Patents by Inventor Stefanie Braun

Stefanie Braun has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).

  • Publication number: 20230069332
    Abstract: The invention relates to a process for starting up a reactor for the continuous production process of polyether carbonate polyols by the addition of alkylene oxide and carbon dioxide in the presence of a DMC catalyst and/or a metal complex catalyst based on the metals cobalt and/or zinc to an H-functional starter substance, in which process: (?) a portion of the H-functional starter substance and/or a suspension medium which has no H-functional groups is mixed in a reactor with a DMC catalyst and/or a metal complex catalyst, the DMC catalyst and/or the metal complex catalyst having a concentration s in the mixture; and (?), after step (?), the H-functional starter substance, alkylene oxide and DMC catalyst and/or a metal complex catalyst are continuously fed into the reactor during the addition process and the resulting reaction mixture is removed from the reactor, and a steady state is achieved.
    Type: Application
    Filed: March 12, 2021
    Publication date: March 2, 2023
    Inventors: Stefanie Braun, Rolf Bachmann, Burkhard Becker, Dirk Becker, Friedhelm Baer, Pascal Bachmann
  • Publication number: 20220411578
    Abstract: A process for continuous production of polyether carbonate polyols by the addition of alkylene oxide and carbon dioxide in the presence of a DMC catalyst or a metal complex catalyst based on the metals cobalt and/or zinc, onto an H-functional starter substance is provided. Wherein (?) the H-functional starter substance, alkylene oxide and catalyst are continuously metered into the reaction during the addition and the resulting reaction mixture is continuously discharged from the reactor, wherein (i) before step (?), a suspension of catalyst in suspension medium and/or H-functional starter substance in the reactor is adjusted to a temperature T1 ranging from 100° C. to 150° C., wherein T1 is at least 10% above a temperature T2 and T2 is a temperature ranging from 50° C. to 135° C., and (ii) from commencement of the addition of alkylene oxide in step (?) the temperature is continuously reduced to the temperature T2.
    Type: Application
    Filed: November 30, 2020
    Publication date: December 29, 2022
    Inventors: Stefanie Braun, Joerg Hofmann, Michael Traving
  • Publication number: 20210277181
    Abstract: The present invention provides a process for removing gaseous constituents dissolved in liquid reaction mixtures in the copolymerization of alkylene oxide and carbon dioxide, characterized in that (?) prior to decompression the liquid reaction mixture has a pressure of 5.0 to 100.0 bar (absolute), wherein the following process stages are performed in the specified sequence: (i) decompression of the reaction mixture by at least 50% of the prevailing pressure, (ii) subsequent droplet separation with first defoaming and (iii) subsequent bubble separation with second defoaming to clarify the liquid phase, wherein the process stages (i) to (iii) are performed one or more times until the resulting reaction mixture has a pressure of 0.01 to <5.00 bar (absolute), and also a process for preparing polyethercarbonate polyols comprising the process stages (i)-(iii).
    Type: Application
    Filed: August 13, 2019
    Publication date: September 9, 2021
    Inventors: Matthias Wohak, Joerg Hofmann, Stefanie Braun, Maria Francisco Casal, Werner Bäcker, Thomas Runowski
  • Publication number: 20210054145
    Abstract: A process for preparing polyethercarbonate polyols by adding alkylene oxide and carbon dioxide onto an H-functional starter substance, wherein, (a) a reactor is initially charged with a portion of H-functional starter substance, optionally together with DMC catalyst and (?) an H-functional starter substance and a suspension medium having no H-functional groups are metered continuously into the reactor during the reaction.
    Type: Application
    Filed: February 13, 2019
    Publication date: February 25, 2021
    Inventors: Joerg Hofmann, Stefanie Braun, Michael Traving
  • Patent number: 10862766
    Abstract: A controller is provided for a Cloud based service handling multiple types of traffic in a telecommunications network, the controller comprising: a first stage configured to automatically model use of Cloud resources allocated to the service for specific workloads of each of a plurality of traffic types, so as provide a variety of models for each traffic type; a second stage configured to automatically reduce the number of and generalise the models so as to provide generalised models for each traffic type applicable to other workloads than the specific loadings; a third stage configured to automatically evaluate accuracy of the generalised models for various combinations of given workloads, in each combination each of the given workloads being of a corresponding traffic type, and to select one of the generalised models dependent upon evaluated accuracy; and a fourth stage configured to control operation of the Cloud resources according to the selected model.
    Type: Grant
    Filed: December 9, 2016
    Date of Patent: December 8, 2020
    Assignee: Alcatel Lucent
    Inventors: Diego Lugones, Jesus Omana Iglesias, Thomas Voith, Stefanie Braun, Jordi Arjona Aroca, Joachim Riemer, Volker Hilt, Jurgen Sienel
  • Patent number: 10836858
    Abstract: The invention relates to a method for producing polyether carbonate polyols by adding alkylene oxides and carbon dioxide to an H-functional starter substance in the presence of a double metal cyanide (DMC) catalyst or in the presence of a metal complex catalyst based on the metals zinc and/or cobalt, wherein (?) alkylene oxide and carbon dioxide are added to an H-functional starter substance in a reactor with a total pressure (absolute) of 5 to 120 bar in the presence of a double metal cyanide catalyst or in the presence of a metal complex catalyst based on the metals zinc and/or cobalt, and a reaction mixture containing the polyether carbonate polyol is obtained, (?) the reaction mixture obtained in step (?) remains in the reactor or is optionally continuously transferred to a downstream reactor at a starting total pressure (absolute) of 5 to 120 bar, the content of free alkylene oxide in the reaction mixture being reduced in the course of a downstream reaction in each case, and the total pressure (absolute)
    Type: Grant
    Filed: June 20, 2017
    Date of Patent: November 17, 2020
    Assignee: Covestro Deutschland AG
    Inventors: Jörg Hofmann, Urs Rauwald, Stefanie Braun, Matthias Wohak, Hartmut Nefzger, Nicole Welsch, Aurel Wolf, Michael Traving, Lars Krueger
  • Publication number: 20190322801
    Abstract: The invention relates to a method for producing polyether carbonate polyols by adding alkylene oxides and carbon dioxide to an H-functional starter substance in the presence of a double metal cyanide (DMC) catalyst or in the presence of a metal complex catalyst based on the metals zinc and/or cobalt, wherein (?) alkylene oxide and carbon dioxide are added to an H-functional starter substance in a reactor with a total pressure (absolute) of 5 to 120 bar in the presence of a double metal cyanide catalyst or in the presence of a metal complex catalyst based on the metals zinc and/or cobalt, and a reaction mixture containing the polyether carbonate polyol is obtained, (?) the reaction mixture obtained in step (?) remains in the reactor or is optionally continuously transferred to a downstream reactor at a starting total pressure (absolute) of 5 to 120 bar, the content of free alkylene oxide in the reaction mixture being reduced in the course of a downstream reaction in each case, and the total pressure (absolute)
    Type: Application
    Filed: June 20, 2017
    Publication date: October 24, 2019
    Inventors: Jörg HOFMANN, Urs RAUWALD, Stefanie BRAUN, Matthias WOHAK, Hartmut NEFZGER, Nicole WELSCH, Aurel WOLF, Michael TRAVING, Lars KRUEGER
  • Patent number: 10421836
    Abstract: The present invention relates to a purifying apparatus for polycarbonate polyols, especially for removal of cyclic alkylene carbonates, comprising an evaporation unit (1) provided with a heater (10) and having an inlet (6) disposed at the top end thereof and a bottoms vessel (11), and a stripping column (2) connected downstream of the evaporation unit (1) and having a top (21) and a bottom (23), wherein a feed (5) for the polycarbonate polyol to be purified opens into the inlet (6) to the evaporation unit (1) and a gas outlet line (12) and a connecting line which opens into the top (21) of the stripping column (2) and is equipped with a pump (18) depart from the evaporation unit (1), and wherein a gas inlet line (24) for an inert gas opens into the bottom (23) of the stripping column (2) and a product line (27) for the purified polycarbonate polyol departs from the bottom (23) of the stripping column (2) and a gas outlet line (25) departs from the top (21) of the stripping column (2).
    Type: Grant
    Filed: June 29, 2015
    Date of Patent: September 24, 2019
    Assignee: COVESTRO DEUTSCHLAND AG
    Inventors: Jörg Hofmann, Stefanie Braun, Kai Laemmerhold, Matthias Wohak, Cyrus Ahmadzade-Youssefi, Jürgen Bausa
  • Publication number: 20190085121
    Abstract: The present invention provides a process for preparing polyether carbonate polyols from H-functional starter substance, alkylene oxide and carbon dioxide in the presence of a DMC catalyst or in the presence of a metal complex catalyst based on the metals zinc and/or cobalt, wherein the carbon dioxide used has a purity of 99.5000% to 99.9449% by volume.
    Type: Application
    Filed: March 16, 2017
    Publication date: March 21, 2019
    Applicant: COVESTRO DEUTSCHLAND AG
    Inventors: Jörg HOFMANN, Stefanie BRAUN, Aurel WOLF
  • Patent number: 10208162
    Abstract: The present invention relates to a method for producing polyether carbonate polyols by addition of one or more alkylene oxides and carbon dioxide to one or more H-functional starter substances in the presence of at least one DMC catalyst, in which the reaction is conducted in a main reactor (8) and a tubular reactor (11, 17) connected as a post reactor downstream thereof, wherein the method is characterized in that at the outlet (13) of the tubular reactor (11, 17) a temperature is set that is at least 10° C. above the temperature in the inside of the main reactor (8). The invention further relates to a device for carrying out said method.
    Type: Grant
    Filed: June 30, 2015
    Date of Patent: February 19, 2019
    Assignee: COVESTRO DEUTSCHLAND AG
    Inventors: Stefanie Braun, Horst Zwick, Matthias Wohak, Jörg Hofmann, Aurel Wolf, Michael Traving, Rolf Bachmann
  • Patent number: 10125217
    Abstract: The invention relates to a process for producing polyether carbonate polyols through an addition reaction of alkylene oxides and carbon dioxide onto one or more H-functional starter substances in the presence of a double metal cyanide catalyst or in the presence of a metal complex catalyst based on the metals zinc and/or cobalt, characterized in that one or more H-functional starter substances containing at least 1000 ppm of component (K) is/are continuously metered into the reactor during the reaction, where component (K) is selected from at least one compound containing a phosphorus-oxygen bond and a phosphorus compound that can form one or more P—O bonds through reaction with OH-functional compounds.
    Type: Grant
    Filed: October 20, 2014
    Date of Patent: November 13, 2018
    Assignee: COVESTRO DEUTSCHLAND AG
    Inventors: Jörg Hofmann, Hans-Georg Pirkl, Kai Laemmerhold, Hartmut Nefzger, Matthias Wohak, Stefanie Braun, Christoph Gürtler, Aurel Wolf, Jens Langanke
  • Publication number: 20180278485
    Abstract: A controller is provided for a Cloud based service handling multiple types of traffic in a telecommunications network, the controller comprising: a first stage configured to automatically model use of Cloud resources allocated to the service for specific workloads of each of a plurality of traffic types, so as provide a variety of models for each traffic type; a second stage configured to automatically reduce the number of and generalise the models so as to provide generalised models for each traffic type applicable to other workloads than the specific loadings; a third stage configured to automatically evaluate accuracy of the generalised models for various combinations of given workloads, in each combination each of the given workloads being of a corresponding traffic type, and to select one of the generalised models dependent upon evaluated accuracy; and a fourth stage configured to control operation of the Cloud resources according to the selected model.
    Type: Application
    Filed: December 9, 2016
    Publication date: September 27, 2018
    Applicant: Alcatel Lucent
    Inventors: Diego Lugones, Jesus Omana Iglesias, Thomas Voiith, Stefanie Braun, Jordi Arjona Aroca, Joachim Riemer, Volker Hilt, Jurgen Sienel
  • Patent number: 10040901
    Abstract: The invention relates to a method for producing polyether carbonate polyols by binding alkylene oxides and carbon dioxide to one or more H-functional starter substance/s in the presence of a double metal cyanide (DMC) catalyst, characterized in that (y) one or more H-functional starter substance/s and DMC catalyst are continuously metered into the reactor during the binding process, and the free alkylene oxide concentration in the reaction mixture amounts to 1.5 to 5.0 wt %, and the obtained reaction mixture is continuously discharged from the reactor.
    Type: Grant
    Filed: June 30, 2015
    Date of Patent: August 7, 2018
    Assignee: COVESTRO DEUTSCHLAND AG
    Inventors: Jörg Hofmann, Stefanie Braun, Kai Laemmerhold, Aurel Wolf, Michael Traving
  • Publication number: 20170233526
    Abstract: A process for the preparation of polyethercarbonate polyols comprises the reaction of a reaction mixture comprising one or more H-functional starter compounds, one or more alkylene oxides, carbon dioxide and a double metal cyanide (DMC) catalyst. The reaction is conducted in a reactor under stirring with a specific power input into the reaction mixture, expressed as Watts per liter (W/L), of ?0.07 to ?5.00.
    Type: Application
    Filed: August 10, 2015
    Publication date: August 17, 2017
    Inventors: Stefanie Braun, Thomas Ernst Müller, Jörg Hofmann, Kabir Rakibul, Walter Leitner, Muhammad Afzal Subhani
  • Publication number: 20170198092
    Abstract: The present invention relates to a method for producing polyether carbonate polyols by addition of one or more alkylene oxides and carbon dioxide to one or more H-functional starter substances in the presence of at least one DMC catalyst, in which the reaction is conducted in a main reactor (8) and a tubular reactor (11, 17) connected as a post reactor downstream thereof, wherein the method is characterized in that at the outlet (13) of the tubular reactor (11, 17) a temperature is set that is at least 10° C. above the temperature in the inside of the main reactor (8). The invention further relates to a device for carrying out said method.
    Type: Application
    Filed: June 30, 2015
    Publication date: July 13, 2017
    Inventors: Stefanie Braun, Horst Zwick, Matthias Wohak, Jörg Hofmann, Aurel Wolf, Michael Traving, Rolf Bachmann
  • Patent number: 9676905
    Abstract: The invention relates to a method for producing polyether carbonate polyols by attaching alkylene oxides and carbon dioxide to one or more H-functional starters in the presence of a double-metal cyanide catalyst, characterized in that (alpha) a suspending agent which contains no H-functional groups is provided in a reactor, (ss) optionally, a moiety of alkylene oxide is added to the mixture from step (alpha) at temperatures of 90 to 150 DEG C., and the addition of the alkylene oxide compound is then interrupted; and (gamma) one or more H-functional starters are continuously metered into the reactor during the reaction.
    Type: Grant
    Filed: August 23, 2013
    Date of Patent: June 13, 2017
    Assignee: Covestro Deutschland AG
    Inventors: Thomas Ernst Müller, Christoph Gürtler, Jörg Hofmann, Matthias Wohak, Stefanie Braun, Aurel Wolf, Ilja Peckermann
  • Publication number: 20170152345
    Abstract: The present invention relates to a purifying apparatus for polycarbonate polyols, especially for removal of cyclic alkylene carbonates, comprising an evaporation unit (1) provided with a heater (10) and having an inlet (6) disposed at the top end thereof and a bottoms vessel (11), and a stripping column (2) connected downstream of the evaporation unit (1) and having a top (21) and a bottom (23), wherein a feed (5) for the polycarbonate polyol to be purified opens into the inlet (6) to the evaporation unit (1) and a gas outlet line (12) and a connecting line which opens into the top (21) of the stripping column (2) and is equipped with a pump (18) depart from the evaporation unit (1), and wherein a gas inlet line (24) for an inert gas opens into the bottom (23) of the stripping column (2) and a product line (27) for the purified polycarbonate polyol departs from the bottom (23) of the stripping column (2) and a gas outlet line (25) departs from the top (21) of the stripping column (2).
    Type: Application
    Filed: June 29, 2015
    Publication date: June 1, 2017
    Inventors: Jörg Hofmann, Stefanie Braun, Kai Laemmerhold, Matthias Wohak, Cyrus Ahmadzade-Youssefi, Jürgen Bausa
  • Publication number: 20170137569
    Abstract: The invention relates to a method for producing polyether carbonate polyols by binding alkylene oxides and carbon dioxide to one or more H-functional starter substance/s in the presence of a double metal cyanide (DMC) catalyst, characterized in that (y) one or more H-functional starter substance/s and DMC catalyst are continuously metered into the reactor during the binding process, and the free alkylene oxide concentration in the reaction mixture amounts to 1.5 to 5.0 wt %, and the obtained reaction mixture is continuously discharged from the reactor.
    Type: Application
    Filed: June 30, 2015
    Publication date: May 18, 2017
    Inventors: Jörg Hofmann, Stefanie Braun, Kai Laemmerhold, Aurel Wolf, Michael Traving
  • Publication number: 20160264727
    Abstract: The invention relates to a process for producing polyether carbonate polyols through an addition reaction of alkylene oxides and carbon dioxide onto one or more H-functional starter substances in the presence of a couble metal cyanide catalyst or in the presence of a metal complex catalyst based on the metals zinc and/or cobalt, characterized in that one or more H-functionalstarter substances containing at least 1000 ppm of component (K) is/are continuously metered into the reactor during the reaction, where component (K) is selected from at least one compound containing a phosphorus-oxygen bond and a phosphorus compound that can form one or more P—O bonds through reaction with OH-functional compounds.
    Type: Application
    Filed: October 20, 2014
    Publication date: September 15, 2016
    Inventors: Jöerg Hofmann, Hans-Georg PIRKL, Kai LAEMMERHOLD, Hartmut NEFZGER, Matthias WOHAK, Stefanie BRAUN, Christoph GÜRTLER, Aurel WOLF, Jens LANGANKE
  • Publication number: 20150259475
    Abstract: The invention relates to a method for producing polyether carbonate polyols by attaching alkylene oxides and carbon dioxide to one or more H-functional starters in the presence of a double-metal cyanide catalyst, characterized in that (alpha) a suspending agent which contains no H-functional groups is provided in a reactor, (ss) optionally, a moiety of alkylene oxide is added to the mixture from step (alpha) at temperatures of 90 to 150 DEG C., and the addition of the alkylene oxide compound is then interrupted; and (gamma) one or more H-functional starters are continuously metered into the reactor during the reaction.
    Type: Application
    Filed: August 23, 2013
    Publication date: September 17, 2015
    Inventors: Thomas Ernst Müller, Christoph Gürtler, Jörg Hofmann, Matthias Wohak, Stefanie Braun, Aurel Wolf, Ilja Peckermann