Patents Issued in May 9, 2024
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Publication number: 20240150232Abstract: A vehicle window, includes at least one transparent glass pane and an IR-reflective coating on a surface of the glass pane, wherein the IR-reflective coating includes n metallic layers and (n+1) dielectric layer modules, wherein the layer modules are implemented as dielectric layers or layer sequences and wherein the layer modules and the metallic layers are arranged alternatingly such that each metallic layer is arranged between two layer modules, where n is a natural number greater than or equal to 1, wherein each metallic layer is implemented as a discontinuous layer of metal nanocrystals, which has regions that are occupied by metal nanocrystals and regions that are not occupied by nanocrystals. The uppermost layer module has a dielectric anti-reflection layer with a refractive index of at most 1.7.Type: ApplicationFiled: February 23, 2022Publication date: May 9, 2024Inventors: Julie RUFF, Sebastian JANZYK, Jan HAGEN
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Publication number: 20240150233Abstract: Glass-based articles comprise stress profiles providing improved fracture resistance. The glass-based articles herein provide high fracture resistance after multiple drops.Type: ApplicationFiled: January 12, 2024Publication date: May 9, 2024Inventors: Timothy Michael Gross, Xiaoju Guo, Jason Thomas Harris, Peter Joseph Lezzi, Alexandra Lai Ching Kao Andrews Mitchell, Pascale Oram, Kevin Barry Reiman, Rostislav Vatchev Roussev, Ljerka Ukrainczyk
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Publication number: 20240150234Abstract: A glass article includes lithium aluminosilicate, includes a first surface, a second surface opposed to the first surface, a first compressive region extending from the first surface to a first compression depth, a second compressive region extending from the second surface to a second compression depth, and, a tensile region disposed between the first compression depth and the second compression depth, where a stress profile of the first compressive region has a first local minimum point at which the stress profile is convex downward and a first local maximum point at which the stress profile is convex upward, where a depth of the first local maximum point is greater than a depth of the first local minimum point, and where a stress of the first local maximum point is greater than a compressive stress of the first local minimum point.Type: ApplicationFiled: January 12, 2024Publication date: May 9, 2024Inventors: Su Jin SUNG, Byung Hoon KANG, Seung KIM, Young Ok PARK, Gyu In SHIM
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Publication number: 20240150235Abstract: Reaction schemes involving acids and bases; reactors comprising spatially varying chemical composition gradients (e.g., spatially varying pH gradients), and associated systems and methods, are generally described.Type: ApplicationFiled: December 22, 2023Publication date: May 9, 2024Applicant: Massachusetts Institute of TechnologyInventors: Yet-Ming Chiang, Leah Ellis, Andres Badel
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Publication number: 20240150236Abstract: The present invention relates to apparatus for thermal treatment of a mineral starting material, wherein the apparatus comprises a calciner, wherein the calciner comprises at least a first calciner section and a second calciner section, wherein the first calciner section is arranged vertically, wherein the second calciner section is arranged at an incline, wherein the second calciner section has an angle ? between the horizontal and the flow direction of the second calciner section, wherein the angle ? is between 20° and 80°, wherein the first calciner section has a first hydraulic diameter dh,1, wherein the second calciner section has a second hydraulic diameter dh,2, wherein the second hydraulic diameter dh,2 is less than or equal to the first hydraulic diameter dh,1 multiplied by the sine of the angle ?.Type: ApplicationFiled: March 18, 2022Publication date: May 9, 2024Applicants: thyssenkrupp Polysius GmbH, thyssenkrupp AGInventors: Eike WILLMS, Patrick BRUNELOT, Martin UHDE, Olaf ONTRUP, Constantin KIMMIG, Jost LEMKE
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Publication number: 20240150237Abstract: Method for grinding a solid in a vertical roller mill (VRM) and a cement composition prepared by the disclosed methods. A method comprises grinding a solid comprising a cement clinker under a water spray in the presence of a grinding stabilizing additive, wherein the grinding stabilizing additive comprises: (i) an alkanol amino acid compound or a disodium or dipotassium salt thereof having the structural formula: (ii) a glycol; or a mixture of (i) and (ii), wherein the water spray level is reduced by at least 5% compared to a control. Cement compositions prepared by the disclosed methods have the pre-hydration level (Wk) equal to or less than 1.5%. The values and preferred values of R1-3 are disclosed herein.Type: ApplicationFiled: December 1, 2023Publication date: May 9, 2024Inventors: Joshua Detellis, Jeffrey Thomas, Josephine H. Cheung, David F. Myers
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Publication number: 20240150238Abstract: A filtering well has a body defining an inner volume, the body having a mineral membrane made of a pervious concrete composition in order to filter water flow into the inner volume of the body. An outlet conduit is in fluid communication with the inner volume for discharging water therefrom. The outlet conduit is formed in the mineral membrane of the body. Other aspects are also disclosed.Type: ApplicationFiled: March 10, 2022Publication date: May 9, 2024Inventors: Serge BAILLARGEON, Eric BARD
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Publication number: 20240150239Abstract: Roofing granules comprising agglomerated inorganic material, and building materials, such as shingles, that include such roofing granules. By fabricating roofing granules from agglomerating inorganic material, in combination with a binder composition having a wetting agent, it is possible to increase the yield of the fabricated roofing granules and tailor the particle size distribution so as to provide optimal shingle surface coverage, thus reducing shingle weight and usage of raw materials. Additionally, the use of agglomeration permits the utilization of by-products from conventional granule production processes.Type: ApplicationFiled: November 8, 2023Publication date: May 9, 2024Inventor: Peter Wilson
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Publication number: 20240150240Abstract: Synthetic aggregate that includes a plurality of agglomerations. Each of the plurality of agglomerations may include a core; and a shell material disposed on the core. According to various embodiments, the construction aggregate may be non-flammable. According to various embodiments, at least one agglomeration of the plurality of agglomerations may have a plurality of cores. The core may include coal, a coal byproduct, and combinations thereof. According to various embodiments, the coal may be a type such as lignite, sub-bituminous, bituminous, and anthracite. The coal byproduct may be fly ash, bottom ash, shale coal, or coal gob.Type: ApplicationFiled: April 26, 2022Publication date: May 9, 2024Inventors: Arnold HILL, Walter SHERWOOD, William EASTER
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Publication number: 20240150241Abstract: The present invention relates to a novel method for the production of an encapsulated system for the self-healing of cracks formed within the matrix of building materials, preferably cementitious materials, such as concrete, mortar or render. Further, the invention refers to a novel encapsulated system comprising a cement-based active core and a hydrated cement-based protective shell, and to the use of said encapsulated system for the self-healing of cementitious materials such as concrete or mortar.Type: ApplicationFiled: March 4, 2022Publication date: May 9, 2024Applicant: National Centre for Scientific Research DemokritosInventors: Ioannis Karatasios, Stamatoula Papaioannou, Maria Amenta, Dimitrios Gournis, Vassilios Kilikoglou
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Publication number: 20240150242Abstract: A three-part epoxy grout composition comprises a liquid epoxy blend, a liquid hardener, and a graded particulate aggregate, wherein the dry aggregate particles are pretreated with an applied adhesion promoter in an amount of 0.01 to 5% by weight. The volume of pretreated aggregate particles, when mixed with the epoxy blend and the hardener, comprises at least 70% by volume of the cured grout. Pretreatment of the aggregate by coating with adhesion promoter allows more efficient use of chemicals along with improved strength. Related methods are also disclosed.Type: ApplicationFiled: November 8, 2022Publication date: May 9, 2024Inventors: Lawrence S. Shapiro, Michael K. Harvey, Scott Atom Saverse, Douglas A. Cheney, Zbigniew Andrew Szczepaniak, Brandon Michael Belcher, Paul Matz, Timothy Patrick Fitzgerald, Shawn Thomas Noble
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Publication number: 20240150243Abstract: It discloses a sustained release grouting material, a preparation method and an application thereof; the sustained release grouting material comprises a water swelling core and a water-soluble sustained release coating, the water swelling core is composed of bentonite, SAP and xanthan gum, which is granulated by disc granulator relying on the cohesiveness of xanthan gum; the water-soluble sustained-release coating is prepared by mixing water-soluble starch, polyvinyl alcohol, poloxamer, lubricant and plasticizer with deionized water to obtain a film-forming solution, and the film-forming solution is coated on a coating machine; the invention uses a coating machine to coat a layer of slow-release coating on the surface of the water-absorbing expansion core, and adjusts the coating thickness by controlling the mass ratio of the coating film-forming liquid to the water-absorbing expansion core particles, so as to realize the controllable water absorption onset time of the expansion core.Type: ApplicationFiled: November 6, 2023Publication date: May 9, 2024Applicant: SHANDONG UNIVERSITY OF SCIENCE AND TECHNOLOGYInventors: Lihua Wang, Chunfeng Li, Zhijie Wen, Zengguang Pang, Xiaoming Fan, Qinghua Shu, Shifu Sun, Qingbiao Wang, Chunquan Dai, Weiwei Han, Shunrong Wang
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Publication number: 20240150244Abstract: Perlite-free, lightweight setting-type joint compounds which comprise calcium sulfate hemihydrate with a dry density of less than 50 lb/ft3, a foaming agent having a HLB value of at least 10 and preferably comprising an alkylbenzene sulfonic acid having a linear alkyl chain containing 8 to 14 carbons and/or a salt thereof, and a combination of rheology modifiers. Methods for building wallboard assemblies and methods for wall patch and repair projects that include applying the perlite-free, lightweight setting-type joint compounds to a substrate.Type: ApplicationFiled: June 2, 2023Publication date: May 9, 2024Inventors: Alexander J. DONOVAN, Naveen PUNATI
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Publication number: 20240150245Abstract: Embodiments of the present disclosure generally relate to methods and materials for fabricating building materials and other components from coal. More specifically, embodiments of the present disclosure relate to materials and other components, such as char clay plaster, char brick, and foam glass fabricated from coal, and to methods of forming such materials. In an embodiment is provided a building material fabrication method. The method includes mixing an organic solvent with coal, under solvent extraction conditions, to form a coal extraction residue, and heating the coal extraction residue under pyrolysis conditions to form a pyrolysis char, the pyrolysis conditions comprising a temperature greater than about 500° C. The method further includes mixing the pyrolysis char with water and with one or more of clay, cement, or sand to create a mixture, and molding and curing the mixture to form a building material. Pyrolysis char-containing materials are also disclosed.Type: ApplicationFiled: January 12, 2024Publication date: May 9, 2024Inventors: GANG TAN, Tengyao JIANG, Jennifer Tanner EISENHAUER, Richard HORNER
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Publication number: 20240150246Abstract: Embodiments of the present disclosure generally relate to methods and materials for fabricating building materials and other components from coal. More specifically, embodiments of the present disclosure relate to materials and other components, such as char clay plaster, char brick, and foam glass fabricated from coal, and to methods of forming such materials. In an embodiment is provided a building material fabrication method. The method includes mixing an organic solvent with coal, under solvent extraction conditions, to form a coal extraction residue, and heating the coal extraction residue under pyrolysis conditions to form a pyrolysis char, the pyrolysis conditions comprising a temperature greater than about 500° C. The method further includes mixing the pyrolysis char with water and with one or more of clay, cement, or sand to create a mixture, and molding and curing the mixture to form a building material. Pyrolysis char-containing materials are also disclosed.Type: ApplicationFiled: January 12, 2024Publication date: May 9, 2024Inventors: Gang TAN, Tengyao JIANG, Jennifer Tanner EISENHAUER, Richard HORNER
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Publication number: 20240150247Abstract: A control process for controlling a production process for calcined clays with a calciner including, capture of at least one temperature in the calciner, taking of at least one sample of the calcined clay, production of a reproducible size distribution of the sample, adjustment of the sample mass, conditioning of the sample to a first measuring temperature and of an alkali to a first measuring temperature, combining of the sample with an alkali, temporal capture of the energy generated by the sample-alkali mixture, quantitative evaluation of the time-energy profile captured for the first exothermic reaction and determination of the amount of energy released by the sample, correlation of the amount of energy captured with the temperature and residence time captured, and comparison with previously captured combinations, temperature and residence time values.Type: ApplicationFiled: March 15, 2022Publication date: May 9, 2024Applicants: thyssenkrupp Polysius GmbH, thyssenkrupp AGInventors: Michael ENDERS, Guido GRUND
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Publication number: 20240150248Abstract: The present invention relates to a low-temperature co-fired ceramic powder and a preparation method and application thereof. The material composition of the low-temperature co-fired ceramic powder is xRO-yM2O3-zXO2, where R is at least one of Mg, Ca, Ba, Zn, Cu, and Pb, M is at least one of B, Al, Co, In, Bi, Nd, Sm, and La, X is at least one of Si, Ge, Sn, Ti, Zr, and Hf, 0?x?85 wt %, 15 wt %?y?90 wt %, 10 wt %?z?85 wt %, and x+y+z=1; and the low-temperature co-fired ceramic powder is obtained by high-temperature melting, quenching, and recrystallization treatment. The temperature of high-temperature melting is 1,200° C. to 1,600° C., and the temperature of recrystallization treatment is 500° C. to 900° C.Type: ApplicationFiled: November 17, 2021Publication date: May 9, 2024Inventors: Feng LIU, Yongyuan LIANG, Tan LV, Hangfeng JIN
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Publication number: 20240150249Abstract: When a large-sized silicon nitride substrate having high thermal conductivity is produced, a portion where the thermal conductivity is low is generated, which causes reduction in yield (pass rate). Provided is a silicon nitride substrate in which ?e/?c, which is a ratio of a thermal conductivity ?c at a center portion of the substrate to a thermal conductivity ?e at an end portion of the substrate, is 0.85 to 1.15. Preferably, the silicon nitride substrate has a size of 150 mm×150 mm or more. In the silicon nitride substrate, the ?c and the ?e each are preferably 100 W/m·K or more.Type: ApplicationFiled: March 15, 2022Publication date: May 9, 2024Inventors: Youichirou KAGA, Rei FUKUMOTO, Kei SHIMADA
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Publication number: 20240150250Abstract: Methods and systems are provided for producing silicon carbide. The system comprises an enclosure configured to be maintained under vacuum conditions and at a processing temperature above a melting temperature of silicon, a vapor production system configured to supply a silicon vapor to the enclosure, and a transportation system configured to provide a stream of graphite powder into the enclosure, retain the graphite powder within the enclosure for a processing time sufficient to react the graphite powder with the silicon vapor to produce a silicon carbide powder, and then provide a stream of the silicon carbide powder out of the enclosure.Type: ApplicationFiled: November 7, 2022Publication date: May 9, 2024Applicant: HONEYWELL INTERNATIONAL INC.Inventors: Mehrad Mehr, Bahram Jadidian
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Publication number: 20240150251Abstract: Methods for repairing a defect in a multilayered coating on a silicon-containing substrate are provided, along with the resulting compared component. The method includes: applying a first patch slurry into the defect; drying the first patch slurry to form a dried first patch layer; applying a second patch slurry into the defect and on the dried first patch layer; and drying the second patch slurry to form a second dried patch layer.Type: ApplicationFiled: November 3, 2022Publication date: May 9, 2024Inventors: Atanu Saha, Don Mark Lipkin, Sreerama Prasad R, Mamatha Nagesh, Nicholas Edward Antolino
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Publication number: 20240150252Abstract: The present invention comprises one or more organic solvents that create a non-aqueous organo solvent delivery system. (NOSDS), and one or more Organo Polycarboxylate functionalities, OPCF, that results in a stable, non-aqueous solution that can easily, safely, evenly and economically coat nitrogen source granules and/or be added to a mobile liquid form of a nitrogen source such as an aqueous dispersion, pressurized ammonia gas or molten urea and/or molten modified urea. Using these solvents provides more flexibility for nitrogen source manufacturers to produce nitrogen sources designed for a particular soil or plant. The liquid solutions are comprised of NOSDS and OPCFs and one or more of a) nitrification inhibitors, b) urease inhibitors, c) pesticides, d) fungicides, e) herbicides, f) insecticides and g) micronutrients.Type: ApplicationFiled: January 12, 2024Publication date: May 9, 2024Inventors: Gary David McKnight, Randall Linwood Rayborn
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Publication number: 20240150253Abstract: A method of increasing organic carbon in a soil is disclosed. The method includes inoculating the soil and/or a plant growing in the soil with one or more fungal strains from at least one genus selected from the group consisting of Acrocalymma, Clonostachys, Leptodontidium, Periconia, Phaeosphaeria, Thozetella, Trichoderma, and a combination thereof, wherein the one or more fungal strains are in an amount effective to increase organic carbon in the soil compared to a non-inoculated control soil. Also disclosed is a method of enhancing plant growth, comprising: applying to a plant, a plant part, or the locus surrounding the plant with one or more fungal strains from at least one genus selected from the group consisting of Acrocalymma, Clonostachys, Leptodontidium, Periconia, Phaeosphaeria, Thozetella, Trichoderma, and a combination thereof in an amount effective to enhance the growth of the plant as compared to an untreated control plant.Type: ApplicationFiled: January 6, 2024Publication date: May 9, 2024Inventors: Ray RILEY, Andres Reyes, Abed Chaudhury, Suresh Subashchandrabose, Ahsanul Haque, Neeraj Purushotham, Raghvendra Sharma, Tegan Nock, Gyongyver Korosi, Brooke Bruning, Grace Scott, Venkatachalam Lakshmanan
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Publication number: 20240150254Abstract: A system and method for preparing a microbial supplement, and applying the supplement to plants, trees and other items to promote their growth. The supplement comprises seawater, including microbes that naturally exist in seawater. Seawater is harvested containing microbes in an inactive or dormant state. The seawater undergoes a filtration, mineralization and oxygenation process to reduce sodium chloride levels, to increase the levels of desirable minerals in the seawater and to oxygenate the seawater to keep the microbes alive, though in a dormant or inactive state. The microbes are maintained in an inactive or dormant state through the preparation process, but become active when the supplement is applied to plants or trees, thereby promoting agricultural growth.Type: ApplicationFiled: November 8, 2023Publication date: May 9, 2024Inventor: Parshuram Nirajan Shastri
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Publication number: 20240150255Abstract: A composition that includes (a) at least one of basalt, metabasalt, diabase, andesite, meta-andesite, phyllite, rhyolite, or a combination thereof, with the at least one of basalt, metabasalt, diabase, andesite, meta-andesite, phyllite, rhyolite, or a combination thereof being present at 30 wt % to 70 wt % based on a total weight of the composition, (b) an organic portion that is present at 20 wt % to 65 wt % based on the total weight of the composition, and (c) a binder. The composition is in the form of a plurality of particles. The composition can find applications in agriculture, horticulture, and gardening, and can be used, e.g., as soil amendment.Type: ApplicationFiled: October 31, 2023Publication date: May 9, 2024Inventors: Raju Khatiwada, Peter Wilson, Jason Clark
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Publication number: 20240150256Abstract: Thermite mixtures shaped or cast into a desired solid form and having sufficient structural integrity to withstand rough handling and challenging operating conditions, and methods of making such solid forms, are provided. When reacted, the thermite mixtures advantageously produce little or no offgas. The solid thermite forms may further include other materials that confer advantageous physical or chemical properties before, during, or after reaction of the thermite mixture.Type: ApplicationFiled: December 18, 2023Publication date: May 9, 2024Inventor: John A. Bognar
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Publication number: 20240150257Abstract: The invention describes a monopropellant fuel that is a mixture in water of a water-soluble hydrocarbon fuel and hydrogen peroxide, where the hydrocarbon fuel and hydrogen peroxide are present in an approximately stoichiometric amount calculated to produce only carbon dioxide and water, wherein water is present in an amount at least 30% of the total weight of the monopropellant fuel.Type: ApplicationFiled: November 8, 2022Publication date: May 9, 2024Applicant: James R Moden, Inc.Inventor: Kenneth Moden
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Publication number: 20240150258Abstract: The present disclosure provides a fire starter that does not require oxygen from the air to ignite or maintain a flame and makes it easy to ignite using one or no fingers, such as teeth. A fire starter includes a burnable casing forming a sealed chamber. A first burnable mixture and a second burnable mixture are separately disposed in the sealed chamber. The first burnable mixture can form a flame without oxygen from the air. An igniter is disposed in the sealed chamber adjacent to the first burnable mixture and configured to generate a first thermal event to ignite the first burnable mixture without oxygen from the air. The first burnable mixture combusts during the first thermal event and triggers a second thermal event to ignite the second burnable mixture. An actuator is configured to activate the igniter to generate the first thermal event without using more than one finger.Type: ApplicationFiled: November 3, 2022Publication date: May 9, 2024Applicant: 3rd Light IP Holdings LLCInventors: James ROSE, John PERRIAM
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Publication number: 20240150259Abstract: The invention relates to a process for producing olefins from oxygenates with variable production of ethylene and propylene. According to the invention, the process is switched from a state 1 with lower ethylene production to a state 2 with higher ethylene production in that: the fraction C2re of the ethylene product stream which is recycled to the OTO reactor is lowered from a first value C2re,1 to a second value C2re,2, resulting in a change dC2re=C2re,1?C2re,2, the fraction C4+re of the C4+ product stream containing C4+ olefins which is recycled to the OTO reactor is lowered from a first value C4+re,1 to a second value C4+re,2, resulting in a change dC4+re=C4+re,2?C4+re,1, where the changes dC2re and dC4+re in a mass flow ratio dC4+re/dC2re, where the mass flow ratio is between 70% and 130%.Type: ApplicationFiled: November 7, 2023Publication date: May 9, 2024Inventors: Stephane HAAG, Martin GORNY, Bryce WILLIAMS, Thomas RENNER
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Publication number: 20240150260Abstract: A process for producing ethylene comprising introducing fuel, ethane/higher hydrocarbons, oxygen, steam to annular jet vortex chamber having combustion upstream of cracking to provide swirling fluid flow pattern producing cracking product (ethylene, acetylene, ethane, methane, 10-60 wt. % water, CO2, CO, hydrogen, oxygenates) having first temperature; cooling cracking product with residence <2,000 milliseconds yielding first cooled product having second temperature lowered by ?30° C.; cooling first cooled product yielding second cooled product having third temperature lowered by ?300° C.Type: ApplicationFiled: March 7, 2022Publication date: May 9, 2024Inventors: Zheng Liu, Murali Gopalakrishnan, Stephen Keith Turner, Sreekanth Pannala
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Publication number: 20240150261Abstract: A method for producing a target compound, includes distributing feed mixture at a temperature in a first temperature range to a plurality of parallel reaction tubes of a shell-and-tube reactor. The method further includes subjecting the feed mixture in first tube sections of the reaction tubes to heating to a temperature in a second temperature range, and in second tube sections of the reaction tubes arranged downstream of the first tube sections to oxidative catalytic conversion using one or more catalysts arranged in the second tube sections. The heating is performed, at least in part, using a catalyst arranged in the first tube sections and having a light-off temperature in the first temperature range.Type: ApplicationFiled: March 14, 2022Publication date: May 9, 2024Inventors: Mathieu Zellhuber, Martin Schubert, Andreas Meiswinkel, Wolfgang Muller, Ernst Haidegger, Gerhard Mestl, Klaus Wanninger, Peter Scheck
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Publication number: 20240150262Abstract: Producing a product hydrocarbon includes subjecting a feed mixture containing a feed hydrocarbon and oxygen to selective oxidation to obtain a product mixture containing product hydrocarbon and water. A subsequent mixture is formed from a portion of the product mixture by separating a portion of the water. Oxygen in the feed mixture is partially converted during the selective oxidation, so that the product mixture has a first residual oxygen content and the subsequent mixture has a second residual oxygen content. Detection of the first and/or the second residual oxygen content is performed using a first measuring device. A second measuring device at the end of the catalyst bed detects temperature. Using a process control and/or evaluation unit, measurement data of the first and/or second measuring device(s) are detected and are evaluated and/or processed while obtaining follow-up data. Process control is carried out on the basis of the follow-up data.Type: ApplicationFiled: March 14, 2022Publication date: May 9, 2024Inventors: Mathieu Zellhuber, Martin Schubert, Andreas Meiswinkel, Anina Wohl
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Publication number: 20240150263Abstract: A process for producing a target compound includes forming a feed mixture containing at least one reactant compound. The feed mixture is distributed to parallel reaction tubes of one or more shell-and-tube reactors and subjected to oxidative catalytic conversion in the reaction tubes. Steam is added to the feed mixture in an amount such that a steam fraction of the feed mixture is 5 to 95 vol %, oxygen is added to the feed mixture in the form of a fluid containing at least 95 vol % oxygen, and the oxidative catalytic conversion is carried out using one or more catalysts containing the metals molybdenum, vanadium, niobium and optionally tellurium.Type: ApplicationFiled: March 14, 2022Publication date: May 9, 2024Inventors: Mathieu Zellhuber, Martin Schubert, Andreas Meiswinkel, Gerhard Mestl, Klaus Wanninger, Peter Scheck, Anina Wohl
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Publication number: 20240150264Abstract: The invention relates to a process for obtaining isobutene from an isobutene containing C4-hydrocarbon mixture (1) in a plant comprising an etherification unit (3), a first distillation unit (5), an ether cleavage unit (10) and a second distillation unit (12), the process comprising: (a) contacting the C4-hydrocarbon mixture (1) with a primary alcohol (2) and reacting the mixture with the primary alcohol in the presence of an acidic catalyst to form the corresponding alkyl tert-butyl ether in the etherification unit (3); (b) distilling the reaction mixture (4) from the etherification unit (3) in the first distillation unit (5), a C4-hydrocarbon raffinate being withdrawn as the overhead product (6), and the alkyl tert-butyl ether being withdrawn as the bottom product (7); (c) vaporizing the bottom product from the first distillation unit (5) in an evaporator (8) obtaining a vapor stream (9); (d) reacting the vapor stream (9) of step (c) in the presence of an acidic catalyst obtaining isobutene and the primaryType: ApplicationFiled: March 1, 2022Publication date: May 9, 2024Inventors: Suman THOTLA, Hans-Guenter Wagner, Randolf HUGO, Gerrit WATERS, Michael HUEBNER, Markus NEUDERT, Thomas ROUSSIERE
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Publication number: 20240150265Abstract: A terpene extraction process may include the steps of: (A) providing a container with a biomass containing extractable materials including both water and terpenes; (B) passing a first gas over the biomass; (C) moving at least a portion of the extractable materials from the biomass into the first gas to form a second gas; (D) moving the second gas into a cold trap assembly to cool the second gas; (E) measuring a water vapor content of the second gas; (F) comparing the water vapor content to a predetermined value; and (G) stopping the extraction process when the water vapor content is less than the predetermined value.Type: ApplicationFiled: November 7, 2023Publication date: May 9, 2024Inventors: William KIMMERLE, Kyle KIMMERLE
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Publication number: 20240150266Abstract: Chemical processes are disclosed that react iron tetracarbonyl dichloride with an alkyl phosphate producing carbon monoxide and a compound represented by the formula FeCl2—(O?P(OR)3)n where n is an integer. Simultaneously or subsequently an alkene with carbon tetrachloride may be reacted in the presence of the compound represented by the formula FeCl2—(O?P(OR)3)n where n is an integer to produce a chlorinated hydrocarbon.Type: ApplicationFiled: November 13, 2023Publication date: May 9, 2024Inventor: Randolph Belter
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Publication number: 20240150267Abstract: The present disclosure provides a process for producing trifluoroiodomethane, the process comprising providing a reactant stream comprising hydrogen iodide and at least one trifluoroacetyl halide selected from the group consisting of trifluoroacetyl chloride, trifluoroacetyl fluoride, trifluoroacetyl bromide, and combinations thereof, reacting the reactant stream in the presence of a first catalyst at a first reaction temperature from about 25° C. to about 400° C. to produce an intermediate product stream comprising trifluoroacetyl iodide, and reacting the intermediate product stream in the presence of a second catalyst at a second reaction temperature from about 200° C. to about 600° C. to produce a final product stream comprising the trifluoroiodomethane.Type: ApplicationFiled: December 8, 2023Publication date: May 9, 2024Inventors: Haridasan K. Nair, Glenn Matthies, Rajiv Ratna Singh, Terris Yang, Haiyou Wang, Ryan J. Hulse, Rajiv Banavali
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Publication number: 20240150268Abstract: Processes for converting methane into methanol are disclosed in which methane, water, and a supported chromium (VI) catalyst are contacted with a light beam at a wavelength in the UV-visible spectrum in an oxidizing atmosphere in a single reactor to form a reaction product comprising methanol, followed by discharging a reactor effluent containing the reaction product from the single reactor, and then separating methanol from the reaction product. Processes to produce methanol using additional reactors also are described, as well as related methanol production systems.Type: ApplicationFiled: October 26, 2023Publication date: May 9, 2024Inventors: Jamie N. Sutherland, James Hillier, Gregory G. Hendrickson, Max P. McDaniel
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Publication number: 20240150269Abstract: The present application describes process for preparing an ortho-allylated hydroxy aryl compounds such as compounds of Formula (1) by reacting an allylic alcohol with a hydroxy aryl compound in the presence of aluminum compound selected from alumina and aluminum alkoxides and in a non-protic solvent wherein at least one carbon atom ortho to the hydroxy group in the hydroxy aryl compound is unsubstituted. The present application also includes compounds of Formula (1).Type: ApplicationFiled: September 26, 2023Publication date: May 9, 2024Applicant: McMaster UniversityInventors: Jakob Magolan, Nicholas Jentsch, Xiong Zhang, Mathew Piotrowski, Patrick Darveau, Meghan Fragis, Jarrod Johnson, Nicole Ritchie, Arnav Kaul
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Publication number: 20240150270Abstract: A method of selectively recovering a lipophilic target substance. An insoluble adsorbent is exposed to a solution of the target substance in a lipophilic solvent. Adsorption of the adsorbent with the target substance is facilitated by addition of hydrophilic solvent, which is less hydrophobic than the lipophilic solvent, to the solution during or after exposure of the solution to the insoluble adsorbent, lowering the temperature of the solution or evaporating a portion of the lipophilic solvent. The adsorbent Is isolated from the solution. For desorbing and recovering the target substance, a hydrophobic dissociation fluid may be combined with the adsorbent, a temperature of the adsorbent may be increased or a portion of the hydrophilic solvent may be evaporated. A solution may be exposed to one or more adsorbents for recovering additional lipophilic target substances, recovering hydrophilic target substances or removing unwanted substances.Type: ApplicationFiled: November 13, 2023Publication date: May 9, 2024Applicant: GROW GROUP PLCInventors: Christopher James Cordier, Sadaf Saad Anjum, Benjamin Thomas Langley, Ian Joseph Atkinson
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Publication number: 20240150271Abstract: The present invention is directed to methods for the preparation of (CnF2n+1)O-substituted arenes and heteroarenes and the direct perfluoralkoxy lation of arenes and heteroarenes with a (CnF2n+1)O-group, respectively. characterized in that a peroxide reagent according to the general formula (I): (CnF2n+1)2 (I) is fragmented in the presence of an electron transferring catalyst under (CnF2n+1)O-radical formation, and said (CnF2n+1)O-radical then substitutes a C—H bond of an arene or heteroarene C—H bond with a (CnF2n+1)O-group, wherein in the above formulae, n is an integer in the range from 1 to 4.Type: ApplicationFiled: February 21, 2022Publication date: May 9, 2024Applicant: Solvay SAInventors: Sebastian Hasenstab-Riedel, Matthew Hopkinson, Stefan Dix, Paul Golz, Jonas Rachid Schmid, Holger Pernice, Sebastian Gutmann
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Publication number: 20240150272Abstract: A processes for purifying glycol ethers, comprises (a) providing a glycol ether to a first vessel, the glycol ether, the glycol ether having the following formula: R1—O— (CHR2CHR3) O)nR4; wherein R1 is an alkyl group having 1 to 9 carbon atoms or a phenyl group; wherein R2 and R3 each individually is hydrogen, a methyl group or an ethyl group, provided that when R3 is a methyl group or an ethyl group, R2 is hydrogen and provided that when R2 is a methyl group or an ethyl group, R3 is hydrogen; wherein R4 is hydrogen, an alkyl group having 1 to 4 carbon atoms, an acetyl group, or a propionyl group; and wherein n is an integer of 1 to 3; (b) filling the first vessel with inert gas; (c) heating the glycol ether in the first vessel to a sub-boiling temperature, wherein the sub-boiling temperature is at least 15° C.Type: ApplicationFiled: May 19, 2021Publication date: May 9, 2024Inventors: Qi Jiang, Kaoru Ohba, Yujun Liu
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Publication number: 20240150273Abstract: Disclosed are an abietane type diterpene compound, a preparation method and an application thereof, relating to the technical field of anti-tumor compounds, where the compound has a chemical structure as shown in the following formula I: Leucosceptrum canum is extracted to prepare the abietane type diterpene compound according to the present application, and the prepared compound is effectively applied in inhibiting human lung cancer cell A549 and human myeloid leukemia cell HL-60.Type: ApplicationFiled: January 31, 2023Publication date: May 9, 2024Inventors: Mingfeng XU, Xiaohong DENG, Jinfeng LIANG, Yidi CHEN, Jing REN, Qin ZHU
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Publication number: 20240150274Abstract: A method for producing adipic acid and cyclohexanone oxime from cyclohexane is provided. Cyclohexane and NOx undergo oxidation-nitration reaction to produce a mixture of adipic acid, nitrocyclohexane, nitrogen oxides and by-product A, from which adipic acid and nitrocyclohexane are separated. The nitrocyclohexane is catalytically hydrogenated with hydrogen to produce cyclohexanone oxime and a small amount of cyclohexylamine, where cyclohexanone oxime is collected, and the cyclohexylamine is partially oxidized with molecular oxygen to obtain cyclohexanone oxime and by-product B. Without separation, or after removing part or all of water from the reaction mixture, under the action of a catalyst, the reaction mixture undergoes hydrogenation and amination simultaneously or sequentially, or the hydrogenation alone, and separation to give cyclohexanone oxime.Type: ApplicationFiled: August 15, 2023Publication date: May 9, 2024Inventors: He'an LUO, Kuiyi YOU, Jian JIAN, Pingle LIU, Wenjin NI, Qiuhong AI
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Publication number: 20240150275Abstract: Antifouling compositions are provided. The antifouling compositions include a dispersing agent including an imidazoline, a solvator including a phthalate, and a promoter agent including an acylamide. Methods of mitigating fouling caused by the polymerization of monomers using the compositions of the disclosure are also provided. The methods of mitigating fouling of monomers include a step of adding a composition of the disclosure to the monomer. In some instances, the monomer is an ethylenically unsaturated monomer, such as (meth)acrylic acid, methyl methacrylate, an acrylic acid ester, methacrylamide sulfate, vinyl acetate, acrylonitrile, acrolein, an acrylate, a methacrylate, 1,3-butadiene, styrene, isoprene, and any combination thereof. Methods of preparing the antifouling compositions are also provided.Type: ApplicationFiled: October 20, 2023Publication date: May 9, 2024Applicant: ECOLAB USA Inc.Inventor: Meng KONG
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Publication number: 20240150276Abstract: The present invention relates to a process for the solidification of hexyl 2-[4-(diethylamino)-2-hydroxybenzoyl]benzoate (INCI diethylamino hydroxybenzoyl hexyl benzoate, DHHB), wherein the process comprises the step of (a) applying a shear rate of 800 s?1 or more to liquid hexyl 2-[4-(diethylamino)-2-hydroxybenzoyl]benzoate and (b) adding seed crystals of hexyl 2-[4-(diethylamino)-2-hydroxybenzoyl]benzoate.Type: ApplicationFiled: March 1, 2022Publication date: May 9, 2024Inventors: Daniel Ruben SELZER, Eva KLEINMANN, Axel BINDER, Helmut KRONEMAYER, Philipp STAEHLE
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Publication number: 20240150277Abstract: The present invention includes compounds of formula (I) and methods for its preparation and treatment of disorders with activated peroxisome preoliferator-activated receptor gamma (PPARG), particularly cancer.Type: ApplicationFiled: August 31, 2023Publication date: May 9, 2024Applicants: Bayer Aktiengesellschaft, The Broad Institute, Inc., Dana-Farber Cancer Institute, Inc.Inventors: Stephan SIEGEL, Knut EIS, Timo STELLFELD, Léa Aurelie BOUCHÉ, Elisabeth POOK, Joseph Peter BLUCK, Philip LIENAU, Constantia PANTELIDOU, Isabel Sophie JERCHEL-FURAU, Ulf BRÜEGGEMEIER, Sven CHRISTIAN, Detlev SÜLZLE, Anders Roland FRIBERG, Simon HOLTON, Christian LECHNER, Stefan KAULFUSS, Hanna MEYER, Douglas ORSI, Steven James FERRARA, Jonathan GOLDSTEIN, Matthew MEYERSON, Christopher LEMKE
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Publication number: 20240150278Abstract: A process for converting caprolactam to aminocapronitrile (ACN), the process comprising contacting a caprolactam feed stream with ammonia to produce a first crude product stream; separating the first crude product stream to produce an intermediate product stream comprising ACN and caprolactam recovery stream; and purifying the intermediate product stream to produce a purified product stream comprising greater than 95 wt % aminocapronitrile.Type: ApplicationFiled: November 3, 2023Publication date: May 9, 2024Applicant: Ascend Performance Materials Operations LLCInventors: C. Alex Diaz, Mikhail I. Khramov, Scott G. Moffatt
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Publication number: 20240150279Abstract: Stably consolidated compounds assembled from a statin and a metformin analog, and metabolically labile dual prodrugs assembled from the same, methods of making both, and methods of using them to treat metabolic diseases such as cancers are described.Type: ApplicationFiled: February 1, 2022Publication date: May 9, 2024Applicant: The University of ToledoInventors: Paul Erhardt, Shi-He Liu, Francis Charles Brunicardi, Divya Andy
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Publication number: 20240150280Abstract: Novel 85Rb-enriched rubidium salt compounds of general formula 1, below and novel compounds of general formula 2, below. Compositions that contain at least one of the novel compounds and optionally further contain an antitumor drug. Methods that entail administering such compounds and compositions to treat cancer, optionally in combination with a conventional form of cancer therapy, such as chemotherapy and radiation treatment. When administered with a conventional form of cancer therapy, the compounds and compositions of the invention may be administered before, simultaneously with, or after administration of the conventional form of cancer therapy.Type: ApplicationFiled: November 1, 2023Publication date: May 9, 2024Applicant: Vector Vitale IP LLCInventors: Peter NOVAK, Maxim TEMNIKOV, Oleksandr BALAKIN
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Publication number: 20240150281Abstract: The present invention relates to the field of organic synthesis and more specifically it concerns a process for preparing a compound of formula (I). Moreover, the present invention comprises also analytical methods of measuring the amount of thiol or thioether compounds having less than 6 carbon atoms in the thiol of formula R—SH and a composition of matter comprising at most 50 ?g/kg of thiol or thioether compounds having less than 6 carbon atoms and at most 1 ppm of any compound of formula (I?).Type: ApplicationFiled: February 8, 2022Publication date: May 9, 2024Inventors: Gilles ODDON, Erik FREROT, Ramez BOSHRA