Superplastic (e.g., Dynamic Recrystallization, Etc.) Patents (Class 148/564)
  • Patent number: 12215595
    Abstract: A method of assembling a radial turbine rotor includes manufacturing turbine blades, a flowpath ring, and a hub. The method includes fixing the turbine blades circumferentially around the flowpath ring by a blade joint between the turbine blades and the flowpath ring to form a ring assembly. The method includes spinning the hub and moving the hub into engagement with the flowpath ring to locate the hub radially inwardly of the flowpath ring and to form a hub joint between the flowpath ring and the hub.
    Type: Grant
    Filed: September 22, 2023
    Date of Patent: February 4, 2025
    Assignee: Rolls-Royce North American Technologies Inc.
    Inventors: Michel S. Smallwood, Stanford Clemens
  • Patent number: 11749520
    Abstract: A discharge chamber for a deep ultraviolet (DUV) light source includes a housing; and a first electrode and a second electrode in the housing, the first electrode and the second electrode being separated from each other to form a discharge region between the first electrode and the second electrode, the discharge region being configured to receive a gain medium including at least one noble gas and a halogen gas. At least one of the first electrode and the second electrode includes a metal alloy including more than 33% and less than 50% zinc by weight.
    Type: Grant
    Filed: August 25, 2021
    Date of Patent: September 5, 2023
    Assignee: Cymer, LLC
    Inventor: Leyla Ramin
  • Patent number: 11441216
    Abstract: A method of forming a part from sheet metal alloy is provided, for example, forming a part from aluminium alloy. The method comprises heating (A) the sheet metal alloy to a temperature at which solution heat treatment of the alloy occurs and so as to achieve solution heat treatment. The sheet is cooled (B) at at least the critical cooling rate for the alloy and then placed between dies to form (C) it into or towards the part.
    Type: Grant
    Filed: November 4, 2019
    Date of Patent: September 13, 2022
    Assignees: IMPERIAL INNOVATIONS LIMITED, IMPRESSION TECHNOLOGIES LIMITED
    Inventors: George Adam, Daniel Balint, Trevor Dean, John Dear, Omer El Fakir, Alistair Foster, Jianguo Lin, Liliang Wang
  • Patent number: 10829830
    Abstract: The present disclosure relates to a middle high temperature pressure vessel steel plate having excellent resistance against a post weld heat treatment (PWHT) and a manufacturing method therefor. The pressure vessel steel plate includes 0.05 to 0.17 wt % of C, 0.50 to 1.00 wt % of Si, 0.3 to 0.8 wt % of Mn, 1.0 to 1.5 wt % of Cr, 0.3 to 1.0 wt % of Mo, 0.003 to 0.30 wt % of Ni, 0.003 to 0.30 wt % of Cu, 0.005 to 0.06 wt % of Sol.Al, 0.015 wt % or less of P, and 0.020 wt % or less of S; additionally two or more elements selected from 0.002 to 0.025 wt % of Nb, 0.002 to 0.03 wt % of V, and 0.002 to 0.15 wt % of Co; and Fe and unavoidable impurities as the reminder, wherein a microstructure of a central portion of the steel plate is formed in a mixed structure of 20 area % or more of tempered martensite and the residue bainite.
    Type: Grant
    Filed: November 3, 2016
    Date of Patent: November 10, 2020
    Assignee: POSCO
    Inventor: Soon-Taik Hong
  • Patent number: 10604828
    Abstract: The present invention relates to an Al—Zn alloy with improved strength and elongation comprising more than 20 parts by weight of zinc relative to the total weight of the alloy and comprising discontinuous precipitates or lamellar precipitates, formed forcibly in 5% or more per unit area. According to the present invention, the tensile strength and the elongation of an Al—Zn alloy are simultaneously improved.
    Type: Grant
    Filed: June 8, 2017
    Date of Patent: March 31, 2020
    Assignee: KOREA INSTITUTE OF MACHINERY & MATERIALS
    Inventors: Seung-Zeon Han, Jee-Hyuk Ahn, Min-Soo Kim
  • Patent number: 9592547
    Abstract: A method of manufacturing an annular material includes: a forging process of making a discoid forged material by forging an alloy material; and a ring rolling process of making an annular material by performing ring rolling on an annular intermediate made by forming a through-hole in the forged material. In the forging process, hot forging which achieves an absolute value ??1 of a strain in a circumferential direction of the forged material that is greater than or equal to 0.3, an absolute value ?h of a strain in a height direction of the forged material that is greater than or equal to 0.3, and a ratio ?h/??1 between the absolute values of the strains that is in a range of 0.4 to 2.5 is performed at least two or more times.
    Type: Grant
    Filed: December 10, 2012
    Date of Patent: March 14, 2017
    Assignee: MITSUBISHI MATERIALS CORPORATION
    Inventors: Hideo Takizawa, Yuji Ishiwari, Hiroaki Kikuchi, Jun Ohsone
  • Patent number: 9574259
    Abstract: A method for producing a high-strength magnesium alloy material includes (a) a step of preparing a magnesium alloy workpiece having a top face and a side face; and (b) a step of applying a compressive load ?p (MPa) from the top face side of the workpiece and performing a uniaxial forging process on the workpiece. Step (b) is performed while suppressing deformation of the workpiece widening outward and under conditions including (i) ?p>?f (where ?f is the compressive breaking stress (MPa) of the workpiece); (ii) a plastic deformation rate is less than or equal to 10%, and (iii) a strain rate is less than or equal to 0.1/sec.
    Type: Grant
    Filed: June 19, 2012
    Date of Patent: February 21, 2017
    Assignee: The University of Electro-Communications
    Inventor: Hiromi Miura
  • Patent number: 9005377
    Abstract: Methods for modifying a physical characteristic of finished endodontic instruments made from one or more superelastic alloys is described which include heat treating one or more finished endodontic instruments in a salt bath for a specific time (e.g., from about four hours to about six hours), at a specified temperature (e.g., from about 475° C. to about 550° C.), and preferably at a specified pH range.
    Type: Grant
    Filed: June 13, 2013
    Date of Patent: April 14, 2015
    Assignee: D & S Dental, LLC
    Inventors: Derek E. Heath, Steven J. A. Treadway
  • Patent number: 8918996
    Abstract: Processes for fabricating components to have two or more regions with different grain structures, and components produced by such processes. First and second preforms are fabricated to comprise interface surfaces at which the preforms can be joined together. The first and second preforms are formed of first and second precipitation-strengthened alloys, respectively, and the first alloy differs from the second alloy by having a higher solvus temperature or a higher grain refiner content. The preforms are joined together to form an article comprising first and second portions formed by the first and second preforms, respectively, and corresponding to first and second regions of the component, respectively, and the interface surfaces of the preforms form a joint between the first and second portions of the article. A supersolvus heat treatment is performed on the article so that greater grain growth occurs in the second portion than in the first portion.
    Type: Grant
    Filed: May 4, 2011
    Date of Patent: December 30, 2014
    Assignee: General Electric Company
    Inventors: Andrew Ezekiel Wessman, David Paul Mourer
  • Patent number: 8916009
    Abstract: A method for manufacturing a nonlinear superelastic file comprising the steps of: providing a superelastic file having a shaft and a file axis; providing a fixture including a file groove being defined by one or more displacement members, the file groove configured for receiving the shaft; inserting at least a portion of the shaft into the fixture along the file groove, the portion of the shaft including a first portion of the shaft; contacting the first portion of the shaft with a first displacement member of the one or more displacement members such that the first portion of the shaft is displaced from the file axis thereby forming a first offset portion of the shaft; heating the portion of the shaft while inserted in the fixture to a temperature of at least about 300° C. for a time period of at least about 1 minute to shape-set the portion of the shaft thereby forming a shape-set nonlinear file.
    Type: Grant
    Filed: November 18, 2011
    Date of Patent: December 23, 2014
    Assignee: DENTSPLY International Inc.
    Inventors: Dan Ammon, Vincent Shotton, Yong Gao, Randall Maxwell
  • Patent number: 8911573
    Abstract: Medical instruments, particularly, endodontic instruments with unique limited memory characteristics, and methods for making such instruments. One embodiment includes heat treating a finished endodontic instrument. A related embodiment includes electropolishing a finished endodontic instrument and then heat treating the endodontic instrument.
    Type: Grant
    Filed: February 14, 2012
    Date of Patent: December 16, 2014
    Assignee: D & S Dental, LLC
    Inventors: Derek E. Heath, Steven J. A. Treadway, Bobby J. Bennett
  • Patent number: 8752752
    Abstract: A composite steel plate includes at least two steel sheets rolled to form a plate. One of the sheets has a composition that varies in a depthwise direction, between nanocrystalline and micron grained. The plate is made by treating a steel sheet to produce a composition in the sheet that varies in a depthwise direction of the sheet between nanocrystalline and micron grained, stacking the treated sheet with at least one other steel sheet, and rolling the stacked sheets to form the plate.
    Type: Grant
    Filed: March 9, 2009
    Date of Patent: June 17, 2014
    Assignee: Hong Kong Polytechnic University
    Inventors: Jian Lu, Junbao Zhang, Aiying Chen
  • Patent number: 8475711
    Abstract: Processes for producing a nickel-titanium alloy are disclosed. The processes are characterized by the production of nickel-titanium alloy articles having improved microstructure. A pre-alloyed nickel-titanium alloy is melted and atomized to form molten nickel-titanium alloy particles. The molten nickel-titanium alloy particles are cooled to form nickel-titanium alloy powder. The nickel-titanium alloy powder is consolidated to form a fully-densified nickel-titanium alloy preform that is hot worked to form a nickel-titanium alloy article. Any second phases present in the nickel-titanium alloy article have a mean size of less than 10 micrometers measured according to ASTM E1245-03 (2008) or an equivalent method.
    Type: Grant
    Filed: February 14, 2011
    Date of Patent: July 2, 2013
    Assignee: ATI Properties, Inc.
    Inventor: C. Craig Wojcik
  • Patent number: 8398789
    Abstract: Superelastic and/or shape memory nickel-titanium alloys having an increased fatigue life that is superior to known nickel-titanium alloys are disclosed. The nickel-titanium alloys have a minimum fatigue life that may be at least about 10 million strain cycles at a strain of at least about 0.75. The minimum fatigue life may be due, at least in part, to the nickel-titanium alloy having at least one of an oxygen concentration of less than about 200 ppm, a carbon concentration of less than about 200 ppm, the absence of oxide-based and/or carbide-based inclusions having a size greater than about 5 microns (?m), the presence of an R-phase, or combinations of the foregoing. Articles manufactured from such fatigue-resistant nickel-titanium alloys can be more durable because they are more resistant to repetitive strain and crack propagation.
    Type: Grant
    Filed: November 26, 2008
    Date of Patent: March 19, 2013
    Assignee: Abbott Laboratories
    Inventors: Sophia L. Wong, Zhicheng Lin, Alan G. Tahran, Jr.
  • Publication number: 20120155501
    Abstract: A method of manufacturing an electrode, in which a solid metal material is extruded through a channel angular extrusion die to form the electrode. The solid metal material comprises copper and at least about 10 wt % zinc, and more particularly, between about 20 and about 40 wt % zinc. Prior to extrusion, the solid metal material may be formed by casting, hot forging, machining and/or hot isostatic pressure such that the solid metal material has dimensions corresponding to the CAE die. After extrusion, the solid metal material can be rolled and/or cut to a desired electrode shape.
    Type: Application
    Filed: December 16, 2010
    Publication date: June 21, 2012
    Applicant: Honeywell International Inc.
    Inventors: Stephane Ferrasse, Frank Alford, Kay Dean Bowles
  • Patent number: 8177927
    Abstract: A method of making articles made of shape memory alloys having improved fatigue performance and to methods of treating articles formed from shape memory alloy materials by pre-straining the articles (or desired portions of the articles) in a controlled manner so that the resultant articles exhibit improved fatigue performance. The shape memory articles are preferably medical devices, more preferably implantable medical devices. They are most preferably devices of nitinol shape memory alloy, most particularly that is superelastic at normal body temperature. The pre-straining method of the present invention as performed on such articles includes the controlled introduction of non-recoverable tensile strains greater than about 0.20% at the surface of a desired portion of a shape memory alloy article. Controlled pre-straining operations are performed on the shape-set nitinol metal to achieve non-recoverable tensile strain greater than about 0.
    Type: Grant
    Filed: August 31, 2010
    Date of Patent: May 15, 2012
    Assignee: W. L. Gore & Associates, Inc.
    Inventors: Bret A. Dooley, Christopher C. Lasley, Michael R. Mitchell, Robert R. Steele, Eric M. Tittelbaugh
  • Patent number: 8128764
    Abstract: A method for refining the microstructure of titanium alloys in a single thermomechanical processing step, wherein the titanium alloy comprises boron. In some embodiments, the method comprises the steps of first adding boron to the titanium alloy then subjecting the boron-containing titanium alloy to a thermomechanical processing step. Also provided is a method for achieving superplasticity in titanium alloys comprising the steps of selecting a boron-containing titanium alloy, determining the temperature and strain rate necessary to achieve beta superplasticity, and applying sufficient temperature and strain rate to the boron-containing titanium alloy to deform the alloy to the desired shape. Also provided methods of forming titanium alloy parts and the parts prepared by these methods.
    Type: Grant
    Filed: December 13, 2004
    Date of Patent: March 6, 2012
    Inventors: Daniel B. Miracle, Seshacharyulu Tamirisakandala, Radhakrishna B. Bhat, Jaimie S Tiley
  • Publication number: 20110259481
    Abstract: There is provided a high strength steel plate including, by weight: 0.03% to 0.20% C, 0.15% to 0.55% Si, 0.9% to 1.5% Mn, 0.001% to 0.05% Al, 0.030% or less P, 0.030% or less S, 0.30% or less Cr, 0.2% or less Mo, 0.6% or less Ni, 0.07% or less V, 0.04% or less Nb, 5 ppm to 50 ppm Ca, 0.005% to 0.025% Ti, 0.0020% to 0.0060% N, 0.0005% to 0.0020% B, the balance of F and unavoidable impurities. The steel plate may be formed of tempered martensite, and conditions for cooling and recrystallization controlled rolling are optimized so as to control an average grain size of a microstructure and an aspect ratio of structure grains. Accordingly, a superior high-strength steel plate that can be used for an atomic plant, for example, an atomic plant rated at IOOOMW or more by having a tensile strength of at least 650 MPa and an impact toughness of at least 200 J at ?5O ° C., and a method of manufacturing the same can be provided.
    Type: Application
    Filed: December 21, 2009
    Publication date: October 27, 2011
    Applicant: POSCO
    Inventors: Soon-Taik Hong, Sung-Ho Jang, Ki-Hyun Bang
  • Patent number: 7976649
    Abstract: A method of fabricating a superplastically formable strip or a superplastically formable foil from TiAl6V4 with a thickness of no more than 0.9 mm, preferably less than or equal to 0.5 mm, comprises the steps: a) hot rolling a sheet metal made of TiAl6V4; b) thermal pre-treatment of the hot-rolled sheet metal at a temperature between 650 and 850° C.; and c) cold rolling the hot-rolled and thermally pre-treated sheet metal at a forming rate of at least 30%, wherein the forming rate per single pass amounts to between 1 and 15%, to form a strip or a foil with a thickness of no more than 0.9 mm, wherein the cold-rolled strip or the cold-rolled foil is not annealed.
    Type: Grant
    Filed: August 20, 2008
    Date of Patent: July 12, 2011
    Assignee: GfE Fremat GmbH
    Inventors: Joachim Klose, Ella Rehtanz, Christiane Rothe, Ines Eulitz, Werner Beck
  • Patent number: 7971770
    Abstract: A friction stir method includes providing a joining tool, a mold comprising a top surface and a cutout defined from the top surface, and a workpiece comprising a treatable layer and arranged on the top surface of the mold. The joining tool resists the workpiece, and rotates and moves to agitate the treatable layer of the workpiece along an extending direction of the cutout of the mold, until a protrusion integrated with the workpiece is formed in the cutout of the mold.
    Type: Grant
    Filed: March 31, 2010
    Date of Patent: July 5, 2011
    Assignees: Hong Fu Jin Precision Industry (ShenZhen) Co., Ltd., Hon Hai Precision Industry Co., Ltd., FINE TECH Corporation
    Inventors: Koichi Nakagawa, Qing Liu, Isao Shiozawa, Takeo Nakagawa
  • Publication number: 20110146853
    Abstract: A method for refining the microstructure of titanium alloys in a single thermomechanical processing step, wherein the titanium alloy comprises boron. In some embodiments, the method comprises the steps of first adding boron to the titanium alloy then subjecting the boron-containing titanium alloy to a thermomechanical processing step. Also provided is a method for achieving superplasticity in titanium alloys comprising the steps of selecting a boron-containing titanium alloy, determining the temperature and strain rate necessary to achieve beta superplasticity, and applying sufficient temperature and strain rate to the boron-containing titanium alloy to deform the alloy to the desired shape. Also provided methods of forming titanium alloy parts and the parts prepared by these methods.
    Type: Application
    Filed: December 13, 2004
    Publication date: June 23, 2011
    Applicant: OHIO UNIVERSITY
    Inventors: Daniel B. Miracle, Seshacharyulu Tamirisakandala, Radhakrishna B. Bhat, Jaimie S. Tiley
  • Publication number: 20100326571
    Abstract: An article made of an alloy, and a method for making the article, are presented. The alloy is substantially free of martensite, and comprises the following composition: at least about 75 weight percent titanium; up to about 10 weight percent of a beta stabilizing component; from about 3 weight percent to about 15 weight percent of an alpha stabilizing component; and from about 0.05 weight percent to about 5 weight percent germanium. Another embodiment is a method for fabricating an article. The method comprises providing a billet made of an alloy as described above, and stabilizing the billet microstructure to form a stabilized billet; the method may further comprise superplastically processing the stabilized billet to form a processed item.
    Type: Application
    Filed: June 30, 2009
    Publication date: December 30, 2010
    Applicant: GENERAL ELECTRIC COMPANY
    Inventors: Andrew David Deal, Radhakrishna Badekila Bhat, Richard DiDomizio, Judson Sloan Marte, Pazhayannur Ramanathan Subramanian
  • Patent number: 7850058
    Abstract: A method of superplastic forming of titanium packs and an associated assembly is provided. The titanium packs can include sheets having different granular structures so that the different sheets are adapted to superplastically form at different temperatures. One or more of the sheets can be formed at a temperature that is below the superplastic forming temperature of another sheet in the pack. In some cases, the occurrence of markoff can be reduced or eliminated.
    Type: Grant
    Filed: November 10, 2005
    Date of Patent: December 14, 2010
    Assignee: The Boeing Company
    Inventors: Thomas J. Connelly, Kent W. Dunstan, William T. Williams, III, Peter N. Comley, Larry D. Hefti
  • Patent number: 7789979
    Abstract: Articles made of shape memory alloys having improved fatigue performance and to methods of treating articles formed from shape memory alloy materials by pre-straining the articles (or desired portions of the articles) in a controlled manner so that the resultant articles exhibit improved fatigue performance. The shape memory articles are preferably medical devices, more preferably implantable medical devices. They are most preferably devices of nitinol shape memory alloy, most particularly that is superelastic at normal body temperature. The pre-straining method of the present invention as performed on such articles includes the controlled introduction of non-recoverable tensile strains greater than about 0.20% at the surface of a desired portion of a shape memory alloy article. Controlled pre-straining operations are performed on the shape-set nitinol metal to achieve nonrecoverable tensile strain greater than about 0.20% at or near the surface of selected regions in the nitinol metal article.
    Type: Grant
    Filed: May 2, 2003
    Date of Patent: September 7, 2010
    Assignee: Gore Enterprise Holdings, Inc.
    Inventors: Bret A. Dooley, Christopher C. Lasley, Michael R. Mitchell, Robert R. Steele, Eric M. Tittelbaugh
  • Patent number: 7763129
    Abstract: A method of forming a component from a gamma-prime precipitation-strengthened nickel-base superalloy so that, following a supersolvus heat treatment the component characterized by a uniformly-sized grain microstructure. The method includes forming a billet having a sufficiently fine grain size to achieve superplasticity of the superalloy during a subsequent working step. The billet is then worked at a temperature below the gamma-prime solvus temperature of the superalloy so as to form a worked article, wherein the billet is worked so as to maintain strain rates above a lower strain rate limit to control average grain size and below an upper strain rate limit to avoid critical grain growth. Thereafter, the worked article is heat treated at a temperature above the gamma-prime solvus temperature of the superalloy for a duration sufficient to uniformly coarsen the grains of the worked article, after which the worked article is cooled at a rate sufficient to reprecipitate gamma-prime within the worked article.
    Type: Grant
    Filed: April 18, 2006
    Date of Patent: July 27, 2010
    Assignee: General Electric Company
    Inventors: David Paul Mourer, Brian Francis Mickle, Shesh Krishna Srivatsa, Eric Scott Huron, Jon Raymond Groh, Kenneth Rees Bain
  • Patent number: 7563488
    Abstract: The invention relates to a process for manufacturing a sputter target. The process comprises the steps of—providing a target holder (12); —applying an intermediate layer (14) on said target holder; —applying a top layer (16) on top of said intermediate layer; said top layer comprising a material having a melting point which is substantially higher than the melting point of said target material; —heating the target holder coated with said intermediate layer and said top layer.
    Type: Grant
    Filed: July 10, 2002
    Date of Patent: July 21, 2009
    Assignee: NV Bekaert SA
    Inventors: Wilmert De Bosscher, Hilde Delrue, Johan Vanderstraeten
  • Patent number: 7534314
    Abstract: A density reducing high carbon containing or UHC-steel and particular a superplastic steel, which besides iron and impurities conventionally accompanying steel, contains the following alloy components in wt. %: 0.8 to 2.5% C 3.5 to 15% Al 0.5 to 4% Cr 0.01 to 4% Si up to 4% Ni, Mn, Mo, Nb, Ta, V, and/or W, wherein the steel includes as additional alloy components 0.1 to 0.85 Sn, and 0 to 3% Ti, Be and/or Ga.
    Type: Grant
    Filed: June 13, 2006
    Date of Patent: May 19, 2009
    Assignee: Daimler AG
    Inventors: Georg Frommeyer, Arndt Gerick, Tilmann Haug, Wolfgang Kleinekathöfer
  • Publication number: 20090050242
    Abstract: A method of fabricating a superplastically formable strip or a superplastically formable foil from TiAl6V4 with a thickness of no more than 0.9 mm, preferably less than or equal to 0.5 mm, comprises the steps: a) hot rolling a sheet metal made of TiAl6V4; b) thermal pre-treatment of the hot-rolled sheet metal at a temperature between 650 and 850° C.; and c) cold rolling the hot-rolled and thermally pre-treated sheet metal at a forming rate of at least 30%, wherein the forming rate per single pass amounts to between 1 and 15%, to form a strip or a foil with a thickness of no more than 0.9 mm, wherein the cold-rolled strip or the cold-rolled foil is not annealed.
    Type: Application
    Filed: August 20, 2008
    Publication date: February 26, 2009
    Inventors: Joachim KLOSE, Ella REHTANZ, Christiane ROTHE, Ines EULITZ, Werner BECK
  • Patent number: 7270720
    Abstract: In a method of bending a rod- or rod-like unfinished workpiece of a single crystal material of a Cu alloy the workpiece is bent at an elevated temperature so as to provide for a predetermined curvature and then the workpiece is further heated whereby the curvature is established but the superelasticity is lost, the workpiece is cooled down and then tempered at another raised temperature for at least one hour and is then immediately quenched in a cooling medium.
    Type: Grant
    Filed: April 30, 2004
    Date of Patent: September 18, 2007
    Assignee: Forschungszentrum Karlsruhe GmbH
    Inventors: Klaus-Peter Brhel, Harald Fischer
  • Patent number: 7165435
    Abstract: Work hardened sheets of formable metal are annealed by thermal conduction and heated to a forming temperature. In a preferred embodiment, the sheet is placed on a flat surface of a heated lower platen to partially heat and soften the sheet and an opposing heated upper platen is brought close enough to the sheet to contribute heat but not to constrain the sheet as it expands. The platens are then both brought close to the sheet to heat it to its forming temperature largely by thermal conduction.
    Type: Grant
    Filed: July 25, 2005
    Date of Patent: January 23, 2007
    Assignee: GM Global Technology Operations, Inc.
    Inventors: James G. Schroth, Richard H. Hammar, Paul E. Krajewski, Leonard L. Pollum, Susan Elizabeth Hartfield-Wunsch
  • Patent number: 6890394
    Abstract: A method is disclosed for heating a cold worked sheet of superplastically formable metal composition to recrystallize its microstructure to a formable condition and/or to heat the sheet to a temperature for an immediate forming operation. The sheet is placed between two electrical resistance heated platens maintained at a suitable temperature for recrystallizing and/or heating the metal sheet through its side surfaces. In a preferred embodiment a critical gap is maintained between the platens and the sheet to permit rapid conductive heating of the expanding sheet without marring its surfaces.
    Type: Grant
    Filed: December 18, 2002
    Date of Patent: May 10, 2005
    Assignee: General Motors Corporation
    Inventors: John E. Carsley, Richard Harry Hammar, John Robert Bradley
  • Patent number: 6866180
    Abstract: Friction stir processing (FSP) modifies the surface microstructure of metals so that thick-section metal workpieces can be bent over large angles without formation of surface cracks. A thick 2519-T8 aluminum plate (25.4 mm thick and 50.8 mm wide) was friction stir processed across the pre-tensile surface to a depth of 6.3 mm, and was then bent at room temperature over a punch with radius 38.1 mm into a v-shaped die to an 80° bend angle. Whereas unprocessed workpieces of this type exhibited surface cracking at 31° bend angle and failed at 40° bend angle, no cracking was evident for the friction stir processed workpiece up to 80° bend angle.
    Type: Grant
    Filed: February 18, 2003
    Date of Patent: March 15, 2005
    Assignee: Rockwell Scientific Licensing, LLC
    Inventors: Murray W. Mahoney, William H. Bingel
  • Patent number: 6835254
    Abstract: A method is disclosed for heating a cold worked sheet of superplastically formable metal composition to recrystallize its microstructure to a suitably formable condition and further to heat the sheet to a temperature for an immediate forming operation. The method utilizes a combination of hot air convection heating and infrared radiation to rapidly accomplish the heating. High temperature infrared heating elements provide most of the energy during an initial high heating rate phase and then those elements are shut off and heating is completed with controlled temperature hot air to prevent overheating of the sheet metal.
    Type: Grant
    Filed: December 9, 2002
    Date of Patent: December 28, 2004
    Assignee: General Motors Corporation
    Inventors: Richard Harry Hammar, John E. Carsley, John Robert Bradley
  • Publication number: 20040118488
    Abstract: A method is disclosed for heating a cold worked sheet of superplastically formable metal composition to recrystallize its microstructure to a formable condition and/or to heat the sheet to a temperature for an immediate forming operation. The sheet is placed between two electrical resistance heated platens maintained at a suitable temperature for recrystallizing and/or heating the metal sheet through its side surfaces. In a preferred embodiment a critical gap is maintained between the platens and the sheet to permit rapid conductive heating of the expanding sheet without marring its surfaces.
    Type: Application
    Filed: December 18, 2002
    Publication date: June 24, 2004
    Inventors: John E. Carsley, Richard Harry Hammar, John Robert Bradley
  • Publication number: 20040108022
    Abstract: A method is disclosed for heating a cold worked sheet of superplastically formable metal composition to recrystallize its microstructure to a suitably formable condition and further to heat the sheet to a temperature for an immediate forming operation. The method utilizes a combination of hot air convection heating and infrared radiation to rapidly accomplish the heating. High temperature infrared heating elements provide most of the energy during an initial high heating rate phase and then those elements are shut off and heating is completed with controlled temperature hot air to prevent overheating of the sheet metal.
    Type: Application
    Filed: December 9, 2002
    Publication date: June 10, 2004
    Inventors: Richard Harry Hammar, John E. Carsley, John Robert Bradley
  • Patent number: 6712916
    Abstract: A shaped metallic component is formed by friction stirring at least a segment of a single piece of bulk metal to impart superplasticity thereto and thereby yield a single superplastic metal blank from the single piece of bulk metal. The metal blank is then deformed by a metal deformation process such as forging, rolling, drawing, bending, extruding, gas forming, punching, and stamping.
    Type: Grant
    Filed: December 21, 2001
    Date of Patent: March 30, 2004
    Assignees: The Curators of the University of Missouri
    Inventors: Rajiv S. Mishra, Murray W. Mahoney
  • Patent number: 6704981
    Abstract: A method of forming sheets of superplastically formable material into a three dimensional article, the sheets being joined together along diffusion bonds to form discrete cells, at least one gas path being provided through the bond between cells. The sheets are heated to a temperature at which they exhibit superplastic properties and a gas injected between the sheets to expand the cells, the gas paths allowing the injected gas to pass from cell to cell. The edges of the gas paths are locally heated to change the microstructure of the sheets in the edge areas, which reduces the flow resistance of the edges under superplastic forming conditions and thereby reduces the propensity of the diffusion bonds bordering the gas transfer holes to peel apart under the forces of the inert gas exerted on the sheets at the gas transfer paths.
    Type: Grant
    Filed: September 9, 2002
    Date of Patent: March 16, 2004
    Assignee: BAE Systems plc
    Inventors: George Strickland, Adam B Marriott
  • Publication number: 20030179117
    Abstract: An information recording medium which ensures high reliability and favorable overwrite cyclability is provided, even when an interface layer is not provided between a recording layer and a dielectric layer. The recording layer 4 and the dielectric layers 2 and 6 are formed on the surface of the substrate 1. In the recording layer 4, a phase change is generated between a crystal phase and an amorphous phase by irradiation of light or application of an electric energy. The dielectric layers 2 and 6 are Zr—Cr—O-based material layers comprising Zr, Cr and O, preferably consisting essentially of material expressed, for example, with the formula (ZrO2)M(Cr2O3)100-M (mol %) wherein 20≦M≦80.
    Type: Application
    Filed: December 17, 2002
    Publication date: September 25, 2003
    Inventors: Rie Kojima, Takashi Nishihara, Haruhiko Habuta, Noboru Yamada
  • Publication number: 20030140992
    Abstract: The invention relates to a method for producing magnesium alloys with a superplastic structure using a deformation process, followed by quick cooling. The magnesium-based alloy is initially pre-heated to a temperature of 340-380° C. and is subsequently deformed. The semi-finished product thus obtained is cooled down at high speed to an ambient temperature immediately after deformation.
    Type: Application
    Filed: December 4, 2002
    Publication date: July 31, 2003
    Inventors: Ulrich Draugelates, Antonia Schram, Claus-Christian Kedenburg, Talant Ryspaev
  • Patent number: 6547895
    Abstract: The superplastic forming of suitable metal alloy sheets into strong components, such as automobile body structures or panels, is improved and accomplished faster by simultaneously forming two or more substantially identical, relatively thin sheets, preferably about 2 mm or less in thickness, rather than a single sheet of the same overall thickness. For example, two or more layers of thin AA5083 sheets can be stretched formed together at about 500° C. with greater deformation and elongation than a single sheet of comparable thickness.
    Type: Grant
    Filed: January 25, 2001
    Date of Patent: April 15, 2003
    Assignee: General Motors Corporation
    Inventors: John Robert Bradley, John E. Carsley, Jacob Lyjak
  • Patent number: 6485585
    Abstract: Pre-straining and thermal recrystallization processes for maximizing formability in SPF sheet alloys of aluminum, magnesium, iron and titanium can be modified to form sheet products with roughened or textured surfaces for low-slip applications or coating adherence or decorative applications. By determination of suitable pre-strain levels and recrystallization/forming temperatures for s sheet metal stock, relatively large grained microstructures are formed in the sheet that yield useful surface texture during forming.
    Type: Grant
    Filed: February 26, 2001
    Date of Patent: November 26, 2002
    Assignee: General Motors Corporation
    Inventor: Paul Edward Krajewski
  • Publication number: 20020117238
    Abstract: Pre-straining and thermal recrystallization processes for maximizing formability in SPF sheet alloys of aluminum, magnesium, iron and titanium can be modified to form sheet products with roughened or textured surfaces for low-slip applications or coating adherence or decorative applications. By determination of suitable pre-strain levels and recrystallization/forming temperatures for s sheet metal stock, relatively large grained microstructures are formed in the sheet that yield useful surface texture during forming.
    Type: Application
    Filed: February 26, 2001
    Publication date: August 29, 2002
    Inventor: Paul Edward Krajewski
  • Publication number: 20020112793
    Abstract: In a joining method for a frame of spectacles, and in more particular to a method for joining a bridge or a temple to a lens rim, a joining method for a frame of spectacles comprises deforming a joining portion of a member made of a shape memory alloy material so as to be insertable into a pipe for joining the member to a lens rim, and joining the joining portion of the member to the pipe by returning the joining portion of the member to an original shape before the deformation after the member is inserted into the pipe.
    Type: Application
    Filed: January 15, 2002
    Publication date: August 22, 2002
    Applicant: KOREA INSTITUTE OF SCIENCE AND TECHNOLOGY
    Inventor: Kwang Koo Jee
  • Patent number: 6350329
    Abstract: A method for producing new superplastic alloys by inducing in an alloy the formation of precipitates having a sufficient size and homogeneous distribution that a sufficiently refined grain structure to produce superplasticity is obtained after subsequent PSN processing. An age-hardenable alloy having at least one dispersoid phase is selected for processing. The alloy is solution heat-treated and cooled to form a supersaturated solid solution. The alloy is plastically deformed sufficiently to form a high-energy defect structure useful for the subsequent heterogeneous nucleation of precipitates. The alloy is then aged, preferably by a multi-stage low and high temperature process, and precipitates are formed at the defect sites. The alloy then is subjected to a PSN process comprising plastically deforming the alloy to provide sufficient strain energy in the alloy to ensure recrystallization, and statically recrystallizing the alloy.
    Type: Grant
    Filed: June 14, 1999
    Date of Patent: February 26, 2002
    Inventors: Lillianne P. Troeger, Edgar A. Starke, Jr., Roy Crooks
  • Patent number: 6328827
    Abstract: In order to obtain sheets made of a nickel-based superalloy of type 718 having properties of superplasticity, the sheets are manufactured with a final cycle comprising the steps of: a) solution treatment at 1060° C. for 15 minutes; b) precipitation at 730° C. to 800° C. for 1 to 2 hours; c) cold rolling at a ratio greater than 60%, and d) recrystallization at 900° C. for 30 minutes. Superplastic deformation of such sheets is carried out at about 970±10° C. and under pressures inducing stresses between 45 and 60 MPa.
    Type: Grant
    Filed: July 5, 1995
    Date of Patent: December 11, 2001
    Assignee: Societe Nationale d'Etude et de Construction de Moteurs d'Aviation “Snecma”
    Inventors: Mohamed Bouzidi, Philippe Caburet, Pierre Clement, André Claude Félix Collot, Jean-Lou Lebrun, Benoit Marty
  • Patent number: 6322646
    Abstract: A method for making a superplastically formable, aluminum alloy product which consists essentially of: about 2-3.8 wt. % magnesium; at least one dispersoid-forming element selected from the group consisting of: up to about 1.6 wt. % manganese, up to about 0.2 wt. % zirconium, and up to about 0.3 w. % chromium; at least one nucleation-enhancing element for recrystallization selected from: about 0.11-1.0 wt. % silicon, up to about 1.5 wt. % copper, and combinations thereof. Said alloy product has greater than about 300% elongation at a strain rate of about 0.0001-0.003/sec and a superplastic forming temperature between about 1000-1100° F. due, in part to the preferred thermomechanical processing steps applied to its intermediate plate or slab product forms.
    Type: Grant
    Filed: June 12, 2000
    Date of Patent: November 27, 2001
    Assignee: Alcoa Inc.
    Inventors: Dhruba J. Chakrabarti, Roger D. Doherty
  • Publication number: 20010014404
    Abstract: The present invention provides a superplastic aluminum alloy in which fine particles not substantially dispersion hardening are dispersed in a sufficient amount to effect grain boundary pinning to suppress crystal grain growth during hot working thereby ensuring manifestation of superplasticity over wide ranges of working temperature and strain rate.
    Type: Application
    Filed: July 17, 1997
    Publication date: August 16, 2001
    Applicant: TOYOTA JIDOSHA KABUSHIKI KAISHA
    Inventors: YOSHIHARU MIYAKE, YOSHIHISA SERZAWA, YUKIO OKOCHI
  • Patent number: 6261391
    Abstract: The present invention disclosed is an aluminum alloy plate for super plastic molding capable of cold pre-molding before super plastic molding. The alloy plate comprises Mg at from 2.0 to 8.0% (weight %, the same shall apply hereinafter) Be at from 0.0001 to 0.01%, at least one of Mn at from 0.3 to 2.5%, Cr at from 0.1 to 0.5%, Zr at from 0.1 to 0.5% and V at from 0.1 to 0.5%. Additionally, the alloy plate may comprise an Fe amount and an Si amount each within a range of 0.0 to 0.2%; amounts of Na and Ca within ranges of 3 ppm or less and 5 ppm or less, respectively; while the remainder of the alloy plate consists of Al and inevitable impurities. The resulting alloy plate a crystalline structure is a non-recrystallized crystal structure; the 90° critical bending radius is 7.5 times the plate thickness or less; and the yield strength ratio before and after the final annealing is 70% or more. The invention also discloses production methods for the alloy plate.
    Type: Grant
    Filed: March 10, 1995
    Date of Patent: July 17, 2001
    Assignees: Honda Giken Kogyo Kabushiki Kaisha, Sky Aluminum Co., Ltd.
    Inventors: Hideaki Ikeda, Masanori Kosugi, Shizuo Kimura, Mamoru Matsuo, Tsutomu Tagata, Nobuyuki Matsumoto
  • Publication number: 20010001969
    Abstract: An alloy containing 3.0 to 8.0 wt. % of Mg, 0.001 to 0.1 wt. % of Ti, and amounts of Fe and Si (as impurities) as small as 0.06 wt. % or less, the balance being Al and unavoidable impurities, wherein the number per square millimeter of grains of an Al—Fe—Si compound having a diameter of 1 &mgr;m or more is 2000 or less, the mean crystal grain diameter is 25 to 200 &mgr;m and the elongation is 350% or more as worked at 350 to 550° C. and a strain rate of 10−2 to 100/s. This alloy may further contain a small amount of Cu, Mn and/or Cr and is formed at 350 to 550° C. and a strain rate of 10−3 to 100/s. An aluminum alloy sheet with excellent high strain rate superplastic formability and therefore capable of being formed at high temperature and high speed is obtained and the use of this sheet shortens the forming time to improve productivity.
    Type: Application
    Filed: January 16, 1998
    Publication date: May 31, 2001
    Applicant: Hideo Yoshida et al
    Inventors: HIDEO YOSHIDA, HIROKI TANAKA, KOUICHIROU TAKIGUCHI
  • Patent number: 6077368
    Abstract: A Ni--Ti superelastic alloy demonstrates superelastic properties at normal temperatures from about 0 and 30.degree. C. The superelastic alloy allows shape alteration when the temperature is in excess of 40.degree. C. The Ni--Ti superelastic alloy is produced by plastic working a composition containing essentially Ni and Ti, and subjecting the composition to heat treatment at a temperature between 600 and 800.degree. C. to impart shape memory. When the Ni--Ti superelastic alloy is used in an eyeglass frame, it allows the shape of the pad arms to be adjusted at temperatures above about 40.degree. C.
    Type: Grant
    Filed: May 17, 1999
    Date of Patent: June 20, 2000
    Assignee: Furukawa Electric Co., Ltd.
    Inventors: Masayuki Nakamura, Mikio Takeuchi