Abstract: A process, a process plant and equipment for conversion of a feedstock rich in oxygenates to a hydrocarbon including directing the feedstock in combination with a recycle gas stream to a hydroprocessing step, to provide a two-phase hydroprocessed process stream including at least hydrogen, methane and hydrocarbons, combining a methane lean stream of hydrocarbons being liquid at ambient temperature, with a methane donor stream being either (i) the two-phase hydroprocessed process stream including methane or (ii) a gaseous stream derived from the two-phase hydroprocessed process stream by phase separation, to provide a multiple-phase combined stream, separating the multiple-phase combined stream into at least a hydrogen rich gas stream and a rich liquid hydrocarbon stream, in a desorption step desorbing an amount of methane from the rich liquid hydrocarbon stream, to provide a methane rich gas phase and a liquid product stream of hydrocarbons.

Abstract: A hydrotreatment unit for an oxygenate feedstock is provided, the unit including: a hydrotreatment reactor; a first cooling unit; a high-pressure separator and a low pressure flash unit. The hydrotreatment unit is arranged to feed at least a part of the hydrogen-rich stream from the high-pressure separator to the hydrotreatment reactor; and the hydrotreatment unit is arranged to feed a part of the degassed hydrocarbon-rich stream from said low pressure flash unit as a hydrocarbon recycle stream to the hydrotreatment reactor. Also, a method for hydrotreating an oxygenate feedstock using the hydrotreatment unit.

Abstract: In a method for the hydroprocessing of renewable feeds in a hydroprocessing unit (unit A), comprising the use of sour waste water from the same or another unit (unit B), which is processing feeds containing sulfur and nitrogen, as wash water in unit A, thereby changing the pH of the waste water from unit A to lower the risk of carbonic acid corrosion of corrodible steel parts in unit A, the renewable material in unit A is directed to contact a material that is catalytically active in hydrogenating the renewable material in the presence of hydrogen, and the effluent is combined with the wash water stream which contains hydrogen sulfide and/or ammonia.

Abstract: In a method for the hydroprocessing of renewable feeds in a hydroprocessing unit (unit A), comprising the use of sour waste water from the same or another unit (unit B), which is processing feeds containing sulfur and nitrogen, as wash water in unit A, thereby changing the pH of the waste water from unit A to lower the risk of carbonic acid corrosion of corrodible steel parts in unit A, the renewable material in unit A is directed to contact a material that is catalytically active in hydrogenating the renewable material in the presence of hydrogen, and the effluent is combined with the wash water stream which contains hydrogen sulfide and/or ammonia.

Abstract: A quench zone mixing apparatus that occupies a low vertical height and has an improved mixing efficiency and fluid distribution across the catalyst surface includes a swirl chamber, a rough distribution network, and a distribution apparatus. In the swirl chamber, reactant fluid from a catalyst bed above is thoroughly mixed with a quench fluid by a swirling action. The mixed fluids exit the swirl chamber through an aperture to the rough distribution system where the fluids are radially distributed outward across the vessel to the distribution apparatus. The distribution apparatus includes a plate with a number of bubble caps and associated drip trays that multiply the liquid drip stream from the bubble caps to further symmetrically distribute the fluids across the catalyst surface. Alternatively, deflector baffles may be associated with the bubble caps to provide a wider and more uniform liquid distribution below the plate.

Abstract: A flow distribution device (100) has a vane distributor (111) at least partially disposed within a cartridge (102) and is operationally coupled to a second distributing device (112) that receives output from the vane distributor (111) Especially preferred flow distribution devices (100) are disposed within a vessel containing a contact bed, and may include at least a second vane distributor (112) within the cartridge (102), wherein the vane distributors (111, 112) are preferably swirl-inducing vane distributors (111, 112).

Abstract: A bubble cap (400) has a cap (430) with at least one slot (495) and a riser (420), configured with a skirt height (460) of at least 4 cm, such that 1.5*Skirt Height (cm)+[Slot Length (cm)?Exposed Slot Height (cm)] is greater than or equal to 7.5, and posed such that a liquid fluid and a gas flow co-currently upwardly in a space between the riser (420) and the cap (430).

Abstract: A bubble cap (100) has a riser (120) and a cap (130), separated by a divider (140) that extends to a length at least 50% of a distance measured between the top of the riser (122) and the bottom of the cap (134). In another aspect, the riser (120) and cap (130) cooperate to provide a skirt height (160) of no less than 1.5?. More preferred bubble caps (400) have a relatively high skirt height (460) or long slit length (497), or both. In yet another aspect, flow-redirecting vanes (610) and plates (630) cooperate to provide a rough distribution of fluids to subsequent distribution tray (650).

Abstract: A bubble cap has a riser and a cap, separated by a divider that extends to a length at least 50% of a distance measured between the top of the riser and the bottom of the cap. In another aspect, the riser and cap cooperate to provide a skirt height of no less than 1.5?. More preferred bubble caps have a relatively high skirt height or long slit length, or both. In yet another aspect, flow-redirecting vanes and plates (e.g., mixing chamber floor and splash deck) cooperate to provide a rough distribution of fluids to subsequent distribution tray(s).

Abstract: A quench zone mixing apparatus (16) that occupies a low vertical height and has an improved mixing efficiency and fluid distribution across the catalyst surface includes a swirl chamber (20), a rough distribution network (100), and a distribution apparatus (120). In the swirl chamber (20), reactant fluid from a catalyst bed above is thoroughly mixed with a quench fluid by a swirling action. The mixed fluids exit the swirl chamber (20) through an aperture to the rough distribution system (100) where the fluids are radially distributed outward across the vessel to the distribution apparatus (120). The distribution apparatus (120) includes a plate (122) with a number of bubble caps (130) and associated a drip trace (150) that multiply the liquid drip stream from the bubble caps (130) to further symmetrically distribute the fluids across the catalyst surface. Alternatively, deflector baffles may be associated with the bubble caps (130) to provide a wider and more uniform liquid distribution below the plate (122).

Abstract: A bubble cap (100) has a riser (120) and a cap (130), separated by a divider (140) that extends to a length at least 50% of a distance measured between the top of the riser (122) and the bottom of the cap (134). In another aspect, the riser (120) and cap (130) cooperate to provide a skirt height (160) of no less than 1.5″. More preferred bubble caps (400) have a relatively high skirt height (460) or long slit length (497), or both. In yet another aspect, flow-redirecting vanes (610) and plates (630) cooperate to provide a rough distribution of fluids to subsequent distribution tray (650).

Abstract: The invention is directed to a bubble cap including: a riser having a lower end located within and extending through an aperture in the plate of the distribution apparatus and a top end to define a passageway between the ends; a cap located over the top end of the riser, the cap having a top portion and a downwardly extending skirt portion; at least one spacer located between the riser and the cap to maintain a gap between the top end of the riser and the cap; and a plurality of riser vanes located between the top end of the riser and the top portion of the cap. An annulus (“bubble cap annulus”) is created between the riser and the cap. The riser vanes are preferably flush against the underside of the bubble cap top wall. The riser vanes are spaced from each other to form vane passageways. Preferably, the vane passageways are the only (or sole) means of fluid communication between the bubble cap annulus and the riser passageway.

Abstract: A bubble cap has a cap with at least one, five, or seven slot(s), and a riser, configured with a skirt height of at least 4 cm such that 1.5*Skirt Height (cm)+[Slot Length (cm)−Exposed Slot Height (cm)] 7.5, 15, 22.5, or 30, and posed such that a liquid fluid and a gaseous fluid flow co-currently upwardly in a space between the riser and the cap. In another aspects, flow-redirecting vanes and plates (e.g., mixing chamber floor and splash deck) cooperate to provide a rough distribution of fluids to subsequent distribution tray(s).

Abstract: A quench zone mixing apparatus that occupies a low vertical height and has an improved mixing efficiency and fluid distribution across the catalyst surface includes a swirl chamber, a rough distribution network, and a distribution apparatus. In the swirl chamber, reactant fluid from a catalyst bed above is thoroughly mixed with a quench fluid by a swirling action. The mixed fluids exit the swirl chamber through an aperture to the rough distribution system where the fluids are radially distributed outward across the vessel to the distribution apparatus. The distribution apparatus includes a plate with a number of bubble caps and associated drip trays that multiply the liquid drip stream from the bubble caps to further symmetrically distribute the fluids across the catalyst surface. Alternatively, deflector baffles may be associated with the bubble caps to provide a wider and more uniform liquid distribution below the plate.

Abstract: A quench zone mixing apparatus is supported within a vessel of a reactor by a support structure that includes a concentric hub, which may be formed to act as a torsion tube, and at least a first set of radial beams extending radially outward from the hub and terminating at a support ring that is attached to the reactor vessel wall. In particular, the radial beams comprise a flange that supports the redistribution tray and a web of the beams preferably includes a plurality of openings to allow the passage of fluids across the vessel. In addition, the webs also carry the channels. The radial beams also support the mixing chamber and, in the area between the wall of the mixing chamber and the vessel wall, the radial beams may have a vertical height that slopes downward from the vessel wall to the mixing chamber wall.

Abstract: A quench zone mixing apparatus that occupies a low vertical height and has an improved mixing efficiency and fluid distribution across the catalyst surface includes a swirl chamber, a rough distribution network, and a distribution apparatus. In the swirl chamber, reactant fluid from a catalyst bed above is thoroughly mixed with a quench fluid by a swirling action. The mixed fluids exit the swirl chamber through an aperture to the rough distribution system where the fluids are radially distributed outward across the vessel to the distribution apparatus. The distribution apparatus includes a plate with a number of bubble caps and associated drip trays that multiply the liquid drip stream from the bubble caps to further symmetrically distribute the fluids across the catalyst surface. Alternatively, deflector baffles may be associated with the bubble caps to provide a wider and more uniform liquid distribution below the plate.