Patents by Inventor TAWFIK ABDO SALEH AWADH

TAWFIK ABDO SALEH AWADH has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).

  • Publication number: 20250034461
    Abstract: Carbon nanofiber doped alumina (Al-CNF) supported MoCo catalysts in hydrodesulfurization (HDS), and/or boron doping, e.g., up to 5 wt % of total catalyst weight, can improve catalytic efficiency. Al-CNF-supported MoCo catalysts, (Al-CNF-MoCo), can reduce the sulfur concentration in fuel, esp. liquid fuel, to below the required limit in a 6 h reaction time. Thus, Al-CNF-MoCo has a higher catalytic activity than Al—MoCo, which may be explained by higher mesoporous surface area and better dispersion of MoCo metals on the AlCNF support relative to alumina support. The BET surface area of Al—MoCo may be 75% less than Al-CNF-MoCo, e.g., 166 vs. 200 m2/g. SEM images indicate that the catalyst nanoparticles can be evenly distributed on the surface of the CNF. The surface area of the AlMoCoB5% may be 206 m2/g, which is higher than AlMoCoB0% and AlMoCoB2%, and AlMoCoB5% has the highest HDS activity, removing more than 98% sulfur and below allowed levels.
    Type: Application
    Filed: March 15, 2024
    Publication date: January 30, 2025
    Applicant: King Fahd University of Petroleum and Minerals
    Inventors: Tawfik Abdo Saleh AWADH, Saddam Ahmed AL-HAMMADI
  • Publication number: 20250034460
    Abstract: Carbon nanofiber doped alumina (Al-CNF) supported MoCo catalysts in hydrodesulfurization (HDS), and/or boron doping, e.g., up to 5 wt % of total catalyst weight, can improve catalytic efficiency. Al-CNF-supported MoCo catalysts, (Al-CNF-MoCo), can reduce the sulfur concentration in fuel, esp. liquid fuel, to below the required limit in a 6 h reaction time. Thus, Al-CNF-MoCo has a higher catalytic activity than Al—MoCo, which may be explained by higher mesoporous surface area and better dispersion of MoCo metals on the AlCNF support relative to alumina support. The BET surface area of Al—MoCo may be 75% less than Al-CNF-MoCo, e.g., 166 vs. 200 m2/g. SEM images indicate that the catalyst nanoparticles can be evenly distributed on the surface of the CNF. The surface area of the AlMoCoB 5% may be 206 m2/g, which is higher than AlMoCoB 0% and AlMoCoB 2%, and AlMoCoB 5% has the highest HDS activity, removing more than 98% sulfur and below allowed levels.
    Type: Application
    Filed: March 15, 2024
    Publication date: January 30, 2025
    Applicant: King Fahd University of Petroleum and Minerals
    Inventors: Tawfik Abdo Saleh AWADH, Saddam Ahmed AL-HAMMADI
  • Publication number: 20250034462
    Abstract: Carbon nanofiber doped alumina (Al-CNF) supported MoCo catalysts in hydrodesulfurization (HDS), and/or boron doping, e.g., up to 5 wt % of total catalyst weight, can improve catalytic efficiency. Al-CNF-supported MoCo catalysts, (Al-CNF-MoCo), can reduce the sulfur concentration in fuel, esp. liquid fuel, to below the required limit in a 6 h reaction time. Thus, Al-CNF-MoCo has a higher catalytic activity than Al—MoCo, which may be explained by higher mesoporous surface area and better dispersion of MoCo metals on the AlCNF support relative to alumina support. The BET surface area of Al—MoCo may be 75% less than Al-CNF-MoCo, e.g., 166 vs. 200 m2/g. SEM images indicate that the catalyst nanoparticles can be evenly distributed on the surface of the CNF. The surface area of the AlMoCoB5% may be 206 m2/g, which is higher than AlMoCoB0% and AlMoCoB2%, and AlMoCoB5% has the highest HDS activity, removing more than 98% sulfur and below allowed levels.
    Type: Application
    Filed: April 26, 2024
    Publication date: January 30, 2025
    Applicant: King Fahd University of Petroleum and Minerals
    Inventors: Tawfik Abdo Saleh AWADH, Saddam Ahmed AL-HAMMADI
  • Publication number: 20250011249
    Abstract: A method for enhancing adhesion of a curable composition to a cement-based object includes applying a graphene oxide (GO) containing dispersion on a surface of the cement-based object thereby forming a GO-treated surface on the cement-based object. The method includes disposing the curable composition on the GO-treated surface of the cement-based object. The method includes curing the curable composition by heating thereby forming a GO interfacial layer and an epoxy resin layer. The GO interfacial layer is between the surface of the cement-based object and the epoxy resin layer. The curable composition includes an epoxy monomer and an amine curing agent. The GO interfacial layer has a thickness of from 0.1 to 10 nanometers (nm).
    Type: Application
    Filed: July 6, 2023
    Publication date: January 9, 2025
    Applicant: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Ashraf Awadh BAHRAQ, Mohammed Ali ALOSTA, Ime Bassey OBOT, Omar Saeed Baghabra AL-AMOUDI, Tawfik Abdo Saleh AWADH, Mohammed MASLEHUDDIN
  • Patent number: 12186734
    Abstract: A polymer/activated carbon composite made up of a branched polyethylenimine and magnetic cores involving Fe3O4 disposed activated carbon. The magnetic cores have activated carbonyl groups on the surface. A process for removing organic dyes, such as methyl red, as well as heavy metal ions from a polluted aqueous solution or an industrial wastewater utilizing the composite is introduced. A method of synthesizing the polymer/activated carbon composites is also specified.
    Type: Grant
    Filed: August 19, 2024
    Date of Patent: January 7, 2025
    Assignee: King Fahd University of Petroleum and Minerals
    Inventors: Tawfik Abdo Saleh Awadh, Akram Abdulhakeem Al-Absi
  • Patent number: 12186736
    Abstract: A polymer/activated carbon composite made up of a branched polyethylenimine and magnetic cores involving Fe3O4 disposed activated carbon. The magnetic cores have activated carbonyl groups on the surface. A process for removing organic dyes, such as methyl red, as well as heavy metal ions from a polluted aqueous solution or an industrial wastewater utilizing the composite is introduced. A method of synthesizing the polymer/activated carbon composites is also specified.
    Type: Grant
    Filed: August 19, 2024
    Date of Patent: January 7, 2025
    Assignee: King Fahd University of Petroleum and Minerals
    Inventors: Tawfik Abdo Saleh Awadh, Akram Abdulhakeem Al-Absi
  • Patent number: 12186735
    Abstract: A polymer/activated carbon composite made up of a branched polyethylenimine and magnetic cores involving Fe3O4 disposed activated carbon. The magnetic cores have activated carbonyl groups on the surface. A process for removing organic dyes, such as methyl red, as well as heavy metal ions from a polluted aqueous solution or an industrial wastewater utilizing the composite is introduced. A method of synthesizing the polymer/activated carbon composites is also specified.
    Type: Grant
    Filed: August 19, 2024
    Date of Patent: January 7, 2025
    Assignee: King Fahd University of Petroleum and Minerals
    Inventors: Tawfik Abdo Saleh Awadh, Akram Abdulhakeem Al-Absi
  • Patent number: 12179174
    Abstract: A polymer/activated carbon composite made up of a branched polyethylenimine and magnetic cores involving Fe3O4 disposed activated carbon. The magnetic cores have activated carbonyl groups on the surface. A process for removing organic dyes, such as methyl red, as well as heavy metal ions from a polluted aqueous solution or an industrial wastewater utilizing the composite is introduced. A method of synthesizing the polymer/activated carbon composites is also specified.
    Type: Grant
    Filed: May 17, 2022
    Date of Patent: December 31, 2024
    Assignee: King Fahd University of Petroleum and Minerals
    Inventors: Tawfik Abdo Saleh Awadh, Akram Abdulhakeem Al-Absi
  • Publication number: 20240408575
    Abstract: A polymer/activated carbon composite made up of a branched polyethylenimine and magnetic cores involving Fe3O4 disposed activated carbon. The magnetic cores have activated carbonyl groups on the surface. A process for removing organic dyes, such as methyl red, as well as heavy metal ions from a polluted aqueous solution or an industrial wastewater utilizing the composite is introduced. A method of synthesizing the polymer/activated carbon composites is also specified.
    Type: Application
    Filed: August 19, 2024
    Publication date: December 12, 2024
    Applicant: King Fahd University of Petroleum and Minerals
    Inventors: Tawfik Abdo Saleh AWADH, Akram Abdulhakeem AL-ABSI
  • Publication number: 20240408576
    Abstract: A polymer/activated carbon composite made up of a branched polyethylenimine and magnetic cores involving Fe3O4 disposed activated carbon. The magnetic cores have activated carbonyl groups on the surface. A process for removing organic dyes, such as methyl red, as well as heavy metal ions from a polluted aqueous solution or an industrial wastewater utilizing the composite is introduced. A method of synthesizing the polymer/activated carbon composites is also specified.
    Type: Application
    Filed: August 19, 2024
    Publication date: December 12, 2024
    Applicant: King Fahd University of Petroleum and Minerals
    Inventors: Tawfik Abdo Saleh AWADH, Akram Abdulhakeem AL-ABSI
  • Publication number: 20240408577
    Abstract: A polymer/activated carbon composite made up of a branched polyethylenimine and magnetic cores involving Fe3O4 disposed activated carbon. The magnetic cores have activated carbonyl groups on the surface. A process for removing organic dyes, such as methyl red, as well as heavy metal ions from a polluted aqueous solution or an industrial wastewater utilizing the composite is introduced. A method of synthesizing the polymer/activated carbon composites is also specified.
    Type: Application
    Filed: August 19, 2024
    Publication date: December 12, 2024
    Applicant: King Fahd University of Petroleum and Minerals
    Inventors: Tawfik Abdo Saleh AWADH, Akram Abdulhakeem AL-ABSI
  • Patent number: 12102978
    Abstract: A polymer/activated carbon composite made up of a branched polyethylenimine and magnetic cores involving Fe3O4 disposed activated carbon. The magnetic cores have activated carbonyl groups on the surface. A process for removing organic dyes, such as methyl red, as well as heavy metal ions from a polluted aqueous solution or an industrial wastewater utilizing the composite is introduced. A method of synthesizing the polymer/activated carbon composites is also specified.
    Type: Grant
    Filed: May 17, 2022
    Date of Patent: October 1, 2024
    Assignee: King Fahd University of Petroleum and Minerals
    Inventors: Tawfik Abdo Saleh Awadh, Akram Abdulhakeem Al-Absi
  • Patent number: 11970665
    Abstract: Carbon nanofiber doped alumina (Al—CNF) supported MoCo catalysts in hydrodesulfurization (HDS), and/or boron doping, e.g., up to 5 wt % of total catalyst weight, can improve catalytic efficiency. Al—CNF-supported MoCo catalysts, (Al—CNF—MoCo), can reduce the sulfur concentration in fuel, esp. liquid fuel, to below the required limit in a 6 h reaction time. Thus, Al—CNF—MoCo has a higher catalytic activity than Al-MoCo, which may be explained by higher mesoporous surface area and better dispersion of MoCo metals on the AlCNF support relative to alumina support. The BET surface area of Al-MoCo may be 75% less than Al—CNF—MoCo, e.g., 166 vs. 200 m2/g. SEM images indicate that the catalyst nanoparticles can be evenly distributed on the surface of the CNF. The surface area of the AlMoCoB5% may be 206 m2/g, which is higher than AlMoCoB0% and AlMoCoB2%, and AlMoCoB5% has the highest HDS activity, removing more than 98% sulfur and below allowed levels.
    Type: Grant
    Filed: May 23, 2022
    Date of Patent: April 30, 2024
    Assignee: King Fahd University of Petroleum and Minerals
    Inventors: Tawfik Abdo Saleh Awadh, Saddam Ahmed Al-Hammadi
  • Patent number: 11897789
    Abstract: Polymer/carbon nanotube composites made up of melamine, aldehyde, diaminoalkane monomeric units and carbon nanotubes having activated carbonyl groups. A method for removing heavy metals, such as Pb(II) from an aqueous solution or an industrial wastewater sample with these composites is introduced. A process of synthesizing the polymer/carbon nanotube composites is also described.
    Type: Grant
    Filed: February 2, 2018
    Date of Patent: February 13, 2024
    Assignee: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Othman Charles Sadeq Al Hamouz, Isaiah Olabisi Adelabu, Tawfik Abdo Saleh Awadh
  • Publication number: 20240043288
    Abstract: The invention is directed to use of polystyrene wastes, such as Styrofoam® wastes, and carbon nanofibers to produce a highly hydrophobic composition or composite that can separate oil and water.
    Type: Application
    Filed: October 16, 2023
    Publication date: February 8, 2024
    Applicant: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Tawfik Abdo Saleh AWADH, Nadeem BAIG
  • Patent number: 11807554
    Abstract: Polystyrene waste, such as Styrofoam® waste, and carbon nanofibers may be used to produce highly hydrophobic compositions or composites that can separate oil and water. Methods for purifying an aqueous solution may include: passing the aqueous solution, including a hydrophobic organic substance, over or through a surface including a polystyrene-CNF composition, thereby producing an aqueous product including less of the hydrophobic organic substance; and optionally, passing the aqueous product over or through the surface at least one more time.
    Type: Grant
    Filed: December 6, 2018
    Date of Patent: November 7, 2023
    Assignee: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Tawfik Abdo Saleh Awadh, Nadeem Baig
  • Patent number: 11772990
    Abstract: A method for removing cadmium ions from contaminated water sources and systems via contacting and treatment with composites formed from reaction between melamine, an aldehyde, diaminoalkane monomeric units and carbon nanotubes having activated carbonyl groups.
    Type: Grant
    Filed: April 19, 2018
    Date of Patent: October 3, 2023
    Assignee: King Fahd University of Petroleum and Minerals
    Inventors: Othman Charles Sadeq Al Hamouz, Isaiah Olabisi Adelabu, Tawfik Abdo Saleh Awadh
  • Patent number: 11773201
    Abstract: Crosslinked polymers made up of polymerized units of cyclic diaminoalkane, aldehyde and bisphenol-S or melamine. A method for removing heavy metals, such as Pb(II) from an aqueous solution or an industrial wastewater sample with these crosslinked polymers is introduced. A process of synthesizing the crosslinked polymers is also described.
    Type: Grant
    Filed: December 8, 2022
    Date of Patent: October 3, 2023
    Assignee: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Othman Charles Sadeq Al Hamouz, Mohammed Estatie, Tawfik Abdo Saleh Awadh, Mohamed A. Morsy
  • Patent number: 11760827
    Abstract: Crosslinked polymers made up of polymerized units of cyclic diaminoalkane, aldehyde and bisphenol-S or melamine. A method for removing heavy metals, such as Pb(II) from an aqueous solution or an industrial wastewater sample with these crosslinked polymers is introduced. A process of synthesizing the crosslinked polymers is also described.
    Type: Grant
    Filed: December 8, 2022
    Date of Patent: September 19, 2023
    Assignee: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Othman Charles Sadeq Al Hamouz, Mohammed Estatie, Tawfik Abdo Saleh Awadh, Mohamed A. Morsy
  • Publication number: 20230249991
    Abstract: A composite material of polyurethane foam having a layer of reduced graphene oxide and polystyrene is described. This composite material may be made by contacting a polyurethane foam with a suspension of reduced graphene oxide, drying, and then irradiating in the presence of styrene vapor. The composite material has a hydrophobic surface that may be exploited for separating a nonpolar phase, such as oil, from an aqueous solution.
    Type: Application
    Filed: March 3, 2023
    Publication date: August 10, 2023
    Applicant: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS
    Inventors: Tawfik Abdo Saleh AWADH, Nadeem BAIG