Extracting From Solid Material Patents (Class 127/43)
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Patent number: 5252136Abstract: A sugar composition consisting of from 90 to 99% by weight sugar and from 10 to 1% by weight of a non-gelling water-soluble dietary fibre. The sugar composition has substantially the properties of normal sugar, but contains a significant amount of dietary fibre, with consequent health benefits. A novel type of soluble fibre derived from sugar beet and a method for preparing it are disclosed. The composition may take the form of a concentrate or syrup, or may be in particulate form. The particulate form may be used as a direct sugar substitute. The fibre used may be a novel fibre obtainable by treating sugar beet with water free from chemical reagents at ambient pressure and at an elevated temperature, for example from 95.degree.-98.degree. C.Type: GrantFiled: November 18, 1991Date of Patent: October 12, 1993Assignee: British Sugar PLCInventors: Malcolm Desforges, Julian M. Cooper, Edward L. Williams
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Patent number: 5221357Abstract: Two stage hydrolysis of lignocellulosic material, conditions during the first stage being such as to hydrolyze or depolymerize the hemicellulosic component without substantial degradation of resulting monosaccharides, conditions during the second stage being such as to hydrolyze the cellulose to glucose without substantial degradation of the glucose. The solids left after first stage hydrolysis are disintegrated mechanically thereby greatly facilitating second stage hydrolysis. Hydrolysis in both stages is preferably accomplished by the use of nitric acid. The pH, retention time and temperature in both stages are selected to maximize production of the desired monosaccharide or monosaccharides.Type: GrantFiled: March 28, 1991Date of Patent: June 22, 1993Inventor: David L. Brink
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Patent number: 5194093Abstract: Process for the extraction of the sugar contained in plants such as sugar beets or sugar cane, wherein the concentration of a dilute liquor by the evaporation of water to obtain a liquor from which the sugar may be separated by crystallization, is applied to a liquor to which hydrogen peroxide has been added and the pH of which is between 8 and 9.5 after the addition of hydrogen peroxide.Type: GrantFiled: August 5, 1991Date of Patent: March 16, 1993Assignee: AtochemInventors: Jean-Francois Boussely, Michel Pouillot
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Patent number: 5137744Abstract: A process for preparing a preferred vegetable fiber product is described. A particular process for reducing off-flavor and off-odor problems in materials such as sugarbeet fiber is specifically described. Also, a preferred system for conducting the process, and preferred products are disclosed. In general, the products result from preferred steps of heating, heat-treating, and washing the vegetable fiber material. Food products incorporating the preferred fiber material, and methods for incorporating the preferred fiber material into food products, are described.Type: GrantFiled: September 11, 1989Date of Patent: August 11, 1992Assignee: American Crystal Sugar CompanyInventors: Paul M. Cagley, James O. Kysilka, Terry D. McGillivray
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Patent number: 5127956Abstract: A method for preparing a mixture of fructose, glucose and oligosaccharides prepared from tubers or roots, and the use of the mixtures as a filler bulking agent with a sweet taste.Type: GrantFiled: September 24, 1990Date of Patent: July 7, 1992Assignee: Danisco A/SInventors: Ole C. Hansen, Rud F. Madsen
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Patent number: 5069893Abstract: A polynucleate aluminum hydroxy silicate-sulphate compound (PASS) having the following average composition:Al.sub.A (OH).sub.B (SO.sub.4).sub.C (SiO.sub.X).sub.D (H.sub.2 O).sub.EwhereinA is 1.0;B ranges from 0.75 to 2.0;C ranges from 0.30 to 1.12;D ranges from 0.005 to 0.1;X is greater than 2.0 but less than or equal to 4.0 such that 3=B+2C+2D (X-2);E is larger than 4 when the product is in aqueous form. The compound is useful for water treatment and other applications where an aluminum hydroxide gel system is required. The compound, in aqueous solution, has a long storage life.Type: GrantFiled: December 1, 1989Date of Patent: December 3, 1991Assignee: Handy Chemicals LimitedInventors: Dieter Haase, Nelu Spiratos, Carmel Jolicoeur
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Patent number: 5002614Abstract: The lipid content, i.e. "cane wax", is extracted from cane molasses by the steps of:(a) adjusting the cane molasses with sufficient alkali to pH 8.0 and 12.4;(b) adding to the pH adjusted molasses a lower alcohol in an amount to provide an alcohol concentration in the range of between 85 and 60 Vol % while heating to 60.degree. C..+-.10.degree. C., and removing the resultant residual solids as a sludge to yield a clarified liquid;(c) reducing the alcohol concentration of the clarified liquid to 50-15 Vol %;(d) adjusting the temperature of the resultant liquid to 45.degree. C..+-.10.degree. C. and then cooling the same to a temperature 20.degree. C..+-.15.degree. C. and efficient to precipitate the lipids therefrom; and(e) recovering the precipitated lipids routinely by isolation or filtration.Type: GrantFiled: April 4, 1989Date of Patent: March 26, 1991Assignee: Daiichi Seito Kabushiki KaishaInventors: Sadao Miyagi, Kenichi Ohshiro, Akio Sakugawa
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Patent number: 4997489Abstract: The invention relates to a process for recovering sugar, sugar alcohol and organic acids comprising citric, malic and quinic acids from a juice extracted from almond hulls. Residues from the extraction is also recovered.Type: GrantFiled: May 8, 1989Date of Patent: March 5, 1991Inventor: Israel N. Rabinowitz
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Patent number: 4950752Abstract: A method is provided for obtaining concentrated solutions of mucilaginous material by heating plants in an aqueous alkaline medium to form a mixture of solid and liquid, then rapidly expressing the liquid from a thin layer of plant in the apparatus. Apparatus for successively expressing liquid from batches of liquid-solid mixture, said apparatus including a porous septum at the open face of a chamber, the chamber being intermittently sealed to the septum, and having a piston to press the mixture against the septum to express liquid through the septum, the solid residue from each batch being conveyed beyond the unsealed chamber as the next batch is being conveyed into it.Type: GrantFiled: August 19, 1987Date of Patent: August 21, 1990Assignee: Carratech, Inc.Inventor: R. John Whitaker
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Patent number: 4908067Abstract: A continuous hydrolysis process for the hydrolysis of wood and wood derived products into sugars and other products, wherein woodchip or other feedstock is formed into a slurry which is acidified, pressurized and heated before being hydrolyzed in reactors J. Three heat exchangers L1, L2 and L3 form a closed circuit in which exchanger L2 recovers heat from the slurry, L1 returns heat to the slurry and L3 makes up lost heat. The slurry is cooled before pressure reduction by pressure reducing means N and separation of the solids and liquid. The cooling prevents flashing to steam of part of the liquid in the slurry so that the process is single phase where generation of steam is avoided. After separation the solids can proceed to further processing or to discharge as lignin as indicated by arrow B. The liquid can proceed to further processing or discharge as indicated by arrow D.Type: GrantFiled: January 21, 1988Date of Patent: March 13, 1990Assignee: Jack T. H. JustInventor: Jack T. H. Just
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Patent number: 4816078Abstract: The invention concerns a process for production of L-arabionose in crystalline form. Starting material are extracted sugar beet pulp or other L-araban containing plant materials. These are heated in an autoclave as an aqueous suspension in the presence of Ca(OH).sub.2. The so obtained solution is chromatographed on a cationic exchanger in the Ca-form. The araban containing fraction is hydrolyzed after adding H.sub.2 SO.sub.4, neutralized and rechromatographed on a cationic exchanger in Ca-form. After concentrating the arabinose containing fractions L-arabinose is obtained in form of crystals by cooling crystallization.Type: GrantFiled: January 21, 1988Date of Patent: March 28, 1989Assignee: Suddeutsche Zucker-AktiengesellschaftInventors: Hubert Schiweck, Manfred Vogel
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Patent number: 4804418Abstract: Processing and outfit for the extraction of cane sugar by pressing canes and magma between several pairs of fluted rollers, wherein each pair of rollers is completely submerged in a tank (C) and fed through a hopper (13), and wherein a constant recirculation of the magma, from each tank towards the corresponding hopper, with a significant flow rate on the one hand, and a countercurrent circulation of the bagasse and the juice with a lower flow rate in the different tanks (C.sub.1, C.sub.2, C.sub.3) corresponding to the different pairs of rollers on the other, are combined.Type: GrantFiled: September 19, 1986Date of Patent: February 14, 1989Assignee: Maguin S. A., B. P.Inventor: Alain Gautier
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Patent number: 4758283Abstract: This invention relates to a process for readily and efficiently preparing L-rhamnose with the use of a marine alga belonging to the family Monostromaceae, Ulvales.According to the process of the present invention, rhamnan sulfate is extracted from a marine alga belonging to the family Monostromaceae such as Monostroma nitidium Wittrock and the obtained extract is hydrolyzed by adding acid(s) thereto followed by heating or treating thereof with a cation exchange resin followed by heating to thereby give a solution containing free L-rhamnose.Since the solution thus obtained contains a large amount of salts, the removal of these salts is significantly important in the preparation of L-rhamnose. In the present invention, an effective process therefor is combined with a conventional method by using an ion exchange resin to thereby establish an efficient desalting process.Type: GrantFiled: December 22, 1986Date of Patent: July 19, 1988Assignee: Towa Chemical Industry Co. Ltd.Inventors: Motohiro Takemura, Mochihiro Iljima, Yoshiaki Tateno, Naoki Okamoto, Masaaki Fuse
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Patent number: 4664716Abstract: A system for extracting soluble substances from fiberous material by lixiviation is followed by various steps of compression and maceration exerting moderate compression on the fiberous material up to 14 Bar. Hereby, special arrangements are made to saturate the fiberous material to maximum absorption between each pressure application. Moisture content of the spent fiberous material is reduced with a special roller assembly with the application of low and high pressure. Heat is used to facilitate the extraction process and to suppress biological alterations of matter involved. With heat exchange between raw material and extracted solvent, overall heat economy is improved. Fiberous material is used as filter aid to reduce contamination of extracted solvent with foreign matter. The system is particularly suitable for the extraction of sugar from sugar cane.Type: GrantFiled: August 2, 1984Date of Patent: May 12, 1987Assignee: Voith S/A - Maquinas e EquipamentosInventor: Wilhelm Leibig
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Patent number: 4627880Abstract: To produce an unprocessed complete cane sugar with approximately the color and flavor of fresh sugarcane juice and still containing valuable amino acids and vitamins, only up to 50% of the sugarcane juice in terms of the weight of the cane is pressed from ripe, de-leaved, and clean sugarcane with a high sucrose content, the juice is pasteurized at a temperature above the second flocculation point of the waxes, fats, proteins, and pentosans, the flocculate is gently separated out, the purified juice gently thickened below the pasteurization temperature, and the resulting syrup converted into a dry and pourable product by suddenly extracting the residual water.Type: GrantFiled: February 27, 1985Date of Patent: December 9, 1986Assignee: Pfeifer & LangenInventors: Arnold Langen, Herta Benecke, Udo Breithaupt
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Patent number: 4589923Abstract: Liquids, such as sugar cane juices, are removed from fibrous materials by an apparatus which receives the fibrous, felt type or matted materials in strand form, for example from a sugar cane diffuser. Two hollow compression rollers having perforated circumferential walls are pressed toward each other for working in a compression range of about 0.5 kg/cm.sup.2 to about 50 kg/cm.sup.2, and form a material feed-in gap facing substantially upwardly. The rollers are arranged above liquid collecting troughs. Lateral funnel forming walls sealingly close the ends of the feed-in gap so that the rollers together with these lateral walls form a feed-in funnel. Material entraining members cover the holes in the perforated circumferential roller walls but with a spacing between the outer roller wall surface and the respective entraining member to form a liquid flow channel into each hole. The material is supplied into the feed-in gap through a substantially vertically extending chute reaching to or into said funnel.Type: GrantFiled: November 2, 1984Date of Patent: May 20, 1986Assignee: Braunschweigische MaschinenbauanstaltInventor: Werner Gruenewald
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Patent number: 4547226Abstract: The sugar content of citrus press liquor is enhanced by separating citrus solids, extracting fructose, glucose, and sucrose from the solids, and recombining the aqueous extract to increase the sugar content thereof. By inversion of the sucrose present in the sugar-enhanced press liquor, a high fructose syrup can be readily obtained which is indistinguishable from high fructose corn syrup. When separation is effected by centrifugation, a biocidally active colloidal phase is formed from which citrus terpenes and limonene can be extracted, resulting in a press liquor suitable for fermentation. The solid residue remaining after extraction can also be recycled with the remaining press cake.Type: GrantFiled: August 3, 1983Date of Patent: October 15, 1985Assignee: IGI Biotechnology, Inc.Inventors: Robert A. Milch, Patricia Guerry-Kopecko, Carol Koeble-Smith, Edward M. Sybert
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Patent number: 4543129Abstract: The liquid content of sugar cane bagasse is reduced by a low pressure process having a substantially longer duration than the duration of prior art high pressure liquid removal processes. For this purpose the liquid containing bagasse, as it emerges from a diffuser, is exposed to a relatively slowly increasing yet low pressure as compared to prior art high pressures, whereby the bagasse travels with a substantially constant speed sequentially through a dewatering zone, wherein a further compaction takes place, a preliminary squeeze-out zone and a final squeeze-out zone. During the preliminary squeeze-out the pressure above an open surface area or section without a sieve or screen is about 0.2 kg/cm.sup.2. During the final squeeze-out the pressure (p) is about p/0.6D>0.003, wherein D is the diameter, in mm, of a squeeze-out roller. The pressing duration t in seconds is also related to the squeeze-out roller diameter D such that D:t is smaller than a constant value K.Type: GrantFiled: January 24, 1984Date of Patent: September 24, 1985Inventor: Willy Kaether
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Patent number: 4488912Abstract: The sugar content of citrus press liquor is enhanced by separating citrus solids, extracting fructose, glucose, and sucrose from the solids, and recombining the aqueous extract to increase the sugar content thereof. By inversion of the sucrose present in the sugar-enhanced press liquor, a high fructose syrup can be readily obtained which appears indistinguishable from high fructose corn syrup. When separation is effected by centrifugation, a colloidal phase is formed from which limonene and biocidal flavanoids can be extracted, resulting in a press liquor suitable for fermentation to alcohol. The solid residue remaining after extraction can also be recycled with the remaining press cake.Type: GrantFiled: August 4, 1982Date of Patent: December 18, 1984Assignee: IGI Biotechnology, Inc.Inventors: Robert A. Milch, Patricia Guerry-Kopecko, Carol Koeble-Smith, Edward M. Sybert
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Patent number: 4484012Abstract: A method for hydrolyzing coffee extraction residue materials to produce manno-saccharides having a degree of polymerization from 1 to 10 and subsequently neutralizing and reducing said mixture of manno-saccharides to their corresponding alcohols. The coffee material, preferably spent coffee grounds from a commercial percolation system, is hydrolyzed in a Plug Flow tubular reactor in the presence of an acid catalyst, such as sulfuric acid. Depending on the time, temperature, pressure and catalyst concentration selected, manno-saccharides or mannose is produced. The manno-saccharides or mannose produced are separated from coffee residue material in the form of a syrup and neutralized with calcium hydroxide. The neutralized mixture of manno-saccharides or mannose is reduced to their corresponding alcohols or mannitol.Type: GrantFiled: February 29, 1984Date of Patent: November 20, 1984Assignee: General Foods CorporationInventors: Howard Stahl, Renee Bayha, Charles V. Fulger, Evan J. Turek
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Patent number: 4452641Abstract: The liquid content of sugar cane bagasse is reduced by a low pressure process having a substantially longer duration than the duration of prior art high pressure liquid removal processes. For this purpose the liquid containing bagasse, as it emerges from a diffuser, is exposed to a relatively slowly increasing yet low pressure as compared to prior art high pressures, whereby the bagasse travels with a substantially constant speed sequentially through a dewatering zone, wherein a further compaction takes place, a preliminary squeeze-out zone and a final squeeze-out zone. During the preliminary squeeze-out the pressure above an open surface area or section without a sieve or screen is about 0.2 kg/cm.sup.2. During the final squeeze-out the pressure (p) is about p/0.6D>0.003, wherein D is the diameter, in mm, of a squeeze-out roller. The pressing duration t in seconds is also related to the squeeze-out roller diameter D such that D:t is smaller than a constant value K 16.Type: GrantFiled: July 13, 1983Date of Patent: June 5, 1984Inventor: Willy Kaether
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Patent number: 4428969Abstract: Date fruits are extracted by a wet grinding operation after addition of water and subsequent filtration of the homogenized product with the aid of a cellulosic filter aid. The date pits may be used as the filter aid. A fermentation may be carried out before the filtration. A high concentrate feed material is thus obtained.Type: GrantFiled: December 11, 1978Date of Patent: January 31, 1984Assignee: Chemap AGInventors: Hans Muller, Rudolf Gayler, Nikolas Rapsomanikis
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Patent number: 4421852Abstract: High fructose syrups are obtained from Jerusalem artichoke tubers and other naturally-occurring inulin-containing materials by extraction of the inulin and any related fructans from the tubers with water, elimination of some low molecular weight nitrogenous species and minerals from the aqueous extract by ultrafiltration, enzymatic hydrolysis of the inulin to fructose and glucose, separation of the reducing sugars from higher molecular species by ultrafiltration, and evaporative concentration of the purified reducing sugars solution to a syrup. The processing also removes colorants initially present in the aqueous extract. The dissolved solids in the syrup comprise at least 90 wt % reducing sugars and these sugars are constituted at least 60 wt %, often at least 75 wt %, by fructose with the balance glucose.Type: GrantFiled: August 9, 1982Date of Patent: December 20, 1983Inventors: Ernst Hoehn, Curtis J. McKay, E. Donald Murray
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Patent number: 4328043Abstract: Sugar extraction efficency from sugar-containing plant tissue, such as sugarbeet cossettes or the like, is increased by contacting the sugar-containing plant tissue near the juice end of a diffusion process with diffusion water in the presence of an effective amount of carbon dioxide.Type: GrantFiled: October 14, 1980Date of Patent: May 4, 1982Assignee: Great Western Sugar CompanyInventors: Arthur H. Freytag, Rodney D. Cooke
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Patent number: 4326892Abstract: Method of improving the recovery of sugar from sugar beets comprising washing the sugar beets to remove impurities therefrom, wholly or partially removing the outer layer of the washed sugar beets, slicing the sugar beets thus obtained and extracting the sliced sugar beets with an aqueous solution to form a sugar juice.Apparatus for wholly or partially removing the surface layer of washed sugar beets, the apparatus comprising two spaced rows of rotatable cylindrical brushes mounted so as to advance sugar beets in the space between the rows while subjecting them to the influence of the brushes to wholly or partially remove the outer layer of the sugar beets.Type: GrantFiled: December 11, 1979Date of Patent: April 27, 1982Assignee: Aktieseiskabet de Danske SukkerfabrikkerInventors: Rud F. Madsen, Werner K. Nielsen
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Patent number: 4310361Abstract: A sugar cane mill facility for the extraction with imbibition of sugar from sugar cane.This mill is characterized by the fact that it includes a fourth roller placed in front of the upper roller, against which it presses and, above the inlet roller and mounted on a mobile support, means acting upon the said support in order to flexibly push the fourth roller towards the upper roller, adjustable stops hindering these two rollers from coming together, and a trash plate placed between the fourth roller and the inlet roller integral with the said mobile support. The juices extracted by pressure between the upper roller and the fourth roller can be recycled to the bagasse layer feeding the mill, either with the juices which have passed through this layer, or with the juices extracted by pressure between the upper roller and the inlet and outlet rollers.Type: GrantFiled: December 11, 1980Date of Patent: January 12, 1982Assignee: Fives-Cail BabcockInventor: Jean-Pierre Georget
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Patent number: 4285735Abstract: A process for making a fructose polymer mixture containing chiefly inulin and inulides with minor amounts of impurities is based on the finding that inulin is in a soluble metastable state at room temperature as it exists in the dahlia tuber. Novel steps in the process are the separation, without the use of heat or adding water, of the water soluble from the ground dahlia tuber within about 10 minutes after grinding, followed by separation by coagulation of protein color and flavor bodies by heating at the boiling temperature from 3 to 10 minutes. No chemical defecating agent, such as lime water is used or required. The resulting clear extract is concentrated to 40% to 70% solids. Dry product is recovered by crystallizing the concentrated extract at 1.degree. to 15.degree. C. The product differs from inulin in that the product, in addition to inulin, also contains inulides, protein, color, flavor bodies, and minerals.Type: GrantFiled: March 10, 1980Date of Patent: August 25, 1981Inventors: William A. Mitchell, Charles E. Mitchell, Pat R. Mitchell
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Patent number: 4273590Abstract: Process for obtaining beet pulp of high dry-solids content from a sugar extraction process by mechanically pressing the pulp, mixing salts of polyvalent cations, an acid or both with the pressed pulp, further pressing the admixture and thermally drying the admixture. The salts of the polyvalent cations are preferably calcium chloride, aluminum chloride and ferric chloride and are added in an amount of from 0.5 to 10%, preferably from 1.5 to 4%, relative to the pulp dry-solids content. The liquid from the second pressing can be concentrated by evaporation and at least part can be recycled to produce the initial solution of the salts. The remainder of the concentrated liquid can be added to the pressed admixture before or after drying to further increase the dry-solids content.Type: GrantFiled: February 19, 1980Date of Patent: June 16, 1981Assignee: Suddeutsche Zucker-AktiengesellschaftInventors: Theodor Cronewitz, Hubert Schiweck
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Patent number: 4147557Abstract: The feed blanket is conditioned prior to entering the mill to provide more uniformity of thickness and to control maximum thickness. Overfeeding is prevented by self-regulated by-passing of excess feed. Plural mills of a milling tandem can be made to operate in a parallel fashion while the remaining ones continue to operate in their usual series fashion.Type: GrantFiled: February 3, 1978Date of Patent: April 3, 1979Inventor: Aryan R. Mayo
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Patent number: 4138272Abstract: A process for the obtention of fructose and fructose-rich syrups from xerophyte plants, particularly of the genus Amarillidaceae, such as Agave, comprises separately collecting the plant material consisting of the leaf portions and the core portions of the plant; admixing and washing with water said plant materials; chopping the washed plant material to form small pieces and recovering the juices released by the chopping operation; subjecting the chopped material to an extraction process with an aqueous liquor expressing the residual solid plant material to expel the enriched extractant therefrom; admixing the plant juice and extractant to obtain a mixed juice, settling and clarifying said mixed juice; acidulating the liquid phase of the process at a preselected moment in the sequence, such that the settled and clarified juice will be brought to a pH of from about 3 to about 4; allowing said acidulated liquid phase to stand for a period of time of from about 2 to 3 hours at a temperature of from about 85.Type: GrantFiled: November 15, 1977Date of Patent: February 6, 1979Inventors: Enrique Zepeda-Castillo, deceased, by Isaura N. Vda. de Zepeda, executrix
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Patent number: 4119435Abstract: Soybean polysaccharides are produced by extracting a residue which is obtained after the separation of soy proteins from soybean, with an aqueous alkaline solution and recovering the resultant solid fraction.Type: GrantFiled: June 3, 1977Date of Patent: October 10, 1978Assignee: Takeda Chemical Industries, Ltd.Inventors: Yukihiro Nakao, Kasumi Miyashita, Jun Toda
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Patent number: 4063960Abstract: Method of treating cut sugar cane, which comprises depositing the cane on a conveyor, spraying steam on the cane to melt and remove wax and field dirt on the surface of the cane, and removing the melted wax and condensed steam below said conveyor. Sugar cane juice, produced by subjecting the steamed cane to roller action, is treated with active carbon to yield a clarified juice. The clarified juice is evaporated to form direct white sugar and edible molasses. The wax is collected, purified and molded into cakes. Adding an alkaline material to the expressed juice precipitates out soaps.Type: GrantFiled: May 2, 1972Date of Patent: December 20, 1977Inventor: Lewis A. Paley
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Patent number: 4046789Abstract: Bakery-type wastes as they occur in the food industry and which contain substantial amounts of fats, sugar, proteins and starch are recovered by removing the fat- and oil-component from the waste by a solvent extraction-filtration step followed by recovery of the sugar and starch protein mixture for reuse in the industry.Type: GrantFiled: December 2, 1975Date of Patent: September 6, 1977Assignee: Chemap AGInventors: Hans Muller, Louis Grob
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Patent number: 4043832Abstract: An apparatus and process for extracting sugar from sugar cane in which a blanket of fiberized cane is passed through a series of compression and maceration operations. The compression is performed at low pressures (for example, 40 to 160 pounds per square inch) between a pair of rollers. During compression, the extracted juice is removed through the perforate surface of the lower roller. The extracted juice removed during compression is supplied as imbibition liquid to a prior operation.Type: GrantFiled: April 5, 1976Date of Patent: August 23, 1977Assignee: CF&I Engineers, Inc.Inventors: Wilhelm J. Leibig, Clarence R. Steele, Frank B. Price