Including Particulate Material Patents (Class 131/342)
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Publication number: 20110036366Abstract: A filter material adapted for use as a filter element of a smoking article is provided, the filter material including at least one segment of fibrous tow having a plurality of degradable particles dispersed therein, the degradable particles comprising a starch material. Exemplary starch materials include naturally-occurring starch, hydroxyalkylated starch, starch esters, ionically modified starch, oxidized starch, hydrolyzed starch, plasticized starch, gelatinized starch, grafted starch, crosslinked starch, transglycosylated starch, starch ethers, and mixtures thereof, as well as blends of starch with other polymers. Filter elements and smoking articles, such as cigarettes, that contain the filter material are also provided. A method of preparing polymer fibers for use in filter elements is also provided, the method including adding the starch material to a fiber precursor solution prior to fiber extrusion or dry-blending the starch material with the polymer material to be formed into fibers.Type: ApplicationFiled: August 11, 2009Publication date: February 17, 2011Inventor: Andries D. Sebastian
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Patent number: 7827996Abstract: Smoking articles which involve the use of amphiphile-modified sorbents are disclosed. The amphiphile-modified sorbent has at least one amphiphilic compound bound to an inorganic molecular sieve substrate. The amphiphile-modified sorbent selectively removes certain constituents from cigarette smoke, while maintaining other constituents, such as those that contribute to flavor. Methods for making cigarette filters and smoking articles using amphiphile-modified sorbents, as well as methods for smoking a cigarette containing an amphiphile-modified sorbent, are also provided.Type: GrantFiled: December 22, 2003Date of Patent: November 9, 2010Assignee: Philip Morris USA Inc.Inventors: Jay A Fournier, Zhaohua Luan
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Patent number: 7806817Abstract: A process for making a crimped tow of filaments suitable for forming a bale of crimped tow for conversion to cigarette filter rods comprising, presenting an uncrimped tow of filaments in a banded condition, adhesively bonding to the filaments of the banded tow (3), porous particles having absorbent surfaces imparting filtration capacity for tobacco smoke constituents, and crimping the banded tow, wherein the process comprises the steps, of: (i) pre-treating the particles to load them with a material capable of generating a gaseous emission from the particles thus forming pre-treated particles; (ii) applying to the filaments of the banded tow, the pre-treated particles and an adhesive for bonding the particles to the filaments; and subsequently (iii) treating the tow to generate the gaseous emission from the pre-treated particles so as to limit deactivation of the absorbent particle surfaces by the adhesive.Type: GrantFiled: March 8, 2005Date of Patent: October 5, 2010Assignee: Acetate Products Ltd.Inventors: Craig Day, John Travers
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Patent number: 7784471Abstract: A smoking article such as a cigarette comprises a tobacco rod and a filter component having a cavity filled with spherical beaded carbon. As mainstream tobacco smoke is drawn through the filter component, targeted gas phase smoke constituents are removed as the smoke passes through the carbon. During the filter manufacturing process the spherical beaded carbon flows like a liquid and substantially completely fills the cavity. Point-to-point contact between the spherical beads together with substantially complete filling of the cavity produces minimal channeling of ambulatory gas phase as well as maximum contact between the gas phase and the carbon surface of the spherical beads during smoking.Type: GrantFiled: April 11, 2006Date of Patent: August 31, 2010Assignee: Philip Morris USA Inc.Inventors: John B. Paine, III, Zuyin Yang, Kent B. Koller, Jay A. Fournier, Charles E. Thomas, Jr., Timothy S. Sherwood, Zhaohua Luan, Shuzhong Zhuang, Jose G. Nepomuceno, Diane L. Gee, Georgios D. Karles
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Patent number: 7784470Abstract: A smoking article such as a cigarette comprises a tobacco rod and a filter component having a cavity filled with spherical beaded carbon. As mainstream tobacco smoke is drawn through the filter component, targeted gas phase smoke constituents are removed as the smoke passes through the carbon. During the filter manufacturing process the spherical beaded carbon flows like a liquid and substantially completely fills the cavity. Point-to-point contact between the spherical beads together with substantially complete filling of the cavity produces minimal channeling of ambulatory gas phase as well as maximum contact between the gas phase and the carbon surface of the spherical beads during smoking.Type: GrantFiled: January 9, 2003Date of Patent: August 31, 2010Assignee: Philip Morris USA Inc.Inventors: John B. Paine, III, Zuyin Yang, Kent B. Koller, Jay A. Fournier, Charles E. Thomas, Jr., Timothy S. Sherwood, Zhaohua Luan, Shuzhong Zhuang, Jose M. G. Nepomuceno, Diane L. Gee, Georgios D. Karles
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Patent number: 7669604Abstract: A filter element incorporating an adsorbent material is provided. The filter element may comprise a first section of filter material and a second section of filter material spaced apart to form a compartment therebetween. The compartment may be filled with one or more adsorbents or the compartment may be divided into two regions, wherein one compartment region is filled with an adsorbent and the other compartment region is either filled with an ion-exchange resin or remains empty. The section of filter material adjacent to the tobacco rod may include one or more channels therethrough for passaging smoke directly from the tobacco rod into the adsorbent-filled compartment. The mouth end section of filter material may contain a breakable capsule, wherein the breakable capsule is filled with a flavoring agent capable of altering the taste characteristics of mainstream smoke.Type: GrantFiled: September 30, 2003Date of Patent: March 2, 2010Assignee: R.J. Reynolds Tobacco CompanyInventors: Evon Llewellyn Crooks, Joanne Naomi Taylor, Paul Fischer Bernasek
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Patent number: 7647932Abstract: A smoking article, such as a cigarette, includes a lighting end and a mouth end. The lighting end is a longitudinally extending segment comprising smokable material that is intended to be lit and burned, and the resulting smoke generated by the burning of that smokable material is intended to be drawn into the mouth of the smoker through the mouth end of smoking article. A mouth end piece is located at the mouth end of the smoking article, and the mouth end piece allows the smoking article to be placed in the mouth of the smoker to be drawn upon. The smoking article further incorporates an aerosol-generation system that is located between the lighting end segment and the mouth end piece. The aerosol-generation system includes (i) a heat generation segment located adjacent to the lighting end segment, and (ii) an aerosol-generation region located between the heat generation segment and the mouth end piece. The aerosol-generation region incorporates an aerosol-forming material (e.g., glycerin and flavors).Type: GrantFiled: August 1, 2005Date of Patent: January 19, 2010Assignee: R.J. Reynolds Tobacco CompanyInventors: Daniel V. Cantrell, William J. Casey, III, Evon L. Crooks, Billy T. Conner, Joanne N. Taylor, Jeffrey A. Willis, Dempsey B. Brewer, Jr., Wayne E. Davis, Jr., James R. Stone
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Publication number: 20090260645Abstract: A tobacco product comprising nanocrystalline particles and methods of reducing the levels of undesirable compounds in tobacco smoke are provided. The nanocrystalline particles are effective sorbents of numerous toxic compounds released by burning tobacco and may be incorporated into the tobacco itself, incorporated into a filter element, or incorporated into the fibers of a wrapping paper.Type: ApplicationFiled: April 14, 2009Publication date: October 22, 2009Applicant: NANOSCALE CORPORATIONInventors: David Brotton, Olga B. Koper
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Patent number: 7552735Abstract: A cigarette filter for removing gas phase constituents from mainstream cigarette smoke as the smoke is drawn through the filter primarily comprises an activated carbon fiber filter section including a bundle of activated carbon fibers. Particulate adsorbent materials such as granules, beads or course powders may be dispersed amongst the activated carbon fibers to aid in removal of the gas phase constituents. Additionally, the activated carbon fiber filter section may be used in combination with a separate bed or beds of particulate adsorbent material. In one embodiment, the activated carbon fibers are positioned within a helical groove on the outside of a threaded rod within the activated carbon fiber filter section. Relatively smaller amounts of activated carbon fibers produce the same smoke constituent reduction as larger amounts of particulate adsorbent material.Type: GrantFiled: April 11, 2003Date of Patent: June 30, 2009Assignee: Philip Morris USA Inc.Inventors: Lixin Xue, Jose G. Nepomuceno, Shuzhong Zhuang, Timothy Scott Sherwood, John Bryant Paine, III, Jay A Fournier, Charles Edwin Thomas, Jr., Kent Brian Koller, Liqun Yu
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Patent number: 7549427Abstract: A novel nanocatalyst is disclosed containing titanium oxide, iron oxide, and calcium oxide. The catalyst comprises a layer of iron oxide in the gamma form supported on a titanium oxide core. Addition of calcium cations helps to stabilize the iron oxide in the gamma form. The iron oxide layer is on the order of a few nanometers thick on the surface of the titanium oxide core, in an “egg-in-shell” structure. The nanocatalyst is highly active in promoting the oxidation of compounds such as hydroquinone, catechol, other hydrocarbons, chlorinated phenols, and carbon monoxide, even at moderately elevated temperatures. The catalyst remains active in a pyrolytic environment for extended periods of time, and possesses high redox cycling potential. The efficiency of the catalyst is not strongly affected by coking in a combustion environment.Type: GrantFiled: July 13, 2005Date of Patent: June 23, 2009Assignee: Board of Supervisors of Louisiana State University and Agricultural and Mechanical CollegeInventors: Harold B. Dellinger, Slawomir M. Lomnicki
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Publication number: 20080190439Abstract: A method and apparatus for tobacco smoke filter production wherein a train of tobacco smoke filtering material, whilst continuously advanced longitudinally, is gathered towards rod shape and then shaped to and secured in rod form, and wherein there is discontinuous pneumatic injection of particulate additive through an injector conduit laterally into the gathering material to form separate additive pockets embedded in and spaced along the continuously produced rod.Type: ApplicationFiled: December 5, 2005Publication date: August 14, 2008Inventors: Serge Veluz, Alexis Louvet
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Publication number: 20080023016Abstract: A novel nanocatalyst is disclosed containing titanium oxide, iron oxide, and calcium oxide. The catalyst comprises a layer of iron oxide in the gamma form supported on a titanium oxide core. Addition of calcium cations helps to stabilize the iron oxide in the gamma form. The iron oxide layer is on the order of a few nanometers thick on the surface of the titanium oxide core, in an “egg-in-shell” structure. The nanocatalyst is highly active in promoting the oxidation of compounds such as hydroquinone, catechol, other hydrocarbons, chlorinated phenols, and carbon monoxide, even at moderately elevated temperatures. The catalyst remains active in a pyrolytic environment for extended periods of time, and possesses high redox cycling potential. The efficiency of the catalyst is not strongly affected by coking in a combustion environment.Type: ApplicationFiled: July 13, 2005Publication date: January 31, 2008Inventors: Harold B. Dellinger, Slawomir M. Lomnicki
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Patent number: 7237558Abstract: A filter element incorporating an adsorbent material is provided. The filter element may comprise a first section of filter material and a second section of filter material spaced apart to form a compartment therebetween. The compartment may be filled with one or more adsorbents or the compartment may be divided into two regions, wherein one compartment region is filled with an adsorbent and the other compartment region is either filled with an ion-exchange resin or remains empty. The section of filter material adjacent to the tobacco rod may include one or more channels therethrough for passaging smoke directly from the tobacco rod into the adsorbent-filled compartment. The mouth end section of filter material may contain a breakable capsule, wherein the breakable capsule is filled with a flavoring agent capable of altering the taste characteristics of mainstream smoke.Type: GrantFiled: September 30, 2003Date of Patent: July 3, 2007Assignee: R. J. Reynolds Tobacco CompanyInventors: Melissa Ann Clark, Evon Llewellyn Crooks, Paul Eugene Braxton, Chandra Kumar Banerjee, Sharon Pitts Dunlap, Timothy Brian Nestor
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Patent number: 7228861Abstract: A cigarette filter has filter sections including filter materials individually wrapped with plug wrap paper, forming paper for wrapping the filter sections integrally, and tipping paper covering the forming paper so as to connect the filter sections to a cigarette section to form a cigarette, wherein activated charcoal and an inorganic mineral-based porous material carrying ferrous sulfate/L-ascorbic acid are contained as adsorbents in at least one of the filter materials and a space between the filter materials.Type: GrantFiled: January 30, 2004Date of Patent: June 12, 2007Assignee: Japan Tobacco, Inc.Inventors: Ichiro Atobe, Fumihiro Omori
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Patent number: 7025067Abstract: A filter for tobacco smoke inhaling/generating/producing device, comprising stipulated amounts of specific grain sizes or combination of grain sizes of activated charcoal for effectively reducing from the mainstream smoke the level of p-benzosemiquinone (p-BSQ), a relatively stable highly reactive major harmful oxidant, without significantly affecting the flavor and taste of the smoke while providing comfortable mouthful of smoke and nicotine delivery, so that the charcoal filter cigarettes becomes potentially less hazardous safer cigarettes and may be acceptable to the smokers with marked reduction in health risk; the charcoal filters also effectively reduce the level of nitric oxide and tar from the mainstream smoke.Type: GrantFiled: February 13, 2002Date of Patent: April 11, 2006Assignee: Council of Scientific and Industrial ResearchInventor: Indu Bhusan Chatterjee
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Patent number: 6907885Abstract: This invention is a highly efficient filter containing fibers that contain small particle size adsorbents/absorbents such as carbon and/or silica to selectively reduce targeted components in mainstream cigarette smoke. The invention relates to a novel class of highly efficient cigarette smoke filters made from much smaller solid fine particles (preferably 1-50 micrometers in diameter) impregnated in shaped fibers that possess open or semi-opened micro-cavity. The invention further relates to a cigarette having a plug/space/plug or plug/space configuration and having the impregnated filters resided in the space in bonded non-woven or freely unbounded manner to allow controlled TPM delivery.Type: GrantFiled: February 11, 2003Date of Patent: June 21, 2005Assignee: Philip Morris USA Inc.Inventors: Lixin Luke Xue, Kent B. Koller, Qiong Gao
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Patent number: 6863074Abstract: Cigarette filters, methods for making cigarettes and methods for smoking cigarettes are provided, which involve the use of an unfunctionalized porous polyaromatic resins, which is capable of removing at least some of at least one gas phase constituent from mainstream smoke through sorption. The unfunctionalized porous polyaromatic resin may be a polymerization product of non-polar styrene and divinyl benzene. Various gas phase constituent can be removed from mainstream tobacco smoke, such as dienes, furans, pyrroles, aromatics and ketones, for example. The cigarette filters and cigarettes can provide low resistance-to-draw and/or high total particulate matter delivery. Additionally, the unfunctionalized porous polyaromatic resin may further include flavorant(s).Type: GrantFiled: August 30, 2002Date of Patent: March 8, 2005Assignee: Philip Morris USA Inc.Inventors: Lixin Xue, Charles Edwin Thomas, Jr., Liqun Yu, Kent B. Koller
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Patent number: 6857431Abstract: Nanocomposite copper-ceria catalysts are provided, which comprise copper oxide nanoparticles, copper nanoparticles, or a mixture thereof combined with ceria nanoparticles. Methods for making such catalysts are also provided, which involve the steps of (i) combining ceria nanoparticles in an aqueous suspension with copper 2,4-pentanedionate to form a slurry; (ii) heating the slurry formed in step (i) under an inert gas atmosphere or an oxygen-argon atmosphere, at a temperature and for a time sufficient to cause decomposition of the copper 2,4-pentanedionate to form copper nanoparticles and/or copper oxide nanoparticles that are combined with the ceria nanoparticles; and (iii) optionally, subjecting the product formed in step (ii) to a heat treatment process under conditions effective to convert at least some of the copper nanoparticles to copper oxide nanoparticles.Type: GrantFiled: December 9, 2002Date of Patent: February 22, 2005Assignee: Philip Morris USA Inc.Inventors: Sarojini Deevi, Sohini PalDey
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Publication number: 20040237984Abstract: A cigarette filter that includes a multiple section filter which reduces the level of predetermined smoke constituents. The filter (130) consists of a fibrous filter plug (132) located at the mouth-end of the cigarette, a section (136) containing a selective adsorbent material, and a section (134) containing a general adsorbent material. The selective adsorbent material, such as a phenol-formaldchyde resin matrix surface-functionalized with mainly primary and secondary amine functional groups, removes specific smoke constituents from the tobacco smoke. The general adsorbent material, such as activated charcoal, is preferably capable of adsorbing a range of chemical compounds without a high degree of specificity. Structurally, the fibrous filter plug, the selective adsorbent section, and the general adsorbent section are co-axially aligned it tandem.Type: ApplicationFiled: January 30, 2004Publication date: December 2, 2004Inventors: James N Figlar, Brian E Tucker, F Kelley St Charles
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Publication number: 20040200490Abstract: A cigarette filter includes two or more filter sections of the following filter sections a filter section added with a liquid fatty acid ester or a liquid fatty acid having a viscosity of 1 to 300 cP, a filter section added with a glycol having a viscosity of 1 to 300 cP, and a filter section added with a charcoal.Type: ApplicationFiled: April 29, 2004Publication date: October 14, 2004Inventors: Michihiro Inagaki, Kazuhiko Katayama, Takako Ikeda
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Publication number: 20040200491Abstract: A process for the on line production of cigarette filters comprises the steps of conveying a continuous thin flexible substrate past a source of smoke altering particulate material, such as adsorbents, catalysts and flavorants. An electrostatic charge is applied onto the substrate upstream of the source of particulate material. A layer of particulate material from the source is deposited onto the substrate with the thickness of the layer depending upon the strength of the electrostatic charge. The coated substrate is then cut into pieces, and the pieces are placed into the cavities between spaced apart filter components. In an alternative process, filter paper is coated with smoke altering particulate material by electrostatic deposition techniques, and spaced apart filter components are placed onto the particulate coated filter paper which is then folded around the filter components.Type: ApplicationFiled: April 9, 2003Publication date: October 14, 2004Inventors: Georgios D. Karles, Henry M. Dante, Xuan Pham, Barry S. Smith
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Publication number: 20040187881Abstract: A cigarette comprises a tobacco rod and a multi-component filter comprising a bed of adsorbent and a flavor-releasing filter segment located downstream of the bed of adsorbent. In the preferred embodiment, the adsorbent is also flavor-bearing and comprises high surface area, activated carbon. As mainstream smoke is drawn through the upstream portion of the filter, gas phase smoke constituents are removed and flavor is released from the adsorbent bed. Thereafter additional flavor is released into the mainstream smoke as it passes through the flavor-releasing filter segment. Ventilation is provided to limit the amount of tobacco being combusted during each puff and is arranged at a location spaced downstream from the adsorbent bed to lower mainstream smoke velocity through the adsorbent bed.Type: ApplicationFiled: March 16, 2004Publication date: September 30, 2004Inventors: Richard Jupe, Ronald William Dwyer, Don Earl Laslie, Arlington L. Finley, Barbara G. Taylor, Cecil M. Smith, Vivian E. Willis
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Publication number: 20040182400Abstract: A cigarette filter has filter sections including filter materials individually wrapped with plug wrap paper, forming paper for wrapping the filter sections integrally, and tipping paper covering the forming paper so as to connect the filter sections to a cigarette section to form a cigarette, wherein activated charcoal and an inorganic mineral-based porous material carrying ferrous sulfate/L-ascorbic acid are contained as adsorbents in at least one of the filter materials and a space between the filter materials.Type: ApplicationFiled: January 30, 2004Publication date: September 23, 2004Inventors: Ichiro Atobe, Fumihiro Omori
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Publication number: 20040182401Abstract: A cigarette filter has filter sections including filter materials individually wrapped with plug wrap paper, forming paper for wrapping the filter sections integrally, and tipping paper covering the forming paper so as to connect the filter sections to a cigarette section to form a cigarette, wherein activated charcoal and silica/alumina are contained as adsorbents in at least one of the filter materials and a space between the filter materials.Type: ApplicationFiled: January 30, 2004Publication date: September 23, 2004Inventors: Ichiro Atobe, Fumihiro Omori
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Patent number: 6789547Abstract: Catalytically active carbons are used in cigarette filters for selective oxidation of selected gas phase components in cigarette smoke. The carbons are impregnated with transition metals and sulfur and/or nitrogen ligation. The catalytic activity of the carbon is significantly improved by introducing catalytically active sites by heat treatment in the range of 500-1000° C. in the presence of transition metals and nitrogenous or sulfurous materials. Furthermore, introduction of such metalliferous sites into a active carbon can improve the absorptive affinity of the active carbon for classes of compounds, including aliphatic dienes and aromatic hydrocarbons.Type: GrantFiled: October 30, 2001Date of Patent: September 14, 2004Assignee: Philip Morris IncorporatedInventor: John B. Paine, III
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Publication number: 20040173229Abstract: The present invention provides smoking articles comprising ultrafine particles. In an embodiment, a combustible material component of a smoking article may comprise ultrafine particles. In other embodiments, ultrafine particles are incorporated into a smoking article in proximity to a combustible material component. The present invention also provides methods for altering smoke chemistry.Type: ApplicationFiled: March 5, 2003Publication date: September 9, 2004Inventors: Evon Llewellyn Crooks, Stephen Benson Sears, Stephen Keith Cole, Chandra Kumar Banerjee, Joanne Naomi Taylor
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Patent number: 6779529Abstract: A cigarette filter includes a multiple section filter which reduces the level of predetermined smoke constituents. The filter includes a fibrous filter plug section, a selective adsorbent section, and a general adsorbent section co-axially aligned in tandem. The selective adsorbent section includes a selective absorbent material which is a phenol-formaldehyde resin matrix surface-functionalized with mainly primary and secondary amine functional groups which removes specific smoke constituents from the tobacco smoke. The general adsorbent section is a material capable of adsorbing a range of chemical compounds without a high degree of specificity.Type: GrantFiled: June 24, 2002Date of Patent: August 24, 2004Assignee: Brown & Williamson Tobacco CorporationInventors: James N. Figlar, Brian E. Tucker, F. Kelley St. Charles
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Patent number: 6761174Abstract: A cigarette comprises a tobacco rod and a multi-component filter comprising a bed of adsorbent and a flavor-releasing filter segment located downstream of the bed of adsorbent. In the preferred embodiment, the adsorbent is also flavor-bearing and comprises high surface area, activated carbon. As mainstream smoke is drawn through the upstream portion of the filter, gas phase smoke constituents are removed and flavor is released from the adsorbent bed. Thereafter additional flavor is released into the mainstream smoke as it passes through the flavor-releasing filter segment. Ventilation is provided to limit the amount of tobacco being combusted during each puff and is arranged at a location spaced downstream from the adsorbent bed to lower mainstream smoke velocity through the adsorbent bed.Type: GrantFiled: February 22, 2002Date of Patent: July 13, 2004Assignee: Philip Morris IncorporatedInventors: Richard Jupe, Ronald William Dwyer, Don Earl Laslie, Arlington L. Finley, Barbara G. Taylor, Cecil M. Smith, Vivian E. Willis
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Publication number: 20040107973Abstract: A system and method for adding material such as foam material to spaced cavities within a cigarette filter. A belt is provided and adapted to be driven synchronously with a moving cigarette filter rod. A plurality of injection needles protrude from the belt at spaced intervals, with the spacing between the needles coinciding with a spacing between the cavities within a cigarette filter rod. A chamber containing an expandable foam material is in fluid communication with one or more of the injection needles at one or more positions along a path traveled by the injection needles.Type: ApplicationFiled: December 9, 2002Publication date: June 10, 2004Inventor: Charles Gary Atwell
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Publication number: 20030234025Abstract: The present invention relates to a new use of Pini Resina for removing toxic substances from a gas. In particular, the invention provides a cigarette filter comprising a filter layer containing Pini Resina, which can remove the toxic substances derived from a burning cigarette.Type: ApplicationFiled: June 21, 2002Publication date: December 25, 2003Applicant: ROYAL DYNESTY TECH.CO., LTDInventor: Hsin-Shiu Chuang
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Publication number: 20030183237Abstract: This invention is a highly efficient filter containing fibers that contain small particle size adsorbents/absorbents such as carbon and/or silica to selectively reduce targeted components in mainstream cigarette smoke. The invention relates to a novel class of highly efficient cigarette smoke filters made from much smaller solid fine particles (preferably 1-50 micrometers in diameter) impregnated in shaped fibers that possess open or semi-opened micro-cavity. The invention further relates to a cigarette having a plug/space/plug or plug/space configuration and having the impregnated filters resided in the space in bonded non-woven or freely unbounded manner to allow controlled TPM delivery.Type: ApplicationFiled: February 11, 2003Publication date: October 2, 2003Inventors: Lixin Luke Xue, Kent B. Koller, Qiong Gao
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Publication number: 20030168070Abstract: A process of impregnating fine adsorbent particles such as carbon dust or APS silica gel powder into the micro-cavities of shaped fibers comprises the steps of continuously conveying shaped fibers with micro-cavities to a reservoir of the fine adsorbent particles. The fibers pass through the reservoir to thereby produce relative motion between the fibers and the particles. Additionally, impact forces are created between the shaped fibers and the fine particles to assist in impregnating the particles into the micro-cavities of the fibers. Any excess particles are removed from the fibers outside the reservoir, and subsequently the shaped fibers impregnated with fine adsorbent particles are collected for later use in filter applications such as cigarette filter and air filter applications, for example.Type: ApplicationFiled: November 14, 2002Publication date: September 11, 2003Inventors: Lixin Luke Xue, Kent B. Koller, Qiong Gao, Tim Sherwood, Charles E. Thomas, George R. Scott, Liqun Yu
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Publication number: 20030159703Abstract: Flavored carbon useful as a filtering material of a smoking article such as a cigarette is made by applying liquid flavorant to activated carbon particles in a fluidized bed. The flavored carbon can be used to impart desired taste to mainstream smoke while removing one or more components from mainstream smoke.Type: ApplicationFiled: February 22, 2002Publication date: August 28, 2003Inventors: Zuyin Yang, Jose G. Nepomuceno, Barbara G. Taylor
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Publication number: 20030154993Abstract: A smoking article such as a cigarette comprises a tobacco rod and a filter component having a cavity filled with spherical beaded carbon. As mainstream tobacco smoke is drawn through the filter component, targeted gas phase smoke constituents are removed as the smoke passes through the carbon. During the filter manufacturing process the spherical beaded carbon flows like a liquid and substantially completely fills the cavity. Point-to-point contact between the spherical beads together with substantially complete filling of the cavity produces minimal channeling of ambulatory gas phase as well as maximum contact between the gas phase and the carbon surface of the spherical beads during smoking.Type: ApplicationFiled: January 9, 2003Publication date: August 21, 2003Inventors: John B. Paine, Zuyin Yang, Kent B. Koller, Jay A. Fournier, Charles E. Thomas, Timothy S. Sherwood, Zhaohua Luan, Shuzhong Zhuang, Jose M. G. Nepomuceno, Diane L. Gee, Georgios D. Karles
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Publication number: 20030140932Abstract: The invention relates to a ventilated filter cigarette with a wrapped one-part tobacco strand (11) and with a filter (20) having a ventilation means, said filter consisting of at least two filter parts (22,23). ventilation holes (14) are provided in the area of the mouth side filter part (22). Moreover, the mouth side filter part (22) is formed of a one-part filter segment, whereas the strand side filter part (23) is a filter segment (23) with a core (24) and a sleeve (26), and thus forms a so-called coaxial filter part or a coaxial filter.Type: ApplicationFiled: January 24, 2003Publication date: July 31, 2003Inventors: Henning Seidel, Solvey Knorr, Inga Gurke
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Patent number: 6591839Abstract: A filter material for reducing the content of harmful substances in tobacco smoke. The filter material comprises a ground and not additionally activated expanded clay produced without adding foreign substances, and zeolite as the filter material. The filter is suitable for tobacco products such as cigarettes, cigars and cigarillos, and for smoking articles such as tobacco pipes and cigarette and cigar holders.Type: GrantFiled: March 28, 2001Date of Patent: July 15, 2003Inventors: Dieter Meyer, Hans-Peter Braun
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Patent number: 6584979Abstract: This invention is a highly efficient filter containing fibers that contain small particle size adsorbents/absorbents such as carbon and/or silica to selectively reduce targeted components in mainstream cigarette smoke. The invention relates to a novel class of highly efficient cigarette smoke filters made from much smaller solid fine particles (preferably 1-50 micrometers in diameter) impregnated in shaped fibers that possess open or semi-opened micro-cavity. The invention further relates to a cigarette having a plug/space/plug or plug/space configuration and having the impregnated filters resided in the space in bonded non-woven or freely unbounded manner to allow controlled TPM delivery.Type: GrantFiled: April 20, 2001Date of Patent: July 1, 2003Assignee: Philip Morris IncorporatedInventors: Lixin Luke Xue, Kent B. Koller, Qiong Gao
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Publication number: 20030079755Abstract: A tobacco filter device includes a plurality of filter units superimposedly rechargeably filled in a sleeve member, having a bowl member connected to an outer end (smoking end) of the sleeve member and a mouthpiece connected to an inner end (mouth end) of the sleeve member, whereby upon smoking of tobacco or a cigarette as loaded or inserted in the bowl portion, the filter unit or units positioned on an outer portion of the sleeve member adjacent to the smoking end, after being saturated with smoking waste including tar and nicotine, may be pushed outwardly and discarded from the outer end of the sleeve member as thrusted and urged by a fresh (new) filter unit (or units) as recharged into the inner (mouth) end of the sleeve member, thereby still keeping use of those filter units not yet saturated and loaded in the rear portion of the sleeve member, without wasting the useful filter units.Type: ApplicationFiled: October 24, 2002Publication date: May 1, 2003Inventor: Te-San Liu
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Publication number: 20030070686Abstract: A cigarette filter includes a multiple section filter which reduces the level of predetermined smoke constituents. The filter includes a fibrous filter plug section, a selective adsorbent section, and a general adsorbent section co-axially aligned in tandem. The selective adsorbent section includes a selective absorbent material which is a phenol-formaldehyde resin matrix surface-functionalized with mainly primary and secondary amine functional groups which removes specific smoke constituents from the tobacco smoke. The general adsorbent section is a material capable of adsorbing a range of chemical compounds without a high degree of specificity.Type: ApplicationFiled: June 24, 2002Publication date: April 17, 2003Applicant: Brown & Williamson Tobacco CorporationInventors: James N. Figlar, Brian E. Tucker, F. Kelley St. Charles
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Patent number: 6530377Abstract: A tobacco smoke filter comprising a porous substrate comprising dry water and a porphyrin dispersed therein. The porous substrate can further comprise microcapsules. The microcapsules can comprise one or more substances selected from the group consisting of chlorophyllin, methylcellulose, sodium pyroglutamate and a vegetable oil. The porous substrate can further comprise sodium pyroglutamate.Type: GrantFiled: November 20, 2000Date of Patent: March 11, 2003Assignee: Filligent LimitedInventors: Craig Lesser, Reid W. Von Borstel
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Patent number: 6478032Abstract: The invention relates to a cigarette paper having a low total filler content, 20% by weight of the paper or less, a proportion of the filler being a filler capable of effecting visible sidestream smoke reduction. The basis weight of the paper is about 30 g m−2 or more. Smoking articles made with such papers provide a synergistic sidestream smoke component reduction when compared with control cigarettes. Papers according to the invention with the addition of various burn additives are also described.Type: GrantFiled: October 18, 1999Date of Patent: November 12, 2002Assignee: British-American Tobacco (Investments) LimitedInventors: Paul David Case, Alan George Stephenson
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Patent number: 6471754Abstract: A purification system for preventing secondhand tobacco smoke from reaching an ambient environment thereabout. Two components of the system include a smoke entrapment intake hood for aggregating the secondhand smoke and an electrostatic suction filter assembly in communication with the entrapment hood for extracting aggregated smoke from the hood, removing untoward particulate from the smoke, and releasing resulting clean air to the environment. The filter assembly includes at least one particulate filter for collecting smoke-borne particulate and at least one appropriately charged or grounded plate for electrostatically collecting charged smoke-borne particulate. An exit port from the filter assembly permits the release of so-cleaned air to the environment as a negative-ion emitter, positioned immediately inside the exit port, introduces charged ions into the cleansed air.Type: GrantFiled: March 16, 2001Date of Patent: October 29, 2002Inventor: Tahsin Ammouri
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Patent number: 6470894Abstract: A composition for inclusion within a cigarette, cigar, pipe or smokeless tobacco. The composition can be included within the tobacco itself, a filter for filtering tobacco smoke once burned or even within the paper or wrapper surrounding the tobacco product. In the cigarette filter, be it internal or external filters, the antioxidant complex is capable of scavenging and neutralizing the free radicals emanating from the burning or heated tobacco and passing through the filter as the smoker inhales. The composition is also capable of reducing free radical damage to the oro-pharyngeal cavity, respiratory tract and lungs resulting from tobacco smoke. The composition includes glutathione and preferably L-glutathione and green tea and/or grape seed extract.Type: GrantFiled: May 11, 2001Date of Patent: October 29, 2002Assignee: Thione International, Inc.Inventors: Theodore Hersh, Rebecca Hersh
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Patent number: 6344239Abstract: A method for producing a tobacco filter material which is either (A) a coating process for coating the surface of a fibrous or particulate cellulose with a cellulose ester having an average substitution degree of about 2.0 to about 2.6 to give a coated cellulose, and wet webbing the coated cellulose into a sheet, or (B) a treating process for treating a naturally-occurring or regenerated cellulose fiber or particle with an organic acid and an organic acid anhydride or organic acid halide in a liquid phase to give a cellulose derivative.Type: GrantFiled: October 20, 1998Date of Patent: February 5, 2002Assignee: Daicel Chemical Industries, Ltd.Inventors: Tanemi Asai, Syu Shimamoto, Hiroyuki Matsumura, Tohru Shibata
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Patent number: 6302114Abstract: The present invention provides a tobacco smoke filter or filter element having a longitudinally extending core (2) and a wrapper (4) engaged around the core (2), the wrapper (4) having particulate additive (6) adhered to one or more portion(s) of the radially inner face thereof with said wrapper (4) being free of additive around its circumference at one or both ends of the core.Type: GrantFiled: October 14, 1992Date of Patent: October 16, 2001Assignee: Cigarette Components LimitedInventors: Paul Francis Clarke, John Charlton
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Patent number: 6257242Abstract: A filter element for reducing or eliminating the harmful vapor phase components of air or smoke. The filter element includes a first section and a second section. The first section is positioned relative to and in fluid communication with the second section and contains an activated carbon fabric. The second section contains a mixture of catalytic activated carbon and coconut activated carbon.Type: GrantFiled: October 18, 1999Date of Patent: July 10, 2001Inventor: Ioannis C. Stavridis
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Patent number: 6164288Abstract: A tobacco smoke filter containing a porous substrate having dry water and microcapsules dispersed therein. The microcapsules contain at least one compound selected from the group consisting of chlorophyllin, methylcellulose, sodium pyroglutamate and a vegetable oil. The tobacco smoke filter can also contain one or more substances such as a porphyrin, and sodium pyroglutamate.Type: GrantFiled: September 17, 1999Date of Patent: December 26, 2000Assignee: Craig LesserInventors: Craig Lesser, Reid W. Von Borstel
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Patent number: 6119699Abstract: A smoking article capable of delivering a regulated smoke composition to a smoker, includes: a) a combustible filler wrapped in a combustible sheath; and b) at least one affinity chromatographic filter unit designed to preferentially remove specific targeted components from the smoke disposed within the sheath adjacent the combustible filler. The filter unit includes a mass of silica or resin particles having chemically bonded to their surfaces functional groups which exhibit preferential affinity for the targeted components and which reversibly bind the targeted components to elute components having a lower affinity than a previously bound component.Type: GrantFiled: December 19, 1997Date of Patent: September 19, 2000Inventor: Michael T. Sung
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Patent number: 6080457Abstract: A smoke filter consists of substrate threads and/or strips each pre-coated with particulate sorbent (e.g. activated carbon granules), gathered together in solid or tubular rod form e.g. within a containing sleeve. When the gathered threads and/or strips form a tubular body, this may be provided with a core.Type: GrantFiled: May 26, 1992Date of Patent: June 27, 2000Assignee: Cigarette Components LimitedInventors: John Charlton, Paul Francis Clarke, Ernest Brian Hayes
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Patent number: 6026819Abstract: Bicomponent fibers comprising a core of a thermoplastic material, preferably polypropylene, and a sheath of a blend of the core-forming polymer and an ethylene-vinyl acetate copolymer are used to produce tobacco smoke filter elements which may be incorporated into tobacco smoke filter products such as filtered cigarettes. The addition of significant quantities of the core-forming material to the ethylene-vinyl acetate used to form the sheath avoids problems experienced heretofore in build-up of polymer in the forming dies using conventional filter-forming equipment. Additionally, the blended sheath-forming polymer improves adhesion between the sheath and the core of the bicomponent fiber and, with the use of polypropylene, improves the hardness of the resultant tobacco smoke filter elements.Type: GrantFiled: February 18, 1998Date of Patent: February 22, 2000Assignee: Filtrona International LimitedInventor: Richard M. Berger