Abstract: The present invention relates to a supported catalyst used for synthesizing polyether amine, a preparation method, and an application. The supported catalyst introduces Mo and CeO2 into Ni and Cu active components. By means of the cooperation of Ni, Cu and Mo, CeO2 and Ni form more active sites, such that the supported catalyst can have high reaction activity and selectivity. By using the supported catalyst to synthesize polyether amine, the amination efficiency and selectivity of polyether polyol can be greatly enhanced, thereby preparing the polyether amine with light color and narrow molecular weight distribution. In addition, the cost of the catalyst can be reduced, a process condition is relatively mild, and the disadvantage of low reaction activity of a nickel-based catalyst in synthesizing small molecule polyether amine can be overcome, such that the supported catalyst has a desirable industrial application prospect.

Abstract: Provided are a system and a method for preparing a polyether amine by catalytic amination of a polyether diol. The preparation method includes: filling a catalyst into the fixed bed reactor; pressurizing the internal pressure of the fixed bed reactor to 10˜13 MPa by a hydrogen gas, and raising the temperature of the fixed bed reactor to 150˜185° C.; adjusting the temperature of the multi-stage preheater so that the feeding temperature of a raw material reaches 125˜135° C.; and simultaneously feeding a polyether diol, liquid ammonia and the hydrogen gas into the multi-stage preheater, and after mixing and preheating, introducing into the fixed bed reactor from the feed inlet of the fixed bed reactor for a continuous catalytic amination reaction. The total amine value of the polyether amine finally obtained by the present invention reaches 28˜32 mgKOH/g, the color reaches 10˜20, and it is colorless transparent liquid.

Abstract: A light emitting filament diode that includes a filament substrate; a plurality of light emitting diodes (LEDs) electrically connected and disposed along a length of the filament substrate; and a phosphorus encapsulant present in direct contact with an upper surface and sidewalk of at least one of the plurality of light emitting diodes (LEDs). No portion of phosphorus encapsulant is present overlying a portion of the filament substrate extending between the sidewalls of adjacently situated light emitting diodes having phosphorus encapsulant present thereon. The light emitting filament diode may a include a transparent encapsulant present over at least the light emitting diode chips.

Abstract: A light emitting diode (LED) structure that includes a stent substrate; and a circuit having a plurality of contact pads arranged along a length of the stent substrate. The structure further includes a plurality of light emitting diode (LED) chips, wherein each light emitting diode chip in the plurality of chips is engaged to a set of contact pads along the length of the metal stent substrate. A continuous phosphor layer is present overlying the plurality of light emitting diode (LED) chips, the continuous phosphor layer including first portions that are in direct contact with at least a light transmission surface of the light emitting diode (LED) chips and second portions that bridge across the space separating adjacently positioned light emitting diode. An encapsulant present over the continuous phosphor layer that is covering at least the light emitting diode chips.

Abstract: The disclosure provides a preparation process of an allyl alcohol polyether with a low potassium and sodium content, comprising the following steps: reacting allyl alcohol with a mixture of epoxypropane and oxacyclopropane to prepare an allyl alcohol oligomer crude product with a molecular weight of 150-1500; reducing the total content of potassium and sodium ions in the allyl alcohol oligomer crude product prepared in step S1 to 2 ppm or less through a cation exchange resin; and reacting the allyl alcohol oligomer product treated in step S2 with the mixture of epoxypropane and oxacyclopropane to prepare allyl alcohol high-molecular-weight polyether with a molecular weight of 2000-5000. According to the present disclosure, the total content of potassium and sodium ions in the product is reduced to 2 ppm or less, and the product has a good double bond protection rate.

Abstract: An apparatus includes memory and processing circuitry coupled to the memory. The processing circuitry is to decode a client-to-client (C2C) enabling signal received from an access point (AP). The C2C enabling signal indicates the AP is configured for Low Power Indoor (LPI) communication at an LPI signal power level. The signal power of the C2C enabling signal received from the AP is determined. Bluetooth (BT) circuitry of the apparatus is configured for BT communication with a wireless device at the LPI signal power level when the signal power of the C2C enabling signal is above a signal power threshold. The BT circuitry is configured to perform a handshake exchange with the wireless device to initiate the BT communication at the LPI signal power level.

Abstract: A tile or plate, includes: an upper plate (3) and a lower plate (4); wherein a plurality of heat conducting cavities (6) are uniformly provided between the upper plate (3) and the lower plate (4) via connecting ribs (5). A solar collection layer is provided on an upper surface of the tile or the plate. Two ends of the tile or the plate are connected with each of the plurality of the heat conducting cavities (6) via transverse connecting pipes (23, 37, 42). The transverse connecting pipes (23, 37, 42) of two neighboring tiles are connected by a ferrule (17) or a hose (36) to form an integrated circulation system. The tile or plate has a large day-lighting area and a high energy conversion rate.

Abstract: The present invention relates to a synthesis method and synthesis reactor of high-selectivity 2-methylallyl chloride by taking isobutylene and chlorine gas as raw materials and performing a gas-phase chlorination reaction in a microchannel reactor with a cooling surface. The isobutylene and the chlorine gas are reacted in a T-shaped microchannel reactor, and the mixing speed is extremely fast. Meanwhile, the huge heat exchange area per unit volume can ensure that the reaction proceeds stably at a substantially constant temperature and has good controllability. Therefore, side reactions caused by excessive local temperature can be effectively suppressed, the reaction selectivity is high, and no coking phenomenon occurs.

Abstract: The present invention relates to a method for preparing 2-methylallyl chloride from 1,2-dichloroisobutane. The method is characterized in that 1,2-dichloroisobutane and a sodium hydroxide aqueous solution are used as raw materials; reactive rectification is performed in a combined rectifying tower to eliminate hydrogen chloride so as to obtain 2-methylallyl chloride. A plate tower is provided at the lower part of the combined rectifying tower; a packing tower is provided at the upper part of the combined rectifying tower; an inner reflux condenser is provided at the top of the combined rectifying tower. The sodium hydroxide aqueous solution is added from a first plate of the plate tower; and 1,2-dichloroisobutane is added from the middle part of the plate tower. The method has the advantages that the raw material 1 and 1,2-dichloroisobutane is fully converted; the selectivity of the 2-methylallyl chloride is high.

Abstract: The present invention relates to a method for preparing 2-methylallyl chloride from 1,2-dichloro-tert-butane. The method is characterized in that 1,2-dichloro-tert-butane and a sodium hydroxide aqueous solution are used as raw materials; reactive rectification is performed in a combined rectifying tower to eliminate hydrogen chloride so as to obtain 2-methylallyl chloride. A plate type tower is provided at the lower part of the combined rectifying tower; a packing tower is provided at the upper part of the combined rectifying tower; an inner reflux condenser is provided at the top of the combined rectifying tower. The sodium hydroxide aqueous solution is added from a first plate of the plate type tower; and 1,2-dichloro-tert-butane is added from the middle part of the plate type tower. The method has the advantages that the raw material 1 and 1,2-dichloro-tert-butane is fully converted; the selectivity of the 2-methylallyl chloride is high.

Abstract: The present invention relates to a synthesis method and synthesis reactor of high-selectivity 2-methylallyl chloride by taking isobutylene and chlorine gas as raw materials and performing a gas-phase chlorination reaction in a microchannel reactor with a cooling surface. The isobutylene and the chlorine gas are reacted in a T-shaped microchannel reactor, and the mixing speed is extremely fast. Meanwhile, the huge heat exchange area per unit volume can ensure that the reaction proceeds stably at a substantially constant temperature and has good controllability. Therefore, side reactions caused by excessive local temperature can be effectively suppressed, the reaction selectivity is high, and no coking phenomenon occurs.

Abstract: A tile or plate, includes: an upper plate (3) and a lower plate (4); wherein a plurality of heat conducting cavities (6) are uniformly provided between the upper plate (3) and the lower plate (4) via connecting ribs (5). A solar collection layer is provided on an upper surface of the tile or the plate. Two ends of the tile or the plate are connected with each of the plurality of the heat conducting cavities (6) via transverse connecting pipes (23, 37, 42). The transverse connecting pipes (23, 37, 42) of two neighboring tiles are connected by a ferrule (17) or a hose (36) to form an integrated circulation system. The tile or plate has a large day-lighting area and a high energy conversion rate.

Abstract: Apparatuses and methods for channel state information reference signal (CSI-RS) configuration in distributed remote radio head (RRH) systems are described. A transmission point selection module can receive a user equipment (UE) signal via a transmission point from a plurality of transmission points sharing a single cell identification. A downlink transmission point can be selected based on the UE signal. The UE can then be configured to report CSI-RS measurements for the selected downlink transmission point.

Abstract: Apparatuses and methods for channel state information reference signal (CSI-RS) configuration in distributed remote radio head (RRH) systems are described. A transmission point selection module can receive a user equipment (UE) signal via a transmission point from a plurality of transmission points sharing a single cell identification. A downlink transmission point can be selected based on the UE signal. The UE can then be configured to report CSI-RS measurements for the selected downlink transmission point.

Abstract: Improved structure and performance are disclosed for lithium cylindrical primary and secondary bobbin cells having an improved cathode and current collector. This collector can be a metal screen, mesh or grid, and may further be treated with carbon or cathode mix components and then wrapped around the cathode and embedded into its surface. This metal grid collector reduces cell impedance, and increases discharge rate capability as well as low temperature performance. The cathode for these cells is surrounded by the anode and may also have a hole through its center to provide improved manufacturability and reduced cost for the cells.

Abstract: A symbol structure is disclosed for use at least with wireless signal transmitters. The symbol structure includes a symbol that is spread over at least two symbol time periods. The symbol may include at least two replicas of the same code. The subcarrier spacing of subcarriers of the symbol has a p/q ratio of the subcarrier spacing of an IEEE 802.16e symbol. In some cases, the symbol includes interspersed null values. The decoding of the symbol involves performing a Fourier transform on the symbol.

Abstract: A hybrid lithium electrochemical cell comprising a spirally wound cathode, separator and anode in a generally cylindrical structure with the packaging materials and terminal structure of a pouch cell. The cell may also contain a welded metal grid outside the pouch cell packaging material to insure a cylindrical shape. The resultant hybrid cell features improved capacity and specific energy.

Abstract: A nonaqueous cell employing an anode such as lithium or lithium alloy, a liquid lithium salt nonaqueous electrolyte, a thermal shutdown separator and a cathode comprising a homogeneous hybrid mixture of carbon fluoride and manganese dioxide, said carbon fluoride or poly-carbon fluoride being represented by the formula (CFx) wherein 0.5?x?1.2 and contained in said mixture in a ratio by weight of about 5 to 99%, preferably about 5 to 50% and said manganese dioxide is heat treated electrolytic manganese dioxide represented by EMD or MnO2. The CFx—MnO2 hybrid cathode cells yield high capacity with high discharge rate and excellent low-temperature performance without voltage delay. The cells are characterized by two significant plateaus in their discharge profiles, the first contributed by MnO2 and the second by CFx.

Abstract: Described herein is an optical multilayered-film filter which provides less interference and a good optical characteristic and is high in productivity. The optical multilayered-film filter wherein dielectric thin films are stacked on each other in a multilayer form in a single direction, comprises a refractive-index inclined laminated portion in which refractive indices of dielectric thin-film layers are successively inclined and changed in a laminating direction, and an alternately-laminated portion in which a dielectric thin-film layer having a high refractive index and a dielectric thin-film layer having a low refractive index are alternately laminated on each other.