Abstract: The present disclosure provides a method of manufacturing a bonding structural test block with defects. The method of manufacturing the bonding structural test block with defects includes: providing a first plate and a second plate; applying an adhesive on an upper surface of the first plate to form an adhesive layer; heating and curing at least partial region of the adhesive layer for the first time; placing the second plate on the adhesive layer; and heating and curing the adhesive layer for the second time to form a boding structural test block. According to the present disclosure, the at least partial region of the adhesive layer is heated and cured for the first time and chemical reaction occurs, so that the at least partial region forms a defect, and controllable manufacturing of the defect is realized. The test block with the defect is subjected to mechanical detection to simulate the actual defective product.

Abstract: The present invention relates to a method for purifying key intermediates of Citalopram, i.e. 4-[4-(dimethylamino)-1-(4-fluorophenyl)-1-hydroxybutyl]-3-hydroxymethylbenzonitrile and a salt thereof. The method comprises dissolving crude 4-[4-(dimethylamino)-1-(4-fluorophenyl)-1-hydroxybutyl]-3-hydroxymethylbenzonitrile (compound of formula I containing formaldehyde impurity) with an organic solvent, adding a washing solution, controlling the temperature, stirring, leaving to stand for layering, and removing the aqueous layer, so as to obtain a purified organic solution of 4-[4-(dimethylamino)-1-(4-fluorophenyl)-1-hydroxybutyl]-3-hydroxymethylbenzonitrile. The method provided by the present invention can effectively remove aldehyde group-containing impurities in the intermediate. The method of the present invention has the advantages of simple operation, cheap raw materials and mild conditions, and is suitable for large-scale industrial production.

Abstract: The provided is a process for separating by absorption the pyrolysis gas from preparation of lower carbon olefins, wherein a primary absorbent and a secondary absorbent are introduced into the demethanizer to separate by absorption the feedstock of the demethanizer through countercurrent contact therewith at a moderate temperature and pressure, thereby to obtain a top fraction primarily comprising hydrogen and methane and a bottom fraction primarily comprising the absorbents and C2+ fraction, wherein the primary absorbent essentially is a mixed Cn or Cn+ fraction, the secondary absorbent essentially is a Cn? alkane fraction or mixed Cn? or Cn?+ fraction, and wherein n and n? are independently 3, 4 or 5 with the proviso when the secondary absorbent is a mixed fraction, n? is not 3.

Abstract: The provided is a process for separating by absorption the pyrolysis gas from preparation of lower carbon olefins, wherein a primary absorbent and a secondary absorbent are introduced into the demethanizer to separate by absorption the feedstock of the demethanizer through countercurrent contact therewith at a moderate temperature and pressure, thereby to obtain a top fraction primarily comprising hydrogen and methane and a bottom fraction primarily comprising the absorbents and C2+ fraction, wherein the primary absorbent essentially is a mixed Cn or Cn+ fraction, the secondary absorbent essentially is a Cn? alkane fraction or mixed Cn? or Cn?+ fraction, and wherein n and n? are independently 3, 4 or 5 with the proviso when the secondary absorbent is a mixed fraction, n? is not 3.