Patents by Inventor William R. Glace
William R. Glace has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).
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Publication number: 20030017435Abstract: A method and system for whitening teeth using at least a whitening gel, a whitening toothpaste, and a whitening rinse. Preferably the system employs a predetermined weight percentage of a peroxide based bleaching agent to effect tooth whitening. In certain formulations the components may use carbamide peroxide or hydrogen peroxide as a bleaching agent. The system may be used at home and preferably does not require clinical visits. The method includes the steps of brushing the teeth daily and before each bleaching with a whitening toothpaste, bleaching the teeth with a whitening gel twice daily, and rinsing with a whitening rinse. Daily brushing with a whitening toothpaste and preferably rinsing with a whitening rinse follow these whitening treatments. A system or kit for whitening teeth includes all of the components necessary to follow the aforementioned method, including a whitening gel, whitening toothpaste, a whitening rinse, and one or more mouth guard trays.Type: ApplicationFiled: July 18, 2001Publication date: January 23, 2003Inventors: Robert L. Ibsen, Kelly Smith-Reynolds, William R. Glace
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Patent number: 6331291Abstract: A thixotropic, smooth-flowing liquid, bulk-water-free dentifrice gel/paste that contains a stable mixture of at least one of amylopectin containing discrete solid particles and modified amylopectin containing discrete solid particles, uniformly suspended in and wetted by an inert essentially anhydrous organic hydroxylated liquid matrix material, and which dentifrice gel/paste is characterized by a high surface sheen. Preferably, the modified homopolysaccharide discrete particles contain esterified amylopectin and/or esterified amylose. The dentifrice gel/paste can be used as a toothpaste, a bleaching gel and a brushing gel.Type: GrantFiled: May 15, 1997Date of Patent: December 18, 2001Inventors: William R. Glace, Robert L. Ibsen, George A. Skoler
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Patent number: 6031016Abstract: A single package adhesive for tooth bonding application comprising a solvent-based homogeneous mixture ofa) an ethylenically unsaturated functional and hygroscopically functional monomer;b) an ethylenically unsaturated functional and hygroscopically functional coupling agent that is capable of (a) chemically reacting with and through the ethylenic bond of the ethylenically unsaturated functional monomer of 1) above and (b) chemically bonding to the surface to which the adhesive is applied;c) a poly-ethylenically unsaturated functional crosslinking agent that is capable of reacting with the monomer of 1) above and the coupling agent of 2) above; andd) a photoinitiator that induces addition polymerization of an ethylenically unsaturated compound.A method for forming a composite and composite structure are included that emply the single package adhesive.Type: GrantFiled: September 18, 1998Date of Patent: February 29, 2000Assignee: Den-Mat CorporationInventors: Robert L. Ibsen, William R. Glace
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Patent number: 5876743Abstract: A process for enhancing the(a) normal healing processes involving a live mammalian body of(i) injured non-dental-related soft tissue, and(ii) non-dental-related osseous material, and(b) for enhancing the biocompatibility and adhesion of bone and/or prosthetic device involved in a non-dental surgical or nonsurgical repair procedure, to ossified and non-ossified tissue components with which they are in contact, where there is an injury to either soft or hard tissue or a non-biocompatible prosthesis is placed in the body, that involves placing at the injury or on the prosthesisa) a primary coating that is a tenaciously-bonded hydrophilic water insoluble crosslinked resin coating,b) that optionally contains a measurable amount of a water/fluid leachable fluoride capable of (a) being leached from the coating in a metered amount, and (b) transporting a small amount of leached fluoride from the coating into the afflicted area ("the primary coating with fluoride").Type: GrantFiled: September 22, 1997Date of Patent: March 2, 1999Assignee: Den-Mat CorporationInventors: Robert L. Ibsen, William R. Glace
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Patent number: 5847020Abstract: A single package adhesive for tooth bonding application comprising a solvent-based homogeneous mixture ofa) an ethylenically unsaturated functional and hygroscopically functional monomer;b) an ethylenically unsaturated functional and hygroscopically functional coupling agent that is capable of (a) chemically reacting with and through the ethylenic bond of the ethylenically unsaturated functional monomer of 1) above and (b) chemically bonding to the surface to which the adhesive is applied;c) a poly-ethylenically unsaturated functional crosslinking agent that is capable of reacting with the monomer of 1) above and the coupling agent of 2) above; andd) a photoinitiator that induces addition polymerization of an ethylenically unsaturated compound.A method for forming a composite and composite structure are included that emply the single package adhesive.Type: GrantFiled: June 6, 1997Date of Patent: December 8, 1998Assignee: Den-Mat CorporationInventors: Robert L. Ibsen, William R. Glace
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Patent number: 5767170Abstract: A single package adhesive for tooth bonding applications which comprises a bulk-water-free solvent-based homogeneous liquid containing:1) An ethylenically unsaturated monomer that possesses a hygroscopic functional group that (a) is capable of chemically reacting with and through the ethylenic bond of the ethylenically unsaturated-functional monomer of 2) below, and (b) provides the capacity for chemical bonding to the surface to which the adhesive is applied.Type: GrantFiled: April 30, 1996Date of Patent: June 16, 1998Assignee: Den-Mat CorporationInventors: Robert L. Ibsen, Alan B. Matthews, William R. Glace
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Patent number: 5707610Abstract: An antibacterial oral hygiene composition in aqueous form comprising:(a) from about 0.05% to about 0.2% by weight of sodium benzoate;(b) from about 0.01% to about 1.0% by weight of a weak carboxylic acid;(c) from about 2.0% to about 5.0% by weight of a buffering agent capable of buffering the composition to a pH of about 3.0 to about 8.0;(d) from 0% to about 1.5% by weight of a surfactant;(e) from 0% to about 0.2% by weight of sodium saccharin, or an amount sufficient to provide a sweetening effect equivalent thereto of a sweetening agent;(f) from 0% to about 2.0% by weight of a flavoring agent; and(g) sufficient water to total 100%.Type: GrantFiled: May 30, 1995Date of Patent: January 13, 1998Assignee: Den-Mat CorporationInventors: Robert L. Ibsen, William R. Glace, Donald L. Pacropis
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Patent number: 5683249Abstract: In the process of implanting a metal dental prosthesis into or on the alveolar bone, to provide anchorage or stabilization either to a tooth or to another prosthesis, which involves surgical exposure of the alveolar bone, providing means for (a) fixing a metal implant in the alveolar bone, and (b) fixing the metal implant to either a tooth or to the other prosthesis, and closing the exposure of the alveolar bone, the improvement which comprises including in respect to such means the step of applying to one or more portions of the implant or to the locus of the implant in the alveolar bone, a primary coating comprising a crosslinked resin that (i) optionally contains leachable fluoride and (ii) is biocompatible with osseous and non-osseous tissue, to effect direct bonding of the implant to the tooth or to the prosthesis, or to bone or to non-osseous tissue or a combination of them. A treated prosthetic is also described.Type: GrantFiled: March 22, 1995Date of Patent: November 4, 1997Assignee: Den-Mat CorporationInventors: Robert L. Ibsen, William R. Glace, Donald R. Pacropis, deceased
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Patent number: 5334625Abstract: An adhesive composition useful for restoration comprising a finely-divided reinforcing filler, a polymerizable matrix material, a bonding agent, a coupling agent, and a thermal initiator.Type: GrantFiled: October 10, 1991Date of Patent: August 2, 1994Assignee: Den-Mat CorporationInventors: Robert L. Ibsen, Donald R. Pacropis, William R. Glace
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Patent number: 5151453Abstract: Two-part dental cement systems based on glass ionomers which are curable on exposure to light. The dental cement systems comprise a two-part blend of sodium N(p-tolyl)glycine-glycidyl methacrylate (Na NTG-GMA) and pyromellitic dianhydride-methyl methacrylate (PMDM) resins and glass ionomers.Type: GrantFiled: August 1, 1990Date of Patent: September 29, 1992Assignee: Den-Mat CorporationInventors: Robert L. Ibsen, Donald R. Pacropis, William R. Glace
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Patent number: 4986981Abstract: A toothpaste characterized by a low abrasion, non-reactive base formulation. The toothpaste has a near neutral or neutral pH. The toothpaste contains a concentration of citric acid, sodium or potassium citrate, papain, and fine-particle-sized aluminum oxide, in particular portions which effectively clean away plaque, mucin and tartar.Type: GrantFiled: July 12, 1989Date of Patent: January 22, 1991Assignee: Den Mat CorporationInventors: William R. Glace, Robert L. Ibsen
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Patent number: 4964911Abstract: A bonding adhesive for dentistry and a method for preparing the surface of dentin, enamel, or other natural or industrial substrates containing or capable of binding metallic ions, for adhesion of composite materials or resins. First, an aqueous solution of phosphoric acid or a mixture of phosphoric and nitric acids along with aluminum oxalate, or phosphoric acid alone, is applied to the surface.Type: GrantFiled: December 16, 1988Date of Patent: October 23, 1990Assignee: Den-Mat CorporationInventors: Robert L. Ibsen, Pacropis, Donald R., William R. Glace
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Patent number: 4859716Abstract: A microfilled dental composite containing from about 30% to about 60% filler. The filler being sub-micron hydrophobic silica particles of about 0.01-0.04 micrometers in diameter. The filler is dispersed in ethoxylated bisphenol A dimethacrylate resin containing suitable aliphatic dimethacrylate diluents up to about 40% by weight and curing agents effecting curing.Type: GrantFiled: November 6, 1987Date of Patent: August 22, 1989Assignee: Den-Mat CorporationInventors: Robert L. Ibsen, William R. Glace
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Patent number: 4738722Abstract: A buffered glass ionomer cement for dental use, including in combination, a mixture of a fine particle, 5-10 microns, powder consisting essentially by weight of______________________________________ silica 20-30% boron oxide 1-10% aluminum oxide 10-20% aluminum fluoride 1-10% calcium fluoride 30-40% phosphorus pentoxide 1-5% ammonium fluoride 1-10% ______________________________________plus five to twenty percent of the weight of the above of zinc oxide and zero to ten percent of titanium dioxide,anda liquid component comprising, by weight polyacrylic acid of low molecular weight, 40% solution in water--100-80% by weight, d-tartaric acid--0-20%. The powder and the liquid component are mixed together in a ratio of from 1:1 to 5:3 by weight.Type: GrantFiled: September 15, 1986Date of Patent: April 19, 1988Assignee: Den-Mat CorporationInventors: Robert L. Ibsen, William R. Glace, Donald R. Pacropis
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Patent number: 4674980Abstract: A filled-resin composition useful for porcelain repair and as a dental composite and therefore made up of non-toxic materials and a method for repairing porcelain or teeth. The composition comprises a methacrylate functional resin usable in dental composites, powdered filler-colorant therein, at least one photoinitiator for the resin in an amount sufficient to initiate polymerization and complete it in depth within about half a minute when exposed to a visible-light output of at least 5,000 foot candles, the photoinitiator being an exciplex of (1) an carbocyclic ketone or acetal and (2) either ethyl-4-dimethyl amino benzoate or ethyl-2-dimethyl amino benzoate, and at least one accelerator-free peroxide curing agent for the resin in an effective amount for completing polymerization within about one-half hour of any portion of the resin not receiving sufficient light to effectuate complete cure before then.Type: GrantFiled: September 22, 1983Date of Patent: June 23, 1987Assignee: Den-Mat, Inc.Inventors: Robert L. Ibsen, William R. Glace, Patricia A. Jensen
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Patent number: 4297266Abstract: A filled-resin dental composite. The filler is a mixture of hydrophobic silica particles about 0.01 to 0.04 micron in diameter and glass particles about 2 to 30 microns in diameter. Preferably, the glass is x-ray opaque. An improved method for restoring carious lesions in a living tooth is presented, using the composite.Type: GrantFiled: February 8, 1980Date of Patent: October 27, 1981Assignee: Den-Mat, Inc.Inventors: Robert L. Ibsen, William R. Glace
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Patent number: 4294349Abstract: A kit containing the components essential for repairing, in situ, damaged or fractured porcelain dental prostheses. Such repair includes cleaning, shaping, and priming the damaged area, applying a bonding agent preferably containing two silanes and a water-displacing solvent, then applying a filling agent comprising vitreous powder and a resin binder, allowing the agent to set and harden, and finishing.Type: GrantFiled: June 11, 1980Date of Patent: October 13, 1981Assignee: Den-Mat, Inc.Inventors: Robert L. Ibsen, William R. Glace
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Patent number: 4264489Abstract: A provisional crown-and-bridge resin comprising a liquid resin component and a powder component. The liquid resin component contains tetrahydrofurfuryl methacrylate as a major ingredient and is free from methyl methacrylate. It also contains an anti-oxidant and an accelerator. The powder component contains poly (ethyl methacrylate) as a major ingredient and a curing agent for the resin component. The powder is mixed with the resin shortly before application at a ratio of about two to about five parts of powder to one part of liquid resin by weight, to give a suitably flowing mixture. The resin component may also contain ethyl methacrylate as a major ingredient and may contain ethoxylated bisphenol A dimethacrylate as a major ingredient. The powder may include a substantial proportion of amorphous silica and preferably incorporates a substantial amount of X-ray opaque barium glass.Type: GrantFiled: January 14, 1980Date of Patent: April 28, 1981Assignee: Den-Mat, Inc.Inventors: Robert L. Ibsen, William R. Glace
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Patent number: RE33100Abstract: A buffered glass ionomer cement for dental use, including in combination, a mixture of a fine particle, 5-10 microns, powder consisting essentially by weight of______________________________________ silica 20-30% boron oxide 1-10% aluminum oxide 10-20% aluminum fluoride 1-10% calcium fluoride 30-40% phosphorus pentoxide .[.1-5%.]..Iadd.1-10%.Iaddend. ammonium fluoride .[.1-10%.]..Iadd.1-5%.Iaddend. ______________________________________plus five to twenty percent of the weight of the above of zinc oxide and zero to ten percent of titanium dioxide, anda liquid component comprising, by weight polyacrylic acid of low molecular weight, 40% solution in water--100-80% by weight, d-tartaric acid--0-20%. The powder and the liquid component are mixed together in a ratio of from 1:1 to 5:3 by weight.Type: GrantFiled: June 29, 1988Date of Patent: October 24, 1989Assignee: DEN-MAT CorporationInventors: Robert L. Ibsen, William R. Glace, Donald R. Pacropis
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Patent number: RE34937Abstract: A bonding adhesive for dentistry and a method for preparing the surface of dentin, enamel, or other natural or industrial substrates containing or capable of binding metallic ions, for adhesion of composite materials or resins. First, an aqueous solution of phosphoric acid or a mixture of phosphoric and nitric acids along with aluminum oxalate, or phosphoric acid alone, is applied to the surface. Second, a solution comprising a solvent and at least one compound selected from the group consisting of .[.(1) N-phenylglycine in a mixture with.]. the alkali metal .[.salt.]. .Iadd.salts .Iaddend.of (.Iadd.1) .Iaddend.N-phenylglycine, (2) .[.a mixture of.]. the adduct of .[.the alkali salts.]. N(p-tolyl)glycine and glycidyl methacrylate, .[.with the mixture N(p-tolyl)glycine and glycidyl methacrylate.]. (3) the addition reaction product .[.of the alkali metal salt.].Type: GrantFiled: October 22, 1992Date of Patent: May 16, 1995Assignee: Den-Mat CorporationInventors: Robert L. Ibsen, William R. Glace, Donald R. Pacropis