Patents by Inventor Takeshi Hagio

Takeshi Hagio has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).

  • Patent number: 11872520
    Abstract: A method for inspecting a separation membrane module has a sealing step for sealing a gas for inspection on a primary side of zeolite membrane. The dynamic molecular diameter for the gas for inspection is greater than 1.07 times the pore diameter in the zeolite membrane. The gas for inspection has the characteristic of having a rate of reduction for a CO2 gas permeation rate in the zeolite membrane of less than 10% when a separation membrane structure is allowed to stand for 60 minutes in the gas for inspection at 25 degrees C. and 0.1 MPaG.
    Type: Grant
    Filed: September 9, 2019
    Date of Patent: January 16, 2024
    Assignee: NGK INSULATORS, LTD.
    Inventors: Katsuya Shimizu, Makiko Ichikawa, Kenji Yajima, Takeshi Hagio
  • Publication number: 20230078309
    Abstract: A drying method for a separation membrane includes supplying a gas for drying to the separation membrane so that a value obtained by dividing the difference between a maximum value and a minimum value of a flow rate of the gas for drying on a membrane surface of the separation membrane by the minimum value of the flow rate is less than or equal to 15%. The gas for drying is less than or equal to 40 degree C. and contains a water-soluble gas that has a solubility in 1 cm3 of water of greater than or equal to 0.5 cm3 in conditions of 40 degree C. and 1 atmosphere.
    Type: Application
    Filed: November 18, 2022
    Publication date: March 16, 2023
    Applicant: NGK Insulators, Ltd.
    Inventors: Kenichi NODA, Takeshi HAGIO
  • Patent number: 11534724
    Abstract: A drying method for a separation membrane includes supplying a gas for drying to the separation membrane so that a value obtained by dividing the difference between a maximum value and a minimum value of a flow rate of the gas for drying on a membrane surface of the separation membrane by the minimum value of the flow rate is less than or equal to 15%. The gas for drying is less than or equal to 40 degree C. and contains a water-soluble gas that has a solubility in 1 cm3 of water of greater than or equal to 0.5 cm3 in conditions of 40 degree C. and 1 atmosphere.
    Type: Grant
    Filed: April 18, 2019
    Date of Patent: December 27, 2022
    Assignee: NGK Insulators, Ltd.
    Inventors: Kenichi Noda, Takeshi Hagio
  • Patent number: 11534725
    Abstract: A zeolite membrane complex comprises: a support; and a zeolite membrane formed on the support. The membrane is of SAT-type zeolite, and in an X-ray diffraction pattern obtained by X-ray irradiation to the zeolite membrane, a peak intensity around 2?=13.9° is 1.5 times or more a peak intensity around 2?=8.5°.
    Type: Grant
    Filed: March 2, 2020
    Date of Patent: December 27, 2022
    Assignee: NGK Insulators, Ltd.
    Inventors: Kenichi Noda, Aya Miura, Ryotaro Yoshimura, Takeshi Hagio
  • Patent number: 11471836
    Abstract: A repair method for a separation membrane including a step of applying a colloidal solution to a surface of a separation membrane formed on a support. The colloidal solution has a predetermined pH. In colloidal solution, repair material particles are dispersed in an aqueous solvent. The repair material particles have an electrical charge that is opposite to an electrical charge of the support at the predetermined pH.
    Type: Grant
    Filed: May 7, 2018
    Date of Patent: October 18, 2022
    Assignee: NGK Insulators, Ltd.
    Inventors: Shinichiro Yamazaki, Takeshi Hagio, Kenichi Noda
  • Patent number: 11402314
    Abstract: A method for inspecting a separation membrane structure includes an assembly step of sealing a separation membrane structure that includes a porous substrate and a separation membrane into a casing, and an inspection step of applying pressure to an inspection liquid that has filled a first main surface side of the separation membrane.
    Type: Grant
    Filed: September 6, 2019
    Date of Patent: August 2, 2022
    Assignee: NGK Insulators, Ltd.
    Inventors: Makoto Miyahara, Makiko Ichikawa, Kenji Yajima, Takeshi Hagio
  • Patent number: 11260348
    Abstract: A dehydration method is a dehydration method for selectively separating water from a mixture that contains water, using a zeolite membrane having an AFX structure, and the method includes a step of supplying the mixture to a supply side space of the zeolite membrane having an AFX structure, and a step of making a pressure difference between the supply side space and a permeation side space of the zeolite membrane having an AFX structure.
    Type: Grant
    Filed: December 4, 2019
    Date of Patent: March 1, 2022
    Assignee: NGK Insulators, Ltd.
    Inventors: Kenichi Noda, Makoto Miyahara, Katsuya Shimizu, Takeshi Hagio
  • Patent number: 11229886
    Abstract: A peak intensity of a (002) plane is greater than or equal to 0.5 times a peak intensity of a (100) plane in an X-ray diffraction pattern obtained by irradiation of X-rays to a membrane surface of the ERI membrane.
    Type: Grant
    Filed: September 17, 2019
    Date of Patent: January 25, 2022
    Assignee: NGK Insulators, Ltd.
    Inventors: Takeshi Hagio, Kenichi Noda, Makoto Miyahara, Katsuya Shimizu, Aya Miura, Ryotaro Yoshimura
  • Patent number: 11219879
    Abstract: An aluminophosphate-metal oxide bonded body including a metal oxide having a bonding surface on a part of the surface thereof, and aluminophosphate that is disposed on the bonding surface of the metal oxide, wherein an alkali metal, an alkaline earth metal or both of these is/are disposed on the bonding surface of the metal oxide, and the content rate of the alkali metal, alkaline earth metal or both is from 0.3 to 30.0% by mass with respect to all of the substances that are disposed on the bonding surface of the metal oxide. An aluminophosphate-metal oxide bonded body that provides a favorable bonded state even for complicated shapes is provided.
    Type: Grant
    Filed: September 28, 2015
    Date of Patent: January 11, 2022
    Assignee: NGK Insulators, Ltd.
    Inventors: Takeshi Hagio, Makoto Miyahara, Tetsuya Uchikawa, Makiko Ichikawa, Kenichi Noda, Kenji Yajima
  • Patent number: 11135545
    Abstract: Provided is a gas separation device configured to separate a non-hydrocarbon gas from a feed gas containing the non-hydrocarbon gas through use of a gas separation membrane, in which a decrease in operating rate can be suppressed, and economic efficiency is satisfactory. A first membrane module (1) and a second membrane module (2) are arranged in parallel to each other with respect to supply lines for a feed gas. Gas lines for regeneration (14, 15) ((24, 25)), which are branched from a permeate gas line (13) ((23)) of the membrane module (1) ((2)), and which are joined to a feed gas line (21) ((11)) configured to supply the feed gas to the membrane module (2) ((1)), are provided. Under a state in which the feed gas is supplied to the membrane module (1), a permeate gas through the membrane module (1) is supplied, as a gas for regeneration, to the membrane module (2) through the gas lines for regeneration (14, 15).
    Type: Grant
    Filed: May 12, 2017
    Date of Patent: October 5, 2021
    Inventors: Hiroaki Hasegawa, Yasushi Fujimora, Aiko Matsuyama, Shuichi Oguro, Keiichi Nishida, Akiko Fukuta, Kenjii Yajima, Makiko Ichikawa, Takeshi Hagio, Naoko Takahashi, Makoto Miyahara, Katsuya Shimizu
  • Patent number: 11103834
    Abstract: A dehydration method is a dehydration method for selectively separating water from a mixture that contains water, and the method includes a step of supplying the mixture to a supply side space of a zeolite membrane having an ERI structure, and a step of making a pressure difference between the supply side space and a permeation side space of the zeolite membrane having an ERI structure.
    Type: Grant
    Filed: December 3, 2019
    Date of Patent: August 31, 2021
    Assignee: NGK Insulators, Ltd.
    Inventors: Kenichi Noda, Makoto Miyahara, Katsuya Shimizu, Takeshi Hagio
  • Patent number: 11008219
    Abstract: A method of synthesis for an aluminophosphate-based zeolite membrane includes a steps of preparing a mixed solution with a pH greater than or equal to 6 and less than or equal to 9 by mixing an acidic phosphorous source with an alkali source, a steps of preparing a starting material solution by adding and mixing an aluminum source to the prepared mixed solution, and a steps of synthesizing an aluminophosphate-based zeolite membrane by hydrothermally synthesizing the starting material solution.
    Type: Grant
    Filed: September 17, 2019
    Date of Patent: May 18, 2021
    Assignee: NGK Insulators, Ltd.
    Inventors: Takeshi Hagio, Kenichi Noda, Makoto Miyahara, Katsuya Shimizu
  • Patent number: 10987637
    Abstract: A DDR-type zeolite seed crystal has an average particle diameter of less than or equal to 0.2 ?m, and an average aspect ratio of less than or equal to 1.3.
    Type: Grant
    Filed: September 18, 2017
    Date of Patent: April 27, 2021
    Assignee: NGK Insulators, Ltd.
    Inventors: Hiroyuki Shibata, Akimasa Ichikawa, Naoto Kinoshita, Takeshi Hagio
  • Patent number: 10906815
    Abstract: A zeolite crystal has an AFX structure and a hexagonal plate shape. Ratio of a maximum Feret diameter (L1) in a plan view with respect to a plate thickness in a side view is greater than or equal to 2.
    Type: Grant
    Filed: September 17, 2019
    Date of Patent: February 2, 2021
    Assignee: NGK Insulators, Ltd.
    Inventors: Takeshi Hagio, Kenichi Noda, Makoto Miyahara, Katsuya Shimizu
  • Patent number: 10894234
    Abstract: A peak intensity of a (004) plane is greater than or equal to 3 times a peak intensity of a (110) plane in an X-ray diffraction pattern obtained by irradiation of X-rays to a membrane surface of an AFX membrane.
    Type: Grant
    Filed: September 17, 2019
    Date of Patent: January 19, 2021
    Assignee: NGK Insultators, Ltd.
    Inventors: Takeshi Hagio, Kenichi Noda, Makoto Miyahara, Katsuya Shimizu
  • Patent number: 10835875
    Abstract: A peak intensity of a (110) plane is greater than or equal to 2.5 times a peak intensity of a (004) plane in an X-ray diffraction pattern obtained by irradiation of X-rays to a membrane surface of the AFX membrane.
    Type: Grant
    Filed: September 17, 2019
    Date of Patent: November 17, 2020
    Assignee: NGK Insulators, Ltd.
    Inventors: Takeshi Hagio, Kenichi Noda, Makoto Miyahara, Katsuya Shimizu, Aya Miura, Ryotaro Yoshimura
  • Publication number: 20200269188
    Abstract: Provided is a gas separation device configured to separate a non-hydrocarbon gas from a feed gas containing the non-hydrocarbon gas through use of a gas separation membrane, in which a decrease in operating rate can be suppressed, and economic efficiency is satisfactory. A first membrane module (1) and a second membrane module (2) are arranged in parallel to each other with respect to supply lines for a feed gas. Gas lines for regeneration (14, 15) ((24, 25)), which are branched from a permeate gas line (13) ((23)) of the membrane module (1) ((2)), and which are joined to a feed gas line (21) ((11)) configured to supply the feed gas to the membrane module (2) ((1)), are provided. Under a state in which the feed gas is supplied to the membrane module (1), a permeate gas through the membrane module (1) is supplied, as a gas for regeneration, to the membrane module (2) through the gas lines for regeneration (14, 15).
    Type: Application
    Filed: May 12, 2017
    Publication date: August 27, 2020
    Inventors: Hiroaki Hasegawa, Yasushi Fujimora, Aiko Matsuyama, Shuichi Oguro, Keiichi Nishida, Akiko Fukuta, Kenjii Yajima, Makiko Ichikawa, Takeshi Hagio, Naoko Takahashi, Makoto Miyahara, Katsuya Shimizu
  • Publication number: 20200197879
    Abstract: A zeolite membrane complex comprises: a support; and a zeolite membrane formed on the support. The membrane is of SAT-type zeolite, and in an X-ray diffraction pattern obtained by X-ray irradiation to the zeolite membrane, a peak intensity around 2?=13.9° is 1.5 times or more a peak intensity around 2?=8.5°.
    Type: Application
    Filed: March 2, 2020
    Publication date: June 25, 2020
    Applicant: NGK INSULATORS, LTD.
    Inventors: Kenichi NODA, Aya MIURA, Ryotaro YOSHIMURA, Takeshi HAGIO
  • Patent number: 10688434
    Abstract: The gas separation method is executed under a condition in which a partial pressure of a first gas (G1) in a feed gas that contains at least mutually different gases being the first gas (G1) and a second gas (G2) becomes less than or equal to a total pressure of a permeate-side space (S2) of a gas separation membrane (30). The gas separation method includes a step of causing flow of a sweep gas that contains at least a third gas (G3) being a different gas from the first gas (G1) and the second gas (G2) into the permeate-side space (S2) of the gas separation membrane (30) while supplying a feed gas to a feed-side space (S1) of the gas separation membrane (30). The permeation rate of the first gas (G1) in the gas separation membrane (30) is greater than the permeation rate respectively of the second gas (G2) and the third gas (G3).
    Type: Grant
    Filed: June 15, 2017
    Date of Patent: June 23, 2020
    Assignee: NGK Insulators, Ltd.
    Inventors: Kenichi Noda, Takeshi Hagio
  • Publication number: 20200122096
    Abstract: A dehydration method is a dehydration method for selectively separating water from a mixture that contains water, and the method includes a step of supplying the mixture to a supply side space of a separation membrane, and a step of making a pressure difference between the supply side space and a permeation side space of the separation membrane. The separation membrane includes a first zeolite membrane that faces the permeation side space and is constituted by a first zeolite and a second zeolite membrane that faces the supply side space and is adjacent to the first zeolite membrane. The second zeolite membrane is constituted by a second zeolite that has the same framework structure as framework of the first zeolite and has a lower Si/Al atom ratio than a Si/Al atom ratio of the first zeolite.
    Type: Application
    Filed: December 5, 2019
    Publication date: April 23, 2020
    Applicant: NGK INSULATORS, LTD.
    Inventors: Kenichi Noda, Makoto Miyahara, Katsuya Shimizu, Takeshi Hagio