Patents by Inventor Walter M. Kalback

Walter M. Kalback has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).

  • Patent number: 5538621
    Abstract: This invention relates to low melting solvated mesophase pitches which are suitable for spinning into carbon fibers. The solvated mesophase pitches have a lower melting point than conventional mesophase pitch but remain substantially anisotropic. The solvated mesophase can be produced as an intermediate during solvent fractionation or supercritical solvent fractionation of mesogen-containing isotropic pitches. The process is enhanced through the ability to recover pseudomesogens with an increased average molecular weight which, in combination with the solvent content, provides a fusible mesophase capable of being spun directly into infusible oriented anisotropic carbon fibers.
    Type: Grant
    Filed: July 28, 1994
    Date of Patent: July 23, 1996
    Assignee: Conoco Inc.
    Inventors: Walter M. Kalback, H. Ernest Romine, Xavier M. Bourrat
  • Patent number: 5259947
    Abstract: This invention relates to low melting solvated mesophase pitches which are suitable for spinning into carbon fibers. The solvated mesophase pitches have a lower melting point than conventional mesophase pitch but remain substantially anisotropic. The solvated mesophase can be produced as an intermediate during solvent fractionation or supercritical solvent fractionation of mesogen-containing isotropic pitches. The process is enhanced through the ability to recover pseudomesogens with an increased average molecular weight which, in combination with the solvent content, provides a fusible mesophase capable of being spun directly into infusible oriented anisotropic carbon fibers.
    Type: Grant
    Filed: September 19, 1991
    Date of Patent: November 9, 1993
    Assignee: Conoco Inc.
    Inventors: Walter M. Kalback, H. Ernest Romine, Xavier M. Bourrat
  • Patent number: 5198101
    Abstract: An improved process for producing an anisotropic pitch product suitable for carbon fiber manufacture. A metal alkylaryl sulfonate is combined with a carbonaceous feedstock substantially free of mesophase pitch, and the combination is heated for a period of time at an elevated temperature while passing a non-oxidative sparging gas such as nitrogen through the feedstock. The process is carried out for a sufficient period of time to produce an anisotropic pitch having from 50 to 100 percent by volume mesophase which is suitable for producing good quality carbon fibers.In one aspect of the invention, an oxidatively reactive gas is used as the sparging gas.
    Type: Grant
    Filed: December 13, 1991
    Date of Patent: March 30, 1993
    Assignee: Conoco Inc.
    Inventor: Walter M. Kalback
  • Patent number: 4904371
    Abstract: An improved process for producing an anisotropic pitch product suitable for carbon fiber manufacture. A carbonaceous feedstock substantially free of mesophase pitch is heated for a period of time at an elevated temperature while passing an oxidatively reactive sparging gas such as a mixture of oxygen and nitrogen through the feedstock. The oxidatively treated feedstock is then subjected to a heat soak, for a longer period of time in the absence of a sparging gas. Thereafter the heat soaked feedstock is heated at an elevated temperature in the presence of a non-oxidative sparging gas for a time period equal to or less than the heat soak to produce an anisotropic pitch having from 50 to 100% by volume mesophase which is suitable for producing good quality carbon fibers.
    Type: Grant
    Filed: October 13, 1988
    Date of Patent: February 27, 1990
    Assignee: Conoco Inc.
    Inventor: Walter M. Kalback