Abstract: A smokeless tobacco pastille configured for insertion into the mouth of a user is provided. The smokeless tobacco pastille can include (i) a tobacco material present in an amount of less than about 40 dry weight percent, based on the total dry weight of the pastille; (ii) at least one natural gum binder present in an amount of at least about 25 dry weight percent; and (iii) a plurality of sugar alcohols present in a total amount of at least about 40 dry weight percent, the predominant component of the plurality of sugar alcohols being isomalt or erythritol, wherein the shape of the smokeless tobacco pastille is moldable in the oral cavity.

Abstract: A fuel element adapted for use in a smoking article is provided, the fuel element including a combustible carbonaceous material in an amount of at least 25% by dry weight, based on the weight of the fuel element, and a particulate ignition aid dispersed throughout the fuel element and selected from ceramic particles, cellulose particles, fullerenes, impregnated activated carbon particles, inorganic salts, and combinations thereof, wherein the average particle size of the ignition aid is less than about 1,000 microns. Also provided are elongate smoking articles having a lighting end and an opposed mouth end, and including the above-noted fuel element configured for ignition of the lighting end.

Abstract: Disclosed are a process and an apparatus for improving tobacco raw material. The process mainly comprises performing an extraction from at least one of tobacco leafs, tobacco flakes, tobacco powder, stalks and cut stems by mixed solvents, conducting a solid-liquid separation for the tobacco raw material, applying the extract liquor of tobacco leaves, flakes and cuts for manufacturing tobacco extract and that of stalks and cut stems for manufacturing fertilizer, diluting and mixing a given amount of tobacco aqueous extract and ethanol extract and removing harmful components so as to get feed liquid, backfilling the feed liquid to the tobacco raw material, and drying the tobacco raw material to a certain dryness to obtain the products. The apparatus is a system composed of a plurality of interconnected independent devices such as extractor, solid-liquid separator, a feed liquid backfiller, etc.

Abstract: A method for producing triacetin from one or more plants of genus Nicotiana is provided. The triacetin can be derived inter alia from Nicotiana species biomass or from seed. In certain embodiments, the triacetin is produced by condensation of glycerin, generated by hydrolysis of acylglycerol-containing starting material derived from tobacco biomass or seed, and acetic acid, also derived from tobacco biomass or seed. The invention also provides articles and compositions including tobacco articles and tobacco compositions that include triacetin produced from one or more plants of genus Nicotiana.

Abstract: A smokeless tobacco product configured for insertion into the mouth of a user of the product is provided, the tobacco product including a water-permeable pouch containing a tobacco formulation, the tobacco formulation including a tobacco material and a plurality of microcapsules dispersed within the tobacco material, the plurality of microcapsules including an outer shell encapsulating an internal payload. The internal payload may include an additive such as water, flavorants, binders, colorants, pH adjusters, buffering agents, fillers, disintegration aids, humectants, antioxidants, oral care ingredients, preservatives, additives derived from herbal or botanical sources, and mixtures thereof. Microencapsulated flavorants include tobacco-containing flavorants, such as tobacco extracts or a particulate tobacco material, sweeteners (e.g., sweeteners containing neotame), and vanillin (optionally in a complexed form).

Abstract: Methods for producing dissolving grade pulp and microcrystalline cellulose from tobacco are provided. The methods include chemical pulping a tobacco input to form a tobacco pulp. Chemical pulping the tobacco input includes combining the tobacco input with a strong base defining a weight from about 5% to about 50% of the tobacco input, and heating the tobacco input and the strong base with an H-factor from about 500 to about 3,300. Further, the methods include bleaching the tobacco pulp to produce a dissolving grade pulp. Bleaching the tobacco pulp may include chlorination of the tobacco pulp with a chlorine dioxide solution, and caustic extraction of the tobacco pulp with a second strong base. A related tobacco-derived microcrystalline cellulose product is also provided, which can be used as a binder, a filler, and/or a texturizer in a tobacco product, such as a smokeless tobacco product.

Abstract: A method of preparing a whitened tobacco material is provided, the method including the steps of (i) extracting a tobacco material with an aqueous solution to give a tobacco pulp and a tobacco extract; (ii) treating the tobacco pulp with at least one of a caustic reagent and an oxidizing agent for a time and at a temperature sufficient to lighten the color of the tobacco pulp to give a whitened tobacco pulp; (iii) clarifying the tobacco extract to remove higher molecular weight components; and (iv) combining the whitened tobacco pulp with a clarified tobacco extract to form a whitened tobacco material. The whitened tobacco material can be isolated and incorporated into a smokeless tobacco product. The invention also provides a smokeless tobacco product incorporating a whitened tobacco material. The smokeless tobacco product may be a snus-type formulation contained within a sealed pouch.

Abstract: The invention provides a multi-layered smokeless tobacco product comprising two or more formulations with varying properties. In some embodiments, the smokeless tobacco products provide combinations of different organoleptic properties within the same product. In certain embodiment, these combinations allow for a modified release profile of active ingredients as the user enjoys the smokeless tobacco product. The invention further provides methods for making and using the smokeless tobacco product.

Abstract: A method for producing triethyl citrate from one or more plants of genus Nicotiana is provided. The triethyl citrate can be derived inter alia from Nicotiana species biomass or from seed. In certain embodiments, the triethyl citrate is produced by condensation of ethanol, generated by fermentation of starting material derived from tobacco biomass or seed, and citric acid, also derived from tobacco biomass or seed. The invention also provides articles and compositions including tobacco articles and tobacco compositions that include triethyl citrate produced from one or more plants of genus Nicotiana.

Abstract: A smokeless tobacco product configured for insertion into the mouth of a user is provided. The smokeless tobacco product includes a tobacco material and a specific starch material that imparts specific textural properties to the product. A process for preparing a smokeless tobacco product with a desired textural property is also provided.

Abstract: A cigarette includes lighting and mouth ends. It may include a smokable segment disposed at the lighting end. It also includes a mouth-end segment; an aerosol-generation system disposed between the lighting and mouth ends, which includes (i) a heat-generation segment adjacent the smokable segment, including a heat source configured to be activated by combustion of a smokable material and an insulation layer of a non-glass material that is woven, knit, or both, and (ii) an aerosol-generating segment with aerosol-forming material disposed between, but physically separate from, each of the heat generation segment and the mouth end; a piece of outer wrapping material that provides an overwrap around at least a portion of the aerosol-generating segment, the heat-generation segment, and at least a portion of the smokable segment; those segments being connected together by the overwrap to provide a cigarette rod; that is connected to the cigarette rod using tipping material.

Abstract: A method for producing triacetin from one or more plants of genus Nicotiana is provided. The triacetin can be derived inter alia from Nicotiana species biomass or from seed. In certain embodiments, the triacetin is produced by condensation of glycerin, generated by hydrolysis of acylglycerol-containing starting material derived from tobacco biomass or seed, and acetic acid, also derived from tobacco biomass or seed. The invention also provides articles and compositions including tobacco articles and tobacco compositions that include triacetin produced from one or more plants of genus Nicotiana.

Abstract: A process of extracting at least one target component from a plant material is provided. The process includes homogenizing a plant material in the presence of an extraction solvent to reduce the plant material to a plant liquid component and a plant pulp component. Each of the components may be further processed to extract specific components therefrom. Specifically, the plant liquid component can be processed to extract a plant-derived starch material, plant-derived proteins, plant-derived sugars, plant-derived sugars, and the like. The plant pulp material can be processed to extract pectin and cellulose. An associated system is also provided.

Abstract: A meltable smokeless tobacco composition configured for insertion into the mouth of a user is provided. The smokeless tobacco composition includes a tobacco material and a lipid having a melting point of about 36° C. to about 45° C. An associated process is also provided. The process includes melting a lipid having a melting point of about 36° C. to about 45° C. to form a molten lipid composition, mixing a tobacco material with the molten lipid composition to form a molten smokeless tobacco composition, and cooling the molten smokeless tobacco composition to form a solidified smokeless tobacco composition.

Abstract: Mixed metal oxide catalysts are prepared by combining first nanoscale particles and second nanoscale particles to form a mixture of nanoscale particles and then the mixture is heated to form a mixed metal oxide catalyst. The mixed metal oxide catalysts, which are capable of reducing the concentration of carbon monoxide in the mainstream smoke of a cigarette during smoking, are incorporated into a smoking article component such as tobacco cut filler, cigarette paper and/or cigarette filter material.

Abstract: A smokeless tobacco product includes a powdered or granular smokeless tobacco formulation that is contained within a moisture-permeable packet or pouch. The smokeless tobacco formulation may include finely ground particles of tobacco in powder-like form and other ingredients such as sweeteners, binders, colorants, pH adjusters, fillers, flavoring ingredients, disintegration aids, antioxidants and preservatives. The tobacco formulation may have a dry or moist form. The container has the form of a pouch or bag, such as is the type commonly used for the manufacture of snus products. The container preferably contains at least one capsule, such as a spherical breakable capsule. The container is intended to be placed in the mouth of the tobacco user, such that the tobacco formulation within the container may be enjoyed by the user. After the tobacco user is finished using the smokeless tobacco product, the container is removed from the user's mouth for disposal.

Abstract: A nontoxic, tobacco-less and flavored material for smoking, and a method of making the same. In one aspect, the invention is a tobacco-less material for smoking comprising: a shredded cellulosic paper having a weight; and a mixture of a humectant and a flavoring agent, the mixture having a weight and absorbed into the shredded cellulosic paper.

Abstract: A process for manufacturing reconstituted tobacco with reduced nitrogenous content by submitting cured tobacco material, including whole leaf, stems, scraps, fines and lamina, as well as burley leaf and stem, to an extraction with a solution containing sodium acetate, sodium hydroxide, potassium hydroxide or mixtures thereof. The extraction process, in addition to denitrifying the tobacco material, also produces reconstituted tobacco paper with characteristics similar to flue cured tobacco leaf.

Abstract: The invention relates to a smokable filler material which attempts to mimic tobacco leaf in its simplest components in order to provide a simpler smoke to the smoker. The smokable filler material comprises aerosol generating means, a substantially non-combustible inorganic filler, a binder and an extract from a flavorful fuel source material. It may also comprise a biopolymer.

Abstract: A smokeable filler material which includes casing material as a fuel material, along with an inorganic filler, a binder and an aerosol generating source. This material has good taste and flavour characteristics and contains relatively little tobacco material.

Abstract: A tobacco flavor-tasting article is manufactured by preparing a heat-irreversibly coagulated glucan sheet containing a tobacco extract. The glucan sheet is prepared by preparing a sheet-like material from a high viscosity aqueous dispersion containing the extract obtained by an extraction treatment of a leaf tobacco, together with a heat-irreversibly coagulating glucan, and heating the sheet-like material to coagulate the glucan. This sheet is cut or pulverized to prepare a tobacco flavor-generating material. On the other hand, a tobacco flavor-adjusting material is prepared by preparing a sheet-like material from a leaf tobacco fibrous residue, which is the residue after the extraction, and cutting the sheet-like material. These tobacco flavor-generating material and tobacco flavor-adjusting material are used in combination to produce a cigarette-like article.

Abstract: A process to improve the smoke quality and mechanical properties of reconstituted tobacco is accomplished by adding tobacco materials to an aqueous solution containing ammonium salts and urea. The resulting first tobacco slurry is then pressurized under steam pressure to at least 60 psi for a period of from 1 to 5 minutes then depressurized rapidly to ambient. The depressurized tobacco is then formed into a second tobacco slurry wherein the soluble components within the tobacco is removed. The resulting tobacco residue is then prepared into a reconstituted tobacco sheet and the extract is then concentrated to a solids level of at least 30 percent by weight of solids which is added back to the reconstituted tobacco sheet for further processing into smoking articles.

Abstract: A process for improving smoke quality and mechanical properties of a cast reconstituted tobacco sheet is accomplished by adding tobacco materials to an aqueous solution containing ammonium salts and ammonium hydroxide. The resulting first tobacco slurry is then pressurized under steam pressure to at least 60 psi for a period of from about 1 to 5 minutes then depressurized rapidly to ambient. The depressurized tobacco is then formed into a second tobacco slurry. The resulting tobacco residue is then cast into a reconstituted tobacco sheet for further processing into smoking articles.

Abstract: The process of the present invention involves extracting components from a tobacco material or other plant material using a solvent having an aqueous character to provide separately an aqueous tobacco extract and a water insoluble tobacco portion. The insoluble tobacco portion is refined and a slurry is produced. The slurry is formed into a predetermined shape, e.g., a formed web. The formed web can be pressed to reduce the moisture content. The tobacco material preferably has a moisture content of at least about 50 percent by weight. The material is contacted with an aqueous mixture of an aerosol precursor material. The ratio of liquid having an aqueous character to aerosol precursor material is typically from about 25 to 75 percent by weight. Immediately after the introduction of the aerosol precursor material, the web is dried at a preselected temperature so that the aerosol precursor material is dispersed evenly throughout the web.

Abstract: A smoking inhibitor ring for placement on a cigarette to limit the length of available cigarette to smoke has concentric aluminum cylindrical, uniformly spaced apart inner and outer walls joined at each end by closures, the insulation space between the inner and outer walls being unfilled and the inner wall having an inner diameter substantially the same as a cigarette. A method of using the inhibitor ring includes placing one and then increasing numbers of the rings on a cigarette to gradually decrease the length of cigarette available to smoke.

Abstract: A tobacco composition includes a tobacco extract and an edible carrier. The composition allows tobacco to be enjoyed orally.

Abstract: A composition is provided for use in the suppression of a smoking habit, containing a tobacco plant extract which includes between 0.1% and 8.0% of nicotine and at least one additional tobacco derivative in a water based solvent.

Abstract: Smokable and/or combustible tobacco material is provided by altering the character of tobacco material.Tobacco material is extracted using a solvent to provide a tobacco extract within the solvent and an extracted tobacco material. The extracted tobacco material is separated from at least a portion of the extract and solvent. The extracted tobacco material is subjected to pyrolysis conditions to provide a pyrolyzed material. The pyrolysis conditions can include a temperature of from about 300.degree. C. to about 1250.degree. C. and a non-oxidizing atmosphere.The pyrolyzed material can then be formed into a predetermined shape such as by extrusion, casting and the like.

Abstract: Reconstituted tobacco has phosphate salts incorporated therein. Tobacco is extracted with water to yield an insoluble portion and an aqueous portion containing water soluble tobacco components. The aqueous portion is contacted with diammonium hydrogen orthophosphate and adjusted to a pH of about 6.5. The extract then is applied to the insoluble portion which has been formed into a sheet-like shape. The resulting tobacco composition is dried to yield a reconstituted tobacco material.

Abstract: Denicotinized tobacco cut filler is provided by (i) providing an aqueous denicotinized tobacco extract, (ii) providing tobacco cut filler which has been extracted with an aqueous liquid, (iii) contacting the aqueous extract with the extracted cut filler, (iv) deliquoring the mixture of aqueous extract and extracted cut filler such that a certain level of the tobacco extract remains in contact with the extracted cut filler, and (v) drying the deliquored cut filler to provide a processed cut filler. Greater than 90 percent of the nicotine present in tobacco cut filler can be removed therefrom using such process steps.

Abstract: Denicotinized tobacco cut filler is provided by (i) extracting the cut filler with an aqueous denicotinized extract and thereby providing a mixture of aqueous extract and extracted cut filler, (ii) deliquoring the mixture of aqueous extract and extracted cut filler such that a certain level of tobacco extract remains in contact with the extracted cut filler, and (iii) drying the deliquored tobacco extract/extracted cut filler to provide a processed cut filler. Greater than 90 percent of the nicotine present in tobacco cut filler can be removed therefrom using such process steps.

Abstract: A process is provided for the selective removal of basic materials from plant products, in particular, for removing nicotine from tobacco without materially affecting the content of the other components of the tobacco. Tobacco is traversed with a solvent at high pressure and in a physical state which is either a liquid at a pressure of from about 500-300 atmospheres or a supercritical fluid wherein nicotine and the other components dissolve in the solvent. As the single means of removing substances from the solvent, the solvent is then passed through an acid-containing trap where the solvent is essentially freed of nicotine. The solvent, depleted of nicotine and enriched in the other components, is then recycled to the tobacco to reextract nicotine.

Abstract: Concentrated tobacco extracts are provided by first extracting water soluble components from tobacco. The aqueous extract then is spray dried to a dry powder form. As such, the extract is in a low solvent form (i.e., the solvent content including moisture content of the extract is less than about 12 weight percent). The spray dried extract is contacted with a lower alcohol such as methanol or ethanol, and certain components are extracted from the spray dried extract. The resulting extracted components are isolated from the alcohol solvent in order to yield a tobacco essence. The essence has a homogeneous, viscous character and exhibits a tobacco aroma. The essence is useful as a flavoring agent for cigarettes and other smoking articles.

Abstract: An apparatus and method for manufacturing tobacco sheet material comprising the steps of acoustic mixing with ultrasonic vibration a slurry containing tobacco components and forming sheets of tobacco material by casting the slurry after acoustic mixing. Additionally, the slurry is mixed with subsonic vibration and low shear mixing before the slurry is acoustic mixed. The slurry may include sized tobacco stems, sized tobacco dust and extract solution.

Abstract: A process for manufacturing reconstituted tobacco from tobacco stems and tobacco fines includes treating the tobacco stems to a fibrous form, and mixing the fibrous tobacco stems with tobacco lamina fines. The mixture is then deposited on a moving mesh screen whereon it is formed into a felt-like mat or sheet of generally uniform thickness. The reconstituted tobacco sheet is then removed from the mesh screen for further processing to produce a tobacco smoking article.

Abstract: Process for the start-up of high-temperature processes for the denitrification of tobacco materials via an anaerobic dissimilatory metabolic pathway of thermophilic organisms. The process advantageously permits the induction of denitrification activity through the use of a seed culture which, itself, is the product of a previous thermophilic denitrification treatment of the same type as that to which the start-up process is directed.

Abstract: An improved method of reducing the nitrate, nitrite and ammonium compound content of an aqueous tobacco extract employing microorganisms is described. The nitrates, nitrites and ammonium compounds are eliminated on a continuous basis via an aerobic assimilatory metabolic pathway by introducing aqueous tobacco extract and necessary additives into a work mixture, containing suitable microorganisms, at a dilution rate which does not exceed the growth rate of the microorganisms while withdrawing a portion of the work mixture at a rate such that the volume of the work mixture remains constant. Optionally the biomass may be removed from the withdrawn mixture.

Abstract: A process for reducing the content of nitrate and/or nitrite salts contained in tobacco is disclosed whereby tobacco is treated, under controlled aerobic conditions, with microorganisms capable of degrading nitrates and/or nitrites to other nitrogen-containing compounds, such as proteins and amino acids.

Abstract: An improved process for the reduction of the nitrate content of tobacco materials via dissimilatory denitrification is disclosed wherein more rapid reduction of nitrate to nitrogen gas is effected by utilizing a vacuum during incubation. The process comprises inoculating nitrate-containing tobacco material with a microorganism capable of dissimilatory denitrification and thereafter incubating the tobacco material under conditions whereby the nitrate is reduced to nitrogen gas via dissimilatory denitrification while applying a vacuum.

Abstract: A process for the reduction of the nitrate and nicotine contents of tobacco by microbial treatment is disclosed wherein tobacco materials are subjected, under controlled conditions, to the action of a microorganism effective to degrade nitrates and alkaloids (nicotine) through a biochemical reaction. The microorganism is combined or grown in the presence of a nitrate containing compound in relatively small quantities. Tobacco treated in accordance with this process has a reduced nitrate and nicotine content, and when incorporated into a tobacco smoking product thereby produces a mild smoke, having reduced nitrogen oxides, hydrogen cyanide and nicotine content. However, there is no loss of desirable flavor, taste and smoking properties.

Abstract: A process for the reduction of the nitrate content of tobacco materials by microbial treatment is disclosed wherein tobacco materials are subjected, under controlled conditions, to the action of a microorganism effective to degrade nitrates through a biochemical reaction. Tobacco materials treated in accordance with this process, when incorporated into a tobacco smoking product, produce a mild smoke having reduced nitrogen oxides and hydrogen cyanide deliveries without loss of desirable flavor, taste or other smoking properties.

Abstract: A method is provided for treating uncured green tobacco whereby the chemical composition of the tobacco can be altered. The method involves expressing protoplasmic juice from green uncured tobacco by means of pressure and thereafter artificially curing the tobacco. The expressed juice may be collected and processed to alter its chemical composition. The processed juice may thereupon be reapplied to tobacco from which juice has been expressed to produce a tobacco product having desired chemical characteristics.