Abstract: The invention concerns a method for analyzing the leaf group composition of a cigarette sample based on tobacco thermal characteristics, which comprises the following steps: (1) Preparing a to-be-analyzed cigarette sample and single-grade tobacco samples; (2) Collecting thermal analysis spectra of the cigarette sample and the single-grade tobacco samples; (3) Using a thermal analysis mapping algorithm to obtain the tobacco leaf composition and proportion of the cigarette sample. The method of the invention can complete the composition analysis of an unknown cigarette in a few minutes, and can obtain a clear formula composition and proportion value that is objective, efficient, versatile, has good repeatability and high sensitivity, and has unique advantages in cigarette analysis in the tobacco industry.

Abstract: A method for evaluating the possibility of a cigarette burning cone to fall off is disclosed. The method uses a manipulator simulation device to simulate the smoking of a cigarette, and measures the maximum deviation of the cigarette burning cone, and then uses angle summing and averaging to add the maximum deviations of the cigarette burning cones measured for multiple cigarettes and obtain an average value, and then evaluates the possibility of the cigarette burning cone to fall by the average value of the maximum deviations of the cigarette burning cone. The method is new, and compared with an existing method using state information of the cigarette burning cone “falling” and “not falling,” the method can more accurately, directly and timely reflect the state of the cigarette burning cone.

Abstract: A method of identifying tobacco carbonyl components using non-targeted mass spectrometry is disclosed, which includes the following steps: (1) preparing a tobacco sample extract; (2) derivatizing (part of) the sample/extract with 2,4-dinitrophenylhydrazine (DNPH); (3) derivatizing (another part of) the sample/extract with DNPH-d3; (4) mixing the derivatized tobacco samples; (5) preparing blank samples; (6) performing ultra performance liquid chromatography (UPLC) and ion trap (Orbitrap) high resolution mass spectrometry (HRMS) on the (derivatized) tobacco samples; (7) processing the LC-MS data; (8) filtering the mass spectrometric characteristic data to retain final chromatographic peaks; and (9) structurally annotating or identifying the retained final chromatographic peaks to obtain the tobacco carbonyl components.

Abstract: A test system and a test method for a lip sticking force of tipping paper for cigarettes are provided. The test system includes an artificial lip and test equipment. The artificial lip is a silica gel block. The test equipment includes a friction meter testing platform, a force measuring sensor, a rigid rope, a pulley, a pulley bracket and a sample loading module. The pulley is installed on the pulley bracket, and the rigid rope slides in the pulley. The rigid rope is L-shaped, a first end of the rigid rope in a horizontal direction is connected to the force measuring sensor, and a second end of the rigid rope in a vertical direction is connected to the sample loading module. The artificial lip is located directly below the sample loading module, and the artificial lip is in contact with the sample loading module at a test position.

Abstract: A device for a cigarette tipping paper anti-adhesion test is disclosed. The device includes the following components: an upper cover (1), a plurality of upper cover semi-cylinders (11) inside the upper cover, having the same radius and arranged in parallel, and a box (2) with a plurality of holes (211) on the box upper surface (21), connected with the inner cavity of the box (2). Each upper cover semi-cylinder has a cross-section with a bow shape. The side wall of the box (2) also has an opening (22). A method for testing anti-adhesion of the cigarette tipping paper using the device is also disclosed. The present device can qualitatively and quantitatively simulate adhesion of tipping paper in various conditions.

Abstract: A device for a cigarette tipping paper anti-adhesion test is disclosed. The device includes the following components: an upper cover (1), a plurality of upper cover semi-cylinders (11) inside the upper cover, having the same radius and arranged in parallel, and a box (2) with a plurality of holes (211) on the box upper surface (21), connected with the inner cavity of the box (2). Each upper cover semi-cylinder has a cross-section with a bow shape. The side wall of the box (2) also has an opening (22). A method for testing anti-adhesion of the cigarette tipping paper using the device is also disclosed. The present device can qualitatively and quantitatively simulate adhesion of tipping paper in various conditions.

Abstract: A test system and a test method for a lip sticking force of tipping paper for cigarettes are provided. The test system includes an artificial lip and test equipment. The artificial lip is a silica gel block. The test equipment includes a friction meter testing platform, a force measuring sensor, a rigid rope, a pulley, a pulley bracket and a sample loading module. The pulley is installed on the pulley bracket, and the rigid rope slides in the pulley. The rigid rope is L-shaped, a first end of the rigid rope in a horizontal direction is connected to the force measuring sensor, and a second end of the rigid rope in a vertical direction is connected to the sample loading module. The artificial lip is located directly below the sample loading module, and the artificial lip is in contact with the sample loading module at a test position.

Abstract: A non-sticking lip tipping paper is disclosed that includes a base paper, a color layer and a surface coating. The color layer is formed by printing and drying a color ink on the base paper; the surface coating includes a water-based glue and is coated thereon after drying the color layer. The water-based glue includes the following components by weight: 30-65 parts of a modified water-based resin solution, 10-20 parts of water, 8-15 parts of ethanol, and 5-12 parts of a water-based additive. The water-based additive is a mixture of a wax emulsion and magnesium silicate in a weight ratio of 1:5. A preparation method and a method of applying the non-sticking lip tipping paper are also disclosed.

Abstract: A non-sticking lip tipping paper is disclosed that includes a base paper, a color layer and a surface coating. The color layer is formed by printing and drying a color ink on the base paper; the surface coating includes a water-based glue and is coated thereon after drying the color layer. The water-based glue includes the following components by weight: 30-65 parts of a modified water-based resin solution, 10-20 parts of water, 8-15 parts of ethanol, and 5-12 parts of a water-based additive. The water-based additive is a mixture of a wax emulsion and magnesium silicate in a weight ratio of 1:5. A preparation method and a method of applying the non-sticking lip tipping paper are also disclosed.

Abstract: A determination method for lip sticking force of cigarette tipping paper is provided. The artificial saliva is used to clamp the tipping paper and the artificial mouth skin that are bonded between two jigs, respectively. The two jigs move relative to each other. Force changes during the test are collected through a force sensor and a displacement sensor. The maximum debonding force obtained by the test is divided by the sticking area of the tipping paper and the artificial mouth skin to obtain the lip sticking force of the cigarette tipping paper per unit area. The present invention can accurately quantify the sticking force of the cigarette tipping paper to lips, can well avoid subjective factor influence and difference characterization brought by traditional personal sensory smoking evaluation, is more objective, efficient, has good repeatability, high sensitivity and simple operation.

Abstract: The present invention relates to a prediction model for a lip sticking force of a cigarette tipping paper, a construction method and a prediction method thereof, which belongs to the technical field of analysis and detection. In the method, the stepwise regression analysis is performed on the lip sticking force and values of the dynamic friction coefficient and the grammage of the cigarette tipping paper to obtain a model for predicting the lip sticking force of the cigarette tipping paper. When checking the accuracy of the model, it is found that the predicted value and the measured value basically fall near the 1:1 line, R2 index is 0.99, and the normalized root mean square error (nRMSE) is 2.64%. The present invention provides a method capable of quickly and simply quantifying a sticking force of the cigarette tipper paper to lips.

Abstract: A determination method for lip sticking force of cigarette tipping paper is provided. The artificial saliva is used to clamp the tipping paper and the artificial mouth skin that are bonded between two jigs, respectively. The two jigs move relative to each other. Force changes during the test are collected through a force sensor and a displacement sensor. The maximum debonding force obtained by the test is divided by the sticking area of the tipping paper and the artificial mouth skin to obtain the lip sticking force of the cigarette tipping paper per unit area. The present invention can accurately quantify the sticking force of the cigarette tipping paper to lips, can well avoid subjective factor influence and difference characterization brought by traditional personal sensory smoking evaluation, is more objective, efficient, has good repeatability, high sensitivity and simple operation.

Abstract: The present invention relates to a prediction model for a lip sticking force of a cigarette tipping paper, a construction method and a prediction method thereof, which belongs to the technical field of analysis and detection. In the method, the stepwise regression analysis is performed on the lip sticking force and values of the dynamic friction coefficient and the grammage of the cigarette tipping paper to obtain a model for predicting the lip sticking force of the cigarette tipping paper. When checking the accuracy of the model, it is found that the predicted value and the measured value basically fall near the 1:1 line, R2 index is 0.99, and the normalized root mean square error (nRMSE) is 2.64%.