Patents by Inventor Stefano Cicale'

Stefano Cicale' has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).

  • Patent number: 9828649
    Abstract: Process for the production of grain-oriented Fe—Si sheets having excellent magnetic characteristics to be used for construction of electrical devices wherein the thickness of hot rolled strip (_>3.5 mm) and the total cold deformation rate (90-98%) are higher than known processes, and wherein hot rolled strip annealing before cold rolling is not scheduled.
    Type: Grant
    Filed: October 3, 2012
    Date of Patent: November 28, 2017
    Assignee: CENTRO SVILUPPO MATERIALI S.P.A.
    Inventors: Stefano Fortunati, Stefano Cicale′, Giuseppe Abbruzzese
  • Patent number: 9328396
    Abstract: The present invention has as objective a procedure for the oriented-grain magnetic sheet that provides particular operative hot rolling mill conditions of silicon steel slabs, by means which it is possible to highly contain the heterogeneities of hot rolled sheet re-crystallization. The use of these operative conditions permits to reduce the growing tendency of the crystallized grain during the annealing of the sheets at a final thickness that precedes the secondary oriented re-crystallization. Contemporarily, the particular operational conditions of hot rolling mill according to the invention permit a fine precipitation of secondary phases useful to the control of the grain growing, starting from a quantity of sulphur (S) and nitrogen (N) in matrix lower than corresponding provided by the conventional technologies and consequently disposable in metallic solid solution before the rolling after the heating of the slabs at temperature values lower than 1300° C.
    Type: Grant
    Filed: June 25, 2012
    Date of Patent: May 3, 2016
    Assignee: CENTRO SVILUPPO MATERIALI S.P.A.
    Inventors: Giuseppe Abbruzzese, Stefano Cicale, Stefano Fortunati
  • Patent number: 8871035
    Abstract: A process for producing grain oriented magnetic sheets by subjecting a steel slab ?100 mm, containing 2.5-3.5% si, to the following operations: optional first heating, to a temperature T1?1250° C.; first rough hot-rolling at T2 between 900 and 1200° C., the reduction ratio (% Rid) being at least 80% in the absence of a subsequent heating or, in the presence of a subsequent heating to T3?1300° C., at least 60% determined by % Rid=80?(T3?T2)/5; second finishing hot-rolling at T4<1300° C. to a rolled-section thickness of 1.5 3.0 mm; cold-rolling, in one or more stages with optional intermediate annealing and with a cold reduction ratio ?60% applied in the last stage; primary recrystallization annealing, optionally in a decarburizing atmosphere; second recrystallization annealing.
    Type: Grant
    Filed: November 18, 2009
    Date of Patent: October 28, 2014
    Assignee: Centro Sviluppo Materiali S.p.A.
    Inventors: Stefano Fortunati, Giuseppe Abbruzzese, Stefano Cicale′
  • Publication number: 20140311629
    Abstract: Process for the production of grain-oriented Fe—Si sheets having excellent magnetic characteristics to be used for construction of electrical devices wherein the thickness of hot rolled strip (_>3.5 mm) and the total cold deformation rate (90-98%) are higher than known processes, and wherein hot rolled strip annealing before cold rolling is not scheduled.
    Type: Application
    Filed: October 3, 2012
    Publication date: October 23, 2014
    Inventors: Stefano Fortunati, Stefano Cicale', Giuseppe Abbruzzese
  • Publication number: 20130174940
    Abstract: A method for the production of hot-rolled steel strip comprising the following steps: providing a steel slab comprising, in weight percentages: Si: 2.5 to 3.5%, C: 0.05 to 0.1%, Mn: 0:05 to 0.1%, Als: 0.015 to 0.026%, N: 0.0050 to 0.0100%, and further comprising S and/or Se so that S+ (32/79) Se is in an amount of 0.018 to 0.030%, and optionally comprising one or more elements chosen among Sb in an amount of 0.015 to 0.035%, Cu in an amount of 0.08% to 0.25%, Sn in an amount of 0.06% to 0.15%, P in an amount of 0.005% to 0.015%, the balance being iron and unavoidable impurities, reheating said slab to a temperature between 1300° C. and 1430° C., roughing hot-rolling said slab to produce a blank having a thickness below 50 mm, finishing hot-rolling of said blank to produce a hot rolled strip in three rolling passes or more, the temperature of said blank during the first pass being above 1150° C.
    Type: Application
    Filed: March 18, 2011
    Publication date: July 11, 2013
    Inventors: Stefano Cicale, Giuseppe Abbruzzese, Marco Antonio Da Cunha, Helcio De Araujo Quintao, Ronaldo Claret Ribeiro Silva, Angelo Jose De Faria Fonseca
  • Publication number: 20130160897
    Abstract: The present invention has as objective a procedure for the oriented-grain magnetic sheet that provides particular operative hot rolling mill conditions of silicon steel slabs, by means which it is possible to highly contain the heterogeneities of hot rolled sheet re-crystallization. The use of these operative conditions permits to reduce the growing tendency of the crystallized grain during the annealing of the sheets at a final thickness that precedes the secondary oriented re-crystallization. Contemporarily, the particular operational conditions of hot rolling mill according to the invention permit a fine precipitation of secondary phases useful to the control of the grain growing, starting from a quantity of sulphur (S) and nitrogen (N) in matrix lower than corresponding provided by the conventional technologies and consequently disposable in metallic solid solution before the rolling after the heating of the slabs at temperature values lower than 1300° C.
    Type: Application
    Filed: June 25, 2012
    Publication date: June 27, 2013
    Applicant: CENTRO SVILUPPO MATERIALI S.P.A.
    Inventors: Giuseppe ABBRUZZZESE, Stefano Cicale, Stefano Fortunati
  • Patent number: 8277573
    Abstract: A process for the production of a grain oriented magnetic strip, made of steel containing 2.3 to 5.0% of silicon, obtained by producing a hot-rolled sheet containing a distribution of second phases capable of controlling the secondary recrystallization by means of a two-step hot-rolling with an intermediate annealing, and by changing it into the final product.
    Type: Grant
    Filed: April 18, 2008
    Date of Patent: October 2, 2012
    Assignee: Centro Sviluppo Materiali S.p.A.
    Inventors: Giuseppe Abbruzzese, Stefano Cicale', Stefano Fortunati
  • Publication number: 20120018049
    Abstract: Process for the production of grain-oriented magnetic sheets, wherein a slab made of steel having a thickness of ?100 mm, containing Si in the range comprised between 2.5 and 3.5% by weight, is subjected to a thermo-mechanical cycle comprising the following operations:—optional first heating to a temperature T1 no higher than 1250° C.·first rough hot-rolling, in a first rough hot rolling mill, to a temperature T2 comprised between 900 and 1200° C., the reduction ratio (% Rid) applied to the first rough hot-rolling being adjusted so as to be:—of at least 80%, in the absence of a subsequent heating to a temperature T3—determined by the following relationship % Rid=80 (T3?T2)/5, in the presence of a subsequent heating to a temperature T3—optional second heating to a temperature T3 >T2·second finishing hot-rolling, in a second fmishing hot rolling mill, to a temperature T4<T3 to a thickness of the rolled section comprised in the range of 1.5 mm-3.
    Type: Application
    Filed: November 18, 2009
    Publication date: January 26, 2012
    Applicant: CENTRO SVILUPPO MATERIALI S.P.A.
    Inventors: Stefano Fortunati, Giuseppe Abbruzzese, Stefano Cicale
  • Publication number: 20100300583
    Abstract: A process for the production of a grain oriented magnetic strip, made of steel containing 2.3 to 5.0% of silicon, obtained by producing a hot-rolled sheet containing a distribution of second phases capable of controlling the secondary recrystallization by means of a two-step hot-rolling with an intermediate annealing, and by changing it into the final product.
    Type: Application
    Filed: April 18, 2008
    Publication date: December 2, 2010
    Applicant: Centro Sviluppo Materiali S.p.A.
    Inventors: Giuseppe Abbruzzese, Stefano Cicale', Stefano Fortunati
  • Patent number: 7198682
    Abstract: A process for the production of electrical steel strips, in which a strip is directly cast from molten steel and contains alloy elements apt to generate a precipitation of sulphides and/or nitrides apt to inhibit the grain growth. The strip is hot rolled in-line with the casting operation at a temperature between 1250 and 1000° C., and in which the strip is coiled after hot rolling at a temperature of less than 780° C. if sulphides are utilized, or at a temperature of less than 600° C. if nitrides, or nitrides plus sulphides, are utilized.
    Type: Grant
    Filed: December 17, 2001
    Date of Patent: April 3, 2007
    Assignee: Thyssenkrupp Acciai Speciali Terni S.p.A.
    Inventors: Stefano Cicale′, Stefano Fortunati, Giuseppe Abbruzzese
  • Patent number: 7192492
    Abstract: In the production of electrical steel strips, a special islab-reheating treatment before hot rolling is carried out so that the maximum temperature within the furnace is reached by the slab well before its extraction from the furnace. During the heating stage and performance at the highest temperatures of the thermal cycle, second phase particles are dissolved and segregated elements are distributed in the metallic matrix, while during cooling and temperature equalising steps of the slab in the furnace a controlled amount of small second phases particles are more homogeneously re-precipitated from the metallic matrix. Differently from all the conventional processes for the production of electrical steels, the slab reheating furnace become a site in which it is performed the precipitation of a controlled amount of second phases particles for the necessary grain growth control during the successive process steps.
    Type: Grant
    Filed: August 8, 2001
    Date of Patent: March 20, 2007
    Assignee: Thyssenkrupp Acciai Speciali Terni S.p.A.
    Inventors: Stefano Fortunati, Stefano Cicale′, Claudia Rocchi, Giuseppe Abbruzzese
  • Patent number: 6964711
    Abstract: A process for the production of grain oriented electrical Fe-Si strips in which a Si-containing alloy is directly cast as a strip between 2.5–5.0 mm thick and cold rolled in one stage, or in more stages with intermediate annealing, to a final thickness of between 0.15–1.0 mm. The strip is then continuously annealed to carry out the primary recrystallization and then annealed to carry out the oriented secondary recrystallization. The process further includes that after solidification of the strip, and before its coiling, a phase transformation from Ferrite to Austenite is induced into the metal matrix for a volume fraction between 25–60%, obtained by controlling the alloy composition so that the Austenite fraction is allowed within the stability equilibrium between the two phases. The strip is then deformed by rolling in-line with the casting step to obtain a deformation higher than 20% in the temperature interval 1000–1300° C.
    Type: Grant
    Filed: December 18, 2001
    Date of Patent: November 15, 2005
    Assignee: Thyssenkrupp Acciai Speciali Terni S.p.A.
    Inventors: Stefano Fortunati, Stefano Cicale′, Giuseppe Abbruzzese
  • Publication number: 20050115643
    Abstract: A process for the production of grain oriented electrical Fe—Si strips in which a Si-containing alloy is directly cast as a strip between 2.5-5.0 mm thick and cold rolled in one stage, or in more stages with intermediate annealing, to a final thickness of between 0.15-1.0 mm. The strip is then continuously annealed to carry out the primary recrystallization and then annealed to carry out the oriented secondary recrystallization. The process further includes that after solidification of the strip, and before its coiling, a phase transformation from Ferrite to Austenite is induced into the metal matrix for a volume fraction between 25-60%, obtained by controlling the alloy composition so that the Austenite fraction is allowed within the stability equilibrium between the two phases. The strip is then deformed by rolling in-line with the casting step to obtain a deformation higher than 20% in the temperature interval 1000-1300° C.
    Type: Application
    Filed: December 18, 2001
    Publication date: June 2, 2005
    Inventors: Stefano Fortunati, Stefano Cicale, Giuseppe Abbruzzese
  • Patent number: 6893510
    Abstract: Process for the production of oriented grain electrical steel strips, in which a silicon steel, comprising at least 30 ppm of S, is directly cast as strip 1.5-4.5 mm thick and cold rolled to a final thickness of between 1.0 and 0.15 mm; characterised by the following staged: Cooling and deformation of the solidified strip to obtain a second phases distribution in which 600 cm?1<Iz<1500 cm?1 and Iy=1.9 Fv/r (cm?1), Fv being the volume fraction of second phases stable at temperatures of less than 800° C., and r being the precipitates mean radius, in cm; Hot rolling between solidification and coiling of the strip at a temperature of not less than 750° C., with a reduction ratio of between 15 and 60%; Cold rolling with reduction ratio of 60-92%; Cold rolled strip annealing at 750-1100° C., with increase of the nitrogen content of at least 30 ppm with respect to the initial composition at the strip core, in nitriding atmosphere.
    Type: Grant
    Filed: December 17, 2001
    Date of Patent: May 17, 2005
    Assignee: Thyssenkrupp Acciai Speciali Terni S.p.A.
    Inventors: Stefano Fortunati, Stefano Cicale', Claudia Rocchi, Giuseppe Abbruzzese
  • Publication number: 20050098235
    Abstract: In the production of electrical steel strips, a special islab-reheating treatment before hot rolling is carried out so that the maximum temperature within the furnace is reached by the slab well before its extraction from the furnace. During the heating stage and performance at the highest temperatures of the thermal cycle, second phase particles are dissolved and segregated elements are distributed in the metallic matrix, while during cooling and temperature equalising steps of the slab in the furnace a controlled amount of small second phases particles are more homogeneously re-precipitated from the metallic matrix. Differently from all the conventional processes for the production of electrical steels, the slab reheating furnace become a site in which it is performed the precipitation of a controlled amount of second phases particles for the necessary grain growth control during the successive process steps.
    Type: Application
    Filed: August 8, 2001
    Publication date: May 12, 2005
    Inventors: Stefano Fortunati, Stefano Cicale, Claudia Rocchi, Giuseppe Abbruzzese
  • Publication number: 20040099342
    Abstract: The present invention refers to a process for the production of electrical steel strips, in which a strip directly cast from molten steel and containing alloy elements apt to generate a precipitation of sulphides and/or nitrides apt to inhibit the grain growth, is hot rolled in-line with the casting operation, at a temperature comprised between (1250) and (1000)° C., and in which said strip is coiled after hot rolling at a temperature of less than (780)° C. if sulphides are utilised, or at a temperature of less than (600)° if nitrides, or nitrides plus sulphides, are utilised. A final product is thus obtained having excellent and constant magnetic properties.
    Type: Application
    Filed: November 13, 2003
    Publication date: May 27, 2004
    Inventors: Stefano Cicale, Stefano Fortunati, Giuseppe Abbruzzese
  • Publication number: 20040069377
    Abstract: Process for the production of oriented grain electrical steel strips, in which a silicon steel, comprising at least 30 ppm of S, is directly cast as strip 1.5-4.5 mm thick and cold rolled to a final thickness of between 1.0 and 0.15 mm; characterised by the following staged: Cooling and deformation of the solidified strip to obtain a second phases distribution in which 600 cm−1<Iz<1500 cm−1 and Iy=1.9 Fv/r (cm−1), Fv being the volume fraction of second phases stable at temperatures of less than 800° C., and r being the precipitates mean radius, in cm.; Hot rolling between solidification and coiling of the strip at a temperature of not less than 750° C., with a reduction ratio of between 15 and 60%; Cold rolling with reduction ratio of 60-92%; Cold rolled strip annealing at 750-1100° C., with increase of the nitrogen content of at least 30 ppm with respect to the initial composition at the strip core, in nitriding atmosphere.
    Type: Application
    Filed: November 13, 2003
    Publication date: April 15, 2004
    Inventors: Stefano Fortunati, Stefano Cicale, Claudia Rocchi, Giuseppe Abbruzzese
  • Patent number: 6488784
    Abstract: By forming, after the annealing of the continuously cast body, a limited number of precipitates apt to the control of the grain growth, and utilising a cold rolling reduction ratio of at least 70%, it is possible to obtain in a subsequent step of continuous nitriding the direct formation of nitrides useful for the grain growth control and subsequently, still in a continuous treatment, to at least start the oriented secondary recrystallization.
    Type: Grant
    Filed: November 6, 2000
    Date of Patent: December 3, 2002
    Assignee: Acciai Speciali Terni S.p.A.
    Inventors: Stefano Fortunati, Stefano Cicale′, Giuseppe Abbruzzese
  • Patent number: 6471787
    Abstract: A process for the production of oriented-grain electrical steel sheet with high magnetic characteristics, and more precisely a process in which the slab obtained from continuous casting is continuously nitrided by a reaction between aluminium and nitrogen is described. Amount, size and distribution of precipitates are controlled, enabling a high-temperature continuous heat treatment during which the primary-recrystallization and a high-temperature nitriding are realized.
    Type: Grant
    Filed: June 22, 1999
    Date of Patent: October 29, 2002
    Assignee: Acciai Speciali Terni S.p.A.
    Inventors: Stefano Cicale', Stefano Fortunati, Giuseppe Abbruzzese
  • Patent number: 6406557
    Abstract: During the treatment of electrical steel, a careful combination of heat treatment of the slab with a specific primary recrystallization and nitriding treatment allows for control of the distribution, quantity and dimensions of precipitates in order to obtain a homogeneous precipitation of nitrogen compounds by direct reaction of the absorbed nitrogen with aluminum during the nitriding step.
    Type: Grant
    Filed: June 17, 1999
    Date of Patent: June 18, 2002
    Assignee: Acciai Speciali Terni S.p.A.
    Inventors: Stefano Fortunati, Stefano Cicale′, Giuseppe Abbruzzese, Susanna Matera