Abstract: The present application discloses a bicyclic ketone compound and a preparation method therefor, and a preparation method for bicyclo[3.2.1]-3-octane-2,4-dione, belonging to the technical field of medicaments. 3-chlorobicyclo[3.2.1]-3-octen-2-one reacts with an alcohol in the presence of a strong alkali and a catalyst under an anhydrous condition to generate 4-alkoxybicyclo[3.2.1]-3-octen-2-one, and then 4-alkoxybicyclo[3.2.1]-3-octen-2-one is hydrolyzed to obtain bicyclo[3.2.1]-3-octane-2,4-dione. In the present application, the intermediate compound III—4-alkoxybicyclo[3.2.1]-3-octen-2-one is generated through the reaction of 3-chlorobicyclo[3.2.1]-3-octen-2-one with a strong alkali and an alcohol, and then a target product bicyclo[3.2.1]-3-octane-2,4-dione can be obtained in high yield through hydrolysis reaction.

Abstract: A multi-objective optimized evaluation method of anti-seismic performance of a slope reinforced by a pile-anchor system is provided. The method includes: training an initial three-dimensional slope numerical calculation model to obtain an target three-dimensional slope numerical calculation model; determining numerical values to be imported into the target three-dimensional slope numerical calculation model according to deformation differences, to obtain a model analysis result; obtaining a simulation operation result according to a reinforcement scheme working condition table of the pile-anchor system; based on the model analysis result and the simulation operation result, evaluating anti-seismic reinforcing performance of the pile-anchor system to obtain comprehensive evaluation values, and then optimizing and evaluating the reinforcement schemes of an overall slope to be reinforced.

Abstract: A method for preparing a phenoxycarboxylate includes 1) allowing a salt of a phenolic compound and a halogenated carboxylate to subject to a condensation reaction in a polar solvent under the action of a catalyst; and 2) adding an acid-containing organic solvent to the condensation reaction liquid in step 1) to perform an acidification, and purifying the precipitated halogenated inorganic salt to obtain a phenoxycarboxylate. A catalyst is added in the condensation process, which can improve the reaction rate, achieve the reaction at room temperature and high material conversion rate, and avoid the problem in the prior art that the reaction needs to be performed at high temperature, about 120° C. After the condensation reaction is completed, the salt is removed by dry filtration (an anhydrous condition) by adding a methanol hydrogen chloride solution. There is no industrial wastewater, raw materials are easily recycled, and the reaction yield is high.

Abstract: A multi-degree-of-freedom active damping mechanism control method, system and a damping mechanism are provided. A skyhook active damping control algorithm is used for controlling an electric cylinder output force in a vertical damping direction, and an adaptive control algorithm with an adaptive rate is used for correcting a load moment of inertia in pitch and roll damping directions. At the same time, a predictive model is established according to a task space linearization equation near an equilibrium point, and states of the system at N future moments are predicted in advance at each moment to achieve optimal control under complex constraints and reduce the influence of system delay. At the same time, the three control methods may further improve the active damping effect of the damping device by combining road information obtained by a visual sensor in real time.

Abstract: Through an intermediate I (a compound having the structural formula as shown in the formula Ia and/or the formula Ib), or a pharmaceutically acceptable salt thereof, or a solvate thereof, and a tautomer Ic of Ib, a bicyclopyrone intermediate II with a high yield can be prepared. Two compounds are docked first under the action of a base to produce an intermediate I, and then the intermediate I is subjected to intramolecular ring closure by an ammonium salt, which can increase the yield of the bicyclopyrone intermediate (II), reduce side reactions, and reduce problems that a reaction of raw materials is easily incomplete due to intramolecular ring closure directly through an ammonium salt. A one-pot method includes producing an intermediate I under the action of a base and then performing a ring-closure reaction to produce a bicyclopyrone intermediate (II) that reduces side reactions, and further increases the yield.

Abstract: The present disclosure relates to semiconductor structures and, more particularly, to electrostatic discharge devices and methods of manufacture. The structure includes: a plurality of regions of a first dopant type; insulator material separating each region of the plurality of regions of the first dopant type; and a substrate contacting the plurality of regions of the first dopant type, the substrate comprising a base region of a second dopant type different than the first dopant type and an outer segment surrounding the plurality of regions of the first dopant type, the outer segment comprises an electrical resistivity higher than the second dopant type.

Abstract: A method for preparing a static/dynamic three-dimensional (3D) microcrack propagation sensor, a sensor and equipment, belongs to the field of sensor technology.

Abstract: An adjustable device for railway to cross active faults is provided to fix a rail and a sleeper, including: a fastener mounting base, disposed between the rail and sleeper; clamping pipes, disposed between the fastener mounting base and the sleeper, the sleeper is provided with a through groove, and the clamping pipes are detachably fixed inside the through groove; control parts, disposed on an inner wall of the clamping pipes, each of the control parts is configured to detect lateral pressures between the fastener mounting base and corresponding one of the clamping pipes, thereby to separate the corresponding one of the clamping pipes from the through groove, the device ensures that the rail will not produce bending deformations after the lateral dislocation of the bottom layer during earthquake events, and ensure that a train or rail repair vehicle can pass at a low speed after earthquake.

Abstract: Embodiments of the disclosure provide an electrostatic discharge (ESD) device, including: an input pad; an underlapped field effect transistor (UL-FET) with a trigger voltage Vt, including: an underlapped drain region coupled to the input pad; a source region coupled to ground; and a gate structure coupled to the input pad; and a blocking layer separating the underlapped drain region from the gate structure of the UL-FET by an underlap distance.

Abstract: The present disclosure relates to semiconductor structures and, more particularly, to electrostatic discharge devices and methods of manufacture. The structure includes: a plurality of regions of a first dopant type; insulator material separating each region of the plurality of regions of the first dopant type; and a substrate contacting the plurality of regions of the first dopant type, the substrate comprising a base region of a second dopant type different than the first dopant type and an outer segment surrounding the plurality of regions of the first dopant type, the outer segment comprises an electrical resistivity higher than the second dopant type.

Abstract: Disclosed is a lateral double-diffused metal oxide semiconductor field effect transistor (LDMOSFET) with a replacement metal gate (RMG) structure that includes a first section, which traverses a semiconductor body at a channel region in a first-type well, and a second section, which is adjacent to the first section and which traverses the semiconductor body at a drain drift region in a second-type well. The RMG structure includes, in both sections, a first-type work function layer and a second-type work function layer on the first-type work function layer. However, the thickness of the first-type work function layer in the first section is greater than the thickness in the second section such that the RMG structure is asymmetric. Thus, threshold voltage (Vt) at the first section is greater than Vt at the second section and the LDMOSFET has a relatively high breakdown voltage (BV). Also disclosed are methods for forming the LDMOSFET.

Abstract: A construction and/or installation method for using phosphogypsum in embankment improvement includes preparing a phosphogypsum-containing embankment mixture, setting moisture content of an embankment mixture, paving a modified phosphogypsum-containing embankment, and reversely layering anti-seepage cushion layers from two sides of the embankment to the center of the embankment. The preparation of a phosphogypsum-containing embankment mixture can include the following: 90 parts by weight of phosphogypsum and 10 parts by weight of cement are weighted, uniformly mixed and stirred to obtain a base material mixture; and 2-4 parts by weight of sodium silicate is weighted and dissolved in water, and an obtained solution is added to the base material mixture to obtain the phosphogypsum-containing embankment mixture.

Abstract: Embodiments of the disclosure provide an electrostatic discharge (ESD) device, including: an input pad; an underlapped field effect transistor (UL-FET) with a trigger voltage Vt, including: an underlapped drain region coupled to the input pad; a source region coupled to ground; and a gate structure coupled to the input pad; and a blocking layer separating the underlapped drain region from the gate structure of the UL-FET by an underlap distance.

Abstract: The present invention provides a method for protecting a soil slope from rain erosion by improving with phosphogypsum and a microbe. The method includes: (1) placing Bacillus pasteurii in a culture medium to prepare a microbial solution, and mixing urea, calcium chloride and water to prepare a cementing solution; (2) mixing a mixture, the microbial solution and water well, and adding the cementing solution and water to prepare an improving mixture slurry; and (3) spraying the improving mixture slurry to a face of the slope twice by wet spraying, mixing the improving mixture slurry with grass seeds well, spraying to the face of the slope once, covering with a non-woven fabric by tying and fixing to the slope, and watering every day.

Abstract: Disclosed is a lateral double-diffused metal oxide semiconductor field effect transistor (LDMOSFET) with a replacement metal gate (RMG) structure that includes a first section, which traverses a semiconductor body at a channel region in a first-type well, and a second section, which is adjacent to the first section and which traverses the semiconductor body at a drain drift region in a second-type well. The RMG structure includes, in both sections, a first-type work function layer and a second-type work function layer on the first-type work function layer. However, the thickness of the first-type work function layer in the first section is greater than the thickness in the second section such that the RMG structure is asymmetric. Thus, threshold voltage (Vt) at the first section is greater than Vt at the second section and the LDMOSFET has a relatively high breakdown voltage (BV). Also disclosed are methods for forming the LDMOSFET.

Abstract: A rock mass shear test system for high-energy accelerator computed tomography (CT) scanning includes double horizontal loading devices, a first bearing device for bearing a static shear box, a second bearing device for bearing a dynamic shear box, and a normal loading device, etc. In the test, the double horizontal loading devices simultaneously apply an identical loading force to the rock mass, and the normal loading device applies a shear force to the rock mass. The double horizontal loading devices are provided in parallel and spaced apart, a loading force is applied in the horizontal direction, and a shear force is applied in the vertical direction, so that the loading cylinder and the rock mass sample are effectively prevented from interfering with each other during the accurate scanning process of the shearing progressive failure process of the rock mass.

Abstract: The present invention provides a method for protecting a soil slope from rain erosion by improving with phosphogypsum and a microbe. The method includes: (1) placing Bacillus pasteurii in a culture medium to prepare a microbial solution, and mixing urea, calcium chloride and water to prepare a cementing solution; (2) mixing a mixture, the microbial solution and water well, and adding the cementing solution and water to prepare an improving mixture slurry; and (3) spraying the improving mixture slurry to a face of the slope twice by wet spraying, mixing the improving mixture slurry with grass seeds well, spraying to the face of the slope once, covering with a non-woven fabric by tying and fixing to the slope, and watering every day.

Abstract: Design and construction method for improving an expansive soil embankment using phosphogypsum and microbes, including the following steps: (1) placing Bacillus pasteurii into a culture medium to prepare a microbial solution, and mixing urea and calcium chloride with water to prepare a cementing fluid; (2) mixing and stirring a mixture, the microbial solution and water, adding the cementing solution well, and mixing the cementing fluid with water to prepare an improved mixture; and (3) leveling and compacting original ground, laying geomembranes, the improved mixture, and geogrids, laying a last layer of geomembrane on the top surface of the embankment after pavement of the embankment, and paving a roadbed. The design and construction method can meet construction requirements of highway embankment projects and roadbed projects of first-grade and other grades of roads, and consume solid waste phosphogypsum.

Abstract: The present invention provides a construction method for ecologically protecting an expansive soil slope by combining phosphogypsum with microbial mineralization. The method includes: (1) placing Bacillus pasteurii in a culture medium to prepare a microbial solution, and mixing urea, calcium chloride and water to prepare a cementing solution; (2) preparing a mixture with phosphogypsum fly ash and soil; mixing the mixture, the microbial solution and water well, and adding the cementing solution and water to prepare an improving mixture slurry; and (3) spraying the improving mixture slurry to a face of the slope by wet spraying, and covering with a non-woven fabric by tying and fixing.