Centrifuging Patents (Class 127/56)
  • Publication number: 20150040889
    Abstract: A process for enabling the production of a particulate composition containing crystalline trehalose dihydrate is provided. Including allowing an ?-glycosyltrehalose-forming enzyme to act on liquefied starch derived from a microorganism of the genus Arthrobacter and a trehalose-releasing enzyme derived from a microorganism of the genus Arthrobacter along with a starch debranching enzyme and a cyclomaltodextrin glucanotransferase; allowing glucoamylase to act on the resulting mixture to obtain a saccharide solution containing ?,?-trehalose; precipitating crystalline ?,?-trehalose dihydrate from the above saccharide solution; collecting the precipitated crystalline ?,?-trehalose dihydrate by a centrifuge; and ageing and drying the collected crystals. Cyclomaltodextrin glucanotransferase derived from a microorganism of the genus Paenibacillus or a mutant enzyme thereof is used to increase the ?,?-trehalose content in the saccharide solution to over 86.
    Type: Application
    Filed: September 12, 2012
    Publication date: February 12, 2015
    Applicant: HAYASHIBARA CO., LTD.
    Inventors: Takashi Shibuya, Seisuke Izawa
  • Patent number: 8808458
    Abstract: The present invention concerns a process that can be realised continuously for the preparation of anhydrous crystalline lactulose from commercial aqueous syrups that contain it, characterised in that the crystallisation and consequent separation of the high-purity lactulose with high yields from the syrup is triggered by mixing the ore pulp (or recycled ore pulp), obtained from a previous lactulose crystallisation phase, with the syrup itself.
    Type: Grant
    Filed: November 12, 2008
    Date of Patent: August 19, 2014
    Assignee: Fresenius Kabi Austria GmbH
    Inventor: Giovanni Cipolletti
  • Patent number: 8617315
    Abstract: A process is proposed for recovery of water in the sugar cane processing in production mills of sugar and alcohol or only alcohol (ethanol). In the process, the thermal energy available in the exhausted steam from the electric energy generation turbines is transferred to the different mixed juice processing phases, with the reuse of the exhausted steam condensates in the boilers and of the other condensates, after using thermal energy, for imbibition, in the juice extraction phase, for cooling in the process, after passing through cooling towers, for other industrial uses and for possible treatment or use in the irrigation out of the productive system in the mill.
    Type: Grant
    Filed: June 24, 2009
    Date of Patent: December 31, 2013
    Assignee: Dedini S/A Industrias de Base
    Inventors: Paulo Eduardo Mantelatto, Celina Kiyomi Yamakawa, Antonio Rogério Perira César, José Luiz Olivério, Fernando Cesar Boscariol, Marcilio Nogueria do Amaral Gurgel
  • Publication number: 20130042858
    Abstract: The portable sugar mill is established on a mobile platform for transport to the harvesting field, so that the juice of the harvested sugar cane may be processed and refined in the field. The portable sugar mill converts the juice, which contains sucrose, into raw sugar crystals (brown sugar) and molasses. The portable sugar mill includes a separator tank, a pre-heating tank, a clarifier, and three successive stages of evaporative crystallization and separation of crystals from syrup. The portable sugar mill has a programmable logic controller and a plurality of sensors, control relays, pumps, motors, heaters, and valves that operate automatically under direction of the programmable logic controller.
    Type: Application
    Filed: August 16, 2012
    Publication date: February 21, 2013
    Inventor: J. EDWIN ROY
  • Patent number: 8097086
    Abstract: A method for preparing a sugar syrup having high fructose content, is implemented using at least one fruit containing sorbitol, particularly apples, pears, plums, prunes, peaches, nectarines, apricots and grapes, from which a first juice is extracted. The first juice is processed in order to obtain a clarified and demineralised sweet juice having a colour lower than 45 ICUMSA and having a conductometric ash content lower than 0.4%. The clarified and demineralised sweet juice is then processed in order to hydrolyse the saccharose into fructose and glucose. The method further includes an isomerisation of the glucose in fructose, and removing the sorbitol naturally occurring in the starting material.
    Type: Grant
    Filed: January 24, 2008
    Date of Patent: January 17, 2012
    Assignees: Nutritis, Institut National des Sciences Appliquees Toulouse
    Inventors: Pierre Lapoujade, Alain Guibert, Francoise Ouarne
  • Patent number: 7582444
    Abstract: Process for improving the separation efficiency of residual solid matter from the liquid phase of an aqueous acid hydrolysate of a naturally occurring polysaccharide comprising dissolved sugars, and residual acid wherein a flocculating agent(s) is added to the aqueous mixture in an effective amount, and a process of producing fermentation products comprising the steps of, (i) hydrolysing a particulate polysaccharide based plant derived material in an acid medium, and thereby forming an aqueous mixture comprising dissolved sugar and solid matter, (ii) subjecting the aqueous mixture to one or more separation stages in which solid matter are removed from the aqueous phase, (iii) adjusting the pH of the obtained aqueous phase to a pH of at least 4, (iv) fermenting the dissolved sugars of the aqueous phase by a microorganism to produce a fermentation product, (v) isolating the fermentation product, wherein in at least one separation stage in step (ii) a flocculating agent is added to the aqueous mixture in an effe
    Type: Grant
    Filed: July 28, 2003
    Date of Patent: September 1, 2009
    Assignee: Ciba Specialty Chemicals Water Treatments Ltd.
    Inventor: Jonathan Hughes
  • Publication number: 20090151715
    Abstract: A method for purifying a sucrose material already in a high purity liquid, crystalline or other form of sucrose, such as raw sugar, utilizing chromatography, or utilizing chromatography in connection with other methods of purification.
    Type: Application
    Filed: February 17, 2009
    Publication date: June 18, 2009
    Applicant: Amalgamated Research LLC
    Inventors: Dennis D. Costesso, Michael M. Kearney
  • Publication number: 20090120430
    Abstract: The present invention concerns a process that can be realised continuously for the preparation of anhydrous crystalline lactulose from commercial aqueous syrups that contain it, characterised in that the crystallisation and consequent separation of the high-purity lactulose with high yields from the syrup is triggered by mixing the ore pulp (or recycled ore pulp), obtained from a previous lactulose crystallisation phase, with the syrup itself.
    Type: Application
    Filed: November 12, 2008
    Publication date: May 14, 2009
    Inventor: Giovanni Cipolletti
  • Patent number: 7455997
    Abstract: A process of producing fermentation product comprising the steps of, (i) forming an acidified suspension of particulate plant derived material comprising a first polysaccharide which is more readily hydrolysable and a second polysaccharide which is more difficult to hydrolysable, (ii) allowing the first polysaccharide to undergo hydrolysis by action of the acid at a temperature of at least 50° C.
    Type: Grant
    Filed: July 28, 2003
    Date of Patent: November 25, 2008
    Assignee: Ciba Specialty Chemicals Water Treatments Ltd
    Inventor: Jonathan Hughes
  • Publication number: 20080017187
    Abstract: The present invention relates to an improved process for extract purification of sugar beet raw juice, especially for reduction of lime consumption during the purification of sugar beet raw juice, to a process for producing a nutrient-rich non-sucrose concentrate from sugar beet raw juice, to the non-sucrose substance concentrate thus produced, to uses of the non-sucrose substance concentrate and to an apparatus for preliming sugar beet raw juice and/or for obtaining the non-sucrose substance concentrate.
    Type: Application
    Filed: October 26, 2004
    Publication date: January 24, 2008
    Inventors: Eric Deneus, Gunter Merkel, Thomas Michelberger, Mohsen Ajdari Rad, Marc Willems
  • Patent number: 7192524
    Abstract: A process for the continuous treatment of sugar cane filter cane mud separates and extracts components including fiber which can be used as an animal feed or a source of energy generation, lignin, beta-carotene, oil containing a high content of phytosterol, refined wax which is a resource of policosanol and which can also be used for many other established purposes, and resin which can be used an additive in asphalt mixtures and tire manufacturing or can be recycled back into the sugar milling process. The process is self contained, requiring the input only of fresh water and chemical additives to adjust pH and coloration.
    Type: Grant
    Filed: January 21, 2005
    Date of Patent: March 20, 2007
    Inventor: Rafael Almagro
  • Patent number: 6736903
    Abstract: A method for producing a work product including the steps of receiving a first fluid composed of a liquid, a target substance and at least one residual substance; passing the first fluid through a first work station for separating the residual substance from the first fluid to produce a secondary fluid substantially composed of the liquid and the target substance; and treating the secondary fluid to reduce the proportion of the liquid relative to the target substance in the secondary fluid to form the work product.
    Type: Grant
    Filed: April 23, 2001
    Date of Patent: May 18, 2004
    Assignee: Sunshine Raisin Corporation
    Inventor: John J. Minazzoli
  • Publication number: 20020153333
    Abstract: A method for producing a work product including the steps of receiving a first fluid composed of a liquid, a target substance and at least one residual substance; passing the first fluid through a first work station for separating the residual substance from the first fluid to produce a secondary fluid substantially composed of the liquid and the target substance; and treating the secondary fluid to reduce the proportion of the liquid relative to the target substance in the secondary fluid to form the work product.
    Type: Application
    Filed: April 23, 2001
    Publication date: October 24, 2002
    Inventor: John J. Minazzoli
  • Patent number: 6440222
    Abstract: A process for producing sugar from beets includes the step of filtering a sucrose-containing feed juice, which has been obtained from macerated sugar beets, through a first ultrafiltration membrane that has a first molecular weight cutoff. This ultrafiltration step produces a first ultrafiltration permeate and a first ultrafiltration retentate. The first ultrafiltration permeate is filtered through a second ultrafiltration membrane that has a second molecular weight cutoff that is lower than the first molecular weight cutoff. This second ultrafiltration step produces a second ultrafiltration permeate and a second ultrafiltration retentate. The second ultrafiltration permeate is nanofiltered through a nanofiltration membrane, thereby producing a nanofiltration permeate and a nanofiltration retentate.
    Type: Grant
    Filed: July 18, 2000
    Date of Patent: August 27, 2002
    Assignees: Tate & Lyle Industries, Limited, Tate & Lyle, Inc.
    Inventors: Michael Donovan, Robert P. Jansen, Richard C. Reisig, Marc Hlavacek, Gordon Walker, John C. Williams
  • Patent number: 5900156
    Abstract: A loading control system for a centrifuge used in, for example, a sugar refining operation, optimizes the introduction of product to be centrifuged. A loading system has an ultrasonic loading probe, a sound tube for delivering the sound signals to the sugar wall and returning to the ultrasonic probe, an analog controllable feed valve and a programmable logic controller which is used to control the operation. The logic program implements a control loop which analyses the signal from the probe and controls the position of the gate accordingly. Preferably, the system also implements a control loop for automatic adjustment of the flow rate and amount of sugar in the machine in order to optimize the loading process.
    Type: Grant
    Filed: June 4, 1997
    Date of Patent: May 4, 1999
    Assignee: Savannah Foods and Industries
    Inventor: Dwayne Zeigler
  • Patent number: 5868851
    Abstract: A process to produce solid glucose from a hydrolyzate consisting of a mixture of glucose, water, and an acid used in the hydrolysis of a biomass material is covered herein. In the process, the hydrolyzate is concentrated, as required, to form two phases: a solid glucose phase and an acidic liquid phase. The phases are formed in a vessel where they are separated for recovery of the acidic liquid phase. The solid glucose phase, containing residual acidic liquid phase, is then extracted to remove most of the residual acid to produce solid glucose mostly free of acid. The recovered acid may then be recycled. The solid glucose may be further processed including purification and also drying.
    Type: Grant
    Filed: August 11, 1997
    Date of Patent: February 9, 1999
    Inventor: Gene E. Lightner
  • Patent number: 5865899
    Abstract: A process for refining a raw sugar, particularly raw sugar from the sugar cane sugar industry, characterized in that it comprises the steps of:(a) remelting of the raw sugar for obtaining a raw sugar syrup,(b) carbonatation or phosphatation of said raw sugar syrup, and(c) tangential microfiltration and/or tangential ultrafiltration of the raw sugar syrup, which has been subjected to carbonatation or phosphatation.The process is completed by the steps of:(d) decolorization of the sugar syrup resulting from step (c), and(e) crystallization and/or demineralization of the sugar syrup resulting from step (d).
    Type: Grant
    Filed: May 29, 1996
    Date of Patent: February 2, 1999
    Assignee: Applexion
    Inventors: Marc-Andre Theoleyre, Stanislas Baudoin
  • Patent number: 5674322
    Abstract: In the process, a starch-containing suspension 1 is divided at admixture of washing liquid 5 in a centrifuge "A" into starch-containing concentrate 2, a first liquid phase 3 with primarily dissolved substances and a second liquid phase 4 with primarily undissolved substances. The first liquid phase 3 is especially suitable as washing liquid in counterflow washing processes as it contains no obstructive undissolved substances. Also, the disposal of this liquid phase is simpler. The second liquid phase 4 with the undissolved substances is generated in higher concentration compared to conventional processes so that the processing of this phase is less cumbersome.
    Type: Grant
    Filed: May 31, 1995
    Date of Patent: October 7, 1997
    Assignee: Westfalia Separator AG
    Inventor: Herbert Kunz
  • Patent number: 5480491
    Abstract: The following description sets forth a new process for the preparation of .gtoreq.98.5% pure crystalline lactulose from commercially available aqueous syrups having the following composition: 50-70% by weight of lactulose, 3-9% by weight of lactose, 3-14% by weight of galactose, 4-7% by weight of other carbohydrates, the total content of carbohydrates different from lactulose being of from 10% to 30%.
    Type: Grant
    Filed: April 18, 1994
    Date of Patent: January 2, 1996
    Assignee: Inalco S.p.A.
    Inventor: Giuseppe Bimbi
  • Patent number: 5468300
    Abstract: Refined sugar is produced directly from sugarcane without using conventional refining processes. Clarification of extracted cane juice is obtained either by ultra-centrifugation or ultra-filtration, and removal of certain compounds responsible for adverse color quality and viscosity is effected through a set of packed columns filled with an absorbent for these compounds. After evaporation and crystallization, refined cane sugar is produced.
    Type: Grant
    Filed: April 7, 1994
    Date of Patent: November 21, 1995
    Assignee: International Food Processing Incorporated
    Inventor: Jean-Pierre Monclin
  • Patent number: 5468301
    Abstract: Refined sugar is produced without using conventional refining processes. Clarification of melted raw cane sugar is obtained either by ultra-centrifugation or ultra-filtration, and removal of certain compounds responsible for adverse color quality and viscosity is effected through a set of packed columns filled with an absorbent for these compounds. After evaporation and crystallization, refined cane sugar is produced.
    Type: Grant
    Filed: August 3, 1994
    Date of Patent: November 21, 1995
    Assignee: International Food Processing Incorporated
    Inventor: Jean-Pierre Monclin
  • Patent number: 5454875
    Abstract: A method is disclosed for softening and purifying molasses or syrup to obtain a clarified syrup that can then easily be handled by conventional ion-exclusion or other techniques for recovery of sugar. The process comprises steps that can be performed at ambient temperature. The molasses or syrup is carbonated at high pH, followed by adding organic solvent(s) such as ethanol. The sludge and liquid phases are separated. The solvent is then recovered, leaving a liquid phase comprising a soft and very clear sugar-containing liquid. The liquid phase may then be used in known systems for sugar recovery such as ion-exclusion chromatographic systems. Organic acids such as aconitic acid may be recovered from the sludge residue.
    Type: Grant
    Filed: July 1, 1994
    Date of Patent: October 3, 1995
    Assignee: Board of Supervisors of Louisiana State University and Agricultural and Mechanical College
    Inventor: Stephen J. Clarke
  • Patent number: 5439526
    Abstract: Disclosed and claimed is a rapid, simple process for fractionating wheat flour into components comprising protein concentrates and prime starch. The claimed method utilizes minimal water and produces a low waste water load. Flour and liquid are mixed to form a dough. Additional liquid is added to the dough and the dough and liquid are vigorously dispersed. The dispersion is centrifuged and forms distinct fractions-layers that are separated for the recovery of vital gluten and prime starch.
    Type: Grant
    Filed: October 1, 1993
    Date of Patent: August 8, 1995
    Assignee: Washington State University Research Foundation
    Inventors: Zuzanna Czuchajowska, Yeshajahu Pomeranz
  • Patent number: 5382294
    Abstract: The object of the present invention is to chromatographically separate the higher and lower molecular weight components of juices, liquors, syrups and/or molasses (e.g., inorganic-organic complexes and organic non-sugars), thereby permitting the lower molecular weight sugar and soluble salt-containing fraction(s) to be further processed into natural sweetener products.
    Type: Grant
    Filed: July 29, 1993
    Date of Patent: January 17, 1995
    Inventors: Nicholas T. Rimedio, Li Fu Chen
  • Patent number: 5286298
    Abstract: An apparatus and method for reducing sugar, crystal impact damage and lump formation in a centrifugal provides a resilient barrier ring which absorbs most of the impact energy of the crystals and which deflects the crystals so they are not struck by trailing high speed crystals. An air flow causes vibration of the barrier ring to prevent crystal sticking which could lead to lump formation. This air flow also reduces moisture content in the sugar housing to further reduce lump formation.
    Type: Grant
    Filed: December 13, 1991
    Date of Patent: February 15, 1994
    Assignee: Silver Engineering Works, Inc.
    Inventors: Ted D. Milner, Robert V. Zimmerman, Myles G. Hill
  • Patent number: 5286299
    Abstract: An apparatus and method for providing reduced crystal damage in a sugar centrifugal includes provisions for avoiding scratching and other crystal damage by eliminating asperities and sharp edges at the transition between the screening zone and the discharge zone of a centrifugal basket. In addition, the distance on an upper shroud ring across which high velocity crystals slide is minimized to reduce the likelihood of scratching crystals on the surface of the shroud ring. Finally, the tangential velocity at which crystals are released from the centrifugal basket is minimized to reduce impact damage to the crystals.
    Type: Grant
    Filed: December 13, 1991
    Date of Patent: February 15, 1994
    Assignee: Silver Engineering Works, Inc.
    Inventor: Ted D. Milner
  • Patent number: 5281275
    Abstract: A sugar centrifugal operates at decreased speed to reduce crystal damage but suffers no loss of sugar crystal/molasses separation rate. This is accomplished by superposing a partial vacuum on the molasses chamber of the centrifugal which promotes removal of syrup and water from the sugar crystals through the centrifugal basket wall. Additional drying of the separated crystals is provided by injection of air above the sugar chamber to replace that which is extracted through the centrifugal basket wall.
    Type: Grant
    Filed: December 13, 1991
    Date of Patent: January 25, 1994
    Assignee: Silver Engineering Works, Inc.
    Inventor: Ted D. Milner
  • Patent number: 5269849
    Abstract: An apparatus and method for reducing sugar, crystal impact damage and lump formation in a sugar centrifugal includes a resilient deflector ring which absorbs most of the impact energy of the crystals while deflecting the crystals out of the path of trailing high speed crystals. An air flow parallel to the local surface of the deflector ring causes vibration of the deflector ring to reduce the tendency for crystals to stick while addition of a supply of water aspirated and atomized by the air flow maintains the ring surface free of syrup build-up which could cause crystals to adhere to the ring surface and form lumps.
    Type: Grant
    Filed: June 25, 1992
    Date of Patent: December 14, 1993
    Assignee: Silver-Weibull
    Inventor: Ted D. Milner
  • Patent number: 5244502
    Abstract: A continuously operable centrifuge for spinning off sugar massecuite has an upwardly conically expanded strainer basket (20) mounted for rotation about a vertical axis (16). A downwardly conically expanding massecuite distributor (40) rotating with the basket reaches into a floor region of the strainer basket substantially coaxially to the strainer basket. The lower rim of the distributor forms a throw-off edge. Inside and in the upper region of the massecuite distributor (40), a distributing cup (30) is for distributing massecuite. The peripheral wall of the massecuite distributor (40) is formed by several ring elements (41), (42, 43) which partly overlap in the axial direction leaving an annular gap (44, 45). The product distributor is surrounded by a downwardly conically expanding stationary bell (51) which forms a further gap or gap space between itself and the rotating rings.
    Type: Grant
    Filed: November 26, 1991
    Date of Patent: September 14, 1993
    Assignee: Braunschweigische Maschinenbauanstalt AG
    Inventors: Helmut Schaper, Heinrich Kurland
  • Patent number: 5213832
    Abstract: In a process for applying a sugar solution to the surface of a cereal product, drying the sugar-coated cereal, collecting the fines produced therefrom and recycling the collected fines back into the original sugar solution the improvement that the fines can be contacted with water to form a slurry of dissolved sugar and insoluble cereal which is then separated into a liquid sugar fraction and an insoluble cereal fraction by centrifugation in a solid bowl centrifuge.
    Type: Grant
    Filed: April 9, 1991
    Date of Patent: May 25, 1993
    Assignee: Kraft General Foods, Inc.
    Inventors: Bruce A. Johnson, David A. Cronk
  • Patent number: 5209856
    Abstract: A process and device for the crystallization of sugar syrup is described. Sugar syrup is cooked to provide a massecuite. Thereafter, the massecuite is subjected to at least one stage of continuous mixing under vacuum to promote crystallization of the massecuite. The crystallized massecuite is then separated to separate the crystals from the mother liquor. The mother liquor is thereafter divided into a first discharge which is water syrup poor and a second discharge which is water syrup rich. Substantially all of the first discharge is recycled to the continuous mixing stage under vacuum. Accordingly, the massecuite and the crystals are subjected to a treatment having continuity during mixing under vacuum to maintain homogeneity of the sugar crystals.
    Type: Grant
    Filed: September 26, 1990
    Date of Patent: May 11, 1993
    Assignee: Beghin-Say, S.A.
    Inventors: Jacques Cuel, Claude Longue-Epee
  • Patent number: 5196068
    Abstract: A water-conducting lance, fitted with a spray nozzle at an end thereof, is fixed to the top of a massecuite-separating centrifuge which has a rotating basket, to dispose the nozzle in adjacency to the top of the basket. The nozzle addresses the top of the basket, perpendicularly, and sprays pre-wetting water onto sugar crystals thereat, to insure a good mix of the crystals with subsequent mixing liquid (also water) in a mixing liquid zone, in order that a lump-free high brix magma will be produced.
    Type: Grant
    Filed: November 18, 1991
    Date of Patent: March 23, 1993
    Assignee: Silver Engineering Works, Inc.
    Inventor: Ted D. Milner
  • Patent number: 5114489
    Abstract: An annular compartment is disposed below the mixing ring of a rotating-basket, massecuite-separating centrifuge, to receive the magma therein. Eductors arrayed in the compartment receive hot water, and ingest magma, to eject the mix therethrough and to centrifuge the mix, while melting the sugar crystals in the magma. The melted crystals, now high brix sugar liquid, is overflowed into a companion compartment; from thence the liquid is passed over a weir, into a sub-compartment, for subsequent discharge.
    Type: Grant
    Filed: November 29, 1990
    Date of Patent: May 19, 1992
    Assignee: Silver Engineering Works, Inc.
    Inventors: Ted D. Milner, Robert V. Zimmerman
  • Patent number: 5104453
    Abstract: In a method and apparatus for eliminating liquid components and fine-grained components from a sugar suspension, control variables for controlling the centrifuge are obtained from a measurement of the quantity of material per unit of surface area in the filter cake formed in the centrifuge during the centrifuging process. In particular, a radiometric measurement can be used for this purpose. From the time course of the measurements obtained, relationships with the physical composition of the filter cake at the instant of measurement are derived and used to adjust process control variables, such as the quantity of water to be added and the length of the washing phase. The control of such a process can be made fully automatic, with optical quality, using a single continuous measurement.
    Type: Grant
    Filed: June 30, 1989
    Date of Patent: April 14, 1992
    Assignee: Laboratorium Prof. Dr. Rudolph Berthold
    Inventor: Gerhard W. Kappler
  • Patent number: 4955363
    Abstract: A method of recovering lactose from milk whey or cheese whey with a high yield, wherein the whey is concentrated, part of the lactose is crystallized, and the crystals are separated and dried; the mother liquor is purified by heating it to about 60.degree. to 70.degree. C. at a pH of about 5.8 to 7.0 and by removing the resultant precipitate by centrifugation; the purified mother liquor is fractionated chromatographically, using sulphonated polystyrene resin which is in sodium ion form and cross-linked by a 3-6% per weight divinylbenzene and which is even-grained, the flow rate is about 0.4 to 1.5 m.sup.3 /h, the temperature about 50.degree. to 75.degree. C., and the pH about 5.5 to 7; whereafter elution is carried out with water, and the following fractions are recovered: a protein fraction which may also contain salts, an intermediate fraction which is recirculated to the fractionating step, and a lactose fraction which is passed to the crystallization step.
    Type: Grant
    Filed: October 12, 1988
    Date of Patent: September 11, 1990
    Assignee: Valio Meijerien Keskusosuusliike
    Inventors: Matti E. Harju, Heikki O. Heikkila
  • Patent number: 4758283
    Abstract: This invention relates to a process for readily and efficiently preparing L-rhamnose with the use of a marine alga belonging to the family Monostromaceae, Ulvales.According to the process of the present invention, rhamnan sulfate is extracted from a marine alga belonging to the family Monostromaceae such as Monostroma nitidium Wittrock and the obtained extract is hydrolyzed by adding acid(s) thereto followed by heating or treating thereof with a cation exchange resin followed by heating to thereby give a solution containing free L-rhamnose.Since the solution thus obtained contains a large amount of salts, the removal of these salts is significantly important in the preparation of L-rhamnose. In the present invention, an effective process therefor is combined with a conventional method by using an ion exchange resin to thereby establish an efficient desalting process.
    Type: Grant
    Filed: December 22, 1986
    Date of Patent: July 19, 1988
    Assignee: Towa Chemical Industry Co. Ltd.
    Inventors: Motohiro Takemura, Mochihiro Iljima, Yoshiaki Tateno, Naoki Okamoto, Masaaki Fuse
  • Patent number: 4488912
    Abstract: The sugar content of citrus press liquor is enhanced by separating citrus solids, extracting fructose, glucose, and sucrose from the solids, and recombining the aqueous extract to increase the sugar content thereof. By inversion of the sucrose present in the sugar-enhanced press liquor, a high fructose syrup can be readily obtained which appears indistinguishable from high fructose corn syrup. When separation is effected by centrifugation, a colloidal phase is formed from which limonene and biocidal flavanoids can be extracted, resulting in a press liquor suitable for fermentation to alcohol. The solid residue remaining after extraction can also be recycled with the remaining press cake.
    Type: Grant
    Filed: August 4, 1982
    Date of Patent: December 18, 1984
    Assignee: IGI Biotechnology, Inc.
    Inventors: Robert A. Milch, Patricia Guerry-Kopecko, Carol Koeble-Smith, Edward M. Sybert
  • Patent number: 4448790
    Abstract: The present invention is concerned with a process by means of which the fraction of grain flour that remains after separation of the main part of the starch and of the gluten-type protein, when the grain contains gluten, is divided into two products of food quality. One of these products consists mainly of the albumin-globulin-type, water soluble proteins and the other one, a syrupy product, consists mainly of sugars obtained as products of hydrolysis of small-particle starch of grain. The homogenous slurry obtained after separation of ordinary grain starch and gluten from the grain flour by known methods is heated at a temperature of at least 120.degree. C., treated at a temperature of at the most 90.degree. C. simultaneously by means of alpha-amylase and beta-glucanase, the produced protein precipitate is separated from the sludge, washed, and dried. The remaining clear fraction is sugared by means of amyloglucosidase of fungalamylase.
    Type: Grant
    Filed: January 19, 1982
    Date of Patent: May 15, 1984
    Assignee: Oy Vehna AB
    Inventors: Marja-Leena Sarkki, Martti Soderstrom, Hannu Maunula, Annika Korhonen
  • Patent number: 4339280
    Abstract: A seeding magma for seeding a solution of a crystallizable product is prepared from a suspension the crystals in a liquid phase. This suspension is delivered into a continuously rotating conical basket of a centrifugal drier. The basket has an upper output end and a screen is mounted therein. Rotation of the basket causes the suspension to be subjected to centrifugal forces causing crystals of a size interior to the mesh size of the screen to pass with the liquid phase through the screen and larger crystals to be retained on the screen and centrifugally displaced towards the upper output end and ejected therefrom. These crystals are forcefully projected against an impact surface disposed around the output end of the basket whereby the projected crystals are crushed on impact with the surface. The crushed crystals are recycled into the suspension delivered into the basket while the liquid phase with the crystals passed through the screen is removed for preparing the seeding magma.
    Type: Grant
    Filed: September 22, 1980
    Date of Patent: July 13, 1982
    Assignee: Fives-Cail Babcock
    Inventor: Andre Mercier
  • Patent number: 4118248
    Abstract: A method for releasing compacted sugar crystals from a screen after centrifugation uses braking force for stopping rotation of the centrifuge. The brake stops rotation of the screen without simultaneously stopping rotation of the crystals accumulated adjacent the screen. The centrifuge may include one or more apertures in the base of the drum for exit of the sugar crystals.
    Type: Grant
    Filed: March 17, 1977
    Date of Patent: October 3, 1978
    Inventor: Jorge Halder Lacher
  • Patent number: 4101338
    Abstract: Process for fractionating carbohydrate-containing materials, such as molasses, by contact with an ion exclusion resin wherein a first portion of the material and a second, less dense portion of the material are sequentially fed to the resin. This scheme of adding the carbohydrate-containing material to the column of ion exclusion resin lessens the channeling problem. Also, a process for treating molasses comprising adding ferric ions to the molasses to form a precipitate and passing the so-treated molasses through an ion exclusion resin.
    Type: Grant
    Filed: April 27, 1976
    Date of Patent: July 18, 1978
    Assignee: Sucrest Corporation
    Inventors: Robert M. Rapaport, Anthony Monti, Raymond D. Moroz, Charles B. Broeg
  • Patent number: 4052304
    Abstract: An air and massecuite warming device comprising a pair of nested, concentric frusto-conical tubular members positioned above a massecuite separating centrifuge in which steam is directed into the chamber formed between the nested members. The steam is discharged from the inner member by a plurality of nozzles located in the conical wall of the inner member forming a vortex. Before contacting the massecuite, the steam mixes with the air drawn through the centrifuge, raising the air temperature. This warm air reduces the massecuite viscosity by increasing the temperature of the massecuite and the temperature of the centrifuge elements contacting the massecuite thereby increasing the centrifuge separation capacity and improving the purity of the sugar produced.
    Type: Grant
    Filed: July 21, 1976
    Date of Patent: October 4, 1977
    Assignee: CF&I Engineers, Inc.
    Inventor: Mathieu J. Vertenstein
  • Patent number: 4046590
    Abstract: A process for producing a colorless low-ash, high-purity sugar syrup from cane molasses wherein centrifuged molasses is acidified and treated with an ion exclusion resin. The resin is then eluted with water, and fractions of similar compositions are combined for recycling. The process yields a product similar to refiner's syrup, which is readily further purified by carbon and ion exchange resins to provide a high-quality syrup.
    Type: Grant
    Filed: September 8, 1976
    Date of Patent: September 6, 1977
    Assignee: California and Hawaiian Sugar Company
    Inventor: Richard Riffer
  • Patent number: 4039348
    Abstract: A method of, and a system for, processing or treating raw sugar juice wherein raw sugar juice produced in a crushing mill is delivered to a first section of a partitioned surge chamber from which section it is withdrawn and subjected to a degritting process in one or more cyclone separators, the juice which is relatively free of heavy solids being subsequently delivered to a second section of the partitioned surge chamber from which section it is withdrawn for clarification in a clarifier and from which clarifier mud is withdrawn for subsequent treatment in one or more centrifugal separators, the removal of heavy solids, such as dirt and grit, during the degritting process being such as to reduce wear and erosion of the components in the centrifugal separators for processing the clarifier mud.
    Type: Grant
    Filed: April 14, 1975
    Date of Patent: August 2, 1977
    Assignee: Dorr-Oliver Incorporated
    Inventor: Richard James Hunwick
  • Patent number: 4036694
    Abstract: Beet juice is purified, then concentrated and treated in several steps for boiling and centrifugal separation to effect recovery of sucrose therefrom. The molasses remaining after the separation of sucrose from massecuite is treated with .alpha.-galactosidase to effect hydrolysis of raffinose present in the molasses. The resultant raffinose hydrolyzate is introduced into a calcium saccharate-forming step, wherein quicklime is continuously added to the hydrolyzate to form saccharate within the hydrolyzate. From the calcium saccharate-forming step, nearly the same volume of the saccharate-containing solution as that of the raffinose hydrolyzate fed therein is forwarded to a filtering and washing step. The resultant saccharate cake is sent back to the step for purification.
    Type: Grant
    Filed: September 23, 1975
    Date of Patent: July 19, 1977
    Assignee: Hokkaido Sugar Co., Ltd.
    Inventors: Shinichi Meguro, Shinsaku Imafuku, Kazuo Kawamura, Shigeki Hashimoto, Shigeyoshi Narita
  • Patent number: 4033879
    Abstract: The present centrifuge is especially adapted for centrifuging massecuite in the production of sugar. Two functional and structural units are separated from each other in such a manner that each unit may be supported independently of the other unit, yet so as to properly cooperate with each other. Thus, an inner housing and the rotating drum with the drive means for the drum form an inner, integral unit while an outer housing and a cover as well as the massecuite supply means form a further, outer integral unit. A carrier member, preferably in the form of a hollow channel, extends from the inner housing through the outer housing to support the drum drive means outside of the outer housing, but as part of the inner unit.
    Type: Grant
    Filed: July 15, 1975
    Date of Patent: July 5, 1977
    Assignee: Braunschweigische Maschinenbauanstalt
    Inventors: Peter Natt, Heinrich Kurland
  • Patent number: 4009045
    Abstract: Sugar is continuously crystallized from a sugar bearing solution in a single stage vacuum pan by a method and apparatus comprising means for and the steps of continuously supplying a sugar bearing solution of a constant, desired purity to the vacuum pan by combining a relatively low purity sugar bearing solution flow stream with a relatively high purity sugar bearing solution flow stream while regulating the ratio of relatively low to relatively high purity sugar bearing solution in the combined flow stream, continuously supplying sugar seed crystals having a relatively uniform crystal size distribution to the vacuum pan, continuously boiling at least a portion of the sugar bearing solution and sugar seed crystals in the vaccum pan to form a boiling massecuite, and continuously removing at least a portion of the massecuite from the vacuum pan.
    Type: Grant
    Filed: April 21, 1976
    Date of Patent: February 22, 1977
    Assignee: Godchaux-Henderson Sugar Co., Inc.
    Inventor: Peter H. Petri
  • Patent number: 4008098
    Abstract: A high concentration sugar solution is produced by contacting sugar crystals as they emerge from a centrifuging basket, with pressurized solvent liquid sprayed from a plurality of nozzles to form a turbulent mist of solvent and to envelope the sugar crystals which are forced to travel through said turbulent mist of solvent to impinge upon a baffle guide ring. The turbulent flow of solvent mist and solvent enveloped sugar crystals is guided along said baffle guide ring to a back-up location, where sugar solution, air, and liquid mist are forced through a gap and over a damming ring wall surrounding the gap. The centrifuge for performing the foregoing process includes a centrifuging basket with an upper rim over which the sugar crystals emerge. A solvent supply ring with nozzles facing toward the rim is arranged above the upper basket rim. The baffle guide ring curves downwardly and surrounds an inner housing which in turn surrounds the basket.
    Type: Grant
    Filed: December 10, 1975
    Date of Patent: February 15, 1977
    Assignee: Braunschweigische Maschinenbauanstalt
    Inventors: Walter Dietzel, Siegfried Matusch, Helmut Schaper, Erwin Zeichner
  • Patent number: 3994743
    Abstract: Method and apparatus for treating fresh, unheated sugar cane juice which involves adding a sufficient amount of an aqueous alkaline slurry containing powdered active carbon to the juice to raise the pH of the juice to 6.8-8.5. The resulting mud is separated and a water white juice is obtained. The water white juice is concentrated to form a direct white sugar and an edible molasses having a natural maple flavor and odor. The juice may be subjected to a preliminary cyclone separation and the sugar cane from which the juice is obtained may be subjected to a steam-cleaning operation to remove cane wax and dirt.
    Type: Grant
    Filed: November 19, 1973
    Date of Patent: November 30, 1976
    Inventor: Lewis A. Paley
  • Patent number: 3973984
    Abstract: Continuously operable sugar centrifuge comprises a number of centrifuging channels forming part of a conical frustum and being symmetrically distributed relative to a rotational axis. Preferably, two channels are arranged to receive the massecuite through massecuite supply conduits connected to the upper ends of the centrifuging channels. The lower ends of the centrifuging channels are connected through radially extending sugar discharge conduits leading to a sugar outlet arranged coaxially with the drive shaft of the centrifuge. The sugar conduits have a radial dimension so that their outer ends extend outside of the centrifuging channels. The outer ends of the sugar conduits are provided with funnels facing with their open face in the direction of rotation of the centrifuge whereby an air stream transports the sugar radially inwardly from the centrifuging channels to the sugar outlet.
    Type: Grant
    Filed: October 23, 1975
    Date of Patent: August 10, 1976
    Assignee: Braunschweigische Maschinenbauanstalt
    Inventor: Volkmar Hentschel