Abstract: The present invention provides a method for the preparation of an insensitive high enthalpy explosive Dihydroxylammonium 5,5?-bistetrazole-1,1?-diolate (TKX-50) in the presence of N,N-dimethylformamide, N,N-dimethylacetamide, or N-Methyl-2-pyrrolidone as a solvent via a four-step, one-pot reaction route to obtain a final product after four reaction steps. The more dangerous intermediate diazidoglyoxime may be solved by the one-pot method without the need of isolation. Further, the cyclization reaction is carried out in the presence of dropwisely added concentrated sulfuric acid to replace hydrochloric gas so no hydrochloric gas generator is needed to greatly reduce the amount of waste acid so as to effectively reduce the cost by avoiding using hydrochloric gas steel cylinders which require much safety equipment.

Abstract: The present invention provides a method for the preparation of an insensitive high enthalpy explosive Dihydroxylammonium 5,5?-bistetrazole-1,1?-diolate (TKX-50) in the presence of N,N-dimethylformamide, N,N-dimethylacetamide, or N-Methyl-2-pyrrolidone as a solvent via a four-step, one-pot reaction route to obtain a final product after four reaction steps. The more dangerous intermediate diazidoglyoxime may be solved by the one-pot method without the need of isolation. Further, the cyclization reaction is carried out in the presence of dropwisely added concentrated sulfuric acid to replace hydrochloric gas so no hydrochloric gas generator is needed to greatly reduce the amount of waste acid so as to effectively reduce the cost by avoiding using hydrochloric gas steel cylinders which require much safety equipment.

Abstract: The present invention provides a freely rotatable electrical conduction structure including at least two cylindrical electrical conduction portions, an insulated material portion and at least two electrical conduction terminals. The at least two cylindrical electrical conduction portions are arranged separately along an axis, wherein the inner surface of each cylindrical electrical conduction portion is welded with an end of a conducting wire. The insulated material portion is combined with the at least two cylindrical electrical conduction portions via injection molding to form a circular shaft assembly. The at least two electrical conduction terminals correspond to the at least two cylindrical electrical conduction portions respectively, and each electrical conduction terminal partially projects to form an arc contact portion configured to abut onto the outer peripheral surface of its corresponding cylindrical electrical conduction portion.

Abstract: The present invention provides a freely rotatable electrical conduction structure including at least two cylindrical electrical conduction portions, an insulated material portion and at least two electrical conduction terminals. The at least two cylindrical electrical conduction portions are arranged separately along an axis, wherein the inner surface of each cylindrical electrical conduction portion is welded with an end of a conducting wire. The insulated material portion is combined with the at least two cylindrical electrical conduction portions via injection molding to form a circular shaft assembly. The at least two electrical conduction terminals correspond to the at least two cylindrical electrical conduction portions respectively, and each electrical conduction terminal partially projects to form an arc contact portion configured to abut onto the outer peripheral surface of its corresponding cylindrical electrical conduction portion.