Patents by Inventor Waleed WAFA AL DAJANI

Waleed WAFA AL DAJANI has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).

  • Patent number: 11401252
    Abstract: The present invention relates to a method of producing furfural and extracting lignin from a hemi-cellulosic biomass solution comprising a total quantity of C5 sugars, comprising the steps of heating the hemi-cellulosic biomass solution to a temperature of at least about 200° C.; acidifying the hemi-cellulosic biomass solution with acid to produce the furfural in vapor phase; and condensing the furfural to recover furfural in solution, wherein the furfural is produced at a total molar yield of at least 70% of moles of furfural produced/the total moles C5 sugars present in the initial hemi-cellulosic biomass solution. Low molecular weight lignin can also be recovered from the hemi-cellulosic biomass solution prior to furfural production by membrane concentration, acidification, coagulation and filtration.
    Type: Grant
    Filed: April 20, 2017
    Date of Patent: August 2, 2022
    Assignee: FPInnovations
    Inventors: Naceur Jemaa, Adil Mazar, Waleed Wafa Al Dajani, Michael Paleologou
  • Publication number: 20210040273
    Abstract: Novel meltable lignin compositions having tailored compatibilities, moisture/water-resistant adhesion characteristics, and low to medium glass transition temperatures (30 to 120° C.) desirable for applications in the manufacturing of various products and the integration in the formulations of adhesives, coatings, plastics, composites and masterbatches, are obtained by blending at low temperatures (0-120° C.) dry lignins (0 to 10% moisture), in their hydrogen or protonated forms—hereby referred to as H-forms (pH=2.3-6.5 for a 10% aqueous suspension), with a reactive and/or interactive molecule or combination of molecules.
    Type: Application
    Filed: February 7, 2019
    Publication date: February 11, 2021
    Inventors: Makhlouf LALEG, Naceur JEMAA, Waleed WAFA AL DAJANI, Yaolin ZHANG, Michael PALEOLOGOU
  • Publication number: 20200325111
    Abstract: The present invention relates to a method of producing furfural and extracting lignin from a hemi-cellulosic biomass solution comprising a total quantity of C5 sugars, comprising the steps of heating the hemi-cellulosic biomass solution to a temperature of at least about 200° C.; acidifying the hemi-cellulosic biomass solution with acid to produce the furfural in vapor phase; and condensing the furfural to recover furfural in solution, wherein the furfural is produced at a total molar yield of at least 70% of moles of furfural produced/the total moles C5 sugars present in the initial hemi-cellulosic biomass solution. Low molecular weight lignin can also be recovered from the hemi-cellulosic biomass solution prior to furfural production by membrane concentration, acidification, coagulation and filtration.
    Type: Application
    Filed: April 20, 2017
    Publication date: October 15, 2020
    Applicant: FPInnovations
    Inventors: Naceur JEMAA, Adil MAZAR, Waleed WAFA AL DAJANI, Michael PALEOLOGOU
  • Patent number: 10266989
    Abstract: A process for producing cellulosic fiber with a high curl index is disclosed. The process can include mechanically treating and chemically crosslinking kraft pulp. The mechanical treatment of the pulp can include convolving and mechanically treating a pulp at in a plug screw and steam tube at temperatures above 100° C. and pressures above 3 bar. The mechanically treated pulp can be crosslinked with a crosslinking agent. The product fiber can exhibit a curl index of greater than 0.35, and can be at least 50% higher than the initial curl of the starting pulp material.
    Type: Grant
    Filed: April 1, 2016
    Date of Patent: April 23, 2019
    Assignee: Resolute FP US Inc.
    Inventors: Shaune Hanley, Mark Andrews, Frank Charbonneau, Gary Cothran, Reza Amiri, Rafik Allem, Waleed Wafa Al Dajani
  • Patent number: 9914948
    Abstract: The present disclosure relates to a process for extracting sugars from a pretreated lignocellulosic biomass. This process consists of contacting the pretreated lignocellulosic biomass with low charges of an aqueous peroxy acid (PA) solution to produce a liquid fraction (containing a small amount of lignin and hemicellulose degradation products) and a solid fraction containing cellulose, hemicellulose and lignin. The solid fraction can then be subjected to enzymatic hydrolysis with a variety of cell wall-degrading enzymes to produce a lignin-rich residue and a sugar solution that can be fermented to a variety of (bio)chemicals.
    Type: Grant
    Filed: March 1, 2016
    Date of Patent: March 13, 2018
    Assignee: FPInnovations
    Inventors: Luis Fernando Del Rio, Waleed Wafa Al Dajani, Changbin Mao, Zhirun Yuan
  • Publication number: 20160257982
    Abstract: The present disclosure relates to a process for extracting sugars from a pretreated lignocellulosic biomass. This process consists of contacting the pretreated lignocellulosic biomass with low charges of an aqueous peroxy acid (PA) solution to produce a liquid fraction (containing a small amount of lignin and hemicellulose degradation products) and a solid fraction containing cellulose, hemicellulose and lignin. The solid fraction can then be subjected to enzymatic hydrolysis with a variety of cell wall-degrading enzymes to produce a lignin-rich residue and a sugar solution that can be fermented to a variety of (bio)chem icals.
    Type: Application
    Filed: March 1, 2016
    Publication date: September 8, 2016
    Applicant: FPInnovations
    Inventors: Luis Fernando DEL RIO, Waleed WAFA AL DAJANI, Changbin MAO, Zhirun YUAN