Patents by Inventor XIANWEN LI

XIANWEN LI has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).

  • Patent number: 11313192
    Abstract: The present invention discloses a method for lowering an oil pipe in a gas well without well-killing, a soluble bridge plug and a material preparation method thereof, wherein, the method comprises the steps of: lowering a bridge plug in a wellbore such that the bridge plug blocks the wellbore at a predetermined location in the wellbore; injecting water in the wellbore after the pressure in the wellbore has been relieved so as to replace gases in the wellbore; and lowering an oil pipe in the wellbore to the location of the bridge plug. The method for lowering an oil pipe in a gas well without well-killing, the soluble bridge plug and the material preparation method thereof provided in the present invention successfully solve the problem of high cost for lowering an oil pipe under pressure after a fracturing fluid has been injected into the casing.
    Type: Grant
    Filed: April 4, 2018
    Date of Patent: April 26, 2022
    Inventors: Xianwen Li, Qiaorong Han, Yanming Zhang, Xu Ma, Zhanguo Ma, Yangming Hu, Changjing Zhou, Yuanxiang Xiao, Huaqiang Shi, Baochun Chen, Yonghong Gu, Xiaoyong Wen, Xuan'ang Lai, Yong Ding, Liang Ye, Qianyun Zhao, Xinxing Ma, Yajuan Wang, Man Bi, Hua Shi, Mingfang He, Xiaorui Liu, Wei Gao, Hongying Li, Yun Ling, Ruifen Hao, Lei Shen, Guohui Su, Shaowei Zhou, Shusheng Li, Zhe Li
  • Patent number: 10975294
    Abstract: An injection stimulation agent for water injection well and the preparation method and application thereof are described. The raw material composition of the injection stimulation agent for water injection well comprises: 5.0%-10.0% of sulfamic acid, 10.0%-20.0% of methanol, 10.0%-20.0% of tartaric acid, 10.0%-20.0% of ethylenediamine tetramethylene phosphoric acid, 5.0%-10.0% of sodium polyacrylate, 5.0%-8.0% of cocoyl hydroxyethyl sulfonic acid and the balance of water. Embodiments include a preparation method of the above injection stimulation agent. The injection stimulation agent for water injection well can be used in acidizing treatment process of the reservoir, and can be used directly. The injection stimulation agent can play the role of shrinking swelled clay at the same time of dissolving scale, and finally achieve the purpose of depressurization and enhanced production.
    Type: Grant
    Filed: December 21, 2018
    Date of Patent: April 13, 2021
    Inventors: Lijun Mu, Xianwen Li, Hongjun Lu, Yong Wang, Bin Yao, Zhenning Ji, Suiwang Zhang, Xiaobing Lu, Zhaojie Song, Lei Sui, Zhiying Deng, Erzhen Wang, Wei Wang, Juntao Wang
  • Patent number: 10961442
    Abstract: On-line diverting acids for continuous injection into water injection wells and methods of preparing the diverting acid are disclosed. The on-line diverting acids have a raw material composition of: 5.0-25.0% of hydrochloric acid, 3.0%-6.0% of ammonium fluoride, 4.0%-8.0% of a diverting agent, 3.0%-7.0% of a chelating agent, 1.0-3.0% of a corrosion inhibitor, 1.0-3.0% of an anti-swelling/swelled-clay-shrinking agent and a balance of water. The on-line diverting acids can remove plugging from deep zones of high and low permeability layers, and can be continuously injected to simplify the construction process, to achieve the purpose of reducing the pressure and stimulating the injection.
    Type: Grant
    Filed: January 4, 2019
    Date of Patent: March 30, 2021
    Assignee: PetroChina Company Limited
    Inventors: Lijun Mu, Xianwen Li, Hongjun Lu, Zhiying Deng, Yong Wang, Bin Yao, Zhenning Ji, Suiwang Zhang, Xiaobing Lu, Zhaojie Song, Lei Sui, Erzhen Wang
  • Patent number: 10920127
    Abstract: The present invention provides a method for in-depth profile control and displacement of low-permeability oil reservoirs, comprising: sequentially injecting a flexible and elastic particle-containing pre-slug, a polymer microsphere-containing main slug and a flexible and elastic particle-containing protective slug into an oil layer, and the three slugs have a volume ratio of total injection amount of 1-2:6-8:1-2. The invention provides a method for in-depth profile control and displacement by using styrene-based flexible and elastic particles in combination with the polyacrylamide polymer microsphere, wherein the flexible elastic particles can block cracks and large pore channels of the oil layer, and the polymer microsphere can displace the remaining oil in the oil layer. In the present invention, different slugs of profile control and displacement system are combined to achieve the objective of blocking cracks and large pore channels, displacing crude oil, and improving oil well recovery.
    Type: Grant
    Filed: January 18, 2019
    Date of Patent: February 16, 2021
    Assignee: PETROCHINA COMPANY LIMITED
    Inventors: Tianjiang Wu, Mingke Zheng, Xianwen Li, Haien Yang, Xiaorong Li, Fan Tang, Fangfang Xue, Ronghuan Chen, Rong Zhang, Lijun Zheng, Chunmei Xu, Baoche Liu, Ping Yi, Jiajie Zhu, Weiyu Bi
  • Patent number: 10876043
    Abstract: A chelating agent may be used for reservoir acidification and stimulating injection. The raw material composition of the chelating agent comprises: 10.0%-20.0% of methanesulfonic acid, 10.0%-20.0% of methanol, 10.0%-20.0% of polyaspartic acid, 10.0%-15.0% of epoxy succinic acid, 5.0%-10.0% of sodium cetyl sulfonate, 10.0%-15.0% of cetyltrimethylammonium bromide and the balance of water. The present disclosure also provides a preparation method of the above chelating agent. The chelating agent for reservoir acidification and stimulating injection may be used in an acidizing and stimulating injection process, wherein it can effectively dissolve rock cracks, be used directly without need to be reversed.
    Type: Grant
    Filed: January 23, 2019
    Date of Patent: December 29, 2020
    Assignee: PetroChina Company Limited
    Inventors: Lijun Mu, Xianwen Li, Hongjun Lu, Yong Wang, Bin Yao, Zhenning Ji, Suiwang Zhang, Xiaobing Lu, Zhiying Deng, Lei SUi, Erzhen Wang, Zhaojie Song
  • Patent number: 10781165
    Abstract: Disclosed are a pH-responsive amphoteric surfactant N-lauryl-(?-alkyl)-?-aminopropionic acid and a preparation method and uses thereof. An alkylamine and a solvent are added to a three-necked flask, stirred for complete dissolution, slowly dropwise added with methyl ?-alkyl-acrylate and reacted at room temperature after the ice-water bath is removed. The reaction mixture is refluxed in water bath and evaporated under rotation to remove the solvent and the residual methyl ?-alkyl-acrylate to give N-lauryl-(?-alkyl)-?-aminopropionic acid. Then N-lauryl-(?-alkyl)-?-aminopropionic acid and water are added to a three-necked flask, slowly dropwise added with a sodium hydroxide solution and reacted in water bath to give a crude product, which is filtered and dried to give a purified surfactant sodium N-lauryl-(?-alkyl)-?-aminopropionate. This surfactant is suitable for the foamed acid system and its performance can be switched by adjusting pH due to pH sensitivity.
    Type: Grant
    Filed: June 18, 2019
    Date of Patent: September 22, 2020
    Assignee: Shaanxi University of Science & Technology
    Inventors: Xiaojuan Lai, Zhiqiang Dang, Lei Wang, Shaoyun Ma, Xianwen Li, Wei Tian, Xingen Feng, Yinyin Zhang, Xu Yang
  • Patent number: 10661675
    Abstract: The disclosure provides an Internet-based intelligent mobile charging system and method. The system includes a rescue vehicle APP, a charging rescue vehicle, a rescued vehicle APP and a rescue platform. The rescue vehicle APP includes a first user module, a first order module, a monitoring module and a first communication module; the charging rescue vehicle includes a controller, a global position system (GPS) device, a direct-current charger, an alternative-current charger and a metering module; the rescued vehicle APP includes a second user module, a second order module, a payment module and a second communication module; the rescue platform includes an access module, an order execution module, a vehicle screening module, a rescue vehicle monitoring module, a bill management module and a user certification module.
    Type: Grant
    Filed: June 6, 2018
    Date of Patent: May 26, 2020
    Inventors: Xuekun Yu, Deng Hu, Xianwen Li, Shen Wang
  • Publication number: 20200040682
    Abstract: The present invention discloses a method for lowering an oil pipe in a gas well without well-killing, a soluble bridge plug and a material preparation method thereof, wherein, the method comprises the steps of: lowering a bridge plug in a wellbore such that the bridge plug blocks the wellbore at a predetermined location in the wellbore; injecting water in the wellbore after the pressure in the wellbore has been relieved so as to replace gases in the wellbore; and lowering an oil pipe in the wellbore to the location of the bridge plug. The method for lowering an oil pipe in a gas well without well-killing, the soluble bridge plug and the material preparation method thereof provided in the present invention successfully solve the problem of high cost for lowering an oil pipe under pressure after a fracturing fluid has been injected into the casing.
    Type: Application
    Filed: April 4, 2018
    Publication date: February 6, 2020
    Inventors: Xianwen Li, Qiaorong Han, Yanming Zhang, Xu Ma, Zhanguo Ma, Yangming Hu, Changjing Zhou, Yuanxiang Xiao, Huaqiang Shi, Baochun Chen, Yonghong Gu, Xiaoyong Wen, Xuan'ang Lai, Yong Ding, Liang Ye, Qianyun Zhao, Xinxing Ma, Yajuan Wang, Man Bi, Hua Shi, Mingfang He, Xiaorui Liu, Wei Gao, Hongying Li, Yun Ling, Ruifen Hao, Lei Shen, Guohui Su, Shaowei Zhou, Shusheng Li, Zhe Li
  • Publication number: 20190388858
    Abstract: Disclosed are a pH-responsive amphoteric surfactant N-lauryl-(?-alkyl)-?-aminopropionic acid and a preparation method and uses thereof. An alkylamine and a solvent are added to a three-necked flask, stirred for complete dissolution, slowly dropwise added with methyl ?-alkyl-acrylate and reacted at room temperature after the ice-water bath is removed. The reaction mixture is refluxed in water bath and evaporated under rotation to remove the solvent and the residual methyl ?-alkyl-acrylateto give N-lauryl-(?-alkyl)-?-aminopropionic acid. Then N-lauryl-(?-alkyl)-?-aminopropionic acid and water are added to a three-necked flask, slowly dropwise added with a sodium hydroxide solution and reacted in water bath to give a crude product, which is filtered and dried to give a purified surfactant sodium N-lauryl-(?-alkyl)-?-aminopropionate. This surfactant is suitable for the foamed acid system and its performance can be switched by adjusting pH due to pH sensitivity.
    Type: Application
    Filed: June 18, 2019
    Publication date: December 26, 2019
    Inventors: Xiaojuan LAI, Zhiqiang DANG, Lei WANG, Shaoyun MA, Xianwen LI, Wei TIAN, Xingen FENG, Yinyin ZHANG, Xu YANG
  • Publication number: 20190330519
    Abstract: The present invention provides a chelating agent for reservoir acidification and stimulating injection and its preparation method and application. The raw material composition of the chelating agent comprises: 10.0%-20.0% of methanesulfonic acid, 10.0%-20.0% of methanol, 10.0%-20.0% of polyaspartic acid, 10.0%-15.0% of epoxy succinic acid, 5.0%-10.0% of sodium cetyl sulfonate, 10.0%-15.0% of cetyltrimethylammonium bromide and the balance of water. The present invention also provides a preparation method of the above chelating agent. The chelating agent for reservoir acidification and stimulating injection of the invention is used in an acidizing and stimulating injection process, wherein it can effectively dissolve rock cracks, be used directly without need to be reversed.
    Type: Application
    Filed: January 23, 2019
    Publication date: October 31, 2019
    Inventors: Lijun MU, Xianwen LI, Hongjun LU, Yong WANG, Bin YAO, Zhenning JI, Suiwang ZHANG, Xiaobing LU, Zhiying DENG, Lei SUI, Erzhen WANG, Zhaojie SONG
  • Publication number: 20190316031
    Abstract: The present invention provides an injection stimulation agent for water injection well and the preparation method and application thereof. The raw material composition of the injection stimulation agent for water injection well comprises: 5.0%-10.0% of sulfamic acid, 10.0%-20.0% of methanol, 10.0%-20.0% of tartaric acid, 10.0%-20.0% of ethylenediamine tetramethylene phosphoric acid, 5.0%-10.0% of sodium polyacrylate, 5.0%-8.0% of cocoyl hydroxyethyl sulfonic acid and the balance of water. The present invention further provides a preparation method of the above injection stimulation agent. The injection stimulation agent for water injection well of the present invention can be used in acidizing treatment process of the reservoir, and can be used directly. The injection stimulation agent can play the role of shrinking swelled clay at the same time of dissolving scale, and finally achieve the purpose of depressurization and enhanced production.
    Type: Application
    Filed: December 21, 2018
    Publication date: October 17, 2019
    Inventors: Lijun Mu, Xianwen Li, Hongjun Lu, Yong Wang, Bin Yao, Zhenning Ji, Suiwang Zhang, Xiaobing Lu, Zhaojie Song, Lei Sui, Zhiying Deng, Erzhen Wang, Wei Wang, Juntao Wang
  • Publication number: 20190292438
    Abstract: The present invention provides a method for in-depth profile control and displacement of low-permeability oil reservoirs, comprising: sequentially injecting a flexible and elastic particle-containing pre-slug, a polymer microsphere-containing main slug and a flexible and elastic particle-containing protective slug into an oil layer, and the three slugs have a volume ratio of total injection amount of 1-2:6-8:1-2. The invention provides a method for in-depth profile control and displacement by using styrene-based flexible and elastic particles in combination with the polyacrylamide polymer microsphere, wherein the flexible elastic particles can block cracks and large pore channels of the oil layer, and the polymer microsphere can displace the remaining oil in the oil layer. In the present invention, different slugs of profile control and displacement system are combined to achieve the objective of blocking cracks and large pore channels, displacing crude oil, and improving oil well recovery.
    Type: Application
    Filed: January 18, 2019
    Publication date: September 26, 2019
    Inventors: Tianjiang Wu, Mingke Zheng, Xianwen Li, Haien Yang, Xiaorong Li, Fan Tang, Fangfang Xue, Ronghuan Chen, Rong Zhang, Lijun Zheng, Chunmei Xu, Baoche Liu, Ping Yi, Jiajie Zhu, Weiyu Bi
  • Publication number: 20190276731
    Abstract: The present disclosure provides a diverting agent for diversion acidizing in water injection wells and a preparation method thereof. The diverting agent for diversion acidizing in water injection wells has a raw material composition including: 3%-6% of ethylenediamine, 12%-25% of bromododecane, 10%-20% of a solvent, 10%-20% of an assistant, 14%-28% of oleic acid, 5%-10% of stearic acid salt, 1%-2% of a dispersing agent and a balance of water. The present disclosure also provides a method for preparing the above-mentioned diverting agent for diversion acidizing in water injection wells. The diverting agent for diversion acidizing in water injection wells of the present disclosure can be used for temporary plugging diverting of acid solution in on-line acidification of water injection wells or in acidification operation of oil reservoir with a greater heterogeneity, which has good compatibility with the acid solution and can be used for temporary plugging of high-permeability zones.
    Type: Application
    Filed: January 4, 2019
    Publication date: September 12, 2019
    Inventors: Lijun Mu, Xianwen Li, Hongjun Lu, Zhiying Deng, Yong Wang, Bin Yao, Zhenning Ji, Suiwang Zhang, Xiaobing Lu, Zhaojie Song, Erzhen Wang, Lei Sui
  • Publication number: 20190276730
    Abstract: The present disclosure provides an on-line diverting acid for continuous injection into water injection wells and a preparation method thereof. The on-line diverting acid for continuous injection into water injection wells has a raw material composition of: 5.0-25.0% of hydrochloric acid, 3.0%-6.0% of ammonium fluoride, 4.0%-8.0% of a diverting agent, 3.0%-7.0% of a chelating agent, 1.0-3.0% of a corrosion inhibitor, 1.0-3.0% of an anti-swelling/swelled-clay-shrinking agent and a balance of water. The present disclosure also provides a preparation method of the above-mentioned on-line diverting acid. The on-line diverting acid of the present disclosure can remove plugging from deep zones of high and low permeability layers, and can be continuously injected to simplify the construction process, so as to achieve the purpose of reducing the pressure and stimulating the injection.
    Type: Application
    Filed: January 4, 2019
    Publication date: September 12, 2019
    Inventors: Lijun Mu, Xianwen Li, Hongjun Lu, Zhiying Deng, Yong Wang, Bin Yao, Zhenning Ji, Suiwang Zhang, Xiaobing Lu, Zhaojie Song, Lei Sui, Erzhen Wang
  • Publication number: 20190242231
    Abstract: The present invention provides a method for further forming a plurality of small fractures in a main fracture. If a radial main fracture is further fractured axially to form a plurality of branch fractures, the stimulated volume of the oil and gas reservoir will be achieved to greatly increase the yield of dense oil and gas. The main contribution of the present invention is to form three-dimensional fracture networks for any low-permeability oil reservoirs to achieve stimulated reservoir volume. The concept is that an original main fracture is further fractured to form a plurality of branch fractures (the branch fractures form included angles with the original main fracture), and the locations for forming the branch fractures in the main fracture and even the size and length of the branch fractures can be controlled artificially, so that the branch fractures can be formed by fracturing where needed.
    Type: Application
    Filed: March 21, 2018
    Publication date: August 8, 2019
    Inventors: Desheng ZHOU, Hua YANG, Xianwen LI, Shun LIU, Wenbin CAI, Xianlin MA, Xiong LIU, Yafei LIU
  • Publication number: 20180281613
    Abstract: The disclosure provides an Internet-based intelligent mobile charging system and method. The system includes a rescue vehicle APP, a charging rescue vehicle, a rescued vehicle APP and a rescue platform. The rescue vehicle APP includes a first user module, a first order module, a monitoring module and a first communication module; the charging rescue vehicle includes a controller, a global position system (GPS) device, a direct-current charger, an alternative-current charger and a metering module; the rescued vehicle APP includes a second user module, a second order module, a payment module and a second communication module; the rescue platform includes an access module, an order execution module, a vehicle screening module, a rescue vehicle monitoring module, a bill management module and a user certification module.
    Type: Application
    Filed: June 6, 2018
    Publication date: October 4, 2018
    Inventors: Xuekun YU, DENG HU, XIANWEN LI, SHEN WANG