Patents by Inventor Xujun Hua

Xujun Hua has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).

  • Publication number: 20200207663
    Abstract: Cement composite boards comprising cellulose filaments (CF) and/or CF-containing pulp, are described. The composite boards have at least an improved modulus of rupture when compared with similar board that are free of CF. Methods for producing the CF and/or CF-containing pulp reinforced cement boards are also described. The CF cement composite board comprises: cellulose filaments (CF) and/or CF-containing pulp, and cement, wherein the CF has an aspect ratio of 200 to 5000, comprising a weight % of CF is from 1% to 20% by weight of the composite board. The composite boards herein described may have a modulus of rupture of more than 7 MPa.
    Type: Application
    Filed: May 18, 2018
    Publication date: July 2, 2020
    Applicant: FPInnovations
    Inventors: Xiaolin CAI, Yuxia BEN, Xujun HUA, Michelle RICARD, Carole LAROUCHE, Xiang-Ming WANG
  • Patent number: 10683612
    Abstract: A novel method is disclosed to make cellulose filaments (CF) from wood or other plant fibers with lower energy consumption. The method consists of multi-stage, high consistency refining, followed by low consistency refining or by low consistency, non-refining mechanical treatment, of wood or other plant fibers. The total specific refining energy for the multi-stage, high consistency refining is preferably 2,000-18,000 kWh/t, and more preferably 2,000-12,000 kWh/t. The CF produced can be used as a superior reinforcement additive in the production of paper, tissue or paperboard and in the production of plastic composites. It can also be used as a viscosity or rheology modifier in food products, coatings or drilling muds. The CF produced can also be used to make strong films for application in packaging and in composites.
    Type: Grant
    Filed: September 13, 2017
    Date of Patent: June 16, 2020
    Inventors: Xujun Hua, Guy Roger Njamen Tchapda, Tom Owston, Patrick Neault, Thomas Hu, Yuxia Ben
  • Patent number: 10087580
    Abstract: The present description relates to a process of producing a dry mixed product comprising cellulose filament (CF) and a carrier fiber, and a dry mixed product of re-dispersible cellulose filament and a carrier fiber that permits the CF to retain its dispersibility in water and hence superior reinforcement ability in papermaking furnishes, composite materials, or other materials where CF is used. The process comprises mixing a water suspension of never-dried CF with a cellulose fiber pulp carrier followed by thickening to a suitable concentration so that it can be further processed and dried in a conventional device such as a dryer can of a pulp machine or a flash dryer.
    Type: Grant
    Filed: April 25, 2016
    Date of Patent: October 2, 2018
    Assignee: FPInnovations
    Inventors: Yuxia Ben, Gilles Dorris, Xiaolin Cai, Xujun Hua, Zhirun Yuan, Patrick Neault
  • Publication number: 20180073194
    Abstract: A novel method is disclosed to make cellulose filaments (CF) from wood or other plant fibers with lower energy consumption. The method consists of multi-stage, high consistency refining, followed by low consistency refining or by low consistency, non-refining mechanical treatment, of wood or other plant fibers. The total specific refining energy for the multi-stage, high consistency refining is preferably 2,000-18,000 kWh/t, and more preferably 2,000-12,000 kWh/t. The CF produced can be used as a superior reinforcement additive in the production of paper, tissue or paperboard and in the production of plastic composites. It can also be used as a viscosity or rheology modifier in food products, coatings or drilling muds. The CF produced can also be used to make strong films for application in packaging and in composites.
    Type: Application
    Filed: September 13, 2017
    Publication date: March 15, 2018
    Inventors: Xujun HUA, Guy Roger NJAMEN TCHAPDA, Tom OWSTON, Patrick NEAULT, Thomas HU, Yuxia BEN
  • Patent number: 9856607
    Abstract: Cellulose nanofilaments from cellulose fibers, a method and a device to produce them are disclosed. The nanofilaments are fine filaments with widths in the sub-micron range and lengths up to a couple of millimeters. These nanofilaments are made from natural fibers from wood and other plants. The surface of the nanofilaments can be modified to carry anionic, cationic, polar, hydrophobic or other functional groups. Addition of these nanofilaments to papermaking furnishes substantially improves the wet-web strength and dry sheet strength much better than existing natural and synthetic polymers. The cellulose nanofilaments produced by the present invention are excellent additives for reinforcement of paper and paperboard products and composite materials, and can be used to produce superabsorbent materials.
    Type: Grant
    Filed: May 11, 2011
    Date of Patent: January 2, 2018
    Assignee: FPINNOVATIONS
    Inventors: Xujun Hua, Makhlouf Laleg, Thomas Owston
  • Publication number: 20170150749
    Abstract: The present invention relates to a structurally enhanced agricultural product containing cellulose filaments (CF), and a method for producing the structurally enhanced agricultural material into the sheets. Applying CF improves significantly the wet-web strength of the agricultural material sheets. The method comprises preparation of a pulp slurry of agricultural materials followed by mixing with a water suspension of CF or CF-containing cellulose fibers. The pulp blend is then used to produce an agricultural material sheet by papermaking process.
    Type: Application
    Filed: November 25, 2016
    Publication date: June 1, 2017
    Inventors: Yuxia BEN, Xujun HUA, Michelle RICARD, Xiaoyu WANG
  • Publication number: 20160319482
    Abstract: The present description relates to a process of producing a dry mixed product comprising cellulose filament (CF) and a carrier fibre, and a dry mixed product of re-dispersible cellulose filament and a carrier fibre that permits the CF to retain its dispersibility in water and hence superior reinforcement ability in papermaking furnishes, composite materials, or other materials where CF is used. The process comprises mixing a water suspension of never-dried CF with a cellulose fibre pulp carrier followed by thickening to a suitable concentration so that it can be further processed and dried in a conventional device such as a dryer can of a pulp machine or a flash dryer.
    Type: Application
    Filed: April 25, 2016
    Publication date: November 3, 2016
    Inventors: Yuxia BEN, Gilles DORRIS, Xiaolin CAI, Xujun HUA, Zhirun YUAN, Patrick NEAULT
  • Patent number: 9051684
    Abstract: A method to produce on a commercial scale, high aspect ratio cellulose nanofilaments (CNF) from natural lignocellulosic fibers comprises a multi-pass high consistency refining (HCR) of chemical or mechanical fibers using combinations of refining intensity and specific energy. The CNF produced represents a mixture of fine filaments with widths in the submicron and lengths from tens of micrometers to few millimeters. The product has a population of free filaments and filaments bound to the fiber core from which they were produced. The proportion of free and bound filaments is governed in large part by total specific energy applied to the pulp in the refiner, and differs from other cellulose fibrillar materials by their higher aspect ratio and the preserved degree of polymerization (DP) of cellulose, and are excellent additives for the reinforcement of paper, tissue, paperboard and the like. They display exceptional strengthening power for never-dried paper webs.
    Type: Grant
    Filed: January 19, 2012
    Date of Patent: June 9, 2015
    Assignee: FPINNOVATIONS
    Inventors: Xujun Hua, Makhlouf Laleg, Keith Miles, Reza Amiri, Lahoucine Ettaleb, Gilles Dorris
  • Patent number: 8608906
    Abstract: A method to prepare aqueous furnishes useful as feedstock in the manufacture of very high-mineral content products, particularly paper sheets having mineral filler content up to 90% that display the required physical properties for the intended applications; the furnishes comprise fibrillated long fibers/mineral fillers mixed with anionic acrylic binders and co-additives, in presence or absence of cellulose fibrils; the fibrillated long fibers and cellulose fibrils provide high surface area for greater filler fixation and the reinforcement backbone network that ties all of the product components together; the anionic binders allow rapid and strong fixation of filler particles onto the surfaces of fibrils when mixing is conducted at temperatures higher than the glass transition temperature (Tg) of the binder. The aqueous furnish provides excellent filler retention and drainage during product fabrication.
    Type: Grant
    Filed: September 29, 2011
    Date of Patent: December 17, 2013
    Assignee: FPInnovations
    Inventors: Makhlouf Laleg, Xujun Hua
  • Publication number: 20130017394
    Abstract: A method to produce on a commercial scale, high aspect ratio cellulose nanofilaments (CNF) from natural lignocellulosic fibers comprises a multi-pass high consistency refining (HCR) of chemical or mechanical fibers using combinations of refining intensity and specific energy. The CNF produced represents a mixture of fine filaments with widths in the submicron and lengths from tens of micrometers to few millimeters. The product has a population of free filaments and filaments bound to the fiber core from which they were produced. The proportion of free and bound filaments is governed in large part by total specific energy applied to the pulp in the refiner, and differs from other cellulose fibrillar materials by their higher aspect ratio and the preserved degree of polymerization (DP) of cellulose, and are excellent additives for the reinforcement of paper, tissue, paperboard and the like. They display exceptional strengthening power for never-dried paper webs.
    Type: Application
    Filed: January 19, 2012
    Publication date: January 17, 2013
    Applicant: FPINNOVATIONS
    Inventors: Xujun Hua, Makhlouf Laleg, Keith Miles, Reza Amiri, Lahoucine Ettaleb, Gilles Dorris
  • Publication number: 20120080156
    Abstract: A method to prepare aqueous furnishes useful as feedstock in the manufacture of very high-mineral content products, particularly paper sheets having mineral filler content up to 90% that display the required physical properties for the intended applications; the furnishes comprise fibrillated long fibres/mineral fillers mixed with anionic acrylic binders and co-additives, in presence or absence of cellulose fibrils; the fibrillated long fibres and cellulose fibrils provide high surface area for greater filler fixation and the reinforcement backbone network that ties all of the product components together; the anionic binders allow rapid and strong fixation of filler particles onto the surfaces of fibrils when mixing is conducted at temperatures higher than the glass transition temperature (Tg) of the binder. The aqueous furnish provides excellent filler retention and drainage during product fabrication.
    Type: Application
    Filed: September 29, 2011
    Publication date: April 5, 2012
    Applicant: FPINNOVATIONS
    Inventors: Makhlouf LALEG, Xujun HUA
  • Publication number: 20110277947
    Abstract: Cellulose nanofilaments from cellulose fibers, a method and a device to produce them are disclosed. The nanofilaments are fine filaments with widths in the sub-micron range and lengths up to a couple of millimeters. These nanofilaments are made from natural fibers from wood and other plants. The surface of the nanofilaments can be modified to carry anionic, cationic, polar, hydrophobic or other functional groups. Addition of these nanofilaments to papermaking furnishes substantially improves the wet-web strength and dry sheet strength much better than existing natural and synthetic polymers. The cellulose nanofilaments produced by the present invention are excellent additives for reinforcement of paper and paperboard products and composite materials, and can be used to produce superabsorbent materials.
    Type: Application
    Filed: May 11, 2011
    Publication date: November 17, 2011
    Applicant: FPINNOVATIONS
    Inventors: Xujun HUA, Makhlouf LALEG, Thomas OWSTON
  • Patent number: 7431799
    Abstract: Disclosed is a method for manufacture and application of a polymeric papermaking additive, which can be used in paper manufacture as an agent for improving retention, drainage, product strength and paper machine operation. The additive according to this disclosure is a polymer of epichlorohydrin and contains primary amino groups. Under neutral or acidic conditions these primary amino groups become cationic, which assures good adsorption of the polymer onto anionic fibers and fines of pulps used for production of paper or paperboard. By adsorbing on several fibers or fines, the polymer can increase the retention of fines and fillers. Primary amino groups of this polymer can also form chemical bonds with carbonyl groups of cellulose, lignin and hemicellulose, which are especially abundant in the fibers and fines of mechanical pulps. The cross-linking of fibers and fines by chemical bonds can increase the initial strength of wet web and the strength of rewetted paper.
    Type: Grant
    Filed: February 23, 2005
    Date of Patent: October 7, 2008
    Assignee: FPInnovations
    Inventors: Miroslav Antal, Ivan I. Pikulik, Xujun Hua
  • Patent number: 6998015
    Abstract: A method is disclosed for reducing or inhibiting alkaline darkening of mechanical pulp caused by the presence of calcium carbonate filler during production; the method comprises adding a sulfite, or sulfur-containing reducing agent, especially a sulfite to the mechanical pulp and the filler; the method is usefully applied in the production of mechanical pulp and paper in which calcium carbonate is used as a filler and also in the production of paper at neutral or mildly alkaline conditions.
    Type: Grant
    Filed: November 27, 2001
    Date of Patent: February 14, 2006
    Assignee: Pulp and Paper Research Institute of Canada
    Inventors: Xujun Hua, Makhlouf Laleg
  • Publication number: 20050192402
    Abstract: Disclosed is a method for manufacture and application of a polymeric papermaking additive, which can be used in paper manufacture as an agent for improving retention, drainage, product strength and paper machine operation. The additive according to this disclosure is a polymer of epichlorohydrin and contains primary amino groups. Under neutral or acidic conditions these primary amino groups become cationic, which assures good adsorption of the polymer onto anionic fibres and fines of pulps used for production of paper or paperboard. By adsorbing on several fibres or fines, the polymer can increase the retention of fines and fillers. Primary amino groups of this polymer can also form chemical bonds with carbonyl groups of cellulose, lignin and hemicellulose, which are especially abundant in the fibres and fines of mechanical pulps. The cross-linking of fibres and fines by chemical bonds can increase the initial strength of wet web and the strength of rewetted paper.
    Type: Application
    Filed: February 23, 2005
    Publication date: September 1, 2005
    Inventors: Miroslav Antal, Ivan Pikulik, Xujun Hua
  • Publication number: 20020059999
    Abstract: A method is disclosed for reducing or inhibiting alkaline darkening of mechanical pulp caused by the presence of calcium carbonate filler during production; the method comprises adding a sulfite, or sulfur-containing reducing agent, especially a sulfite to the mechanical pulp and the filler; the method is usefully applied in the production of mechanical pulp and paper in which calcium carbonate is used as a filler and also in the production of paper at neutral or mildly alkaline conditions.
    Type: Application
    Filed: November 27, 2001
    Publication date: May 23, 2002
    Inventors: Xujun Hua, Makhlouf Laleg