Patent number: 9227981
Abstract: The present invention relates to a method of preparation of ?-2,4,6,8,10,12-hexanitro-2,4,6,8,10,12-hexaazaisowurtzitane with reduced impact sensitivity by precipitation of a solution of 2,4,6,8,10,12-hexanitro-2,4,6,8,10,12-hexaazaisowurtzitane in a solvent by an antisolvent, wherein phosphorus(V) oxide is added as a recrystallization promoter to the solution of 2,4,6,8,10,12-hexanitro-2,4,6,8,10,12-hexaazaisowurtzitane in the solvent, the obtained mixture is stirred and filtered, and the filtrate is subsequently precipitated by the addition of the antisolvent.
Type:
Grant
Filed:
October 1, 2012
Date of Patent:
January 5, 2016
Assignee:
UNIVERSITY OF PARDUBICE
Inventors:
Ahmed Ikhlas Mohamed Elbeih, Adela Husarova, Svatopluk Zeman
Publication number: 20140235853
Abstract: The present invention relates to a method of preparation of ?-2,4,6,8,10,12-hexanitro-2,4,6,8,10,12-hexaazaisowurtzitane with reduced impact sensitivity by precipitation of a solution of 2,4,6,8,10,12-hexanitro-2,4,6,8,10,12-hexaazaisowurtzitane in a solvent by an antisolvent, wherein phosphorus(V) oxide is added as a recrystallization promoter to the solution of 2,4,6,8,10,12-hexanitro-2,4,6,8,10,12-hexaazaisowurtzitane in the solvent, the obtained mixture is stirred and filtered, and the filtrate is subsequently precipitated by the addition of the antisolvent.
Type:
Application
Filed:
October 1, 2012
Publication date:
August 21, 2014
Applicant:
UNIVERSITY OF PARDUBICE
Inventors:
Ahmed Ikhlas Mohamed Elbeih, Adela Husarova, Svatopluk Zeman