Abstract: A system and method for sample preparation and/or sample enrichment are provided. The system comprises the following components: a first switch element with a switch element input and at least two mutually exclusive switch element outputs and a second corresponding switch element with at least two mutually exclusive switch element inputs and a switch element output, the first and second switch elements being connected to control means for opening and closing the switch element inputs and switch element outputs; a first distributor element with at least three ports and a second distributor element with at least three ports; as well as a first separation column and a second separation column, the components being in such fluidic communication with each other that by means of different positions of the switch elements it is possible to configure at least two different fluidic paths in the system, wherein said different positions are achievable through the control means.

Abstract: A system and method for sample preparation and/or sample enrichment are provided. The system comprises the following components: a first switch element with a switch element input and at least two mutually exclusive switch element outputs and a second corresponding switch element with at least two mutually exclusive switch element inputs and a switch element output, the first and second switch elements being connected to control means for opening and closing the switch element inputs and switch element outputs; a first distributor element with at least three ports and a second distributor element with at least three ports; as well as a first separation column and a second separation column, the components being in such fluidic communication with each other that by means of different positions of the switch elements it is possible to configure at least two different fluidic paths in the system, wherein said different positions are achievable through the control means.

Abstract: The invention relates to a method and to a circuit configuration for adjusting the voltage level for the electrical data transmission between a transmitting component and a receiving component of one or different assemblies. According to the invention, the voltage level is increased step-wise or continuously until the required value for the correct representation of the signals to be transmitted is reached in the receiving component. Increase of the voltage level is stopped by the transmission of respective information. The inventive method and circuit are advantageous in that the minimum voltage level required for the transmission of data can be precisely adjusted. Power loss can be thereby reduced and adjacent channel interferences through high voltage levels can be reduced to a minimum.

Abstract: The invention relates to a method and to a circuit configuration for adjusting the voltage level for the electrical data transmission between a transmitting component and a receiving component of one or different assemblies. According to the invention, the voltage level is increased step-wise or continuously until the required value for the correct representation of the signals to be transmitted is reached in the receiving component. Increase of the voltage level is stopped by the transmission of respective information. The inventive method and circuit are advantageous in that the minimum voltage level required for the transmission of data can be precisely adjusted. Power loss can be thereby reduced and adjacent channel interferences through high voltage levels can be reduced to a minimum.

Abstract: A touch probe 9 for a coordinate measuring apparatus is proposed which includes a touch probe chassis 29 adapted to be attached to the coordinate measuring apparatus, a support for the sensing stylus 39 which is mounted on the touch probe chassis 29 so as to be deflectable from a rest position and on which a sensing stylus 47 is mountable for contacting a workpiece 17, a deflection measuring system 55, 57 for detecting a deflection of the support for the sensing stylus 39 with respect to the touch probe chassis 29 and an inspection optics 61 for inspecting a tip 49 of the sensing stylus 47. The touch probe 1 is characterized in that at least one of the components support for the sensing stylus 39 and touch probe chassis 29 comprises a transverse support 39 which extends transversely to a direction of extension of the sensing stylus 47 and which is transparent to light in at least a portion thereof and which is disposed in a beam path 69 of the inspection optics 61.

Abstract: The switching network serves for the transmission of digital data signals within a broadband communication system. This switching network is thereby constructed of individual switching elements (KE) that form at least one multi-stage funnel due to a connection to one another. The section for the assemblies of the switching network is selected such that at least one complete funnel is accommodated on the respective assembly. The respective assembly thereby has its external data inputs provided with unidirectionally designed optical/electrical transducers (OML-E) and has its external data outputs provided with unidirectionally designed electrical/optical transducers (OML-S).

Abstract: A method and arrangement for the advantageous assembly of blocking capacitors for an integrated circuit. An integrated circuit includes a BGA housing having a plurality of preferably ball-shaped connector pins. A printed circuit board is also provided, having conductor paths to which the housing of the integrated circuit is electrically and mechanically contacted by means of the connector pins. At least one blocking capacitor is spatially arranged between two connector pins of the housing and also between the printed circuit board and housing of the integrated circuit.

Abstract: A touch probe 9 for a coordinate measuring apparatus is proposed which includes a touch probe chassis 29 adapted to be attached to the coordinate measuring apparatus, a support for the sensing stylus 39 which is mounted on the touch probe chassis 29 so as to be deflectable from a rest position and on which a sensing stylus 47 is mountable for contacting a workpiece 17, a deflection measuring system 55, 57 for detecting a deflection of the support for the sensing stylus 39 with respect to the touch probe chassis 29 and an inspection optics 61 for inspecting a tip 49 of the sensing stylus 47. The touch probe 1 is characterized in that at least one of the components support for the sensing stylus 39 and touch probe chassis 29 comprises a transverse support 39 which extends transversely to a direction of extension of the sensing stylus 47 and which is transparent to light in at least a portion thereof and which is disposed in a beam path 69 of the inspection optics 61.

Abstract: A device for transmitting high-frequency signals over data lines which are fixed on conventional circuit boards at a specific angle to optical fiber bundles forming the circuit boards.

Abstract: The invention relates to an opto-electric module, comprising a printed circuit board (L) which as an electrical interface has a number of plug-in contacts (SK) running parallel in the area of a first face for directly plugging the module into an assembly. As an optical interface, said printed circuit board is also connected to an optical element (OE) in the area of a second face. The component side and the back of said printed circuit board are also covered at least partly by a housing part (GK, KK).

Abstract: Reaction mixtures obtained by Beckmann rearrangement of cyclohexanone oxime with sulfuric acid or oleum are neutralized by a process which comprises the following steps:(a) mixing the reaction mixture with recycled ammonium sulfate mother liquor whose concentration is chosen so that no solid ammonium sulfate is precipitated during the neutralization,(b) neutralization by feeding gaseous ammonia which contains water or an aqueous ammonium sulfate solution in finely divided liquid form through a plurality of nozzle orifices into the solution of the reaction mixture in the ammonium sulfate mother liquor at elevated temperatures,(c) separation of crude lactam from the aqueous ammonium sulfate solution,(d) evaporation of the ammonium sulfate solution under reduced pressure and with separation of the crystalline ammonium sulfate from the ammonium sulfate mother liquor and(e) recycling of the ammonium sulfate mother liquor to stage a).

Abstract: Water-immiscible solvents are removed from offgases containing same by washing with water-containing caprolactam.

Abstract: Caprolactam is obtained by cleaving oligomers of caprolactam by a process in which the oligomers, in a liquid or solid state, are introduced into a fluidized alumina bed and cleaved at from 290.degree. to 400.degree. C. in the presence of steam, and, in addition to the amount of inert gas required to fluidize the alumina bed, from 0.1 to 3 times this amount of inert gas is introduced above the fluidized bed.

Abstract: In a process for continuously extracting caprolactam from an aqueous solution, containing caprolactam and its oligomers, with organic solvents, by introducing the aqueous solution into the upper part of an extraction zone and organic solvents into the lower part, and taking off a solution of caprolactam in organic solvents at the upper end and an aqueous phase containing caprolactam oligomers at the lower end, the improvement that liquid aromatic hydrocarbons are used and the extraction is carried out at a pH of from 2.0 to 6.0.

Abstract: A process for the preparation of caprolactam wherein, in a first stage, cyclohexanone-oxime is vaporized, in the presence of inert gases, by bringing it into contact with a fluidized bed of inert solid particles at from 150.degree. to 250.degree. C., and the mixture of cyclohexanone-oxime vapor and inert gases is passed into a second stage, where the cyclohexanone-oxime is rearranged to caprolactam at from 230.degree. to 450.degree. C. over a supported catalyst, containing boron trioxide, in a fluidized bed.

Abstract: A process for rapidly cooling gases which contain caprolactam vapor and which have been obtained by catalytic rearrangement of cyclohexanone-oxime in the gas phase in the presence of a supported catalyst containing boric acid, wherein a finely divided coolant at from 90.degree. to 200.degree. C. is fed into a cooling zone from above, gases which are at 330.degree.-400.degree. C. and contain caprolactam vapor are introduced radially at high speed through nozzle orifices over the downstream portion of the cooling zone, and are cooled to 100.degree.-200.degree. C. by thorough mixing with the finely divided coolant, and the cooled mixture is discharged.

Abstract: In a process for the preparation of .epsilon.-caprolactam by catalytic rearrangement of cyclohexanone-oxime in the gas phase at from 230.degree. to 450.degree. C. over a supported catalyst, containing boron trioxide, in a fluidized bed, wherein the catalyst is removed from the fluidized bed at the rate at which it becomes spent and is treated, in a fluidized state, with gases containing molecular oxygen at from 600.degree. to 900.degree. C., after which boron trioxide or boric acid is added to the fluidized catalyst, at from 300.degree. to 900.degree. C., before the catalyst is returned to the fluidized bed, the improvement that boron trioxide or boric acid of particle size from 0.05 to 1.5 mm is fed to the fluidized catalyst at one or more points.

Abstract: In a process for the continuous extraction of caprolactam from crude lactam by means of benzene in counter-current, in which crude lactam is fed into the upper part of an extraction zone and benzene into the lower part, a solution of caprolactam in benzene is taken off at the top and an aqueous solution containing impurities is taken off at the bottom, the improvement that water is additionally fed into the upper part of the extraction zone and a part of the aqueous solution, containing impurities, obtained at the bottom of the extraction zone is recycled into the extraction zone. Caprolactam is used for the manufacture of nylon.

Abstract: A process for obtaining coarsely crystalline pure ammonium sulfate from reaction mixtures which have been obtained by Beckmann rearrangement of cyclohexanone-oxime with sulfuric acid or oleum, by neutralizing the mixtures with ammonia at an elevated temperature, with the addition of recycled ammonium sulfate mother liquor, the concentration being so chosen that during the neutralization no solid ammonium sulfate precipitates, separating the crude caprolactam from the ammonium sulfate solution, crystallizing ammonium sulfate by evaporating the ammonium sulfate solution under reduced pressure, separating off the crystallized ammonium sulfate and recycling the mother liquor to the neutralization stage. The neutralization is carried out at from 80.degree. to 115.degree. C. under autogenous pressure and the ammonium sulfate solution obtained after separating off the crude lactam is evaporated under a pressure of from 200 to 600 mm Hg while cooling to from 72.degree. to 101.degree. C.

Abstract: Caprolactam is obtained by cleaving oligomers of caprolactam by a process in which the oligomers, in a liquid or solid state, are introduced into a fluidized alumina bed and cleaved at from 290.degree. to 400.degree. C. in the presence of steam, and, in addition to the amount of inert gas required to fluidize the alumina bed, from 0.1 to 3 times this amount of inert gas is introduced above the fluidized bed.