With Working Patents (Class 148/667)
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Patent number: 11554399Abstract: Systems and methods for quenching an extrudate using an atomized spray of liquid are described. A system includes a billet die at a proximal end configured to accept a billet and form an extrudate, a quench chamber located adjacent to the billet die for receiving the extrudate and comprising at least one pulsed width modulation (PWM) atomizing spray nozzle and a control module in communication with the at least one PWM atomizing spray nozzle and configured to independently control a liquid pressure, a gas pressure, a spray frequency, a duty cycle and flow rate of each at least one PWM atomizing spray nozzle.Type: GrantFiled: November 20, 2019Date of Patent: January 17, 2023Assignee: Tesla, Inc.Inventor: Jared E. Ottmann
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Patent number: 10196722Abstract: The invention relates to the method for manufacturing a rolled product of variable thickness made of heat-treatable aluminum alloy in which hot rolling is performed to achieve a variation in thickness of at least 10% lengthwise between the thickest part and the thinnest part; the rolled product of variable thickness obtained undergoes solution heat-treatment and quenching with permanent set of at least 1% in the thickest part before natural or artificial ageing. The products obtained according to the invention exhibit improved mechanical strength of at least 5% in the thinnest part and improved fracture toughness of at least 15% in the thickest part. The products according to the invention are notably useful in the fabrication of aircraft upper or lower wing skins the “buy to fly” ratio and the properties are simultaneously improved.Type: GrantFiled: November 7, 2013Date of Patent: February 5, 2019Assignee: CONSTELLIUM ISSOIREInventors: Jean-Christophe Ehrstrom, Armelle Danielou, Timothy Warner
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Patent number: 9752220Abstract: There are provided a magnesium alloy coil stock having good flatness and a method for producing the magnesium alloy coil stock, and a magnesium alloy structural member that uses the coil stock and a method for producing the magnesium alloy structural member. The coil stock is obtained by coiling a sheet composed of a magnesium alloy in a cylindrical shape, and the internal diameter of the coil stock is 1000 mm or less. The coil stock can be produced by rolling a cast material obtained by subjecting a magnesium alloy to continuous casting, subjecting the rolled sheet to warm leveling, and coiling the worked sheet in a cylindrical shape while the temperature just before coiling is decreased to 100° C. or less.Type: GrantFiled: November 22, 2010Date of Patent: September 5, 2017Assignee: SUMITOMO ELECTRIC INDUSTRIES, LTD.Inventors: Takahiko Kitamura, Ryuichi Inoue, Nobuyuki Mori, Yukihiro Oishi, Osamu Mizuno, Nozomu Kawabe
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Patent number: 9523141Abstract: Provided is an Mg alloy and a method for producing same able to demonstrate high strength without requiring an expensive rare earth element (RE). The high-strength Mg alloy containing Ca and Zn within a solid solubility limit and the remainder having a chemical composition comprising Mg and unavoidable impurities is characterized in comprising equiaxial crystal particles, there being a segregated area of Ca and Zn along the (c) axis of a Mg hexagonal lattice within the crystal particle, and having a structure in which the segregated area is lined up by Mg3 atomic spacing in the (a) axis of the Mg hexagonal lattice. The method for producing the high-strength Mg alloy is characterized in that Ca and Zn are added to Mg in a compounding amount corresponding to the above composition and, after homogenization heat treating an ingot formed by dissolution and casting, the above structure is formed by subjecting the ingot to hot processing.Type: GrantFiled: November 6, 2012Date of Patent: December 20, 2016Assignees: TOYOTA JIDOSHA KABUSHIKI KAISHA, NATIONAL UNIVERSITY CORPORATION KOBE UNIVERSITY, NATIONAL INSTITUTE FOR MATERIALS SCIENCEInventors: Kota Washio, Akira Kato, Toshiji Mukai, Alok Singh, Hidetoshi Somekawa
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Patent number: 9017602Abstract: A method of forming a wrought material having a refined grain structure is provided. The method comprises providing a metal alloy material having a depressed solidus temperature and a low temperature eutectic phase transformation. The metal alloy material is molded and rapidly solidified to form a fine grain precursor that has fine grains surrounded by a eutectic phase with fine dendritic arm spacing. The fine grain precursor is plastic deformed at a high strain rate to cause recrystallization without substantial shear banding to form a fine grain structural wrought form. The wrought form is then thermally treated to precipitate the eutectic phase into nanometer sized dispersoids within the fine grains and grain boundaries and to define a thermally treated fine grain structure wrought form having grains finer than the fine grains and the fine dendritic arm spacing of the fine grain precursor.Type: GrantFiled: February 4, 2011Date of Patent: April 28, 2015Assignee: Thixomat, Inc.Inventors: Raymond F. Decker, Jack Huang, Sanjay G. Kulkarni, Stephen E. Lebeau, Ralph E. Vining
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Publication number: 20150083285Abstract: A magnesium alloy of the present invention has the chemical composition that contains 0.02 mol % or more and less than 0.1 mol % of at least one element selected from yttrium, scandium, and lanthanoid rare earth elements, and magnesium and unavoidable impurities accounting for the remainder. A magnesium alloy member of the present invention is produced by hot plastic working of the magnesium alloy in a temperature range of 200° C. to 550° C., followed by an isothermal heat treatment performed in a temperature range of 300° C. to 600° C. The magnesium alloy is preferred for use in applications such as in automobiles, railcars, and aerospace flying objects. The magnesium alloy and the magnesium alloy member can overcome the yielding stress anisotropy problem, and are less vulnerable to the rising price of rare earth elements.Type: ApplicationFiled: May 28, 2013Publication date: March 26, 2015Inventors: Hidetoshi Somekawa, Yoshiaki Osawa, Toshiji Mukai, Alok Singh, Kota Washio, Akira Kato
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Publication number: 20140373982Abstract: The present invention discloses a magnesium alloy sheet with low Gd content and high ductility and its hot rolling technology, which belongs to the field of metal material technology. The chemical components of the magnesium alloy sheet, based on the mass percent, take up respectively: 0.9˜2.1% as Zn, 0.2˜0.8% as rare earth element, namely Gd, 0˜0.9% as Mn, and the rest as Mg. The magnesium alloy sheet of the present invention is added with relatively lower rare earth element, Gd, which reduces the alloy costs; in addition, magnesium alloy has good rolling performance, which can realize continuous, multi-pass and large-deformation rolling, and also ensure the sheets rolled have non-basal texture and high room-temperature elongation which reaches 35˜50%, wherein the elongation, ?, in the rolling direction is no less than 35% and that in the horizontal direction no less than 45%.Type: ApplicationFiled: August 2, 2013Publication date: December 25, 2014Applicant: Institute of Metal Research Chinese Academy of SciencesInventors: Rongshi Chen, Hong Yan, Enhou Han, Wei Ke
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Publication number: 20140348696Abstract: A method for increasing formability of magnesium alloy sheet and the magnesium alloy sheet prepared by the same are provided, in which the method includes the following steps: forming {10-12} twins in magnesium alloy sheet (step 1); and annealing the magnesium alloy sheet of step 1 (step 2). The present invention also provides the magnesium alloy sheet containing {10-12} twins prepared by the method. Accordingly, the room temperature formability and the warm formability are increased by forming {10-12} twins through deformation on the magnesium alloy sheet and subsequently performing annealing, because it is possible to artificially form {10-12} twins without increasing dislocations in the magnesium alloy sheet and accommodate the deformation generated during the forming via annihilation of the twins.Type: ApplicationFiled: August 11, 2014Publication date: November 27, 2014Applicant: Korea Institute of Machinery and MaterialsInventors: Sung Hyuk Park, Young Min Kim, Ha Sik Kim, Chang Dong Yim, Bong Sun You, Seong Gu Hong, Chong Soo Lee, Jeong Hun Lee, Hyung Lae Kim
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Patent number: 8657973Abstract: Magnesium-based alloy wire excelling in strength and toughness, its method of manufacture, and springs in which the magnesium-based alloy wire is utilized are made available. The magnesium-based alloy wire contains, in mass %, 0.1 to 12.0% Al, and 0.1 to 1.0% Mn, and is provided with the following constitution. Diameter d that is 0.1 mm or more and 10.0 mm or less; length L that is 1000d or more; tensile strength that is 250 MPa or more; necking-down rate that is 15% or more; and elongation that is 6% or more. Such wire is produced by draw-forming it at a working temperature of 50° C. or more, and by heating it to a temperature of 100° C. or more and 300° C. or less after the drawing process has been performed.Type: GrantFiled: October 2, 2012Date of Patent: February 25, 2014Assignees: Sumitomo Electric Industries, Ltd., Sumitomo (SEI) Steel Wire Corp.Inventors: Yukihiro Oishi, Nozomu Kawabe
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Patent number: 8636853Abstract: An Mg alloy provided with high strength and high ductility by matching the strength and ductility in tensile deformation and compressive deformation at the same levels is provided. The Mg alloy of the present invention is characterized by having a chemical composition consisting of Y: 0.1 to 1.5 at % and a balance of Mg and unavoidable impurities and having a microstructure with high Y regions with Y concentrations higher than an average Y concentration distributed at nanometer order sizes and intervals. The present invention further provides an Mg alloy characterized by having a chemical composition consisting of Y: more than 0.1 at % and a valance of Mg and unavoidable impurities, having a microstructure with high Y regions with Y concentrations higher than an average Y concentration distributed at nanometer order sizes and intervals and having an average recrystallized grain size within the range satisfying the following formula 1: ?0.87c+1.10<log d<1.14c+1.Type: GrantFiled: March 26, 2008Date of Patent: January 28, 2014Assignees: Toyota Jidosha Kabushiki Kaisha, National Institute for Materials ScienceInventors: Tetsuya Shoji, Akira Kato, Toshiji Mukai, Hidetoshi Somekawa
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Patent number: 8591674Abstract: A method of enhancing the ductility of magnesium alloy sheets containing 85% or more by weight of magnesium is described. An annealed, substantially strain free, sheet of generally uniform grain size is locally deformed in local regions to develop strained ‘islands’ of a predetermined strain embedded in a substantially strain-free matrix and then annealed. The deformed regions undergo recrystallization and grain growth while the remainder of the sheet suffers only minor change in grain size, leading to sheet with grains having a bimodal size distribution. The ductility of alloys processed in this way is significantly greater than the ductility of the unprocessed, uniform grain size alloy without compromise to the tensile strength of the alloy.Type: GrantFiled: November 11, 2011Date of Patent: November 26, 2013Assignee: GM Global Technology Operations LLCInventors: Sushil Kumar Mishra, Shashank Tiwari, Asim Tewari, Jon T. Carter, Deepika Sachdeva
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Publication number: 20130213528Abstract: A magnesium alloy member capable of achieving a mechanical strength and a high-temperature fatigue strength sufficient for a compressor for in automotive air conditioners The magnesium alloy member is formed by subjecting a cast material of a magnesium alloy containing, on the basis of mass %, from 0.3% to 10% calcium (Ca), from 0.2% to 15% aluminum (Al), and from 0.05% to 1.5% manganese (Mn), and containing calcium (Ca) and aluminum (Al) at a calcium/aluminum mass ratio of from 0.6 to 1.7, with the balance being magnesium (Mg) and inevitable impurities to plastic working (extrusion processing) at from 250° C. to 500° C. This makes it possible to obtain a magnesium alloy member having a room-temperature 0.2% proof stress of 300 MPa or more and a 150° C. fatigue strength of 100 MPa or greater.Type: ApplicationFiled: October 28, 2011Publication date: August 22, 2013Inventors: Sueji Hirawatari, Hidenori Hosoi, Tsuyoshi Fukui, Makoto Fukushima, Shigeharu Kamado, Tomoyuki Honma
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Publication number: 20130218292Abstract: A method for producing an implant and the implant itself, particularly an intraluminal endoprosthesis, wherein the implant is produced from a preferably hollow cylindrical semifinished article (10), wherein the semifinished article contains magnesium or a magnesium alloy, the method comprising preparing the semifinished article (10), and shaping the semifinished article at a temperature of between 250° C. and 550° C. using a tool, which has a metallic lubricant containing gallium and/or a gallium compound on at least a part of its surface that will come into contact with the semifinished article.Type: ApplicationFiled: February 11, 2013Publication date: August 22, 2013Applicant: BIOTRONIK AGInventor: Biotronik AG
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Patent number: 8506733Abstract: The present invention provides a magnesium-based composite material that can achieve excellent performance such as high tensile strength not only at ordinary temperature but also at high temperature. The magnesium-based composite material of the present invention is Al2Ca-containing magnesium-based composite material, wherein said composite material is obtained by a solid-phase reaction of an aluminum-containing magnesium alloy and an additive, said additive being calcium oxide, and said composite material contains Al2Ca formed in the solid-phase reaction. In the magnesium-based composite material, CaO, in combination with Al2Ca, can be dispersed.Type: GrantFiled: March 11, 2009Date of Patent: August 13, 2013Assignee: Topy Kogyo KabusikikaisyaInventors: Keitaro Enami, Shoji Ono, Masaki Ohara, Takanori Igarashi
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Patent number: 8505353Abstract: The present invention relates to a method of manufacturing magnesium alloy processing materials capable of improving low cycle fatigue life. The manufacturing method for magnesium alloy processing materials with improved low cycle fatigue life comprises pre-straining a magnesium alloy processing material which is processed.Type: GrantFiled: August 12, 2009Date of Patent: August 13, 2013Assignee: Postech Academy-Industry FoundationInventors: Sung-Hyuk Park, Chong-Soo Lee, Seong-gu Hong, Byoung-Ho Lee
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Patent number: 8480823Abstract: A metal induction forming method includes providing a metal sheet, cold forming the metal sheet by applying shaping pressure to the metal sheet, heating the metal sheet while applying shaping pressure to the metal sheet and quenching the metal sheet.Type: GrantFiled: June 17, 2010Date of Patent: July 9, 2013Assignee: The Boeing CompanyInventors: Marc R. Matsen, William Dykstra
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Publication number: 20130118657Abstract: A method of enhancing the ductility of magnesium alloy sheets containing 85% or more by weight of magnesium is described. An annealed, substantially strain free, sheet of generally uniform grain size is locally deformed in local regions to develop strained ‘islands’ of a predetermined strain embedded in a substantially strain-free matrix and then annealed. The deformed regions undergo recrystallization and grain growth while the remainder of the sheet suffers only minor change in grain size, leading to sheet with grains having a bimodal size distribution. The ductility of alloys processed in this way is significantly greater than the ductility of the unprocessed, uniform grain size alloy without compromise to the tensile strength of the alloy.Type: ApplicationFiled: November 11, 2011Publication date: May 16, 2013Applicant: GM GLOBAL TECHNOLOGY OPERATIONS LLCInventors: Sushil Kumar Mishra, Shashank Tiwari, Asim Tewari, Jon T. Carter, Deepika Sachdeva
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Patent number: 8357250Abstract: The formability of coiled and annealed (O-temper) magnesium alloy sheet material in high temperature forming operations is sometimes adversely affected by small amounts of cold work introduced into the fine grained material during handling of the coil and unwinding it to obtain blank workpieces for hot stamping, hot blow forming, or the like. When necessary, the formability of the sheet material with regions of hard worked microstructure may be improved by predetermining a recovery heat treatment using small portions of the material in formability tests. The recovery heat treatment, determined for the specific coiled stock, may then be applied to the material of the coil as it is used in making vehicle body panels or the like.Type: GrantFiled: July 29, 2008Date of Patent: January 22, 2013Assignee: GM Global Technology Operations LLCInventors: Paul E. Krajewski, Ravi Verma, Jon T. Carter, Joshua D. Lasceski
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Patent number: 8333924Abstract: Provided is a high-strength and high-toughness magnesium alloy which has practical level of both the strength and the toughness for expanded applications of the magnesium alloys, and is a method for manufacturing thereof. The high-strength and high-toughness magnesium alloy of the present invention contains: a atom % in total of at least one metal of Cu, Ni, and Co; and b atom % in total of at least one element selected from the group consisting of Y, Dy, Er, Ho, Gd, Tb, and Tm, while a and b satisfying the following formulae (1) to (3), 0.2?a?10??(1) 0.2?b?10??(2) 2/3a?2/3<b.Type: GrantFiled: March 20, 2007Date of Patent: December 18, 2012Assignees: National University Corporation Kumamoto University, Chiba UniversityInventors: Yoshihito Kawamura, Michiaki Yamasaki, Takaomi Itoi, Mitsuji Hirohashi
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Publication number: 20120288398Abstract: The present invention relates to a cold-rolling method for cold-rolling a wrought Mg alloy with a weak or non-basal texture as well as a cold-rolled sheet, the method comprising the steps of: pre-treating a billet of the wrought Mg alloy with a weak or non-basal texture, and then cold rolling it; wherein the weak or non-basal texture plane of said billet is selected as a rolling plane, and the rolling direction is parallel to the rolling plane; and said billet is cold rolled at room temperature to a sheet or foil with a thickness of 0.1 to 100 mm, wherein single-pass or multi-pass rolling is used, and the cold rolling is followed by an annealing at 200 to 400° C. for 10 min to 48 h.Type: ApplicationFiled: April 30, 2012Publication date: November 15, 2012Applicant: Institute of Metal Research, Chinese Academy of SciencesInventors: Rongshi Chen, Di Wu, Enhou Han, Wei Ke
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Patent number: 8308878Abstract: Magnesium-based alloy wire excelling in strength and toughness, its method of manufacture, and springs in which the magnesium-based alloy wire is utilized are made available. The magnesium-based alloy wire contains, in mass %, 0.1 to 12.0% Al, and 0.1 to 1.0% Mn, and is provided with the following constitution. Diameter d that is 0.1 mm or more and 10.0 mm or less; length L that is 1000 d or more; tensile strength that is 250 MPa or more; necking-down rate that is 15% or more; and elongation that is 6% or more. Such wire is produced by draw-forming it at a working temperature of 50° C. or more, and by heating it to a temperature of 100° C. or more and 300° C. or less after the drawing process has been performed.Type: GrantFiled: May 16, 2002Date of Patent: November 13, 2012Assignees: Sumitomo Electric Industries, Ltd., Sumitomo (SEI) Steel Wire Corp.Inventors: Yukihiro Oishi, Nozomu Kawabe
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Patent number: 8293031Abstract: A magnesium alloy, comprising: Y: 0.5-10? Zn: 0.5-6?? Ca: 0.05-1?? Mn: ??0-0.5 Ag: 0-1 Ce: 0-1 Zr: 0-1 or Si: 0-0.4, wherein the amounts are based on weight-percent of the alloy and Mg, and manufacturing-related impurities constitute the remainder of the alloy to a total of 100 weight-percent. Also disclosed is a method for manufacturing such an alloy and a biodegradable implant formed therefrom.Type: GrantFiled: July 27, 2007Date of Patent: October 23, 2012Assignee: Biotronik VI Patent AGInventors: Bodo Gerold, Heinz Mueller, Joerg Loeffler, Anja Haenzi, Peter Uggowitzer
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Patent number: 8282748Abstract: The invention relates to a method for producing metal matrix composite materials, including at least one proportion of magnesium or one magnesium alloy and involving at least one production step in which a thixomolding ensues. According to the invention, an Mg2Si phase having a volume fraction of at least 2% is incorporated in a metal matrix preferably comprised of magnesium or of a magnesium alloy. The inventive method uses the thixomolding method for the in-situ production of a metallic composite material and is advantageous in that a broad range of adjustable volume fractions of the Mg2Si phase in the composite material results whereby enabling the properties of the composite material to be individually modified. The inventive metal matrix composite material is particularly suited for producing thermally stressed parts of motor vehicles such as pistons or the like.Type: GrantFiled: October 16, 2004Date of Patent: October 9, 2012Assignee: Mahle GmbHInventors: Florian Moll, Lutz Oemisch, Ulrich Bischofberger, Karl Ulrich Kainer, Norbert Hort, Hajo Dieringa, Hagen Frank
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Patent number: 8268235Abstract: An implant consisting entirely or in part of a biocorrodible magnesium alloy having the composition Gd: 2.7-15.0 wt %, Zn: 0-0.5 wt %, Zr: 0.2-1.0 wt %, Nd: 0-4.5 wt %, Y: 0-2.0 wt %, where magnesium and impurities due to the production process account for the remainder to a total of 100 wt %.Type: GrantFiled: December 17, 2009Date of Patent: September 18, 2012Assignee: Biotronik VI Patent AGInventor: Bodo Gerold
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Patent number: 8142578Abstract: A process for manufacturing a process for manufacturing a part made of a magnesium alloy is disclosed. The process includes a step of forging a block of the alloy followed by a heat treatment. The alloy is a casting alloy based on 85% magnesium, and containing, by weight: 0.2 to 1.3% zinc; 2 to 4.5% neodymium; 0.2 to 7.0% rare-earth metal with an atomic number from 62 to 71; 0.2 to 1% zirconium. The forging is carried out at a temperature above 400° C. In particular the temperature is set between 420 and 430° C. and the forging step comprises a plastic deformation carried out at a slow rate. The process allows one to produce parts such as elements of casing for aeronautical machines, operating at a temperature of around 200° C. and having good aging properties.Type: GrantFiled: July 19, 2007Date of Patent: March 27, 2012Assignees: Hispano Suiza, Manoir IndustriesInventors: Pascal Cantrel, Sophie Lubin, Christian Henri Paul Mauhe, Isabelle Robert, Jean Stracchi
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Patent number: 8123877Abstract: A heat-resistant magnesium alloy is for casting, and includes Ca in an amount of from 1 to 15% by mass, Al in a summed amount of from 4 to 25% by mass with the amount of Ca, and the balance being Mg and inevitable impurities when the entirety is taken as 100% by mass. The heat-resistant magnesium alloy is not only inexpensive, but also effects an advantage that cracks are inhibited from occurring when being cast. For example, a process for producing heat-resistant magnesium alloy cast product includes the step of pressure pouring an alloy molten metal, which has a target composition around Mg—3% Ca—3% Al—from 0.2 to 0.3% Mn, into a cavity of metallic die, which is preheated to a die temperature of from 130 to 140° C. in advance. The process makes it possible to produce die-cast products, which are free from cast cracks.Type: GrantFiled: October 18, 2007Date of Patent: February 28, 2012Assignee: Kabushiki Kaisha Toyota JidoshokkiInventors: Motoharu Tanizawa, Kyoichi Kinoshita, Eiji Kishi, Katsufumi Tanaka, Yuki Okamoto, Takayuki Kato
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Publication number: 20110315282Abstract: The quasicrystal phase and/or quasicrystal-like phase particles, which is composed of the Mg—Zn—Al, are dispersed into Mg-base alloy material for strain working. The microstructure in this material does not include the dendrite structure, and the size of the magnesium matrix is 40 ?m or less than 40 ?m. The present invention shows that the quasicrystal phase and/or quasicrystal-like phase is able to form by addition of the Zn and Al elements except for the use of rare earth elements. In addition, the excellent trade-off-balancing between strength and ductility and reduction of the yield anisotropy, which are the serious issues for the wrought processed magnesium alloys, is able to obtain by the microstructure controls before the strain working process.Type: ApplicationFiled: January 19, 2010Publication date: December 29, 2011Inventors: Hidetoshi Somekawa, Yoshiaki Osawa, Alok Singh, Toshiji Mukai
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Patent number: 8062439Abstract: A magnesium alloy sheet having an adequate strength and an excellent bendability is provided along with a method of manufacturing such an alloy sheet. The method comprises, rolling a magnesium alloy sheet through a reduction roll, the alloy thereof containing about 0.1-10.0 mass % of Al and about 0.1-4.0 mass % of Zn, wherein the magnesium alloy sheet has a surface temperature of about 100° C. or below at the time just before it is fed in the reduction roll, and the reduction roll has a surface temperature in the range of about 100° C. to 300° C. Particularly, when executing multipass rolling, at least the last pass is accomplished in non-preheat rolling wherein the magnesium alloy sheet and the reduction roll have specified surface temperatures, respectively.Type: GrantFiled: June 3, 2003Date of Patent: November 22, 2011Assignee: Sumitomo Electric Industries, Ltd.Inventors: Kenichi Shimizu, Nozomu Kawabe, Akira Kishimoto
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Publication number: 20110272069Abstract: A magnesium-based alloy consisting of, by weight: 0.5 to 1.5% manganese, 0.05 to 0.5% rare earth of which more than 70% is lanthanum, 0 to 1.5% zinc and 0 to 0.1% strontium, the balance being magnesium except for incidental impurities.Type: ApplicationFiled: August 29, 2008Publication date: November 10, 2011Applicant: CAST CRC LIMITEDInventors: Matthew Robert Barnett, Christopher Huw John Davies, Aiden Graeme Beer
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Patent number: 7967928Abstract: Methods of extruding magnesium-based casting alloys are provided. The magnesium alloys have relatively high strength and castibility, as well as an improved ductility and extrudability for wrought alloy applications. The magnesium-based wrought alloy comprises aluminum (Al) of between about 2.5 to about 3.5 wt. %, manganese (Mn) of less than about 0.6 wt. %, zinc (Zn) of less than about 0.22 wt. %, other impurities of less than about 0.1 wt. %, and a balance of magnesium (Mg). The disclosure provides various methods of forming extruded structural components, including automotive components, and methods of forming such wrought alloys.Type: GrantFiled: October 1, 2007Date of Patent: June 28, 2011Assignee: GM Global Technologies Operations LLCInventors: Aihua A Luo, Anil K Sachdev
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Patent number: 7879165Abstract: The present invention provides a method for producing a magnesium alloy sheet capable of producing a magnesium alloy sheet having excellent plastic workability such as press workability. The method of the present invention includes rolling a magnesium alloy blank with a reduction roll. The rolling includes controlled rolling performed under the following conditions (1) and (2) wherein M (% by mass) is the Al content in a magnesium alloy constituting the blank: (1) the surface temperature Tb (° C.) of the magnesium alloy blank immediately before insertion into the reduction roll satisfies the following expression: 8.33×M+135?Tb?8.33×M+165 wherein 1.0?M?10.0; and (2) the surface temperature Tr of the reduction roll is 150° C. to 180° C.Type: GrantFiled: March 24, 2006Date of Patent: February 1, 2011Assignee: Sumitomo Electric Industries, Ltd.Inventors: Nobuyuki Mori, Nozomu Kawabe
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Patent number: 7871476Abstract: A magnesium alloy exhibiting high strength and high ductility, characterized in that it comprises 0.03 to 0.54 atomic % of certain solute atoms belonging to 2 Group, 3 Group or Lanthanoids of the Periodic Table and having an atomic radius larger than that of magnesium and the balanced amount of magnesium, and has a fine crystal grain structure wherein solute atoms having an average crystal grain diameter of 1.5 ?m or less and being unevenly present in the vicinity of crystal grain boundaries at a concentration being 1.5 to 10 times that within crystal grains, wherein an atom selected from the group consisting of Ca, Sr, Ba, Sc, Y, La, Ce, Pr, Nd, Pm, Sm, Eu, Gd, Th, Dy, Ho, Er, Tm, Yb and Lu can be used as the above solute atom; and a method for producing the magnesium alloy. The above magnesium alloy is novel and achieves high strength and high ductility at the same time.Type: GrantFiled: June 28, 2005Date of Patent: January 18, 2011Assignee: National Institute for Materials ScienceInventors: Toshiji Mukai, Kazuhiro Hono, Hidetoshi Somekawa, Tomoyuki Honma
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Publication number: 20100163141Abstract: An Mg alloy provided with high strength and high ductility by matching the strength and ductility in tensile deformation and compressive deformation at the same levels is provided. The Mg alloy of the present invention is characterized by having a chemical composition consisting of Y: 0.1 to 1.5 at % and a balance of Mg and unavoidable impurities and having a microstructure with high Y regions with Y concentrations higher than an average Y concentration distributed at nanometer order sizes and intervals. The present invention further provides an Mg alloy characterized by having a chemical composition consisting of Y: more than 0.1 at % and a valance of Mg and unavoidable impurities, having a microstructure with high Y regions with Y concentrations higher than an average Y concentration distributed at nanometer order sizes and intervals and having an average recrystallized grain size within the range satisfying the following formula 1: ?0.87c+1.10<log d<1.14c+1.Type: ApplicationFiled: March 26, 2008Publication date: July 1, 2010Applicants: TOYOTA JIDOSHA KABUSHIKI KAISHA, National Institute for Materials ScienceInventors: Tetsuya Shoji, Akira Kato, Toshiji Mukai, Hidetoshi Somekawa
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Patent number: 7677134Abstract: A forged product is made of a magnesium alloy and includes a through hole making portion to make a through hole that runs in a predetermined direction, and a bottom portion that lies on a plane intersecting with the predetermined direction. The through hole includes a first portion that has been formed by a forging process and a second portion that has been formed after the forging process. The second portion of the through hole has shifted toward the bottom portion with respect to the middle of the through hole in the predetermined direction.Type: GrantFiled: December 17, 2007Date of Patent: March 16, 2010Assignee: Yamaha Hatsudoki Kabushiki KaishaInventors: Toru Kitsunai, Osamu Matsushita
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Publication number: 20100012234Abstract: The present invention relates to a process for manufacturing a process for manufacturing a part made of a magnesium alloy, comprising a step of forging a block of said alloy followed by a heat treatment, characterized in that the alloy is a casting alloy based on 85% magnesium, and containing, by weight: 0.2 to 1.3% zinc; 2 to 4.5% neodymium; 0.2 to 7.0% rare-earth metal with an atomic weight from 62 to 71; 0.2 to 1% zirconium, and in that the forging is carried out at a temperature above 400° C. In particular the temperature is set between 420 and 430° C. and the forging step comprises a plastic deformation carried out at a slow rate. The process allows to produce parts such as elements of casing for aeronautical machines, operating at a temperature of around 200° C. and having good aging properties.Type: ApplicationFiled: July 19, 2007Publication date: January 21, 2010Applicants: Hispano Suiza, Manoir IndustriesInventors: Pascal Cantrel, Sophie Lubin, Christian Henri Paul Mauhe, Isabelle Robert, Jean Stracchi
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Publication number: 20090032151Abstract: A magnesium base alloy pipe having high strength and toughness is provided along with a method of manufacturing such pipes. A magnesium base alloy pipe, wherein the pipe is produced by drawing a pipe blank of a magnesium base alloy comprising containing either of the following ingredients (1) or (2): (1) about 0.1-12.0 mass % of Al; or (2) about 1.0-10.0 mass % of Zn and about 0.1-2.0 mass % of Zr. The novel alloy pipe is manufactured by a method comprising steps of providing the above-described pipe blank, pointing the pipe blank, and drawing the pointed pipe blank. The drawing step is executed at a drawing temperature above approx. 50° C.Type: ApplicationFiled: September 30, 2008Publication date: February 5, 2009Applicant: SUMITOMO (SEI) STEEL WIRE CORP.Inventors: Yukihiro OISHI, Nozomu Kawabe, Hitoshi Takahashi, Katsumi Wakamatsu
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Publication number: 20090035171Abstract: Provided is a high-strength and high-toughness magnesium alloy which has practical level of both the strength and the toughness for expanded applications of the magnesium alloys, and is a method for manufacturing thereof. The high-strength and high-toughness magnesium alloy of the present invention contains: a atom % in total of at least one metal of Cu, Ni, and Co; and b atom % in total of at least one element selected from the group consisting of Y, Dy, Er, Ho, Gd, Tb, and Tm, while a and b satisfying the following formulae (1) to (3), 0.2?a?10??(1) 0.2?b?10??(2) 2/3a?2/3<b.Type: ApplicationFiled: March 20, 2007Publication date: February 5, 2009Inventors: Yoshihito Kawamura, Michiaki Yamasaki, Takaomi Itoi, Mitsuji Hirohashi
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Publication number: 20080304997Abstract: Disclosed is a wrought magnesium alloy having excellent strength and extrusion or rolling formability, and a method of producing the same. The wrought magnesium alloy comprises 0.1-1.5 at % group IIIa, 1.0-4.0 at % group IIIb, 0.35 at % or less of one selected from the group consisting of groups IIa, IVa, VIIa, IVb, and a mixture thereof, 1.0 at % or less of group IIb, and a balance of Mg and unavoidable impurities and thus has a second phase composite microstructure. The wrought magnesium alloy of the present invention has high strength, toughness, and formability in addition to the electromagnetic wave shield ability of magnesium. Accordingly, the wrought magnesium alloy is a material useful to portable electronic goods, such as notebook personal computers, mobile phones, digital cameras, camcorders, CD players, PDA, or MP3 players, automotive parts, such as engine room hoods, oil pans, or inner panel of door, or structural parts for airplane.Type: ApplicationFiled: March 11, 2005Publication date: December 11, 2008Applicant: PRIMOMETAL CO., LTD.Inventor: Kang-Hyung Kim
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Publication number: 20080279715Abstract: The present invention provides a method for producing a magnesium alloy sheet capable of producing a magnesium alloy sheet having excellent plastic workability such as press workability. The method of the present invention includes rolling a magnesium alloy blank with a reduction roll. The rolling includes controlled rolling performed under the following conditions (1) and (2) wherein M (% by mass) is the Al content in a magnesium alloy constituting the blank: (1) the surface temperature Tb (° C.) of the magnesium alloy blank immediately before insertion into the reduction roll satisfies the following expression: 8.33×M+135?Tb?8.33×M+165 wherein 1.0?M?10.0; and (2) the surface temperature Tr of the reduction roll is 150° C. to 180° C.Type: ApplicationFiled: March 24, 2006Publication date: November 13, 2008Applicant: SUMITOMO ELECTRIC INDUSTRIES, LTD.Inventors: Nobuyuki Mori, Nozomu Kawabe
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Patent number: 7083689Abstract: A method for fabricating a magnesium alloy billet for a thixoforming process capable of enhancing the mechanical properties of a forming product by inducing plastic deformation of an AZ91D magnesium alloy included extrusion and compression and forming a fine recrystallized microstructure from a primary solid phase through an isothermal holding process by a ‘strain induced melt activated process.’ In the case in which the magnesium alloy fabricated according to the present invention is adapted to a material used for a power train part, a chassis part or an interior part of a vehicle, it is possible to fabricate a part having a thick region and a region with a complicated shape. Such a fabrication is impossible in the conventional die casting process.Type: GrantFiled: December 31, 2003Date of Patent: August 1, 2006Assignee: Hyundai Motor CompanyInventor: Soon Chan Park
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Patent number: 7048812Abstract: A magnesium based alloy consists of, by weight: 1.4–1.9% neodymium, 0.8–1.2% rare earth element(s) other than neodymium, 0.4–0.7% zinc, 0.3–1% zirconium, 0–0.3% manganese, and 0–0.1% oxidation inhibiting element(s) the remainder being magnesium except for incidental impurities.Type: GrantFiled: June 20, 2003Date of Patent: May 23, 2006Assignee: Cast Centre Pty LtdInventors: Colleen Joyce Bettles, Christopher Thomas Forwood
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Patent number: 6893515Abstract: The present invention is related to a manufacturing process for highly ductile magnesium alloy, which is processable under plasticization at ambient temperature. The process includes melting in vacuum melt furnace or inert gas protected furnace, teeming into ingot, extrusion or rolling into finished material. Such highly ductile magnesium alloy has extremely excellent plastic deformability at ambient temperature and improves completely the deficiency associated with traditional commercial magnesium alloy that lacks plastic deformability at ambient temperature. The material is suitable for the structural components in automobiles, 3C products, appliances and office automation products.Type: GrantFiled: September 12, 2002Date of Patent: May 17, 2005Assignee: Hsu-Yang Technologies Co., Ltd.Inventors: Jin-Chin Guan, Ming-Tarng Yeh, Jian-Yih Wang
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Patent number: 6818080Abstract: A manufacturing method for a shaped light metal article includes the steps of forming a plastic worked article by plastic working an article for plastic working made of light metal material, and subjecting the plastic worked article to a post-plastic working heat treatment for between 20 minutes and 10 hours at a temperature in a range of 250 to 400° C. As a result, a shaped light metal article is produced with sufficient ductility.Type: GrantFiled: December 4, 2001Date of Patent: November 16, 2004Assignee: Mazda Motor CorporationInventors: Kazuo Sakamoto, Yasuo Uosaki, Nobuo Sakate
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Publication number: 20040206428Abstract: A method for fabricating a magnesium alloy billet for a thixoforming process capable of enhancing the mechanical properties of a forming product by inducing plastic deformation of an AZ91D magnesium alloy included extrusion and compression and forming a fine recrystallized microstructure from a primary solid phase through an isothermal holding process by a ‘strain induced melt activated process.’ In the case in which the magnesium alloy fabricated according to the present invention is adapted to a material used for a power train part, a chassis part or an interior part of a vehicle, it is possible to fabricate a part having a thick region and a region with a complicated shape. Such a fabrication is impossible in the conventional die casting process.Type: ApplicationFiled: December 31, 2003Publication date: October 21, 2004Inventor: Soon Chan Park
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Publication number: 20040163744Abstract: Magnesium-based alloy wire excelling in strength and toughness, its method of manufacture, and springs in which the magnesium-based alloy wire is utilized are made available. The magnesium-based alloy wire contains, in mass %, 0.1 to 12.0% Al, and 0.1 to 1.0% Mn, and is provided with the following constitution. Diameter d that is 0.1 mm or more and 10.0 mm or less; length L that is 1000 d or more; tensile strength that is 250 MPa or more; necking-down rate that is 15% or more; and elongation that is 6% or more. Such wire is produced by draw-forming it at a working temperature of 50° C. or more, and by heating it to a temperature of 100° C. or more and 300° C. or less after the drawing process has been performed.Type: ApplicationFiled: November 29, 2003Publication date: August 26, 2004Inventors: Yukihiro Oishi, Nozomu Kawabe
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Publication number: 20040040635Abstract: The present invention is related to a manufacturing process for highly ductile magnesium alloy, which is processable under plasticization at ambient temperature. The process includes melting in vacuum melt furnace or inert gas protected furnace, teeming into ingot, extrusion or rolling into finished material. Such highly ductile magnesium alloy has extremely excellent plastic deformability at ambient temperature and improves completely the deficiency associated with traditional commercial magnesium alloy that lacks plastic deformability at ambient temperature. The material is suitable for the structural components in automobiles, 3C products, appliances and office automation products.Type: ApplicationFiled: September 12, 2002Publication date: March 4, 2004Applicant: Hsu-Yang Technologies Co., Ltd.Inventors: Jin-Chin Guan, Ming-Tarng Yeh, Jian-Yih Wang
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Patent number: 6544357Abstract: A new class of light or reactive elements and monophase &agr;′-matrix magnesium- and aluminum-based alloys with superior engineering properties, for the latter being based on a homogeneous solute distribution or a corrosion-resistant and metallic shiny surface withstanding aqueous and saline environments and resulting from the control during synthesis of atomic structure over microstructure to net shape of the final product, said &agr;′-matrix being retained upon conversion into a cast or wrought form. The manufacture of the materials relies on the control of deposition temperature and in-vacuum consolidation during vapor deposition, on maximized heat transfer or casting pressure during all-liquid processing and on controlled friction and shock power during solid state alloying using a mechanical milling technique.Type: GrantFiled: January 31, 1997Date of Patent: April 8, 2003Inventors: Franz Hehmann, Michael Weidemann
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Patent number: 6511560Abstract: A thin, forged magnesium alloy casing is integrally constituted by a thin plate with projections on either or both surfaces, and the thin plate is as thin as about 1.5 mm or less. The thin forged casing can be produced by (a) carrying out a first forging step for roughly forging a magnesium alloy plate to form an intermediate forged product under the conditions of a preheating temperature of the magnesium alloy plate of 350-500° C., a die temperature of 350-450° C., a compression pressure of 3-30 tons/cm2, a compressing speed of 10-500 mm/sec. and a compression ratio of 75% or less; and (b) carrying out a second forging step for precisely forging the intermediate forged product under the conditions of a preheating temperature of the intermediate forged product of 300-500° C., a die temperature of 300-400° C., a compression pressure of 1-20 tons/cm2, a compressing speed of 1-200 mm/sec., and a compression ratio of 30% or less.Type: GrantFiled: April 16, 2001Date of Patent: January 28, 2003Assignees: Tokyo Seitan Inc., Sony CorporationInventors: Isao Seki, Shigeo Hama, Shigehiro Taniike, Fukashi Watanabe, Masahiko Kakizaki, Shinji Seki
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Patent number: 6471797Abstract: Disclosed is a quasicrystalline phase-reinforced Mg-based metallic alloy with high warm and hot formability, and making method thereof. The metallic alloy comprises a composition of Mg—1˜10 at % Zn—0.1˜3 at % Y, in which a two-phase region consisting of a quascrystalline phase and a magnesium-based solid solution phase exists. Constituting a matrix structure, the Mg-based solid solution phase (&agr;—Mg) is formed as a primary solid phase upon solidification. The quasicrystalline phase serves as a second phase and forms, together with the Mg-based solid solution phase, a eutectic phase, thereby reinforcing the matrix. The materials obtained through the hot rolling or extrusion of the cast alloy have an increased volume % of the second phase and thus show significantly increased strength.Type: GrantFiled: May 9, 2001Date of Patent: October 29, 2002Assignee: Yonsei UniversityInventors: Do Hyang Kim, Won Tae Kim, Dong Hyun Bae, Eun Soo Park, Seong Hoon Yi
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Patent number: 6350328Abstract: Feed material for use in producing a thixotropic alloy comprising pellets in the form of a solid cylinder having a length to diameter ratio in the range of from 1:1 to 2:1 and a maximum length of 0.250 inch.Type: GrantFiled: June 27, 2000Date of Patent: February 26, 2002Assignee: Rossborough Manufacturing Co. LPInventor: David W. Hostetler