
    Type: Application
    Filed: February 8, 2006
    Publication date: March 5, 2009
    Applicant: NIPPON MINING & METALS CO., LTD.
    Inventors: Atsushi Fukushima, Shiro Tsukamoto
  • Publication number: 20080073640
    Abstract: The method of manufacturing the semiconductor device comprises the step of forming quantum dots 16 on a base layer 10 by self-assembled growth; the step of irradiating Sb or GaSb to the surface of the base layer 10 before or in the step of forming quantum dots 16; the step of etching the surfaces of the quantum dots 16 with an As raw material gas to thereby remove an InSb layer 18 containing Sb deposited on the surfaces of the quantum dots 16; and growing a capping layer 22 on the quantum dots 16 with the InSb layer 18 removed.
    Type: Application
    Filed: May 15, 2007
    Publication date: March 27, 2008
    Applicants: FUJITSU LIMITED, THE UNIVERSITY OF TOKYO
    Inventors: Yasuhiko Arakawa, Denis Guimard, Shiro Tsukamoto, Hiroji Ebe, Mitsuru Sugawara
  • Publication number: 20070108046
    Abstract: Provided is a hollow cathode sputtering target comprising an inner bottom face having a surface roughness of Ra?1.0 ?m, and preferably Ra?0.5 ?m. This hollow cathode sputtering target has superior sputter film evenness (uniformity), generates few arcing and particles, is capable of suppressing the peeling of the redeposited film on the bottom face, and has superior deposition characteristics.
    Type: Application
    Filed: August 24, 2004
    Publication date: May 17, 2007
    Applicant: Nikko Materials Co., Ltd.
    Inventor: Shiro Tsukamoto
  • Patent number: 7122848
    Abstract: The present invention relates to a substrate having an organic metal complex bonded on the surface thereof, which is prepared by the vapor deposition of a sulfur atom onto a substrate followed by bonding of an organic metal complex such as tetrakis-triphenylphosphine palladium [Pd(PPh3)4] to the surface of the substrate; a substrate bonded transition metal catalyst using said substrate; and a method for the preparation thereof. The above substrate and metal catalyst allow the solution of some problems with respect to the safety and stability of an organic metal complex in its use, the removal of trace amounts of metals in a reaction product, waste water treatment and the like.
    Type: Grant
    Filed: April 11, 2005
    Date of Patent: October 17, 2006
    Assignees: Japan Science and Technology Agency, National Institute for Materials Science
    Inventors: Atsushi Nishida, Mitsuhiro Arisawa, Shiro Tsukamoto, Masahiko Shimoda