With Organic Treating Agent (e.g., Solvent, Surfactant, Or Reactant Yielding Soluble Product, Etc.) Patents (Class 134/22.14)
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Patent number: 11021418Abstract: The present invention relates to a method for olefin oligomerization, and can provide a method for olefin oligomerization. The method includes the steps of: introducing an oligomerization transition metal catalyst, olefin monomers, and a solvent into a reactor and performing an olefin oligomerization reaction to produce an oligomer; introducing a catalyst deactivator to a reaction product of the oligomerization reaction to deactivate the catalyst, with the catalyst deactivator including at least one functional group containing at least one selected from the group including oxygen, phosphor, nitrogen, and sulfur and having a number average molecular weight of 400 or more; separating the oligomer through distillation in a distiller; and separating the catalyst deactivator through the bottom end of the distiller.Type: GrantFiled: July 18, 2018Date of Patent: June 1, 2021Assignees: SK Innovation Co., Ltd., SK Global Chemical Co., Ltd.Inventors: Sungreal Son, Hyoseung Park, Inhyoup Song, So Hee Sim, Chansaem Park, Woosung Jung
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Patent number: 10711115Abstract: A process for extruding polypropylene comprising extruding a composition comprising a polypropylene and a second acid scavenger and less than about 10 ppm of a nucleating agent.Type: GrantFiled: May 24, 2018Date of Patent: July 14, 2020Assignee: Milliken & CompanyInventors: Kemper D. Lake, Jr., Christopher T. Kochanowicz, Joseph J. Peterson, Clifford S. Bynum, Keith A. Keller
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Patent number: 10383343Abstract: An installation and method for producing and/or processing confectionery masses which are made from at least one liquid raw material and granular and/or powdery raw materials. The installation includes at least a first mixing container and at least one further product-processing device. The first mixing container has at least one raw-material inlet and a product outlet and a mixing device for mixing the raw materials at least largely homogeneously. At least the mixing container includes at least one spraying device in an upper container region, which at least one spraying device serves to feed the at least one liquid raw material, wherein at least one outlet cone of the spraying device is directed, at least in some regions, toward an inner wall surface of the first mixing container.Type: GrantFiled: August 18, 2016Date of Patent: August 20, 2019Assignee: NETZSCH-Feinmahltechnik GmbHInventors: Theron Harbs, Holger Moeschl, Lars-Peter Weiland, Sergio Devegili
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Patent number: 10302236Abstract: The present invention provides methods and methods for curing a leakage in a pipeline, the method including at least one gel pig and at least one sealant composition; wherein the at least one gel pig and the at least one sealant composition form a pig train, adapted to move along the pipeline to a region of the leakage and to seal the leakage.Type: GrantFiled: December 18, 2015Date of Patent: May 28, 2019Assignee: Curapipe System Ltd.Inventors: Samuel Perstnev, Boris Natapov, Alexander Perstnev, Reonald Ukhanov, Peter Paz
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Patent number: 10209038Abstract: A curtain of a flexible fabric is provided that is deployable to create a physical and visual barrier between an employee and a person perpetuating a crime such as a robbery or assault. The barrier can be in the form of a curtain that is electrified with an extreme high voltage, similar to a stun gun, and which prevents the assailant from approaching an employee or a restricted area. The curtain can be mounted in any area where it is beneficial to limit site and access of a trespasser or an assailant, such as between a cashier at a convenience store and the store's open retail area. The curtain can also be used to create temporary safe rooms or deployed within hallways of a restricted area to limit movement of an intruder.Type: GrantFiled: July 28, 2016Date of Patent: February 19, 2019Inventor: Christopher D. Wallace
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Patent number: 10202514Abstract: The present invention relates to graffiti removal compositions and the use thereof for the removal of graffiti from surfaces. The compositions comprise (i) alkyl esters of one or more soybean oil fatty acids; (ii) one or more aliphatic diesters of dicarboxylic acids; (iii) one or more compounds of the formula R2C(0)OR3, wherein R2 is a C1-C20 alkyl and R3 is C1-C20 alkyl; and (iv) a surfactant.Type: GrantFiled: June 18, 2015Date of Patent: February 12, 2019Assignee: GUARD IT SOLUTIONS PTY LTDInventors: Anthony Leenan, Peter Richardt
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Patent number: 9791108Abstract: A method of hydraulic fracturing is provided which uses metal silicides to generate significant pressure inside a wellbore. The method comprises injecting a fracturing fluid and an aqueous or reacting fluid into the wellbore to react with the fracturing fluid. The fracturing fluid comprises metal silicide, which may be uncoated or coated, and hydrocarbon fluid. The reacting fluid comprises water or a solvent. A method of removing buildup in pipelines such as subsea pipelines which uses metal silicides to generate heat and pressure inside the pipeline is also provided. The method comprises injecting an organic slug and an aqueous slug. The organic slug comprises metal silicide and hydrocarbon fluid. The aqueous slug comprises water. Alternatively, there is also provided a method for purifying flowback water produced from a hydraulic fracturing process comprising adding metal silicide to the flowback water produced from a hydraulic fracturing process.Type: GrantFiled: May 4, 2017Date of Patent: October 17, 2017Assignee: SIGNA CHEMISTRY, INC.Inventors: Paul H. Krumrine, III, James S. Falcone, Jr., Michael Lefenfeld
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Patent number: 9758877Abstract: Methods and compositions are disclosed for inhibiting corrosion on metal surfaces of gas turbine air compressors. The methods comprise contacting the metal surfaces with a corrosion inhibiting composition comprising at least one filming amine.Type: GrantFiled: February 28, 2014Date of Patent: September 12, 2017Assignee: General Electric CompanyInventors: Sal Esposito, Anthony M. Rossi, Mel Joseph Esmacher, Rebecca Evelyn Hefner, Trevor James Dale, Kelsey Elizabeth Beach
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Patent number: 9017488Abstract: A process for quickly removing hydrocarbon contaminants and noxious gases in a safe and effective manner from catalytic reactors, other media packed process vessels and associated equipment in the vapor phase without using steam. The cleaning agent contains one or more solvents, such as terpenes or other organic solvents. The cleaning agent is injected into contaminated equipment, along with a carrier gas, in the form of a cleaning vapor.Type: GrantFiled: July 16, 2014Date of Patent: April 28, 2015Assignee: Refined Technologies, Inc.Inventors: Cody Nath, Barry Baker, Sean Sears
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Patent number: 8999072Abstract: Disclosed are methods and apparatus for cleaning heat exchangers and similar vessels by introducing chemical cleaning solutions and/or solvents while maintaining a target temperature range by direct steam injection into the cleaning solution. The steam may be injected directly into the heat exchanger or into a temporary side stream loop for recirculating the cleaning solution or admixed with fluids being injected to the heat exchanger. The disclosed methods are suitable for removing metallic oxides from a heat exchanger under chemically reducing conditions or metallic species such as copper under chemically oxidizing conditions. In order to further enhance the heat transfer efficiency of heating cleaning solvents by direct steam injection, mixing on the secondary side of the heat exchanger can be enhanced by gas sparging or by transferring liquid between heat exchangers when more than one heat exchanger is being cleaned at the same time.Type: GrantFiled: December 3, 2009Date of Patent: April 7, 2015Assignee: Westinghouse Electric Company LLCInventors: Robert D. Varrin, Jr., Michael J. Little
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Publication number: 20150083165Abstract: Methods for on-line cleaning hot parts of a gas turbine during its operation are provided. A cleaning agent composition is injected into a hot gas path of the gas turbine, and includes a liquid carrier and a descaling material suspending in the liquid carrier. The descaling material includes at least one oxide, in an anhydrous or a hydrated form, that is derived from calcium, magnesium, titanium, iron, aluminium, silicon in the form of silicates having non-fibrous structures, or phosphorus in the form of alkaline-earth phosphates. Cleaning agents are also provided for use in a gas turbine.Type: ApplicationFiled: March 25, 2014Publication date: March 26, 2015Applicant: General Electric CompanyInventor: Michel Moliere
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Patent number: 8986461Abstract: A cleaning composition and process to remove carbon deposits from combustion equipment components is provided. The de-carbonizing composition is packaged in certain embodiments in an aerosol propellant. The inventive composition is also readily used as a liquid or an atomized mist that is readily introduced into the intake manifold through a tube tolerant of engine inlet operational temperatures and conditions. The invention introduces the composition by a process that precludes the need for engine disassembly.Type: GrantFiled: March 17, 2014Date of Patent: March 24, 2015Assignee: Illinois Tool Works, Inc.Inventors: Mark E. Hischier, Gregory Hewgill
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Patent number: 8957005Abstract: A silicon wafer cleaning agent includes at least a water-based cleaning liquid, and a water-repellent cleaning liquid for providing water-repellent to an uneven pattern at least at recessed portions during a cleaning process. The water-repellent cleaning liquid is a liquid composed of a water-repellent compound containing a reactive moiety which is chemically bondable to Si in the silicon wafer, and a hydrophobic group, or is a liquid wherein 0.1 mass % or more of the water-repellent compound relative to the total quantity of 100 mass % of the water-repellent cleaning liquid and an organic solvent are mixed and contained therein. A cleaning process wherein a pattern collapse is easily induced can be improved by using the cleaning agent.Type: GrantFiled: September 15, 2010Date of Patent: February 17, 2015Assignee: Central Glass Company, LimitedInventors: Soichi Kumon, Masanori Saito, Takashi Saio, Hidehisa Nanai, Yoshinori Akamatsu
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Patent number: 8951467Abstract: An embodiment prevents equipment fouling (deposition of unwanted material) in an oil recovery system via implementing passivation of metallic components. By preventing or at least slowing or inhibiting corrosion of equipment or components via passivation, such as passivating heat exchangers, metallic piping, and the like, an embodiment in turn reduces fouling thereof. Other embodiments are described and claimed.Type: GrantFiled: March 15, 2013Date of Patent: February 10, 2015Assignee: Chemtreat, Inc.Inventors: Robert Wright Bedinger, III, Benjamin Edward Niemaseck, Mark Jason Puchovich, John Richardson
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Patent number: 8945314Abstract: A solid composition includes a polysaccharide hybrid polymer composition and a hydratable salt. In one embodiment, the polysaccharide hybrid polymer composition includes a polysaccharide residue present in an amount from approximately 5% to 90% by weight of the polysaccharide hybrid polymer composition and a residue of at least one ethylenically unsaturated monomer present in an amount from approximately 10% to 75% by weight of the polysaccharide hybrid polymer composition.Type: GrantFiled: July 30, 2012Date of Patent: February 3, 2015Assignee: Ecolab USA Inc.Inventors: Kerrie E. Walters, Carter Silvernail
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Patent number: 8940679Abstract: The present invention relates to compositions for deodorizing and cleaning, in particular solid compositions in the form of effervescent tablets which can be reconstituted in water to obtain solutions for cleaning and deodorizing. The compositions comprise one or more Bacillus subtilis strain(s), one or more surfactant(s), one or more fragrance(s), one or more descaling agent(s), and one or more effervescent agent(s). The invention further relates to a kit comprising such tablets, as well as methods for obtaining cleaning and deodorizing tablets and solutions and their use for cleaning and deodorizing.Type: GrantFiled: January 25, 2013Date of Patent: January 27, 2015Assignee: Pollets S.A.Inventor: Abdelhamid Jabrane
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Publication number: 20140352731Abstract: A cleaning composition suitable for removing soil from a variety of surfaces and a method of using the same are provided. Cleaning compositions according to embodiments of the present invention include at least one carbonate ester, including, for example, ethylene carbonate, propylene carbonate, trimethylene carbonate, and combinations thereof. Depending on the specific application, the compositions may also include at least one surfactant and/or at least one thickener. Cleaning compositions as described herein may be particularly useful for removing soil from surfaces of pipes, vessels, and other equipment associated with the production and/or processing of oil and/or natural gas, such as, for example, equipment associated with a hydraulic fracturing process.Type: ApplicationFiled: May 31, 2013Publication date: December 4, 2014Inventors: Tony Atabong, Curtis Shaw
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Publication number: 20140311529Abstract: The present invention relates to [1] a detergent composition for endoscope washers, including a nonionic surfactant (A) represented by the following formula (1), a branched-chain fatty acid having not less than 6 and not more than 10 carbon atoms or a salt thereof (B), a defoaming agent (C) and water, R—O—[(EO)m/(PO)n]—H??(1) wherein R represents a branched-chain alkyl group having not less than 7 and not more than 9 carbon atoms; EO represents an ethanediyloxy group; PO represents a propanediyloxy group; m and n each represent an average molar number of addition of the ethanediyloxy or propanediyloxy group in which m is a number of not less than 1 and not more than 30, and n is a number of not less than 2 and not more than 50; and the mark “/” represents that EO and PO may be added either in a random form or in a block form, and an order of addition of EO and PO is optional; and [2] a method of washing an endoscope using an endoscope washer, including the step of washing the endoscope with a mixture incluType: ApplicationFiled: May 28, 2013Publication date: October 23, 2014Inventors: Masaya Nishio, Tatsuya Sakai
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Patent number: 8853144Abstract: A composition includes a polysaccharide graft polymer composition. In one embodiment, the polysaccharide graft polymer composition includes a polysaccharide residue present in an amount from about 5% to about 90% by weight of the polysaccharide graft polymer composition and a residue of at least one ethylenically unsaturated monomer present in an amount from about 10% to about 75% by weight of the polysaccharide graft polymer composition.Type: GrantFiled: July 30, 2012Date of Patent: October 7, 2014Assignee: Ecolab USA Inc.Inventors: Carter Silvernail, Erik C. Olson, Klin Rodrigues
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Patent number: 8841246Abstract: A composition includes a polysaccharide hybrid polymer composition. In one embodiment, the polysaccharide hybrid polymer composition includes a polysaccharide residue present in an amount from about 5% to about 90% by weight of the polysaccharide hybrid polymer composition and a residue of at least one ethylenically unsaturated monomer present in an amount from about 10% to about 75% by weight of the polysaccharide hybrid polymer composition.Type: GrantFiled: July 30, 2012Date of Patent: September 23, 2014Assignee: Ecolab USA Inc.Inventors: Carter Silvernail, Erik C. Olson, Klin Rodrigues
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Patent number: 8821646Abstract: An irrigation system cleaning formulation contains a sufficient concentration of a water-soluble organic acid which has a pK(1)a of less than about 4.0. A cleansing irrigation water contains a sufficient amount of such cleaning formulation, and a method of cleaning an irrigation system uses such cleaning formulation.Type: GrantFiled: November 18, 2008Date of Patent: September 2, 2014Inventors: John C. Miller, Deborah L. Miller
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Publication number: 20140238444Abstract: The present invention provides a cleaning method by which the performance of a microchip can be recovered and a cleaning liquid. A method for cleaning a microfluidic device comprising: cleaning a channel that is formed in the microfluidic device, has a surface having a polymer coating, and has been brought into contact with a sample containing nucleic acid and/or protein, by bringing the channel into contact with a cleaning liquid comprised only of an organic solvent having solubility in at least the same volume of water at 25° C., or a cleaning liquid containing 50 vol % or more of the organic solvent in a buffer solution. The method wherein the buffer solution has a pH of 8 to 10. The method wherein the buffer solution further contains 3 to 8M of a protein denaturant. The method wherein the buffer solution has a pH of 2 to 4.Type: ApplicationFiled: February 27, 2013Publication date: August 28, 2014Applicant: SHIMADZU CORPORATIONInventor: Akihiro Arai
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Publication number: 20140238437Abstract: The present invention comprises a method and system for the in-situ cleaning of a heat exchanger tube bundle of carbonaceous deposits. Using the method and system, an organic solvent is brought into fluid communication with one or more heat exchanger tube bundles in a closed system. The closed system is formed at the site of operation of the heat exchanger tube bundles and without having to remove the heat exchanger tube bundles from their shells or other associated equipment. Once the closed system is formed, the organic solvent is brought to a temperature at which it is effective to remove carbonaceous deposits from the heat exchanger tube bundle and flowed through the equipment associated with the heat exchanger tube bundles so as to contact the heat exchanger tube bundles and remove carbonaceous deposits that have formed therein.Type: ApplicationFiled: February 26, 2014Publication date: August 28, 2014Applicant: T5 TECHNOLOGIES, INC.Inventors: Michael Tomkins, Robert Larsen
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Patent number: 8765021Abstract: The present invention relates to an aqueous treatment composition for inhibiting corrosion and acid attack on metallic surfaces that comprises a thiourea organic derivative, a polyalkoxylated terpene nonionic surfactant and an acid. The invention also relates to a process for cleaning industrial metallic equipment, in particular heat exchangers in which a heat transfer fluid, generally based on air or on water, flows, with a view to cleaning them and removing scale and other soiling.Type: GrantFiled: March 26, 2009Date of Patent: July 1, 2014Assignee: Rhodia OperationsInventor: Jean-Emile Zanetto
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Patent number: 8734589Abstract: A heat exchanger may be cleaned by introducing compressed nitrogen and a flushing composition through an injection device.Type: GrantFiled: August 23, 2012Date of Patent: May 27, 2014Assignee: The Rectorseal CorporationInventors: Eva Ackerman, Yanwei Cen, William Francis Flynn, Richard Garza
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Patent number: 8691731Abstract: Generating heat within a combination solvent/acid system removes undesirable deposits from petroleum reservoir formations (especially the near well-bore region), oilfield equipment, and petroleum processing equipment. An exothermic reaction occurs between the solvent and the acid and the heat evolved helps remove organic solid deposits. The acids may include organic acid compounds, such as sulfonic acids, sulfuric acid and nitric acid. The solvents may include terpene- and terpene-derivative-containing solvents, including, but not necessarily limited to, limonene, pinene, dipentene, myrcene, turpentines and compounds having at least one double bond, such as methyl furan, dienes, styrene, vinyl acetate and the like. The exothermic reaction produces a great amount of heat, and together with using certain acids and solvents already known as effective to remove paraffin and asphaltene deposition, removing such deposits is improved.Type: GrantFiled: November 5, 2010Date of Patent: April 8, 2014Assignee: Baker Hughes IncorporatedInventors: David W. Jennings, Samuel Asomaning, Michael E. Newberry
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Patent number: 8685173Abstract: The present invention is generally directed toward methods of cleaning and descaling surfaces contaminated with food soils, especially clean-in-place systems. More particularly, the methods according to the present invention also provide for sanitizing of surfaces contaminated with food soils. Thus, there is provided a single cleaning cycle that may clean, sanitize, and descale food-soiled surfaces, and in certain embodiments, without the need for a pre-rinse step, using an acidic detergent composition comprising a fatty alkyl-1,3-diaminopropane or salt thereof in the presence of an acid selected from the group consisting of inorganic acids, organic acids, and mixtures thereof.Type: GrantFiled: July 16, 2009Date of Patent: April 1, 2014Assignee: DeLaval Holding ABInventors: Fahim U. Ahmed, Bruno Van Den Bossche
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Patent number: 8679366Abstract: A composition includes a polysaccharide graft polymer composition and 2-phosphonobutane-1,2,4-tricarboxylic acid. In one embodiment, the polysaccharide graft polymer composition includes a polysaccharide residue present in an amount from approximately 5% to approximately 90% by weight of the polysaccharide graft polymer composition and a residue of acrylic acid, methacrylic acid or a combination thereof present in an amount from approximately 10% to approximately 75% by weight of the polysaccharide graft polymer composition.Type: GrantFiled: July 30, 2012Date of Patent: March 25, 2014Assignee: Ecolab USA Inc.Inventors: Carter Silvernail, Erik C. Olson
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Patent number: 8673088Abstract: A device for combining multiple components into a foam mixture and dispensing the foam mixture into a pipe is described. The multiple components are combined immediately prior to dispensing, which maximizes activity for labile, biologically active components whose degradation accelerates upon combining components. Embodiments of the device are relatively light weight and adapted to removably couple to sewer cleaning vehicles.Type: GrantFiled: September 17, 2010Date of Patent: March 18, 2014Inventor: Thomas P. Suiter, II
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Patent number: 8673089Abstract: Methods of using an aldimine of formula (I) as cleaning agent or ingredient of a cleaning agent composition for reactive polyurethane compositions, especially for reactive polyurethane hot melt adhesives. It has been found that such cleaning agents can greatly reduce the quantity of wastes and in particular mixtures of blocked and nonblocked reactive polyurethane compositions can be used without problem for gluing, without the gluing being negatively influenced in its properties, especially its thermal stability.Type: GrantFiled: November 26, 2010Date of Patent: March 18, 2014Assignee: Sika Technology AGInventors: Doreen Janke, Kai Paschkowski
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Patent number: 8668779Abstract: A method of simultaneously cleaning and disinfecting an industrial water system is described and claimed. The method involves the addition to the water of the industrial water system of a Compound selected from the group consisting of the alkali salts of chlorite and chlorate and mixtures thereof; and an acid, followed by allowing the water in the industrial water system to circulate for several hours. The reaction of the alkali salts of chlorite and chlorate and acid produces chlorine dioxide in-situ in the water of the industrial water system. The chlorine dioxide kills microorganisms and the acid acts to remove deposits upon the water-contact surfaces of the equipment. This cleaning and disinfecting method works in a variety of industrial water systems including cooling water systems.Type: GrantFiled: April 30, 2002Date of Patent: March 11, 2014Assignee: Nalco CompanyInventors: Andrew J. Cooper, Jasbir S. Gill, Amit Gupta, Robert F. Kelly, Douglas G. Kelley, Eric R. Myers
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Patent number: 8647443Abstract: A method of cleaning an automatic biochemical analyzer, wherein the cleaning solution includes: at least one anionic surfactant, at least one nonionic surfactant, an alkali metal hydroxide, an alkali metal citrate, and a buffering agent stabilizing the pH value above 13.0. In some embodiments, the cleaning solution provides low residual rate of proteins, low residual rate of lipids, desirable within-batch repeatability in clinical testing, low level of cross-contamination, and low level of reactant deposit after cleaning, without affecting test results of the biochemical analyzer. In some embodiments, the cleaning solution has no corrosive effects on the liquid path and reaction cup of the analyzer. The ingredients of the cleaning solution may also be biodegradable.Type: GrantFiled: May 20, 2011Date of Patent: February 11, 2014Assignee: Shenzhen Mindray Bio-Medical Electronics Co., Ltd.Inventors: Yuping Zhang, Mulong Liu, Wenjuan Xu, Jun Cheng
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Patent number: 8636918Abstract: A composition includes an anionic polysaccharide hybrid polymer composition and 2-phosphonobutane-1,2,4-tricarboxylic acid. In one embodiment, the polysaccharide hybrid polymer composition includes a polysaccharide residue present in an amount from approximately 5% to approximately 90% by weight of the polysaccharide hybrid polymer composition and a residue of at least one ethylenically unsaturated monomer present in an amount from approximately 10% to approximately 75% by weight of the polysaccharide hybrid polymer composition.Type: GrantFiled: July 30, 2012Date of Patent: January 28, 2014Assignee: Ecolab USA Inc.Inventors: Carter Silvernail, Erik C. Olson
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Patent number: 8632638Abstract: Disclosed is a method for cleaning deposits from one or more parts of an engine fuel delivery system, the method comprising introducing into the engine fuel delivery system a cleaning composition comprising (a) one or more aromatic hydrocarbon solvents; and (b) one or more propylene glycol ethers.Type: GrantFiled: November 15, 2011Date of Patent: January 21, 2014Assignee: Chevron Oronite Company LLCInventors: Felicia Simpson-Green, Damon Vaudrin
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Patent number: 8628625Abstract: A method that uses an L-?-dipalmitoleoyl-phosphatidylcholine (DPPC) surfactant based device that reacts with a substance in a known manner, to detect a substance of interest or to extract a substance of interest from a material is provided. The principles of the present invention are particularly useful in detecting/measuring a substance that is harmful to a human, and also to extracting NACL from saltwater.Type: GrantFiled: October 1, 2007Date of Patent: January 14, 2014Inventor: Mark L. Witten
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Publication number: 20130333729Abstract: Disclosed is a dry cleaning method for removing a composition represented by a compositional formula of MgaZnbOHc (0?a?1, 0?b?1, 0?c?1, and 0.5?a+b?1), which accumulates in a film formation chamber or in an exhaust pipe of an apparatus for forming a composition represented by a compositional formula of MgXZn1?XO (0?x?1) into a film, by using a cleaning gas. This method is characterized by that a cleaning gas containing ?-diketone is used and that the composition is removed by reacting the composition accumulated with the cleaning gas at a temperature of from 100° C. to 400° C. It is possible by this method to remove the composition without opening the apparatus.Type: ApplicationFiled: January 19, 2012Publication date: December 19, 2013Applicant: Central Glass Company, LimitedInventors: Tomonori Umezaki, Yuta Takeda
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Patent number: 8608863Abstract: A method for cleaning a component comprises a first stage including the steps of: (i) loading a component into the cleaning chamber of a flush station, (ii) directing a deionized water stream through first filter means, (iii) introducing carbon dioxide into the filtered water stream, (iv) directing the carbonated water stream into a fluid passage to be cleaned in the component, and (v) collecting the dirty water stream after it passes through the component and directing the collected dirty water stream through second filter means for reuse. The method can further include a second stage including the steps of: (vi) loading the component into a testing chamber of a testing station, (vii) directing a deionized water stream through third filter means, (viii) directing the filtered water stream into the fluid passage in the component, and (ix) collecting the water stream after it passes through the component and directing the collected water stream into a particle counter.Type: GrantFiled: December 8, 2010Date of Patent: December 17, 2013Assignee: Parker-Hannifin CorporationInventor: Jerome Francis Stremel, III
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Patent number: 8562751Abstract: A dry cleaning method of a substrate processing apparatus includes forming a metal oxide by oxidizing a metal film adhered to the inside of a processing chamber of the substrate processing apparatus; forming a complex by reacting the metal oxide with ?-diketone; and sublimating the complex to be removed. A cleaning gas containing oxygen and ?-diketone is supplied into the processing chamber while heating the inside of the processing chamber. A flow rate ratio of oxygen to ?-diketone in the cleaning gas is set such that a formation rate of the metal oxide is lower than a formation rate of the complex.Type: GrantFiled: January 17, 2012Date of Patent: October 22, 2013Assignees: Tokyo Electron Limited, Central Glass Company, LimitedInventors: Isao Gunji, Yusaku Izawa, Hitoshi Itoh, Tomonori Umezaki, Yuta Takeda, Isamu Mori
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Publication number: 20130239991Abstract: A composition for treating a water system to remove scale, microorganisms and biofilm, and corrosion by-products. The composition comprises chelating agents and a surfactant. Depending on the water system being treated, the composition may be a solid dissolved by water in the system being treated or may be a pre-mixed foam or aerosol. A treatment system particularly suitable for flowing water systems comprises a container for holding such a treatment composition and mixing it with a portion of water from the water system, a filter for removing solids dislodged during treatment, and a corrosion monitor. A method for using such a treatment composition comprises draining substantially all existing water in the water system, filling or rinsing the system with fresh water, contacting the treatment composition with substantially all parts of the water system, and draining the treatment composition from the system before resuming normal operations.Type: ApplicationFiled: January 18, 2013Publication date: September 19, 2013Applicant: NCH CorporationInventors: Adrian Denvir, David F. Vela, Christina B. Burton, Katrell D. Copeland, Scott M. Boyette, Robert C. Pearce, III
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Publication number: 20130233350Abstract: A method and system for removing hydrocarbon deposits from a heat exchanger tube bundle using an organic solvent. After contact with a heat exchanger tube bundle, the contaminated organic solvent may be treated to remove solids, base waters, and/or suspended hydrocarbons, and then again contacted with a heat exchanger tube bundle for the removal of hydrocarbon deposits. This allows for the removal of hydrocarbon deposits from a heat exchanger tube bundle in an efficient and environmentally friendly manner. The treatment of the heat exchanger tube bundle is also preferably performed using a method and system by which, through contact of the heat exchanger tube bundle with an organic solvent, a large percentage of hydrocarbon deposits are removed from the heat exchanger tube bundle in a short period of time.Type: ApplicationFiled: March 7, 2012Publication date: September 12, 2013Inventors: Michael Tomkins, Robert Larsen, Gary L. Gardner
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Publication number: 20130192649Abstract: The present invention relates to the acidic cleaning in the beer industry, and more particularly an improved process for acidic cleaning of the various elements and vessels that are used in the preparation of beer and other and other related fermented beverages, said cleaning being carried out by using a formulation comprising at least one alkane sulphonic acid.Type: ApplicationFiled: March 13, 2013Publication date: August 1, 2013Applicant: ARKEMA FRANCEInventor: Arkema France
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Patent number: 8492473Abstract: A purging compound for purging an extruder of polyamides or other polar thermoplastic resins for transitioning to the extrusion of a non-polar thermoplastic resin, includes a non-polar base polymer compounded with an ethylene-methacrylate copolymer, up to 15% of a mineral, and about 1% of a suitable antioxidant.Type: GrantFiled: March 23, 2011Date of Patent: July 23, 2013Assignee: Ingenia Polymers Corp.Inventors: Sushanta Dhar Roy, Viraj Triokekar, Salvatore D'Uva, Ed Hindy
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Patent number: 8480812Abstract: A process for quickly removing hydrocarbon contaminants and noxious gases in a safe and effective manner from catalytic reactors, other media packed process vessels and associated equipment in the vapor phase without using steam. The cleaning agent contains one or more solvents, such as terpenes or other organic solvents. The cleaning agent is injected into contaminated equipment, along with a carrier gas, in the form of a cleaning vapor.Type: GrantFiled: June 4, 2009Date of Patent: July 9, 2013Assignee: Refined Technologies, Inc.Inventors: Cody Nath, Barry Baker, Sean Sears
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Patent number: 8444770Abstract: A method for cleaning components of a system for filling holes in a printed circuit board with a fluid fill material includes removing the components being a dispensing head and a manifold connected to the dispensing head preferably as a single unit. The single unit is retained in that format. Excess fluid material from the dispensing head and manifold is evacuated preferably by passing air through the dispensing head and manifold. Then the dispensing head and manifold is placed in a cleaning tub, and the manifold is attached to a solvent pump line. The dispensing head and manifold is flushed with a flow of solvent from the solvent pump line; and excess solvent from the dispensing head and manifold is evacuated, by passing air through the dispensing head and manifold.Type: GrantFiled: June 29, 2009Date of Patent: May 21, 2013Assignee: TTM Technologies, Inc.Inventors: Tadd Hohlfelder, Brad Moran, Rubin Matthews, Thomas Gannon
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Patent number: 8361238Abstract: A process is provided for removing polymeric fouling on process equipment surfaces to restore the efficiency of such equipment. This is accomplished by contacting the fouled equipment with a solvent comprising at least one non-aromatic hydrocarbon compound, or a mixture of one or more non-aromatic organic compounds and one or more aromatic hydrocarbon compounds, for a period of time sufficient to remove the polymeric fouling.Type: GrantFiled: January 4, 2012Date of Patent: January 29, 2013Assignee: Perigee Solutions International, LLCInventors: Michael R. Dorton, Gary L. Gardner, Sr.
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Patent number: 8353990Abstract: A process is provided for chemically decontaminating the surface of a metallic component. In a first treatment step, an oxide layer formed on the component by corrosion of the material of the component is detached from the surface of the component with a first aqueous treatment solution containing an organic decontamination acid. In a subsequent second treatment step, the surface which is at least partially freed of the oxide layer is treated with an aqueous solution containing an active component for removing particles which adhere to the surface. The active component is formed of at least one anionic surfactant from the group including sulphonic acids, phosphonic acids, carboxylic acids and salts of those acids.Type: GrantFiled: August 17, 2011Date of Patent: January 15, 2013Assignee: Areva NP GmbHInventors: Rainer Gassen, Luis Sempere Belda, Werner Schweighofer, Bertram Zeiler
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Patent number: 8344198Abstract: A processes is provided to inhibit or limit the decomposition of a halide-containing olefin oligomerization catalyst system during recovery of an oligomerization product. The process includes deactivation of an olefin oligomerization catalyst system present in an olefin oligomerization reactor effluent stream by contact with an alcohol under conditions that minimize potential for deactivated catalyst system decomposition. Such conditions include minimization of the water content of the deactivation agent and concentration of the deactivation agent.Type: GrantFiled: March 15, 2004Date of Patent: January 1, 2013Assignee: Chevron Phillips Chemical Company LPInventors: Warren M. Ewert, Bruce E. Kreischer, Ronald D. Knudsen
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Publication number: 20120285489Abstract: [Problem] An object of the present invention is to provide pipe cleaning means that can effectively control introduction of viable bacteria to an inside of an apparatus and contamination occurring in the apparatus and particularly provide a pipe cleaning method and a pipe cleaning mechanism in a luminescence measurement apparatus. [Solution] A cleaning method of a pipe of a luminescence measurement apparatus (10) according to the present invention includes a bacteriolytic process of supplying a sterilization reagent into a supply pipe for hot water or a reagent in the luminescence measurement apparatus (10) and sterilizing an inside of the supply pipe, an ATP removal process of supplying an ATP removal reagent into the supply pipe after the sterilization of the inside of the supply pipe and removing ATP inside the supply pipe, and a process of replacing the ATP removal reagent in the supply pipe with pure water.Type: ApplicationFiled: January 21, 2011Publication date: November 15, 2012Inventor: Noe Miyashita
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Patent number: 8298345Abstract: A heat exchanger may be cleaned by introducing compressed nitrogen and a flushing composition through an injection device.Type: GrantFiled: September 11, 2009Date of Patent: October 30, 2012Assignee: The Rectorseal CorporationInventors: Eva Ackerman, Yanwei Cen, William Francis Flynn, Richard Garza
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Patent number: 8298481Abstract: A method for sterilizing a plastic bottle in an aseptic filling system according to which at least an inner surface or an outer surface of a bottle is sterilized by injecting a heated sterilizing fluid at 65° C.-90° C. while maintaining internal pressure of the bottle at 1 kPa-20 kPa.Type: GrantFiled: October 18, 2011Date of Patent: October 30, 2012Assignee: Toyo Seikan Kaisha, Ltd.Inventors: Takeshi Iwashita, Yonosuke Takahara, Kenichi Kominami, Ken Isogawa