Abstract: An apparatus for gas/liquid separation has a heat-exchanging condensor housed in an adiabaic coolant container, in combination with an adiabatic reservoir for the condensed liquid. The condensor has an inner pipe conduit for a passive coolant which circulates through the conduit, and the container and is cooled by a freezer coil of an outside refrigerator and effectively cools the solvent vapor travelling through a clearance formed between the inner side wall of said condensor and outer side wall of said inner pipe conduit. This feature enables a continuous operation without troublesome replenishing of an active component in a freezing mixture as an active coolant. The adiabatic reservoir receives the condensed liquid and has a visual gauge for monitoring. A communicating plug detachably provided on the shoulder of the adiabatic reservoir serves to supply an auxiliary freeze-protecting solvent into the reservoir, for easy treatment of a solvent which is liable to be solidified by excessive cooling.

Abstract: A chromatographic plate comprising a support having a plurality of linear grooves engraved on the rear is disclosed. Each of said grooves have a uniform depth of a half or less as large as the thickness of the support and serves to guide a cutter. After the chromatographic development, the support may easily be cloven along the grooves into strips together with an adsorbent layer carried by the front of the support to give a sample holder for mass spectrometry.

Abstract: The conventional water-resistant silica or alumina plate for thin layer chromatography is converted into a reverse-phase thin layer chromatographic plate by tri-(lower alkyl)silylating the adsorbent in situ. The adsorbent layer containing the tri-(lower alkyl)silyloxy group is found to be superior to either of the known adsorbent layers containing mono- or di-(lower alkyl)silyloxy groups, or mono-(higher alkyl)silyloxy groups. Optimum conditions for performing a method for preparing the plate are also disclosed.

Abstract: Quantitative determinations by means of mass spectrometry of substances which have hitherto been very difficult to perform are made possible by the employment of the sample holding element of the present invention composed of a porous and gas-permeable aggregate of a skeletal ingredient having refractory and electrical-insulating properties, with a remarkable improvement in sensitivity and accuracy. Determination of mixture samples for their respective components is also effected without any preceding separating step.