Patents by Inventor TAWFIK ABDO SALEH AWADH

TAWFIK ABDO SALEH AWADH has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).

  • Patent number: 11970665
    Abstract: Carbon nanofiber doped alumina (Al—CNF) supported MoCo catalysts in hydrodesulfurization (HDS), and/or boron doping, e.g., up to 5 wt % of total catalyst weight, can improve catalytic efficiency. Al—CNF-supported MoCo catalysts, (Al—CNF—MoCo), can reduce the sulfur concentration in fuel, esp. liquid fuel, to below the required limit in a 6 h reaction time. Thus, Al—CNF—MoCo has a higher catalytic activity than Al-MoCo, which may be explained by higher mesoporous surface area and better dispersion of MoCo metals on the AlCNF support relative to alumina support. The BET surface area of Al-MoCo may be 75% less than Al—CNF—MoCo, e.g., 166 vs. 200 m2/g. SEM images indicate that the catalyst nanoparticles can be evenly distributed on the surface of the CNF. The surface area of the AlMoCoB5% may be 206 m2/g, which is higher than AlMoCoB0% and AlMoCoB2%, and AlMoCoB5% has the highest HDS activity, removing more than 98% sulfur and below allowed levels.
    Type: Grant
    Filed: May 23, 2022
    Date of Patent: April 30, 2024
    Assignee: King Fahd University of Petroleum and Minerals
    Inventors: Tawfik Abdo Saleh Awadh, Saddam Ahmed Al-Hammadi
  • Patent number: 11897789
    Abstract: Polymer/carbon nanotube composites made up of melamine, aldehyde, diaminoalkane monomeric units and carbon nanotubes having activated carbonyl groups. A method for removing heavy metals, such as Pb(II) from an aqueous solution or an industrial wastewater sample with these composites is introduced. A process of synthesizing the polymer/carbon nanotube composites is also described.
    Type: Grant
    Filed: February 2, 2018
    Date of Patent: February 13, 2024
    Assignee: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Othman Charles Sadeq Al Hamouz, Isaiah Olabisi Adelabu, Tawfik Abdo Saleh Awadh
  • Publication number: 20240043288
    Abstract: The invention is directed to use of polystyrene wastes, such as Styrofoam® wastes, and carbon nanofibers to produce a highly hydrophobic composition or composite that can separate oil and water.
    Type: Application
    Filed: October 16, 2023
    Publication date: February 8, 2024
    Applicant: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Tawfik Abdo Saleh AWADH, Nadeem BAIG
  • Patent number: 11807554
    Abstract: Polystyrene waste, such as Styrofoam® waste, and carbon nanofibers may be used to produce highly hydrophobic compositions or composites that can separate oil and water. Methods for purifying an aqueous solution may include: passing the aqueous solution, including a hydrophobic organic substance, over or through a surface including a polystyrene-CNF composition, thereby producing an aqueous product including less of the hydrophobic organic substance; and optionally, passing the aqueous product over or through the surface at least one more time.
    Type: Grant
    Filed: December 6, 2018
    Date of Patent: November 7, 2023
    Assignee: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Tawfik Abdo Saleh Awadh, Nadeem Baig
  • Patent number: 11772990
    Abstract: A method for removing cadmium ions from contaminated water sources and systems via contacting and treatment with composites formed from reaction between melamine, an aldehyde, diaminoalkane monomeric units and carbon nanotubes having activated carbonyl groups.
    Type: Grant
    Filed: April 19, 2018
    Date of Patent: October 3, 2023
    Assignee: King Fahd University of Petroleum and Minerals
    Inventors: Othman Charles Sadeq Al Hamouz, Isaiah Olabisi Adelabu, Tawfik Abdo Saleh Awadh
  • Patent number: 11773201
    Abstract: Crosslinked polymers made up of polymerized units of cyclic diaminoalkane, aldehyde and bisphenol-S or melamine. A method for removing heavy metals, such as Pb(II) from an aqueous solution or an industrial wastewater sample with these crosslinked polymers is introduced. A process of synthesizing the crosslinked polymers is also described.
    Type: Grant
    Filed: December 8, 2022
    Date of Patent: October 3, 2023
    Assignee: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Othman Charles Sadeq Al Hamouz, Mohammed Estatie, Tawfik Abdo Saleh Awadh, Mohamed A. Morsy
  • Patent number: 11760827
    Abstract: Crosslinked polymers made up of polymerized units of cyclic diaminoalkane, aldehyde and bisphenol-S or melamine. A method for removing heavy metals, such as Pb(II) from an aqueous solution or an industrial wastewater sample with these crosslinked polymers is introduced. A process of synthesizing the crosslinked polymers is also described.
    Type: Grant
    Filed: December 8, 2022
    Date of Patent: September 19, 2023
    Assignee: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Othman Charles Sadeq Al Hamouz, Mohammed Estatie, Tawfik Abdo Saleh Awadh, Mohamed A. Morsy
  • Publication number: 20230249991
    Abstract: A composite material of polyurethane foam having a layer of reduced graphene oxide and polystyrene is described. This composite material may be made by contacting a polyurethane foam with a suspension of reduced graphene oxide, drying, and then irradiating in the presence of styrene vapor. The composite material has a hydrophobic surface that may be exploited for separating a nonpolar phase, such as oil, from an aqueous solution.
    Type: Application
    Filed: March 3, 2023
    Publication date: August 10, 2023
    Applicant: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Tawfik Abdo Saleh AWADH, Nadeem BAIG
  • Patent number: 11713422
    Abstract: Carbon nanofiber doped alumina (Al—CNF) supported MoCo catalysts in hydrodesulfurization (HDS), and/or boron doping, e.g., up to 5 wt % of total catalyst weight, can improve catalytic efficiency. Al—CNF-supported MoCo catalysts, (Al—CNF—MoCo), can reduce the sulfur concentration in fuel, esp. liquid fuel, to below the required limit in a 6 h reaction time. Thus, Al—CNF—MoCo has a higher catalytic activity than Al—MoCo, which may be explained by higher mesoporous surface area and better dispersion of MoCo metals on the AlCNF support relative to alumina support. The BET surface area of Al—MoCo may be 75% less than Al—CNF—MoCo, e.g., 166 vs. 200 m2/g. SEM images indicate that the catalyst nanoparticles can be evenly distributed on the surface of the CNF. The surface area of the AlMoCoB5% may be 206 m2/g, which is higher than AlMoCoB0% and AlMoCoB2%, and AlMoCoB5% has the highest HDS activity, removing more than 98% sulfur and below allowed levels.
    Type: Grant
    Filed: May 23, 2022
    Date of Patent: August 1, 2023
    Assignee: King Fahd University of Petroleum and Minerals
    Inventors: Tawfik Abdo Saleh Awadh, Saddam Ahmed Al-Hammadi
  • Publication number: 20230202877
    Abstract: A composite material of polyurethane foam having a layer of reduced graphene oxide and polystyrene is described. This composite material may be made by contacting a polyurethane foam with a suspension of reduced graphene oxide, drying, and then irradiating in the presence of styrene vapor. The composite material has a hydrophobic surface that may be exploited for separating a nonpolar phase, such as oil, from an aqueous solution.
    Type: Application
    Filed: March 3, 2023
    Publication date: June 29, 2023
    Applicant: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Tawfik Abdo Saleh AWADH, Nadeem BAIG
  • Patent number: 11684897
    Abstract: A method for making a titania-polymer nanocomposite by simultaneously forming TiO2 nanoparticles in situ from a TiO2 precursor in the presence of urea and interfacially polymerizing polyamide precursors thereby producing a titania-polymer nanocomposite. A titania-polymer nanocomposite made by this method. A method for removing a dye or metal from water comprising contacting contaminated water with the titania-polymer nanocomposite.
    Type: Grant
    Filed: August 10, 2022
    Date of Patent: June 27, 2023
    Assignee: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Tawfik Abdo Saleh Awadh, Saddam Ahmed Al-Hammadi, Islam Ali Elsayed
  • Patent number: 11642630
    Abstract: A method for making a titania-polymer nanocomposite by simultaneously forming TiO2 nanoparticles in situ from a TiO2 precursor in the presence of urea and interfacially polymerizing polyamide precursors thereby producing a titania-polymer nanocomposite. A titania-polymer nanocomposite made by this method. A method for removing a dye or metal from water comprising contacting contaminated water with the titania-polymer nanocomposite.
    Type: Grant
    Filed: August 10, 2022
    Date of Patent: May 9, 2023
    Assignee: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Tawfik Abdo Saleh Awadh, Saddam Ahmed Al-Hammadi, Islam Ali Elsayed
  • Publication number: 20230140110
    Abstract: Crosslinked polymers made up of polymerized units of cyclic diaminoalkane, aldehyde and bisphenol-S or melamine. A method for removing heavy metals, such as Pb(II) from an aqueous solution or an industrial wastewater sample with these crosslinked polymers is introduced. A process of synthesizing the crosslinked polymers is also described.
    Type: Application
    Filed: December 8, 2022
    Publication date: May 4, 2023
    Applicant: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Othman Charles Sadeq AL HAMOUZ, Mohammed ESTATIE, Tawfik Abdo Saleh AWADH, Mohamed A. MORSY
  • Publication number: 20230116824
    Abstract: Crosslinked polymers made up of polymerized units of cyclic diaminoalkane, aldehyde and bisphenol-S or melamine. A method for removing heavy metals, such as Pb(II) from an aqueous solution or an industrial wastewater sample with these crosslinked polymers is introduced. A process of synthesizing the crosslinked polymers is also described.
    Type: Application
    Filed: December 8, 2022
    Publication date: April 13, 2023
    Applicant: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Othman Charles Sadeq AL HAMOUZ, Mohammed ESTATIE, Tawfik Abdo Saleh AWADH, Mohamed A. MORSY
  • Patent number: 11613479
    Abstract: A composite material of polyurethane foam having a layer of reduced graphene oxide and polystyrene is described. This composite material may be made by contacting a polyurethane foam with a suspension of reduced graphene oxide, drying, and then irradiating in the presence of styrene vapor. The composite material has a hydrophobic surface that may be exploited for separating a nonpolar phase, such as oil, from an aqueous solution.
    Type: Grant
    Filed: July 24, 2019
    Date of Patent: March 28, 2023
    Assignee: King Fahd University of Petroleum and Minerals
    Inventors: Tawfik Abdo Saleh Awadh, Nadeem Baig
  • Patent number: 11583828
    Abstract: A polymer/activated carbon composite made up of a branched polyethylenimine and magnetic cores involving Fe3O4 disposed activated carbon. The magnetic cores have activated carbonyl groups on the surface. A process for removing organic dyes, such as methyl red, as well as heavy metal ions from a polluted aqueous solution or an industrial wastewater utilizing the composite is introduced. A method of synthesizing the polymer/activated carbon composites is also specified.
    Type: Grant
    Filed: July 23, 2019
    Date of Patent: February 21, 2023
    Assignee: King Fahd University of Petroleum and Minerals
    Inventors: Tawfik Abdo Saleh Awadh, Akram Abdulhakeem Al-Absi
  • Publication number: 20220401891
    Abstract: A method for making a titania-polymer nanocomposite by simultaneously forming TiO2 nanoparticles in situ from a TiO2 precursor in the presence of urea and interfacially polymerizing polyamide precursors thereby producing a titania-polymer nanocomposite. A titania-polymer nanocomposite made by this method. A method for removing a dye or metal from water comprising contacting contaminated water with the titania-polymer nanocomposite.
    Type: Application
    Filed: August 10, 2022
    Publication date: December 22, 2022
    Applicant: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Tawfik Abdo Saleh AWADH, Saddam Ahmed AL-HAMMADI, Islam Ali ELSAYED
  • Publication number: 20220401890
    Abstract: A method for making a titania-polymer nanocomposite by simultaneously forming TiO2 nanoparticles in situ from a TiO2 precursor in the presence of urea and interfacially polymerizing polyamide precursors thereby producing a titania-polymer nanocomposite. A titania-polymer nanocomposite made by this method. A method for removing a dye or metal from water comprising contacting contaminated water with the titania-polymer nanocomposite.
    Type: Application
    Filed: August 10, 2022
    Publication date: December 22, 2022
    Applicant: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Tawfik Abdo Saleh AWADH, Saddam Ahmed AL-HAMMADI, Islam Ali ELSAYED
  • Patent number: 11530289
    Abstract: A crosslinked polymer that is in the form of a Mannich polycondensation product including reacted units of a cyclic diaminoalkane, an aldehyde, and bisphenol-S or melamine. Also disclosed is a method for removing heavy metals from an aqueous solution by contacting the aqueous solution having an initial concentration of the heavy metal with the crosslinked polymer to form a mixture, and filtering the mixture to obtain an aqueous solution having a reduced concentration of the heavy metal compared to the initial concentration.
    Type: Grant
    Filed: March 16, 2018
    Date of Patent: December 20, 2022
    Assignee: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Othman Charles Sadeq Al Hamouz, Mohammed Estatie, Tawfik Abdo Saleh Awadh, Mohamed A. Morsy
  • Publication number: 20220297086
    Abstract: A polymer/activated carbon composite made up of a branched polyethylenimine and magnetic cores involving Fe3O4 disposed activated carbon. The magnetic cores have activated carbonyl groups on the surface. A process for removing organic dyes, such as methyl red, as well as heavy metal ions from a polluted aqueous solution or an industrial wastewater utilizing the composite is introduced. A method of synthesizing the polymer/activated carbon composites is also specified.
    Type: Application
    Filed: May 17, 2022
    Publication date: September 22, 2022
    Applicant: King Fahd University of Petroleum and Minerals
    Inventors: Tawfik Abdo Saleh AWADH, Akram Abdulhakeem AL-ABSI