Abstract: An injection moulding process for making a toothbrush involving a stack mould assembly of at least three mould blocks (1, 2, 3, 4) arranged for use along a longitudinal stack axis (A—A), with two end mould blocks (3, 4), and an intermediate mould block (1, 2), with part mould cavities (11A, 21, 31, 41, 51) in the blocks. Plastic toothbrush skeletons are made in a cavity (11A, 21, 31) between the intermediate block (1, 2) and one end block (3), then elastomer parts are made in a cavity (41, 51) between the intermediate block (1, 2) and the other end block (4). Preferably the intermediate block (1) rotates so its part cavity (11A) faces the other end block (4). Stack mould assemblies (1, 2, 3, 4) for this process are provided. The assembly (1, 2, 3, 4) provides a compact mould with high output.

Abstract: A dental cleaning implement such as a toothbrush, having longitudinally disposed first and second parts flexibly joined together. Between the first and second parts is a rotatable member such that when the implement bends the first parts adjacent to the member bear upon the member. The rotatable member has circumferentially disposed relatively softer and harder regions, so that as the member is rotated the parts can be caused to bear compressibly upon selected softer or harder regions.

Abstract: A toothbrush having a head which carries a dental cleaning tool, and a grip handle, the head and handle being disposed along a longitudinal head-handle axis, the toothbrush having a resiliently flexible structure which can resiliently bend under the action of toothbrushing pressure and having adjustment means comprising a longitudinally moveable stiffening member which can be moved longitudinally into greater or lesser engagement with the resiliently flexible structure.

Abstract: The invention relates to modified recombinant allergen mutants which can be obtained from recombinant allergens which are derived from allergens which can be obtained by extraction from natural raw materials such as pollen of the species Phleum pratense. While these modified recombinant allergens stimulate lymphocytes from patients who are allergic to pollent to proliferate and synthesize cytokines, they exhibit a markedly diminished ability to bind to the IgE antibodies which are present in the serum of the T lymphocyte donors and to grass pollen allergen-specific IgEs and can therefore be used for a specific, made-to-release allergy therapy.

Abstract: A process for preparing acyloxybenzenesulfonates by reacting a carboxylic acid derivative with a salt of a phenolsulfonic acid in the presence of an antioxidant, preferably 2,6-di-tert-butyl-4-methylphenol. The addition of such antioxidants gives a product having a high color quality.

Abstract: A toothbrush head having elastomeric oral hygiene parts in the form of elastomeric strips aligned non-perpendicular to the length direction of the head. Preferably adjacent pairs of strips are linked to form a strip of “V” (32A, 32B) cross section. Preferably the head comprises flexibly linked segments (14, 15) and is flexibly linked to the toothbrush handle.

Abstract: A process for preparing acyloxybenzenesulfonates by reacting anhydrous phenolsulfonates with carboxylic acid derivatives comprises conducting the reaction with a salt of a phenolsulfonic acid which has a water content of less than 0.5% by weight and has been contacted with a substance having basic properties.

Abstract: A process for preparing acyloxybenzenesulfonates by reacting a carboxylic acid derivative with a salt of a phenolsulfonic acid in the presence of an antioxidant, preferably 2,6-di-tert-butyl-4-methylphenol. The addition of such antioxidants gives a product having a high color quality.

Abstract: The invention relates to a process for the preparation of acyloxybenzenesulfonates starting from carbonyl halides and salts of phenolsulfonic acid which have a low water content. Surprisingly, it was discovered that acyloxybenzenesulfonates can be prepared in high yields and good grades, irrespective of the grade or reactivity of the phenolsulfonic acid derivative, if the reaction of the phenolsulfonic acid with an alkanecarboxylic acid derivative is carried out in an aliphatic or aromatic solvent in the presence of 0.5 to 25% by weight of a polyglycol ether.

Abstract: The invention relates to a process for the preparation of acyloxybenzenesulfonates starting from carbonyl halides and salts of phenolsulfonic acid which have a low water content. Surprisingly, it was discovered that acyloxybenzenesulfonates can be prepared in high yields and good grades, irrespective of the grade or reactivity of the phenolsulfonic acid derivative, if the reaction of the phenolsulfonic acid with an alkanecarboxylic acid derivative is carried out in an aliphatic or aromatic solvent in the presence of 0.5 to 25% by weight of a polyglycol ether.

Abstract: A process for preparing acyloxybenzenesulfonates by reacting anhydrous phenolsulfonates with carboxylic acid derivatives comprises conducting the reaction with a salt of a phenolsulfonic acid which has a water content of less than 0.5% by weight and has been contacted with a substance having basic properties.

Abstract: An injection moulding process for making a toothbrush involving a stack mould assembly of at least three mould blocks (1, 2, 3, 4) arranged for use along a longitudinal stack axis (A-A), with two end mould blocks (3, 4), and an intermediate mould block (1, 2), with part mould cavities (11A, 21, 31, 41, 51) in the blocks. Plastic toothbrush skeletons are made in a cavity (11A, 21, 31) between the intermediate block (1, 2) and one end block (3), then elastomer parts are made in a cavity (41, 51) between the intermediate block (1, 2) and the other end block (4). Preferably the intermediate block (1) rotates so its part cavity (11A) faces the other end block (4). Stack mould assemblies (1, 2, 3, 4) for this process are provided. The assembly (1, 2, 3, 4) provides a compact mould with high output.

Abstract: This invention discloses an improved method for making salts of acylisethionates using a direct esterification of a fatty acid with one or more salts of a selected hydroxyalkanesulfonic acid in the presence of a catalyst selected from the described group. This method may be used at temperatures below 200 degrees C.