Patents by Inventor Tadahiro Fukuju

Tadahiro Fukuju has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).

  • Publication number: 20240067529
    Abstract: Provide is a porous spherical silica useful as a polish and as a cosmetic material. The porous spherical silica is such that less impurities are contained therein, the particle size distribution thereof is narrow, the D50 thereof is within a predetermined range, and the pore volume thereof is within a predetermined range, the D50 thereof is 2 to 200 ?m, the D10/D90 thereof is at least 0.3, the pore volume thereof is 0.5 mL/g to 8 mL/g, the arithmetic mean value of the breaking compressive test forces of specimens of ten particles is 1.0×101 to 1.0×102 mN, and the alkali metal content thereof is at most 50 ppm. The porous spherical silica can be produced by forming a W/O emulsion using a fumed silica dispersion as an aqueous phase, and pH-adjusting or heating to gelate this emulsion, and thereafter collecting and drying the resultant.
    Type: Application
    Filed: January 12, 2022
    Publication date: February 29, 2024
    Applicant: TOKUYAMA CORPORATION
    Inventors: Noriko YOSHIMURA, Tadahiro FUKUJU
  • Patent number: 11246931
    Abstract: The present invention relates to an active pharmaceutical ingredient carrier and a production method of the same. The active pharmaceutical ingredient carrier includes silica having a volume of a pore with a pore radius of 1 to 100 nm determined by BJH method of 3.0 to 5.0 ml/g, and a peak of a pore radius of 10 to 50 nm determined by BJH method; and an active pharmaceutical ingredient carried by the silica.
    Type: Grant
    Filed: May 17, 2018
    Date of Patent: February 15, 2022
    Assignee: Tokuyama Corporation
    Inventors: Yoshimi Hironaka, Tadahiro Fukuju, Hiromasa Yamamoto
  • Publication number: 20200147220
    Abstract: The present invention relates to an active pharmaceutical ingredient carrier and a production method of the same. The active pharmaceutical ingredient carrier includes silica having a volume of a pore with a pore radius of 1 to 100 nm determined by BJH method of 3.0 to 5.0 ml/g, and a peak of a pore radius of 10 to 50 nm determined by BJH method; and an active pharmaceutical ingredient carried by the silica.
    Type: Application
    Filed: May 17, 2018
    Publication date: May 14, 2020
    Inventors: Yoshimi Hironaka, Tadahiro Fukuju, Hiromasa Yamamoto
  • Patent number: 9216909
    Abstract: An aerogel with excellent thermal insulation performance, average particle size of 1 to 20 ?m and globular shape; and a method of manufacturing it efficiently, is provided. The aerogel has specific surface area by BET method of 400 to 1000 m2/g; pore volume and peak pore radius by BJH method of 3 to 8 mL/g and 10 to 30 nm, respectively; average particle size and average circularity by image analysis method of 1 to 20 ?m and no less than 0.8, respectively. The method includes the steps of: preparing an aqueous silica sol; dispersing the sol into a hydrophobic solvent, thereby forming a W/O emulsion; causing gelation of the sol, thereby converting the emulsion into a dispersion of a gel; replacing water in the gel with a solvent having a small surface tension; treating the gel with a hydrophobing agent; and removing the solvent used in the solvent replacement.
    Type: Grant
    Filed: October 24, 2011
    Date of Patent: December 22, 2015
    Assignee: TOKUYAMA CORPORATION
    Inventors: Tadahiro Fukuju, Hiroshi Numa, Kazuaki Tabata
  • Patent number: 9199853
    Abstract: The present invention provides a globular-shaped metal oxide powder with excellent thermal insulation performance and reduced bulk density, and a method of manufacture thereof, wherein the metal oxide powder has globular independent particles as the main component, and has BET specific surface area of 400 to 1000 m2/g, BJH pore volume of 2 to 8 mL/g, and oil absorption of no less than 250 mL/100g. The present invention also provides a method for manufacturing the hollow and globular shaped metal oxide powder including the step of forming an O/W/O emulsion.
    Type: Grant
    Filed: April 25, 2012
    Date of Patent: December 1, 2015
    Assignee: TOKUYAMA CORPORATION
    Inventors: Wakana Tomimatsu, Tadahiro Fukuju, Hiroshi Numa
  • Patent number: 8877990
    Abstract: A process of making a chlorinated hydrocarbon through a thermal dehydrochlorination step in which an unsaturated compound represented by the following general formula (2) is obtained by thermally decomposing a saturated compound represented by the following general formula (1). CCl3—CCl2-mHm—CCl3-nHn??(1) CCl2?CCl2-mHm-1—CCl3-nHn??(2) (in the above formulas, m is 1 or 2, and n is an integer of 0 to 3.
    Type: Grant
    Filed: June 17, 2010
    Date of Patent: November 4, 2014
    Assignee: Tokuyama Corporation
    Inventors: Tadahiro Fukuju, Kikuo Yamamoto, Masayuki Moriwaki, Yasutaka Komatsu, Akihiro Saito, Shunsuke Hosaka, Dai Tsunoda, Jun Kawakami
  • Publication number: 20140057111
    Abstract: The present invention provides a globular-shaped metal oxide powder with excellent thermal insulation performance and reduced bulk density, and a method of manufacture thereof, wherein the metal oxide powder has globular independent particles as the main component, and has BET specific surface area of 400 to 1000 m2/g, BJH pore volume of 2 to 8 mL/g, and oil absorption of no less than 250 mL/100g. The present invention also provides a method for manufacturing the hollow and globular shaped metal oxide powder including the step of forming an O/W/O emulsion.
    Type: Application
    Filed: April 25, 2012
    Publication date: February 27, 2014
    Applicant: TOKUYAMA CORPORATION
    Inventors: Wakana Tomimatsu Fujimoto, Tadahiro Fukuju, Hiroshi Numa
  • Publication number: 20130189521
    Abstract: An aerogel with excellent thermal insulation performance, average particle size of 1 to 20 ?m and globular shape; and a method of manufacturing it efficiently, is provided. The aerogel has specific surface area by BET method of 400 to 1000 m2/g; pore volume and peak pore radius by BJH method of 3 to 8 mL/g and 10 to 30 nm, respectively; average particle size and average circularity by image analysis method of 1 to 20 ?m and no less than 0.8, respectively. The method includes the steps of: preparing an aqueous silica sol; dispersing the sol into a hydrophobic solvent, thereby forming a W/O emulsion; causing gelation of the sol, thereby converting the emulsion into a dispersion of a gel; replacing water in the gel with a solvent having a small surface tension; treating the gel with a hydrophobing agent; and removing the solvent used in the solvent replacement.
    Type: Application
    Filed: October 24, 2011
    Publication date: July 25, 2013
    Applicant: TOKUYAMA CORPORATION
    Inventors: Tadahiro Fukuju, Hiroshi Numa, Kazuaki Tabata
  • Patent number: 8304589
    Abstract: A process of making a chlorinated hydrocarbon through a thermal dehydrochlorination step in which an unsaturated compound represented by the following general formula (2) is obtained by thermally decomposing a saturated compound represented by the following general formula (1). CCl3—CCl2-mHm—CCl3-nHn??(1) CCl2?CCl2-mHm-1—CCl3-nHn??(2) (in the above formulas, m is 1 or 2, and n is an integer of 0 to 3.).
    Type: Grant
    Filed: February 27, 2012
    Date of Patent: November 6, 2012
    Assignee: Tokuyama Corporation
    Inventors: Tadahiro Fukuju, Kikuo Yamamoto, Masayuki Moriwaki, Yasutaka Komatsu, Akihiro Saito, Shunsuke Hosaka, Dai Tsunoda, Jun Kawakami
  • Publication number: 20120157723
    Abstract: A process of making a chlorinated hydrocarbon through a thermal dehydrochlorination step in which an unsaturated compound represented by the following general formula (2) is obtained by thermally decomposing a saturated compound represented by the following general formula (1). CCl3—CCl2-mHm—CCl3-nHn??(1) CCl2?CCl2-mHm-1—CCl3-nHn??(2) (in the above formulas, m is 1 or 2, and n is an integer of 0 to 3.
    Type: Application
    Filed: February 27, 2012
    Publication date: June 21, 2012
    Inventors: Tadahiro FUKUJU, Kikuo YAMAMOTO, Masayuki MORIWAKI, Yasutaka KOMATSU, Akihiro SAITO, Shunsuke HOSAKA, Dai TSUNODA, Jun KAWAKAMI
  • Publication number: 20120053374
    Abstract: A process of making a chlorinated hydrocarbon through a thermal dehydrochlorination step in which an unsaturated compound represented by the following general formula (2) is obtained by thermally decomposing a saturated compound represented by the following general formula (1). CCl3—CCl2-mHm—CCl3-nHn??(1) CCl2?CCl2-mHm-1—CCl3-nHn??(2) (in the above formulas, m is 1 or 2, and n is an integer of 0 to 3.
    Type: Application
    Filed: June 17, 2010
    Publication date: March 1, 2012
    Inventors: Tadahiro Fukuju, Kikuo Yamamoto, Masayuki Moriwaki, Yasutaka Komatsu, Akihiro Saito, Shunsuke Hosaka, Dai Tsunoda, Jun Kawakami