Abstract: A method for producing a 3D-printed tissue substitute is disclosed, utilizing a 3D printing device including a tank including a yield stress fluid in which the material is printed, the printing material delivered by the cartridge includes polyvinyl alcohol and gelatin, the method including a step following which, after printing the material in the yield stress fluid, a printed intermediate device is solidified in the yield stress fluid by lowering the temperature of the tank. The intermediate device is removed from the tank, rinsed and dried in order to obtain the tissue substitute.

Abstract: A series of alloys of Co, Ni, Al, W, Ta, and Cr, wherein the alloy comprises a solid solution of gamma and gamma prime alloy phases, the Ni content is greater than 25% at. %, the Al content is greater than 10 at. %, the Cr content is greater than 2 at. %, and the Ni:Co ratio is between 0.5 and 1.5. In one or more examples, the alloy further comprises one or more of C, B, and a reactive element metal. Embodiments of the alloy simultaneously possess a high solvus temperature, a high fraction of the strengthening ??-L12 phase, good oxidation resistance and highly favorable solidification characteristics.

Abstract: Forming a precipitation hardened composite material having reinforcing particles and precipitated intermetallic particles dispersed in the binder material may involve heat treating the hard composite material at a temperature above a solvus line for the binder material and below a melting point of the binder material and quenching the hard composite material to a temperature below the solvus line of the binder material. At least some of the precipitated intermetallic particles in the precipitation hardened composite material may have at least one dimension less than 1 micron. Such precipitated intermetallic particles may optionally be grown to larger sizes by heat treating the precipitation hardened composite material at a temperature below the solvus line of the binder material.

Abstract: A sliding shoe for supporting a piston of a hydrostatic axial piston machine against a swash plate includes a sliding face that defines a central concentric pressure pocket that is flat in order to stabilize the sliding shoe. The pressure pocket has radial supply grooves in order to ensure an optimal supply of pressure medium to the pressure pocket from a central mouth opening. The radial supply grooves extend through the pressure pocket and as far as a circumferential groove which surrounds the pressure pocket.

Abstract: A sputtering target for a magnetic recording medium, wherein an average grain area of a B-rich phase is 90 ?m2 or less. A process for producing a sputtering target for a magnetic recording medium, wherein an alloy cast ingot is subject to heat treatment, thereafter subject to primary rolling which includes at least one pass of cold rolling, thereafter subject to secondary rolling, and machined to prepare a target. The obtained sputtering target for a magnetic recording medium has few cracks in the B-rich phase and has a high leakage flux density, and by using this target, it is possible to stabilize the discharge during sputtering, suppress arcing which occurs from cracks in the B-rich phase, and suppress the generation of particles.

Abstract: A process for producing a Co-base alloy which has a basic composition including, in terms of mass proportion, 0.1%-10% Al, 3.0-45% W, and Co as the remainder and has an intermetallic compound of the L12 type [Co3 (Al,W)] dispersed and precipitated therein. Part of the Co may be replaced with Ni, Ir, Fe, Cr, Re, or Ru, while part of the Al and W may be replaced with Ni, Ti, Nb, Zr, V, Ta or Hf. The intermetallic compound [Co3 (Al, W)] has a high melting point, and this compound and the matrix are mismatched little with respect to lattice constant. Thus, the cobalt-base alloy can have high-temperature strength equal to that of nickel-base alloys and excellent structure stability.

Abstract: An article and a method for forming the article are disclosed. The article comprising a composition, wherein the composition comprises, by weight percent, about 13.7% to about 14.3% chromium (Cr), about 9.0% to about 10.0% cobalt (Co), about 3.5% to about 3.9% aluminum (Al), about 3.4% to about 3.8% titanium (Ti), about 4.0% to about 4.4% tungsten (W), about 1.4% to about 1.7% molybdenum (Mo), about 1.55% to about 1.75% niobium (Nb), about 0.08% to about 0.12% carbon (C), about 0.005% to about 0.040% zirconium (Zr), about 0.010% to about 0.014% boron (B), and balance nickel (Ni) and incidental impurities. The composition is substantially free of tantalum (Ta) and includes a microstructure substantially devoid of Eta phase.

Abstract: A cobalt-nickel base alloy is disclosed. The alloy includes, in weight percent: greater than about 4 % of Al, about 10 to about 20 % of W, about 10 to about 40 % Ni, about 5 to 20 % Cr and the balance Co and incidental impurities. The alloy has a microstructure that is substantially free of a CoAl phase having a B2 crystal structure and configured to form a continuous, adherent aluminum oxide layer on an alloy surface upon exposure to a high-temperature oxidizing environment. A method of making an article of the alloy includes: selecting the alloy; forming an article from the alloy; solution-treating the alloy; and aging the alloy to form an alloy microstructure that is substantially free of a CoAl phase having a B2 crystal structure, wherein the alloy is configured to form a continuous, adherent aluminum oxide layer on an alloy surface upon exposure to a high-temperature oxidizing environment.

Abstract: A method of processing a metal alloy includes heating to a temperature in a working temperature range from a recrystallization temperature of the metal alloy to a temperature less than an incipient melting temperature of the metal alloy, and working the alloy. At least a surface region is heated to a temperature in the working temperature range. The surface region is maintained within the working temperature range for a period of time to recrystallize the surface region of the metal alloy, and the alloy is cooled so as to minimize grain growth. In embodiments including superaustenitic and austenitic stainless steel alloys, process temperatures and times are selected to avoid precipitation of deleterious intermetallic sigma-phase. A hot worked superaustenitic stainless steel alloy having equiaxed grains throughout the alloy is also disclosed.

Abstract: The present invention describes a method of manufacturing a near-net shaped hollow shaft useful for high power applications such as gearboxes for wind energy industry. The method involves providing a concast bloom (of a round or rectangular or of any polygonal cross section) or an as-cast round ingot from which a hollow perform is prepared using hollow die punching, followed by process of heat treatment, proof-machining and stress relieving.

Abstract: Method for producing a soft magnetic alloy strip suited to be mechanically cut, having a chemical composition comprising, by weight: 18% ?? Co ? 55%? 0% ? V + W ? 3% 0% ? Cr ? 3% 0% ? Si ? 3% 0% ? Nb ? 0.5%? 0% ? B ? 0.05%?? 0% ? C ? 0.1%? 0% ? Zr + Ta ? 0.5%? 0% ? Ni ? 5% 0% ? Mn ? 2% the rest being iron and impurities from production, according to which a strip obtained by hot rolling a semi-finished product consisting of the alloy is cold-rolled to obtain a cold-rolled strip with a thickness less than 0.6 mm, After the cold rolling, the strip is running annealed by passing it through a continuous furnace at a temperature between the order/disorder transition temperature of the alloy and the ferritic/austenitic transformation point of the alloy, followed by rapid cooling to a temperature below 200° C.

Abstract: This invention provides a technique for rendering bio-toxicity such as allergy toxicity derived from Ni trace impurity, i.e., nickel toxicity, which is unavoidably present in a bio-Co—Cr—Mo alloy or an Ni-free stainless steel alloy unharmful, characterized in that an element selected from the group consisting of the group 4, 5 and 13 elements of the periodic table, particularly an element selected from the group consisting of the group 4 elements of the periodic table, is added to the alloy composition. The additive element is preferably an element selected from the group consisting of zirconium and titanium, more preferably zirconium.

Abstract: Disclosed herein is a method of treating a component comprising solution treating the component for a period of about 4 to about 10 hours at a temperature of about 1750 to about 1850° F.; cooling the component to a temperature of about 1490 to about 1520° F. at an average rate of 1° F./min to about 25° F./min; stabilizing the component at about 1450 to about 1520° F. for a period of from about 1 to about 10 hours; cooling the component to room temperature; precipitation aging the component by heating the component to a first precipitation aging temperature of about 1275 to about 1375° F. for about 3 to about 15 hours; cooling the component at an average rate of 50 to about 150° F./hour to a second precipitation aging temperature of about 1100 to about 1200° F. for a time period of about 2 to about 15 hours; and cooling the component.

Abstract: Disclosed herein is a method of treating a component comprising solution treating the component for a period of about 4 to about 10 hours at a temperature of about 1750 to about 1850°F.; cooling the component to a temperature of about 1580 to about 1650°F. at an average rate of 1°F./min to about 25°F./min; stabilizing the component at about 1580 to about 1650°F. for a period of about 1 to about 10 hours; cooling the component to room temperature; precipitation aging the component at a first precipitation aging temperature of about 1275 to about 1375°F. for about 3 to about 15 hours; cooling the component at an average rate of 50 to about 150°F./hour to a second precipitation aging temperature of about 1100 to about 1200°F. for a time period of about 2 to about 15 hours; and cooling the component.

Abstract: A process for producing a Co-base alloy which has a basic composition including, in terms of mass proportion, 0.1%-10% Al, 3.0-45% W, and Co as the remainder and has an intermetallic compound of the L12 type [Co3 (Al, W)] dispersed and precipitated therein. Part of the Co may be replaced with Ni, Ir, Fe, Cr, Re, or Ru, while part of the Al and W may be replaced with Ni, Ti, Nb, Zr, V, Ta or Hf. The intermetallic compound [Co3 (Al, W)] has a high melting point, and this compound and the matrix are mismatched little with respect to lattice constant. Thus, the cobalt-base alloy can have high-temperature strength equal to that of nickel-base alloys and excellent structure stability.

Abstract: Provided is a Co—Cr—Pt—B-based alloy sputtering target having no more than 10 cracks of 0.1 to 20 ?m in a B-rich phase in a 100 ?m×100 ?m area (field of view). Additionally provided is a method for producing this Co—Cr—Pt—B-based alloy sputtering target including the steps of hot forging or hot rolling a Co—Cr—Pt—B-based alloy cast ingot, thereafter performing cold rolling or cold forging thereto at an elongation rate of 4% or less, and machining the ingot to prepare a target having no more than 10 cracks of 0.1 to 20 ?m in a B-rich phase in a 100 ?m×100 ?m area (field of view), or, hot forging or hot rolling the ingot, thereafter quenching the ingot to ?196° C. to 100° C., and machining the ingot to prepare a target. The target of the present invention has high magnetic flux density and few microcracks in a B-rich layer, and thus stabilizes discharge and minimizes arcing.

Abstract: A Co-base alloy which has a basic composition including, in terms of mass proportion, 0.1%-10% Al, 3.0-45% W, and Co as the remainder and has an intermetallic compound of the Ll2 type [Co3(Al,W)] dispersed and precipitated therein. Part of the Co may be replaced with Ni, Ir, Fe, Cr, Re, or Ru, while part of the Al and W may be replaced with Ni, Ti, Nb, Zr, V, Ta or Hf. The intermetallic compound [Co3(Al, W)] has a high melting point, and this compound and the matrix are mismatched little with respect to lattice constant. Thus, the cobalt-base alloy can have high-temperature strength equal to that of nickel-base alloys and excellent structure stability.

Abstract: A process for manufacturing a component with a base of Co—Cr—Mo alloys having values of average ultimate elongation at 800° C. greater than 10% and of average yielding load at 800° C. greater than 400 MPa, comprising: obtaining a sintered component by additive sintering of powders of Co—Cr—Mo alloys containing carbides irregularly dispersed in the molten matrix; Conducting a first heat treatment on the sintered component for solubilization of the carbides at a temperature of between 1100° C. and 1300° C. for at least 2 hours to form a solubilization intermediate; and cooling the solubilization intermediate at a cooling rate at least equal to that of cooling in air to form a cooled intermediate; and conducting a second heat treatment on the cooled intermediate at a temperature of between 700° C. and 1000° C.

Abstract: A method of producing a seamless, tubular product includes centrifugally casting a corrosion resistant alloy into a tubular workpiece having an inner diameter and an outer diameter. The method then removes material from the inner diameter of the workpiece and subjects the workpiece to at least about a 25% wall reduction at a temperature below a recrystallization temperature of the workpiece using a metal forming process. The metal forming process includes radial forging, rolling, pilgering, and/or flowforming.

Abstract: A Co—Cr—Mo alloy with nitrogen addition composed of 26 to 35% by weight of Cr, 2 to 8% by weight of Mo, 0.1 to 0.3% by weight of N, and balance of Co is subjected to solution treatment and then subjected to isothermal aging treatment holding the alloy at 670 to 830° C. for a predetermined period of time to form a multi-phase structure composed of an ?-phase and a Cr nitride by means of an isothermal aging effect. After cooling, the alloy subjected to reverse transformation treatment in which the alloy is heated at a temperature range of 870 to 1100° C. for reverse transformation to a single ?-phase from the multi-phase structure composed of an ?-phase and a Cr nitride.

Abstract: Cobalt based alloys exhibiting high-temperature mechanical strength in an oxidizing medium are provided. The alloys are free of W and Hf and include the following elements in percentage by weight of the alloy: 23 to 34% Cr; 6 to 12% Ni; 6.0 to 10% Ta; 0.3 to 1.2% C; less than 3% Fe; less than 1% Si; less than 0.5% Mn; less than 0.1% Zr; and a balance of cobalt and impurities. Ta/C molar ratios of the alloys are at least 0.3.

Abstract: A metallic material is made from at least one refractory metal or an alloy based on at least one refractory metal. The metallic material has an oxygen content of about 1,000 to about 30,000 ?g/g and the oxygen is interstitial.

Abstract: A cobalt-nickel base alloy is disclosed. The alloy includes, in weight percent: greater than about 4% of Al, about 10 to about 20% of W, about 10 to about 40% Ni, about 5 to 20% Cr and the balance Co and incidental impurities. The alloy has a microstructure that is substantially free of a CoAl phase having a B2 crystal structure and configured to form a continuous, adherent aluminum oxide layer on an alloy surface upon exposure to a high-temperature oxidizing environment. A method of making an article of the alloy includes: selecting the alloy; forming an article from the alloy; solution-treating the alloy; and aging the alloy to form an alloy microstructure that is substantially free of a CoAl phase having a B2 crystal structure, wherein the alloy is configured to form a continuous, adherent aluminum oxide layer on an alloy surface upon exposure to a high-temperature oxidizing environment.

Abstract: A process of forming a prosthetic implant component, such as the femoral component of a knee replacement prosthesis. The process comprises the steps of: (i) forming a prosthetic component having a shape at least approximating the desired final shape of the component from a metal alloy; (ii) subjecting the component to a relatively elevated temperature and pressure followed by a cooling regime; (iii) machining the surface of the component; (iv) polishing the surface of the component.

Abstract: A Co-based alloy having a fundamental composition of Co—Al binary system containing 3-15% Al and having lamellar structure wherein f.c.c. structure ?-phase and ?(B2)-phase are superimposed on each other in layers, which Co-based alloy is modified so as to have a porous surface layer region effective for chemical retaining capability, sustained release, biocompatibility, etc. through selective removal of either the ?-phase or the ?-phase from the surface layer. As a third component, at least one member selected from among Ni, Fe, Mn, Ga, Cr, V, Ti, Mo, Nb, Zr, W, Ta, Hf, Si, Rh, Pd, Ir, Pt, Au, B, C and P may be contained in a total amount of 0.001 to 60%.

Abstract: Apparatus and methods are provided for cooling workpieces. A cooling gas is directed toward a surface of a workpiece. The workpiece is moved relative to the flow of cooling gas. The cooling gas may include at least a first component that is gaseous at a reference ambient condition and a second component that is a liquid at the ambient condition. The second component may be delivered as a gas or as droplets.

Abstract: A method for producing a filled skutterudite-based alloy includes the steps of melting alloy raw material that includes a rare earth metal R that is at least one species selected from among La, Ce, Pr, Nd, Sm, Eu and Yb, a transition metal T that is at least one species selected from among Fe, Co, Ni, Os, Ru, Pd, Pt and Ag, and metallic antimony Sb to form a melt; and rapidly quenching the melt through strip casting to form a solidified product that is the filled skutterudite-based alloy advantageously usable for a thermoelectric element.

Abstract: A high-temperature member for use in a gas turbine, the member being formed from a new wear-resistant alloy having good wear resistance as well as good ductility, is disclosed. The member was developed to prevent wear and damage that occur due to vibration while the turbine is running. The high-temperature member for use in a gas turbine is formed from a new cobalt-based wear-resistant alloy which is composed of a cobalt-chromium matrix and refractory metals, with the content of hard particles (such as carbide) reduced. The refractory metals promote work hardening, thereby improving wear resistance. The reduced content of hard particles contributes to good ductility.

Abstract: A Co—Cr—Mo-based alloy includes: 63 mass %?Co<68 mass %; 15 mass %?Cr<26 mass %; 10 mass %?Mo<19 mass %; and the balance of inevitable impurities, wherein the total amount of Cr and Mo is from 32 mass % to 37%. The mass magnetic susceptibility of the alloy is 7×4?·10?9 m3/kg or less at room temperature, and the Vickers hardness number (Hv) of the alloy is 400 or more.

Abstract: A method for recovering a catalyst for a fuel cell includes a collection step in which a catalyst is collected by attracting, using a magnetic force, a magnetic material contained in at least one of the catalyst and a carrier on which the catalyst is supported. A system for recovering a catalyst for a fuel cell includes a collection device that attracts, using a magnetic force, a magnetic material contained in at least one of a catalyst and a carrier on which the catalyst is supported.

Abstract: Embodiments of the present invention provide methods of processing cobalt alloys including, in weight percent, from 26 to 30 chromium, from 5 to 7 molybdenum, and greater than 50 cobalt, the methods comprises cold working and aging the alloys such that after aging the cobalt alloys have a hardness of at least Rockwell C 50. Other embodiments provide methods of selectively cold working at least one portion of a cobalt alloy, and subsequently aging the alloy, such after aging, the selectively cold worked portions of the alloy have a higher hardness value then portions of the alloy that were not selectively cold worked. The present invention also discloses cobalt alloys, implants, and articles of manufacture made from cobalt alloys within the present invention.

Abstract: Methods for manufacturing components capable of transporting a liquid including providing a mold, placing at least one core made from a core material into the mold, injecting a component material into the mold about the core to produce a green component, heating the green component to burn out the core and produce a brown component, and sintering the brown component to produce a finished component capable of transporting a liquid wherein the finished component is from about 95% to about 99% dense.

Abstract: A Co based alloy including at least one member selected from among 0.01 to 10% Fe, 0.01 to 30% Ni and 0.01 to 25% Mn, which Co based alloy has a metal structure wherein ?-phase of h.c.p. structure having been generated by heat-induced or stress-induced transformation is formed in a ratio of 10 vol. % or more. According to necessity, there may be added at least one member selected from among 0.01 to 10% Al, 0.01 to 35% Cr, to 20% V, 0.01 to 15% Ti, 0.01 to 30% Mo, 0.01 to 10% Nb, to 3% Zr, 001 to 30% W, 0.01 to 10% Ta, 0.01 to 5% Hf, 0.01 to 8% Si, 0.001 to 3% C, 0.001 to 3% B, 0.001 to 3% P and 0.001 to 3% misch metal. The Co based alloy exhibits high elastic deformation capability and is good in ductility and workability. The Co based alloy is used as a functional material of, for example, sensor or actuator capable of displacement control by magnetic field application.

Abstract: This invention provides a technique for rendering bio-toxicity such as allergy toxicity derived from Ni trace impurity, i.e., nickel toxicity, which is unavoidably present in a bio-Co—Cr—Mo alloy or an Ni-free stainless steel alloy unharmful, characterized in that an element selected from the group consisting of the group 4, 5 and 13 elements of the periodic table, particularly an element selected from the group consisting of the group 4 elements of the periodic table, is added to the alloy composition. The additive element is preferably an element selected from the group consisting of zirconium and titanium, more preferably zirconium.

Abstract: A Co-base alloy which has a basic composition including, in terms of mass proportion, 0.1%-10% Al, 3.0-45% W, and Co as the remainder and has an intermetallic compound of the Ll2 type [Co3(Al,W)] dispersed and precipitated therein. Part of the Co may be replaced with Ni, Ir, Fe, Cr, Re, or Ru, while part of the Al and W may be replaced with Ni, Ti, Nb, Zr, V, Ta or Hf. The intermetallic compound [Co3(Al, W)] has a high melting point, and this compound and the matrix are mismatched little with respect to lattice constant. Thus, the cobalt-base alloy can have high-temperature strength equal to that of nickel-base alloys and excellent structure stability.

Abstract: An article is presented where the article comprises an alloy having a minor phase dispersed within a matrix phase and a plurality of substantially equiaxed grains. The article further comprises a continuous gradient in grain size from a first grain size at an outer surface of the article to a second grain size at an inner portion of the article, wherein the first grain size is less than the second grain size. Methods for forming the article using high deformation processing are also presented, where the processing includes extruding the feedstock material through a die having a twist channel configured to apply a torsional strain to the feedstock material as it passes through the die to form an extruded billet.

Abstract: A metallic structure having a graded microstructure is provided. The metallic structure comprises a graded region comprising a plurality of grains having a gradient in grain size varying as a function of position between a first median grain size at an outer region and a second median grain size at an inner region and a plurality of dispersoids dispersed within the microstructure. The first median grain size is different from the second median grain size. A method of forming a metallic structure having a graded microstructure is also provided. The method comprises: providing a metallic structure comprising at least one reactive species; diffusing at least one reactant at a controlled rate from an outer region of the metallic structure towards an inner region of the metallic structure to form a gradient in reactant activity; reacting the reactant with the reactive species to form a plurality of dispersoids; and heat treating the metallic structure to achieve grain growth so as to form a graded microstructure.

Abstract: Methods are provided for forming a plurality of permanent magnets with two different north-south magnetic pole alignments for use in microelectromechanical (MEM) devices. These methods are based on initially magnetizing the permanent magnets all in the same direction, and then utilizing a combination of heating and a magnetic field to switch the polarity of a portion of the permanent magnets while not switching the remaining permanent magnets. The permanent magnets, in some instances, can all have the same rare-earth composition (e.g. NdFeB) or can be formed of two different rare-earth materials (e.g. NdFeB and SmCo). The methods can be used to form a plurality of permanent magnets side-by-side on or within a substrate with an alternating polarity, or to form a two-dimensional array of permanent magnets in which the polarity of every other row of the array is alternated.

Abstract: A method is provided for separating superalloy metal powder from contaminants, such as process-produced contaminants, by enhancing the magnetic properties thereof in a carburizing atmosphere followed by magnetic separation of the contaminants from the superalloy metal powder to thereby enhance the concentration of the contaminants. Heating or mechanical agitation or both are employed to resist agglomeration of the metal powder before magnetic separation thereof from the contaminants. Certain preferred times and temperatures are disclosed.

Abstract: A method for refining the grain size of alloys which undergo ferromagnetic to paramagnetic phase transformation and an alloy produced therefrom. By subjecting the alloy to a timed application of a strong magnetic field, the temperature of phase boundaries can be shifted enabling phase transformations at lower temperatures.

Abstract: A method is provided for separating superalloy metal powder from contaminants, such as process-produced contaminants, by enhancing the magnetic properties thereof, such as by oxidizing or leaching of chromium, for example, followed by magnetic separation of the contaminants from the superalloy metal powder to thereby enhance the concentration of the contaminants. Heating conditions or mechanical agitation or both are employed to resist agglomeration of the metal powder before magnetic separation thereof from the contaminants. Certain preferred times and temperatures are disclosed.

Abstract: A method of manufacturing a wear resistant shoe (26) includes upsetting (46) one end portion (38) of cylindrical member to work harden that portion to a substantial depth, machining (48) the cylindrical member portion to finished dimensions and surface hardening (56) a face (28 or 34) of the machined cylindrical member portion. The cylindrical member may comprise rod stock of a diameter less than the greatest diameter of the finished shoe and be upset or swaged to axially reduce and radially increase the dimensions of the one end portion. A hollow region (30) is formed in an opposite rod stock end portion and the periphery (50) of the hollow region is crimped about a rounded end (18) of the piston (20). The cold work done during the swaging or forming process provides a foundation for hardened faces comprising balance (28) and auxiliary balance (34) lands, forms a crude shape of the shoe, and imparts work hardening and wear property improvements.

Abstract: A method of manufacturing a wear resistant shoe (26) includes upsetting (46) one end portion (38) of cylindrical member to work harden that portion to a substantial depth, machining (48) the cylindrical member portion to finished dimensions and surface hardening (56) a face (28 or 34) of the machined cylindrical member portion. The cylindrical member may comprise rod stock of a diameter less than the greatest diameter of the finished shoe and be upset or swaged to axially reduce and radially increase the dimensions of the one end portion. A hollow region (30) is formed in an opposite rod stock end portion and the periphery (50) of the hollow region is crimped about a rounded end (18) of the piston (20). The cold work done during the swaging or forming process provides a foundation for hardened faces comprising balance (28) and auxiliary balance (34) lands, forms a crude shape of the shoe, and imparts work hardening and wear property improvements.

Abstract: In accordance with the invention, nanostructured metallic materials having high tensile strength and increased ductility are prepared by providing a metallic material, deforming the metallic material to form a plurality of dislocation cell structures, annealing the material at a temperature from about 0.3 to about 0.7 of its absolute melting temperature, and cooling the annealed metallic material. The result is a nanostructured metal or alloy having increased tensile strength as compared with the corresponding coarse-grained material and substantially greater ductility as compared with nanostructured material made by conventional processes. Using this process applicants have made nanostructured alloys with tensile strengths in excess of 1.5 Gpa and ductility greater than 1 per cent strain-to-failure. They have also made nanostructured metals with tensile strength in excess of 400 MPa and ductility in excess of 50% strain-to-failure.

Abstract: The present invention relates to producing cobalt having a low oxygen and a low oxide inclusion content for use as a sputter target thereby reducing the arcing and metal defects during sputtering commonly associated with high-oxygen cobalt sputter targets. Notably, the method for reducing the oxygen content and the oxide inclusion content in cobalt are separate processes which may be combined in successive order to procuce a low-oxygen cobalt sputter target having a low oxide inclusion content. The reduction in oxygen content preferably is performed prior to reducing the oxide inclusion content. Accordingly, the artisan will appreciate that one process can be performed without the other depending upon whether a reduction in oxygen or oxide inclusions is preferred in a desired cobalt sputter target.

Abstract: The invention relates to a cobalt-based alloy having mechanical strength at high temperature, in particular in an oxidizing or corrosive medium, essentially comprising the following elements (the proportions being shown as percentage by weight of the alloy):

Abstract: An ingot of material which is normally too brittle to allow successful rolling and wrought processing is formed so as to have a thickness-to-width ratio of less than about 0.5 and is annealed in a temperature range of 1000° F. to 2500° F. for a preselected time. The ingot is then rolled in a temperature range of 1500° F. to 2500° F. Additional/optional annealing of the resulting rolled plate in a temperature range of 500° F. to 2000° F., or between room temperature and 1500° F., and/or a final annealing between 500° F. and 1500° F., is possible. Sputtering targets are cut out of the rolled plate and used for the manufacture of storage disks.

Abstract: A high purity cobalt sputter target is disclosed which contains a face centered cubic (fcc) phase and a hexagonal close packed (hcp) phase, wherein the value of the ratio of X-ray diffraction peak intensity, Ifcc(200)/Ihcp(10 1), is smaller than the value of the same ratio in a high purity cobalt material obtained by cooling fcc cobalt to room temperature from the high temperature at which it is molten. High purity cobalt is defined as having an oxygen content of not more than 500 ppm, a Ni content of not more than 200 ppm, contents of Fe, Al and Cr of not more than 50 ppm each, and Na and K of less than 0.5 ppm. The disclosed sputter target is manufactured by subjecting the material to cold-working treatments (less than 4221C). Annealing the material, at a temperature in the range 300-4221C for several hours, between cold working treatments significantly increases the amount of cold work which could be imparted into the material.

Abstract: An ingot of material which is normally too brittle to allow successful rolling and wrought processing is formed so as to have a thickness-to-width ratio of less than about 0.5 and is annealed in a temperature range of 1000° F. to 2500° F. for a preselected time. The ingot is then rolled in a temperature range of 1500° F. to 2500° F. Additional/optional annealing of the resulting rolled plate in a temperature range of 500° F. to 2000° F., or between room temperature and 1500° F., and/or a final annealing between 500° F. and 1500° F., is possible. Sputtering targets are cut out of the rolled plate and used for the manufacture of storage disks.

Abstract: A method of manufacturing a wear resistant shoe (26) includes upsetting (46) one end portion (38) of cylindrical member to work harden that portion to a substantial depth, machining (48) the cylindrical member portion to finished dimensions and surface hardening (56) a face (28 or 34) of the machined cylindrical member portion. The cylindrical member may comprise rod stock of a diameter less than the greatest diameter of the finished shoe and be upset or swaged to axially reduce and radially increase the dimensions of the one end portion. A hollow region (30) is formed in an opposite rod stock end portion and the periphery (50) of the hollow region is crimped about a rounded end (18) of the piston (20). The cold work done during the swaging or forming process provides a foundation for hardened faces comprising balance (28) and auxiliary balance (34) lands, forms a crude shape of the shoe, and imparts work hardening and wear property improvements.