Patents by Inventor Wolfgang Loth
Wolfgang Loth has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).
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Patent number: 9120731Abstract: What is proposed is a process for preparing polyether alcohols by conversion of the following reactants: a) one or more alkylene oxides and optionally carbon dioxide and b) one or more H-functional starter substances, in the presence of a catalyst, to form a liquid reaction mixture, in a reaction unit (1), which is characterized in that the reaction unit (1) has internals (2) which form a multitude of microstructured flow channels which bring about multiple splitting of the liquid reaction mixture into component flow paths and recombination thereof in altered arrangement, the multiple splitting and recombination being repeated several times and the microstructured flow channels having a characteristic dimension which is defined as the greatest possible distance of any particle in the liquid reaction mixture from the wall of a flow channel closest to the particle, in the range from 20 to 10 000 ?m, the result being that the flow profile of the liquid reaction mixture approximates to ideal plug flow as a resultType: GrantFiled: August 8, 2011Date of Patent: September 1, 2015Assignee: BASF SEInventors: Achim Loeffler, Michael Stoesser, Wolfgang Loth, Ralf Boehling, Sirus Zarbakhsh
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Patent number: 9108172Abstract: The present invention relates to a method for the continuous production of a polymer by radical polymerization, wherein at least three materials are mixed with microstructures in one or more mixers and are then polymerized in at least one reaction zone.Type: GrantFiled: September 3, 2013Date of Patent: August 18, 2015Assignee: BASF SEInventors: Wolfgang Mattmann, Wolfgang Loth, Bolette Urtel, Elke Gütlich-Hauk, Christian Hubert Weidl, Andreas Daiβ
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Patent number: 9068023Abstract: The invention relates to a continuous process for the preparation of amphiphilic graft polymers, wherein a vinyl ester component (B) composed of vinyl acetate and/or vinyl propionate (B1) and, if desired, a further ethylenically unsaturated monomer (B2), is polymerized in the presence of a polyalkylene oxide (A), a free radical-forming initiator (C) and, if desired, an additive (D), at a mean polymerization temperature at which the initiator (C) has a decomposition half-time of from 1 to 500 min, in at least one tubular reactor segment with a feed side and an outlet side, through which the reaction mixture comprising at least a part of component (A) to (C), and if desired (D), streams, a tubular reactor segment and the use of the inventive amphiphilic graft polymer. The invention further relates to an inventive amphiphilic graft polymer and the use thereof.Type: GrantFiled: March 7, 2013Date of Patent: June 30, 2015Assignee: BASF SEInventors: Faissal-Ali El-Toufaili, Michaela Heussler, Christian Schwede, Aaron Flores-Figueroa, Rainer Dobrawa, Dieter Boeckh, Wolfgang Loth, Gerd Konrad
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Patent number: 9056926Abstract: A process for preparing aqueous solutions of homo- or copolymers of acrylic acid by means of free-radical polymerization of acrylic acid and optionally water-soluble, monoethylenically unsaturated comonomers in an aqueous medium in the presence of at least one water-soluble initiator and of at least one water-soluble regulator, wherein the polymerization is conducted by means of a continuous process, and wherein, after the polymerization, low molecular weight components are at least partly removed from the resulting aqueous polymer solution. For the polymerization, preference is given to using microstructured mixers and reactors. Preference is given to using at least one reactor and/or mixer with microstructures for the process.Type: GrantFiled: November 2, 2010Date of Patent: June 16, 2015Assignee: BASF SEInventors: Matthias Kleiner, Wolfgang Loth, Markus Brym, Elke Gütlich-Hauk, Bolette Urtel, Ruth Wirschem, Jürgen Detering
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Patent number: 8969493Abstract: The present invention relates to a process and to an apparatus for continuous living polymerization of cationically polymerizable monomers, in which at least three feedstocks are mixed in one or more mixers with microstructures and then polymerized in at least one reaction zone.Type: GrantFiled: April 30, 2009Date of Patent: March 3, 2015Assignee: BASF SEInventors: Wolfgang Mattmann, Wolfgang Loth, Phillip Hanefeld, Elke Guetlich-Hauk, Thomas Wettling, Andreas Daiss
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Patent number: 8703879Abstract: A continuous process for the multistage drying and postcondensation of polyamide pellets in the solid phase comprises 1) carrying out the predrying process in a continuous drying apparatus which is operated in countercurrent mode or in crossflow mode with inert gas or steam, or with a mixture of inert gas and steam, using a pellet temperature in the range from 70 to 200° C., and 2) Carrying out the subsequent continuous postcondensation process in a separate vertical duct with moving bed at a pellet temperature in the range from 120 to 210° C., where the duct is operated in countercurrent mode with inert gas or steam, or with a mixture of inert gas and steam, the inert gas is introduced at least two sites along the duct, and from 15 to 90% of the inert gas is introduced at the base of the vertical duct and from 10 to 85% of the inert gas is introduced in the upper half below the surface of the pellets.Type: GrantFiled: June 19, 2009Date of Patent: April 22, 2014Assignee: BASF SEInventors: Wolfgang Loth, Faissal-Ali El-Toufaili, Achim Stammer, Gad Kory, Achim Gerstlauer, Jens Becker
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Publication number: 20140088280Abstract: The present invention relates to a method for the continuous production of a polymer by radical polymerization, wherein at least three materials are mixed with microstructures in one or more mixers and are then polymerized in at least one reaction zone.Type: ApplicationFiled: September 3, 2013Publication date: March 27, 2014Applicant: BASF SEInventors: Wolfgang Mattmann, Wolfgang Loth, Bolette Urtel, Elke Gütlich-Hauk, Christian Hubert Weidl, Andreas Daiß
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Patent number: 8546468Abstract: The present invention relates to a method for the continuous production of a polymer by radical polymerization, wherein at least three materials are mixed with microstructures in one or more mixers and are then polymerized in at least one reaction zone.Type: GrantFiled: April 30, 2009Date of Patent: October 1, 2013Assignee: BASF SEInventors: Wolfgang Mattmann, Wolfgang Loth, Bolette Urtel, Elke Guetlich-Hauk, Christian Hubert Weidl, Andreas Daisse
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Publication number: 20130253089Abstract: The invention relates to a continuous process for the preparation of amphiphilic graft polymers, wherein a vinyl ester component (B) composed of vinyl acetate and/or vinyl propionate (B1) and, if desired, a further ethylenically unsaturated monomer (B2), is polymerized in the presence of a polyalkylene oxide (A), a free radical-forming initiator (C) and, if desired, an additive (D), at a mean polymerization temperature at which the initiator (C) has a decomposition half-time of from 1 to 500 min, in at least one tubular reactor segment with a feed side and an outlet side, through which the reaction mixture comprising at least a part of component (A) to (C), and if desired (D), streams, a tubular reactor segment and the use of the inventive amphiphilic graft polymer. The invention further relates to an inventive amphiphilic graft polymer and the use thereof.Type: ApplicationFiled: March 7, 2013Publication date: September 26, 2013Applicant: BASF SEInventors: Faissal-Ali El-Toufaili, Michaela Heussler, Christian Schwede, Aaron Flores-Figueroa, Rainer Dobrawa, Dieter Boeckh, Wolfgang Loth, Gerd Konrad
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Publication number: 20130131389Abstract: What is proposed is a process for preparing polyether alcohols by conversion of the following reactants: a) one or more alkylene oxides and optionally carbon dioxide and b) one or more H-functional starter substances, in the presence of a catalyst, to form a liquid reaction mixture, in a reaction unit (1), which is characterized in that the reaction unit (1) has internals (2) which form a multitude of microstructured flow channels which bring about multiple splitting of the liquid reaction mixture into component flow paths and recombination thereof in altered arrangement, the multiple splitting and recombination being repeated several times and the microstructured flow channels having a characteristic dimension which is defined as the greatest possible distance of any particle in the liquid reaction mixture from the wall of a flow channel closest to the particle, in the range from 20 to 10 000 ?m, the result being that the flow profile of the liquid reaction mixture approximates to ideal plug flow as a resultType: ApplicationFiled: August 8, 2011Publication date: May 23, 2013Applicant: BASF SEInventors: Achim Loeffler, Michael Stoesser, Wolfgang Loth, Ralf Boehling, Sirus Zarbakhsh
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Publication number: 20120214941Abstract: A process for preparing aqueous solutions of homo- or copolymers of acrylic acid by means of free-radical polymerization of acrylic acid and optionally water-soluble, monoethylenically unsaturated comonomers in an aqueous medium in the presence of at least one water-soluble initiator and of at least one water-soluble regulator, wherein the polymerization is conducted by means of a continuous process, and wherein, after the polymerization, low molecular weight components are at least partly removed from the resulting aqueous polymer solution. For the polymerization, preference is given to using microstructured mixers and reactors. Preference is given to using at least one reactor and/or mixer with microstructures for the process.Type: ApplicationFiled: November 2, 2010Publication date: August 23, 2012Applicant: BASF SEInventors: Matthias Kleiner, Wolfgang Loth, Markus Brym, Elke Gütlich-Hauk, Bolette Urtel, Ruth Wirschem, Jürgen Detering
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Patent number: 8211987Abstract: The present invention relates to a method for reducing residual volatiles from polymer compositions.Type: GrantFiled: April 12, 2011Date of Patent: July 3, 2012Assignee: BASF SEInventors: Fatemeh Ahmadnian, Wolfgang Loth, Karl-Heinz Wassmer, Andreas Brodhagen, Gerd Konrad
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Publication number: 20110251345Abstract: The present invention relates to a method for reducing residual volatiles from polymer compositions.Type: ApplicationFiled: April 12, 2011Publication date: October 13, 2011Applicant: BASF SEInventors: Fatemeh AHMADNIAN, Wolfgang LOTH, Karl-Heinz WASSMER, Andreas BRODHAGEN, Gerd KONRAD
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Patent number: 8034980Abstract: A process for preparing polyether polyols by reaction of the following starting materials: a) one or more alkylene oxides and, if appropriate, carbon dioxide and also b) one or more H-functional starter substances, in the presence of a catalyst, in a reaction unit having a plurality of parallel layers A, B which are microstructured so that each layer has a multiplicity of channels which are arranged parallel to one another and form a continuous flow path from one side of the plate to the opposite side of this, wherein a distribution device for introduction of the starting materials and the catalyst is provided at one end of the channels of the layers A and a collection device for the reaction mixture is provided at the other end of these is proposed.Type: GrantFiled: May 22, 2007Date of Patent: October 11, 2011Assignee: BASF AktiengesellschaftInventors: Achim Loeffler, Wolfgang Loth, Ralf Boehling, Thomas Ostrowski, Michael Stoesser, Hartwig Voss, Axel Schimpf
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Publication number: 20110092645Abstract: A continuous process for the multistage drying and postcondensation of polyamide pellets in the solid phase comprises 1) carrying out the predrying process in a continuous drying apparatus which is operated in countercurrent mode or in crossflow mode with inert gas or steam, or with a mixture of inert gas and steam, using a pellet temperature in the range from 70 to 200° C., and 2) Carrying out the subsequent continuous postcondensation process in a separate vertical duct with moving bed at a pellet temperature in the range from 120 to 210° C., where the duct is operated in countercurrent mode with inert gas or steam, or with a mixture of inert gas and steam, the inert gas is introduced at least two sites along the duct, and from 15 to 90% of the inert gas is introduced at the base of the vertical duct and from 10 to 85% of the inert gas is introduced in the upper half below the surface of the pellets.Type: ApplicationFiled: June 19, 2009Publication date: April 21, 2011Applicant: BASF SEInventors: Wolfgang Loth, Faissal-Ali El-Toufaili, Achim Stammer, Gad Kory, Achim Gerstlauer, Jens Becker
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Publication number: 20110054071Abstract: The present invention relates to a method for the continuous production of a polymer by radical polymerization, wherein at least three materials are mixed with microstructures in one or more mixers and are then polymerized in at least one reaction zone.Type: ApplicationFiled: April 30, 2009Publication date: March 3, 2011Applicant: BASF SEInventors: Wolfgang Mattmann, Wolfgang Loth, Bolette Urtel, Elke Guetlich-Hauk, Christian Hubert Weidl, Andreas Daisse
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Publication number: 20110028666Abstract: The present invention relates to a process and to an apparatus for continuous living polymerization of cationically polymerizable monomers, in which at least three feedstocks are mixed in one or more mixers with microstructures and then polymerized in at least one reaction zone.Type: ApplicationFiled: April 30, 2009Publication date: February 3, 2011Applicant: BASF SEInventors: Wolfgang Mattmann, Wolfgang Loth, Phillip Hanefeld, Elke Guetlich-hauk, Thomas Wettling, Andreas Daiss
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Publication number: 20100168348Abstract: The invention relates to a process for continuously preparing styrene polymers by anionic spray polymerization, which comprises i) styrene and the initiator solution being mixed in a dynamic or static mixer and then the mixture being sprayed, ii) the resultant droplets passing from the liquid monomer state to the melted polymer state during their free fall in the spraying tower, iii) the melt droplets being collected as a melt at the foot of the tower, the melt having a monomer content of below 1%, preferably below 0.1% (<1000 ppm), and being discharged by suitable means.Type: ApplicationFiled: August 1, 2006Publication date: July 1, 2010Applicant: BASF AKTIENGESELLSCHAFTInventors: Wolfgang Loth, Volker Seidl, Stefan Bruhns, Klaus-Dieter Hungenberg, Juergen Koch, Christian Schade, Claudius Schwittay
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Publication number: 20090203874Abstract: A process for preparing polyether polyols by reaction of the following starting materials: a) one or more alkylene oxides and, if appropriate, carbon dioxide and also b) one or more H-functional starter substances, in the presence of a catalyst, in a reaction unit having a plurality of parallel layers A, B which are microstructured so that each layer has a multiplicity of channels which are arranged parallel to one another and form a continuous flow path from one side of the plate to the opposite side of this, wherein a distribution device for introduction of the starting materials and the catalyst is provided at one end of the channels of the layers A and a collection device for the reaction mixture is provided at the other end of these is proposed.Type: ApplicationFiled: May 22, 2007Publication date: August 13, 2009Applicant: BASF SEInventors: Achim Löffler, Wolfgang Loth, Ralf Böhling, Thomas Ostrowski, Michael Stösser, Hartwig Voss, Axel Schimpf
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Patent number: 6815527Abstract: The continuous process for preparing a polyamide by reacting at least one aminonitrile with water comprises: (1) reacting at least one aminonitrile with water in the presence of an organic liquid diluent at from 90 to 400° C. and from 0.1 to 35×106 Pa in a flow tube containing a Brönsted acid catalyst selected from a beta-zeolite catalyst, a sheet-silicate catalyst or a titanium dioxide catalyst comprising from 70 to 100% by weight of anatase and from 0 to 30% by weight of rutile and in which up to 40% by weight of the titanium dioxide may be replaced by tungsten oxide, to obtain a reaction mixture, (2) further reacting the reaction mixture at from 150 to 400° C.Type: GrantFiled: January 10, 2003Date of Patent: November 9, 2004Assignee: BASF AktiengesellschaftInventors: Peter Bassler, Helmut Winterling, Rolf-Hartmuth Fischer, Wolfgang Loth