Apparatus For Graining And Separating Crystals Patents (Class 159/45)
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Patent number: 11752446Abstract: A plant for concentrating a tartaric acid solution includes a first and a second evaporation unit arranged in series, a pump for feeding a diluted tartaric acid solution into the first evaporation unit, a barometric condenser placed downstream of the second evaporation unit, and a system for feeding a first low-temperature vapor into the first evaporation unit. A process for concentrating tartaric acid includes providing a plant according to the above description, performing a first concentration, by evaporation, of the diluted tartaric acid solution, inside the first evaporation unit, and performing a second concentration, by evaporation, of the partially concentrated tartaric acid solution from the first evaporation unit, inside the second evaporation unit.Type: GrantFiled: August 28, 2020Date of Patent: September 12, 2023Assignee: DISTILLERIE MAZZARI S.P.A.Inventor: Emidio Margheritini
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Patent number: 11377414Abstract: A plant for concentrating a tartaric acid solution includes a first and a second evaporation unit arranged in series, a pump for feeding a diluted tartaric acid solution into the first evaporation unit, a barometric condenser placed downstream of the second evaporation unit, and a system for feeding a first low-temperature vapor into the first evaporation unit. A process for concentrating tartaric acid includes providing a plant according to the above description, performing a first concentration, by evaporation, of the diluted tartaric acid solution, inside the first evaporation unit, and performing a second concentration, by evaporation, of the partially concentrated tartaric acid solution from the first evaporation unit, inside the second evaporation unit. The plant and process have the advantages of ensuring low energy consumption, allowing concentration of solutions tending to crystallization, and allowing the continuous measurement of the tartaric acid concentration to be concentrated.Type: GrantFiled: August 28, 2020Date of Patent: July 5, 2022Assignee: DISTILLERIE MAZZARI S.P.AInventor: Emidio Margheritini
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Patent number: 10815132Abstract: The present invention relates to the waste water treatment field, and discloses apparatus and method for treating waste water containing ammonium salts, which contains NH4+, SO42?, Cl?, and Na+. In the method of the present invention, the pH value of the waste water to be treated is adjusted to a specific range in advance; sodium sulfate crystal and relatively concentrated ammonia are obtained by first evaporation, and then sodium chloride crystal and relatively dilute ammonia is obtained by second evaporation; alternatively, sodium chloride crystal and relatively concentrated ammonia is obtained by third evaporation, and then sodium sulfate crystal and relatively dilute ammonia are obtained by fourth evaporation. The method of the present invention can recover ammonia, sodium sulfate, and sodium chloride from the waste water respectively, so that the resources in the waste water can be reused as far as possible.Type: GrantFiled: April 20, 2018Date of Patent: October 27, 2020Assignees: China Petroleum & Chemical Corporation, Sinopec Catalyst Co., Ltd.Inventors: Xiping Yin, Ye Li, Songyuan Gu, Zhijian Liu, Tao Wang, Jin'ai Gao, Yuhua Chen, Yan Zhou, Ling Yang, Zhiwei Yuan, Hongliang Yi, Tao An, Fuzu Liu, Zhimin Zhang, Shupeng Xu
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Patent number: 10544064Abstract: Method and fluidized bed reactor for the production of granules, such as granules of urea or ammonium nitrate. The reactor comprises at least one granulation compartment with air inlets, and an air moving device downstream the granulation compartment, e.g., downstream one or more scrubbers. The air moving device is configured to draw air through said one or more air inlets into the granulation compartment.Type: GrantFiled: October 28, 2015Date of Patent: January 28, 2020Assignee: YARA INTERNATIONAL ASAInventors: Jaap Voorhans, André Kayaert, Luc Vanmarcke
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Patent number: 10040697Abstract: A method for static mixing in a waste water settling tank to increase the percentage of recovery of entrained solids from the waste water comprising a settling tank having a recirculation ring and a hopper bottom defining a sludge hopper, a fluid deflector centrally disposed within the space contained in the hopper bottom having a flat portion, and an inlet pipe for introduction of waste water containing second entrained solids into the settling tank and having a discharge outlet in proximity to the underside of the deflector dome and a nozzle facing downward. Influent waste water is directed vertically downward toward the flat portion and upward into the center of the fluid deflector which distributes the influent radially into contact, preferably turbulent, with previously introduced waste water containing first entrained solids to cause coalescence of the first and second entrained solids to form larger particles having increased settling velocity.Type: GrantFiled: October 3, 2015Date of Patent: August 7, 2018Assignee: ClearCove Systems, Inc.Inventors: Terry Wright, Qausarali Goriawala
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Patent number: 10040004Abstract: A method for static mixing in a waste water settling tank to increase the percentage of recovery of entrained solids from the waste water comprising a settling tank having a hopper bottom defining a sludge hopper, a deflector dome centrally disposed within the space contained in the hopper bottom, and an inlet pipe for introduction of waste water containing second entrained solids into the settling tank and having a discharge outlet in proximity to the underside of the deflector dome. Influent waste water is directed vertically upward into the center of the deflector dome which distributes the influent radially into contact, preferably turbulent, with previously introduced waste water containing first entrained solids to cause coalescence of the first and second entrained solids to form larger particles having increased settling velocity.Type: GrantFiled: September 11, 2015Date of Patent: August 7, 2018Assignee: ClearCove Systems, Inc.Inventors: Terry Wright, Kimberly A. Miller, Timothy D. McCrossen
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Patent number: 9776104Abstract: Disclosed are processes and apparatuses for producing a crystalline product. The processes and apparatuses may extend the operational time of an evaporative crystallizer by providing an internal volume or large deposit inventory for fouling deposits to reside without impacting the unit operation.Type: GrantFiled: December 14, 2012Date of Patent: October 3, 2017Assignee: Dow Global Technologies LLCInventors: Timothy C. Frank, J. W. Moore, Paul A. Larsen, Pramod D. Patil, Robert M. Whittingslow, Paul A. Gillis
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Patent number: 9440862Abstract: A device and method of accelerating the evaporation of wastewater and concentration of solids wherein an evaporative material contacts wastewater allowing the wastewater to migrate onto the surface of the evaporative material where the sun and wind evaporates the wastewater in an accelerated manner due to the configuration of the evaporative material.Type: GrantFiled: April 29, 2013Date of Patent: September 13, 2016Inventor: Shafiq Ur Rahman
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Patent number: 8894810Abstract: A floating salt farm in which its purpose is to produce crystallized salt and bittern at offshore locations through the evaporation process using extracted seawater. The floating salt farm components can be consisted of a seawater tank, an evaporator tank, a heating tank, a deposit tank, a storage tank, and photovoltaic panels, which these components are installed onto the buoyant foundation. The evaporator tank component can consist of an evaporator plate and an evaporator bin. The evaporator plate, which captures the produced crystallized salt during the evaporation process, has a sieve surface. The contents inside the evaporator bin can affect the properties of the produced crystallized salt and bittern, such as their mineral compositions, during the evaporation process. The seawater can be extracted from desired water depths and/or in the proximity of volcanic sites, in which the seawater can have affected mineral compositions due to volcanic activity.Type: GrantFiled: October 28, 2012Date of Patent: November 25, 2014Assignee: Pioli Systems Inc.Inventor: Jae Hyun Lim
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Publication number: 20140338843Abstract: Disclosed are processes and apparatuses for producing a crystalline product. The processes and apparatuses may extend the operational time of an evaporative crystallizer by providing an internal volume or large deposit inventory for fouling deposits to reside without impacting the unit operation.Type: ApplicationFiled: December 14, 2012Publication date: November 20, 2014Inventors: Timothy C. Frank, J.W. Moore, Paul A. Larsen, Pramod D. Patil, Robert M. Whittingslow, Paul A. Gillis
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Patent number: 8877016Abstract: Systems and methods for solar steam generation are described. The systems and methods include moving at least one frame mounted optical focusing lens to track the sun in two axes and disposing a water boiler at a focus of each optical focusing lens. Raw water is pumped through an inlet at a bottom of each boiler and solar energy is concentrated, using each optical focusing lens, on each boiler, heating the raw water in each boiler and evaporating steam from the raw water. The steam exits each boiler, via a steam outlet pipe. Remaining salts and solids in each boiler are ground by rotation of salt grinding-cleaning gears. These ground salts and solids are drained and/or pumped out of each boiler from an exit in the bottom of each boiler.Type: GrantFiled: November 6, 2011Date of Patent: November 4, 2014Assignee: King Saud UniversityInventors: Mazen A. Ba-abbad, Hany A. Al-Ansary, Essam A. Al-Ammar
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Patent number: 8763426Abstract: A system and method for separating at least a part of the solids from brine having an initial temperature T1, the system comprising a crystallizer comprising a crystallizer inlet for receiving therein said brine, a crystallizer first outlet for discharging vapor having a first pressure P1, evaporated from at least a part of said brine, and a crystallizer second outlet for discharging a slurry having a final temperature T2 lower than said initial temperature T1; a separator comprising a separator inlet for receiving therein said slurry, a separator first outlet for discharging therefrom said part of the solids separated from said slurry, and a separator second outlet for discharging therefrom a remaining liquid having a temperature substantially equal to T2; a compressor comprising a compressor inlet for receiving therein said vapor, and a compressor outlet for discharging therefrom a compressed vapor having a second pressure P2 higher than said pressure P1; and a condenser comprising a condenser first inlet fType: GrantFiled: December 10, 2009Date of Patent: July 1, 2014Assignee: I.D.E. Technologies Ltd.Inventors: Yeshayahu Rotstein, Tuvia Zisner, Joseph Weinberg, Avraham Ophir
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Patent number: 8696870Abstract: Device for desalinating sea water comprising a unit (10) for spraying sea water in the form of droplets, a unit (20) for vaporizing the droplets into steam, a unit (30) for separating steam from salt particles, and a unit (40) for condensing steam into fresh water. The spraying unit comprises a sea water entry (12), an ambient-temperature dry air entry (14), and a device for generating acoustic waves at a frequency greater than 1 MHz focused by means of nozzles (17) receiving the sea water coming from the sea water entry so as to obtain microdroplets having a diameter comprised between about 2.5 microns and about 5 microns.Type: GrantFiled: December 15, 2008Date of Patent: April 15, 2014Inventors: Charles Pallanca, Henri Renggli, Gil Ching
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Patent number: 8636973Abstract: The present invention relates to means and methods for producing crystals or crystalline substances. In particular, crystals or crystalline substances which are useful as pharmaceutical ingredients can be manufactured.Type: GrantFiled: June 22, 2011Date of Patent: January 28, 2014Assignee: Biosyn Arzneimittel GmbHInventors: Thomas Stiefel, Ortwin Kottwitz
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Patent number: 7681643Abstract: A process for conditioning of wastewater treatment brines for deep well injection during recovery of heavy hydrocarbon oils in situ. High pressure steam is used to mobilize oil, which is recovered in a mixture of oil and produced water. The produced water is pre-treated by removing residual oil. The remaining water is acidified and steam stripped to remove non-hydroxide alkalinity and non-condensable gases, and is then fed to a crystallizing evaporator, where it is evaporated from a circulating brine slurry to produce (1) a distillate stream having a trace amount of residual solutes, and (2) evaporator blowdown stream containing, as dissolved or suspended solids, substantially all of the solutes from the produced water feed. The distillate stream is used as boiler feedwater, either directly or after polishing. The evaporator blowdown is conditioned to remove substantially all suspended solids and to produce a clear brine solution for deep well injection.Type: GrantFiled: September 22, 2006Date of Patent: March 23, 2010Assignee: GE Ionics, Inc.Inventor: William F. Heins
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Patent number: 7438129Abstract: A process for treating produced water to generate high pressure steam. Produced water from heavy oil recovery operations is treated by first removing oil and grease. Feedwater is then acidified and steam stripped to remove alkalinity and dissolved non-condensable gases. Pretreated produced water is then fed to an evaporator. Up to 95% or more of the pretreated produced water stream is evaporated to produce (1) a distillate having a trace amount of residual solutes therein, and (2) evaporator blowdown containing substantially all solutes from the produced water feed. The distillate may be directly used, or polished to remove the trace residual solutes before being fed to a steam generator. Steam generation in a packaged boiler, such as a water tube boiler having a steam drum and a mud drum with water cooled combustion chamber walls, produces 100% quality high pressure steam for down-hole use.Type: GrantFiled: June 8, 2005Date of Patent: October 21, 2008Assignee: GE Ionics, Inc.Inventor: William F. Heins
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Patent number: 7428926Abstract: A process for treating produced water to generate high pressure steam. Produced water from heavy oil recovery operations is treated by first removing oil and grease. Pretreated produced water is then fed to an evaporator. Up to 95% or more of the pretreated produced water stream is evaporated to produce (1) a distillate having a trace amount of residual solutes therein, and (2) evaporator blowdown containing substantially all solutes from the produced water feed. The distillate may be directly used, or polished to remove the trace residual solutes before being fed to a steam generator. Steam generation in a packaged boiler, such as a water tube boiler having a steam drum and a mud drum with water cooled combustion chamber walls, produces 100% quality high pressure steam for down-hole use.Type: GrantFiled: June 8, 2005Date of Patent: September 30, 2008Assignee: GE Ionics, Inc.Inventor: William F. Heins
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Patent number: 7150320Abstract: A process for treating produced water to generate high pressure steam. Produced water from heavy oil recovery operations is treated by first removing oil and grease. If necessary, the pH is then adjusted, normally downward, releasing at least some carbonate alkalinity as free carbon dioxide. Pretreated produced water is then fed to an evaporator. Up to 95% or more of the pretreated produced water stream is evaporated to produce (1) a distillate having a trace amount of residual solutes therein, and (2) evaporator blowdown containing substantially all solutes from the produced water feed. The distillate may be directly used, or polished to remove the trace residual solutes before being fed to a steam generator. Steam generation in a packaged boiler, such as a water tube boiler having a steam drum and a mud drum with water cooled combustion chamber walls, produces 100% quality high pressure steam for down-hole use.Type: GrantFiled: June 9, 2004Date of Patent: December 19, 2006Inventor: William F. Heins
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Patent number: 7077201Abstract: An evaporation based method of treating produced water from heavy oil production. A produced water from heavy oil recovery operations treated by first removing oil and grease to a desired level, preferably to about twenty parts per million, or less. If necessary, the pH is then adjusted, normally downward and by acid addition, to release at least some carbonate alkalinity as free carbon dioxide. Preferably, all non-hydroxide alkalinity is removed, or substantially so, by introducing the feedwater into a decarbonator. Feedwater is introduced into an evaporator, and the feedwater is evaporated to a selected concentration factor to produce (1) a distillate having a small amount of residual solutes, and (2) evaporator blowdown containing residual solids. Distillate may be directly used for steam generation in a once-through steam generator, or polished by ion exchange or electrodeionization prior to feed to a packaged boiler.Type: GrantFiled: November 30, 2002Date of Patent: July 18, 2006Assignee: GE Ionics, Inc.Inventor: William F. Heins
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Patent number: 7008516Abstract: According to a method of desalinating sea water, sea water sampled from deep sea is injected into a decompression chamber of a reduced pressure tank having a steam chamber, steam at an atmospheric pressure superheated to a boiling temperature or higher by high-frequency heating is supplied to the steam chamber at a surrounding of the decompression chamber at an interval of a heat conducting wall therebetween, water in the sea water is evaporated by heating sea water in the decompression chamber and the evaporated water is condensed to thereby provide fresh water. Concentrated sea water remains in the decompression chamber and therefore, the method can be utilized also as a method of concentrating sea water. Salt can be obtained by further evaporating the water of the concentrated sea water as necessary.Type: GrantFiled: September 26, 2002Date of Patent: March 7, 2006Inventors: Yoshinobu Kozuka, Yoshimasa Shimbo
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Patent number: 6984292Abstract: There is disclosed a method and apparatus for treating produced water from a heavy oil thermal recovery unit to achieve water recovery and recycle levels of greater than 80% and as high as 100% to achieve zero discharge criteria. The method includes the initial steps of capturing the waste heat energy from the high pressure steam separator located downstream of the steam generators. Further, transferring the heat energy into a heated separator and reboiler exchanger to distill oil reservoir produced water and recover distilled water and a concentrated brine or solid product. The heated separator concentrated stream is circulated through the reboiler exchanger to maintain from 1% to about 50% mass vapour in the stream returning to the heated separator and prevent fouling and scaling. The apparatus includes a low pressure waste energy separator, heated separator and vapour compressor in combination with a forced circulation circuit to generate the distilled water.Type: GrantFiled: January 21, 2003Date of Patent: January 10, 2006Assignee: EnCana CorporationInventors: Steve Kresnyak, Alex Braun
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Patent number: 6866750Abstract: The present invention provides a device and method for desalinating saltwater which utilizes a heatable vessel wherein is placed a sufficient quantity of a salt which will absorb water of crystallisation and which has a dissolution index of not higher than 10?24. Saltwater is then added to the vessel and brought into contact with the salt, so that the salt will bind water from the saltwater and form a crystal hydrate. The excess saltwater with salt concentrate is drained from the vessel. The salt which has absorbed water tom the saltwater and formed a crystal hydrate is then heated in the vessel, and the pure water from the crystal hydrate is released as water vapour, which is collected and cooled to obtain desalinated water.Type: GrantFiled: November 8, 2000Date of Patent: March 15, 2005Assignee: Gougel Industri ABInventors: Michail Gougel, Mark Novikov
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Patent number: 6849155Abstract: This invention provides a concentrator capable of drawing out a concentrate of a constant concentration. The concentrator includes a heater having a heating medium that has been heated to a temperature not less than the boiling point of a solution fed to the concentrator—whereby said heater heats the solution to evaporate the solvent to a vapor to make a mixture of the vapor and a liquid—and a gas-liquid separator for dividing the mixture into the liquid and the vapor. The concentrator provides for returning the liquid separated in the gas-liquid separator to the heater, for drawing out a portion of the liquid separated in the gas-liquid separator, for detecting the concentration of an intended component in the drawn out liquid, and for controlling the liquid draw-out so that when the concentration is above a predetermined threshold, liquid draw-out commences, and when the concentration is below the threshold, liquid draw-out stops.Type: GrantFiled: November 12, 2002Date of Patent: February 1, 2005Assignee: Daicel Chemical Industries, Ltd.Inventors: Kazuyuki Akita, Toshiharu Minoda
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Publication number: 20040211526Abstract: The present invention discloses an improved evaporation method compressing an evaporation material from power into compressed particles or tablets at a predetermined pressure, temperature, and time; since the compressed evaporation material being consistent in crystallization property is more even and denser than powder, therefore the efficiency of the thermal conductivity becomes higher and the efficiency of heating more stable.Type: ApplicationFiled: April 28, 2003Publication date: October 28, 2004Inventors: Shu-Wen Chang, Gwo-Sen Lin, Chi-Min Chen
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Patent number: 6733636Abstract: A method of treating produced water from heavy oil production to provide feedwater for the production of high quality steam. A produced water from heavy oil recovery operations is initially treated by first removing oil and grease to a desired level, preferably to about twenty parts per million, or less. The pH is then adjusted, normally downward and by acid addition, to release at least some carbonate alkalinity as free carbon dioxide. Preferably, all non-hydroxide alkalinity is removed, or substantially so, by introducing the feedwater into a decarbonator. In some cases, the pH may be raised (without, or subsequent to decarbonation, depending upon water chemistry) preferably by caustic addition, to maintain silica solubility in the feedwater.Type: GrantFiled: May 8, 2000Date of Patent: May 11, 2004Assignee: Ionics, Inc.Inventor: William F. Heins
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Patent number: 6699369Abstract: A method for removing dissolved solids, particularly salts, from water. An apparatus for performing the inventive method is disclosed. The aqueous solution to be treated, for example sea water, is atomized using special non-pneumatic nozzles, and sprayed into an evaporation chamber through which air, heated by waste heat, is blown. The micro-droplets undergo rapid evaporation in the chamber, resulting in the separation of the salt solids from the vapor phase of the water. The mixture of suspended solids and water vapor is filtered to remove and collect the salts, and the water vapor is condensed to collect the salt-free water.Type: GrantFiled: August 10, 2001Date of Patent: March 2, 2004Assignee: Aquasonics InternationalInventors: William Francis Hartman, Larry Joe Kepley, Jerry Van Fox
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Patent number: 6649027Abstract: A water reclamation system for a closed environment includes a mixer that receives brine. A processor is downstream of the mixer, with the processor distilling substantially salt-free water from the brine in the substantial absence of salt crystallization. A crystallizer subsystem is downstream of the processor, with the crystallizer subsystem crystallizing salt from the brine and recycling the brine to the mixer.Type: GrantFiled: March 7, 2000Date of Patent: November 18, 2003Assignee: Honeywell International Inc.Inventors: Allen Kent MacKnight, Alex M. Lubman
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Patent number: 6582552Abstract: A liquid evaporation method and apparatus wherein the contamination of the heat transfer surfaces is avoided by using a special circulating fluid. The liquid to be evaporated is heated in direct contact with the circulating fluid and conveyed to a vapor separation tank. In the evaporator according to the invention, heat transfer surface contamination may be limited by mixing the liquid to be evaporated with the circulating fluid only after the heat exchanger so that the heat surface contaminating liquid to be evaporated does not make direct contact with the heat surface.Type: GrantFiled: September 14, 2001Date of Patent: June 24, 2003Assignee: Rinheat OyInventor: Pentti Juhola
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Publication number: 20030094245Abstract: This invention provides a concentrator capable of drawing out a concentrate of a constant concentration.Type: ApplicationFiled: November 12, 2002Publication date: May 22, 2003Inventors: Kazuyuki Akita, Toshiharu Minoda
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Patent number: 6551466Abstract: A method and apparatus for removing a contaminant from a fluid feed stream containing the contaminant. The method includes the steps of providing a feed stream and heating it in a first step to at least partially remove some of the contaminants and recover energy from a concentrate and distillate generated. Further heating the feed stream in a second heating step in a heated separator generates a saturated vapor fraction and a concentrated liquid contaminant fraction. The vapor fraction may be compressed to generate a temperature differential in the reboiler exchanger with the vapor fraction being passed into contact with a reboiler exchanger to provide a stream of condensed vapor from the reboiler. The stream may be circulated through the reboiler exchanger and the heated separator to maintain from about 1% to about 50% by mass vapor in the stream.Type: GrantFiled: December 22, 1999Date of Patent: April 22, 2003Assignee: Aqua Pure Ventures Inc.Inventors: Steve Kresnyak, Edward Warchol, Robert Becker
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Publication number: 20030047290Abstract: The invention relates to a method and installation for the dry fractionation of edible oils and fats and related products, said method comprising the steps of:Type: ApplicationFiled: July 30, 2002Publication date: March 13, 2003Inventors: Marc Hendrix, Marc Kellens
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Patent number: 6500216Abstract: A method and an apparatus of producing natural salt or fresh water by treating sea water in an extremely short period of time and with high efficiently. The distilled water and salt components are treated for expediting crystallization of the salt components by evaporating water components by atomizing sea water and blowing warm wind thereto. During this treatment, there are provided a method and an apparatus of arranging net or cloth at one stage or a plurality of stages in a midway of a flow of the evaporated water components and adhering the salt components on the net or the cloth when the evaporated water components pass through the net or the cloth.Type: GrantFiled: July 30, 1999Date of Patent: December 31, 2002Inventor: Masakatsu Takayasu
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Publication number: 20020117268Abstract: A continuous vacuum pan includes a cylindrical housing having a vertical axis, at least one liquid heating pan within the housing, and a vertical tube, floating calandria within the liquid heating pan. The vertical tube floating calandria has a downcomer between its periphery and the periphery of the liquid heating pan, and a gap is provided between the bottom of the calandria and the bottom of the liquid heating pan. Radially extending baffles in the liquid heating pan define a plurality of compartments located in series with one another, the compartments ranging from a first upstream compartment to a downstream output compartment. Ports are provided in all of the baffles except in the baffle between the output compartment and the first compartment. The ports are spaced from the bottom of the liquid heating pan, permitting communication between the compartments.Type: ApplicationFiled: January 10, 2002Publication date: August 29, 2002Inventors: Paul Martin Schorn, Leon Smith
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Patent number: 6391361Abstract: A method is provided for producing a powdery product from a protein-containing liquid having a dry solid content, providing (1) a first feeding stream of protein-containing liquid, (2) a second feeding stream having a higher content of dry solids than the first feeding stream, (3) mixing the first feeding stream and second feeding stream to obtain a main stream, (4) heating the main stream in a heater, (5) transferring the heated main stream to a separator, (6) flash separating volatile components from the heated main stream and obtaining a main stream protein-containing concentrate, and subjecting at least a part of the main stream protein-containing concentrate to a drying step to obtain a powdery product. The amount of water to be evaporated in the drying step is significantly reduced, requiring smaller drying equipment, less air and less energy, and yields a powdery product having higher “bulk density”.Type: GrantFiled: September 22, 2000Date of Patent: May 21, 2002Assignee: APV Nordic Anhydro A/SInventors: Lars Valentin Peters, Ole Teglhus Kragh
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Patent number: 6335045Abstract: A method for concentration of a liquid food product, the liquid product having a dry solid content of a least 40 percent and the liquid food product comprising crystallizable components, comprising the steps of heating the liquid food product to a temperature above the crystallization temperature of the liquid food product in a first heat exchanger; transferring the heated liquid food product to a first separator; flash separating volatile components from the heated liquid food product; and obtaining a liquid concentrate of the liquid food product.Type: GrantFiled: May 31, 2000Date of Patent: January 1, 2002Assignee: APV Anhydro A/SInventors: Lars Valentin Peters, Ole Teglhus Kragh
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Patent number: 6218592Abstract: A method for the treatment of radioactive evaporator concentrates from the evaporation system of nuclear plants comprises the steps of (a) freeing the evaporator concentrates from undissolved components, (b) crystallizing the sodium sulfate contained in the evaporator concentrates as Glauber's salt (Na2SO4.10 H2O) on an immersion cooler, (c) recrystallizing the Glauber's salt deposited on the immersion cooler, (d) optionally, repeating the recrystallization step (c) once or several times, (e) separating essentially inactive sodium sulfate from the process, and (f) recycling the depleted evaporator concentrates of step (a) to the evaporation system.Type: GrantFiled: March 17, 2000Date of Patent: April 17, 2001Assignee: Kernkraftwerke Gundremmingen Betriebsgesellschaft mbHInventors: Manfred Lasch, Udo Krumpholz
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Patent number: 6086722Abstract: A process for minimizing evaporator scaling during the recovery of liquids and solids from the aqueous effluent discharged during a partial oxidation gasification, wherein the aqueous effluent contains ammonium chloride (NH.sub.4 Cl). The aqueous effluent is evaporated to produce a distillate water and a brine having an NH.sub.4 Cl concentration of about 10 to 60 weight percent. The brine can be further concentrated and ammonium chloride crystals are recovered. The distillate water is recycled to the gasification reaction. No effluent discharges to the environment.Type: GrantFiled: July 9, 1997Date of Patent: July 11, 2000Assignee: Texaco Inc.Inventors: George Henry Webster, Jr., Byron Von Klock, Dinh-Cuong Vuong, John Saunders Stevenson, Steven Robert Johnson
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Patent number: 6027607Abstract: A process for extracting salt from brine contained in at least one open evaporation basin. At least part of the brine is heated in a heating unit located outside the evaporation basis and returned to the evaporation basin. The heating unit is driven by waste heat from a recooling industrial plant. According to this process, climatic values and the degree of recooling are measured and evaluated in a control unit. At least part of the heated brine and some non-heated brine are sprayed by a spraying device of the evaporation basin. The amount of sprayed brine is regulated by the control unit depending on the measured data.Type: GrantFiled: July 31, 1998Date of Patent: February 22, 2000Assignee: Krebs & Co. AGInventor: Vicente Gracia Corniel
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Patent number: 6001246Abstract: A process wastewater treatment plant, and a process relating thereto, which converts process wastewater generated in battery manufacturing and the like into clean process water and sodium sulfate salt by treating the process wastewater to remove impurities and contaminants, including debris, oil/grease, heavy metal oxides, lead and other heavy metals, suspended solids, bacteria, organic compounds, and/or gases, from the wastewater to obtain a clean neutral sodium sulfate brine, subjecting the brine to heat to obtain distilled water and sodium sulfate salt, and purifying the distilled water by reverse osmosis for reuse as clear process water.Type: GrantFiled: May 18, 1998Date of Patent: December 14, 1999Inventor: Charles M. Suenkonis
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Patent number: 5984981Abstract: A salt making method comprising putting a crude salt-water mixture (5) comprising crude salt or rock salt and bittern in a vessel (1), blowing the air from a pipe (7) into the mixture (5) with a pump (9), crystallizing the component salt out of the mixture (5), and precipitating the salt as a common salt (S) at the bottom of the vessel (1). The remainder of the mixture (5) is discharged through a filter (13) into a tank (17), where it is stored as a concentrated brine (15), which is then discharged through a filter layer (16) and a drain (18), and crude salt is dissolved therein to recycle as a crude salt-water mixture. The concentrated brine (15) may be used after being mixed with the extracts of aloe, mozuku (Nemacystis decipiens), rice bran, etc. The air may be blown into the mixture (5) under heating.Type: GrantFiled: August 27, 1997Date of Patent: November 16, 1999Assignee: Showa MiyagiInventor: Showa Miyagi
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Patent number: 5857269Abstract: A process for manufacturing improved granulated fatty alcohol sulfates. The process includes slowly drying and mechanically mixing the fatty alcohol sulfate.Type: GrantFiled: March 11, 1996Date of Patent: January 12, 1999Assignee: Zohar Detergent FactoryInventors: Oded Vashitz, Amatzia Galler
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Patent number: 5575923Abstract: An improved salt basket for dewatering solids, particularly salts resulting from evaporation of industrial wastewaters. The salt basket system includes a pressurizable vessel having a screen floor situated above a bottom liquid collection head, an inlet for the brine/solids slurry from which solids are to be separated and dried, an inlet for air, an inlet for steam (the latter two inlets may be combined, where convenient), an inlet for solids free feed, and a drain outlet (these two may be combined where convenient into a combination feed/drain connection). Preferably, an automated system for introducing feed brine and for removing the solids product is provided. For safety, a pivotally attached lower door has a hydraulic failsafe closure mechanism and locking safety latches to prevent the door from inadvertently opening.Type: GrantFiled: June 7, 1995Date of Patent: November 19, 1996Assignee: Ionics, IncorporatedInventors: Robert L. Solomon, Ferris C. Standiford, Joseph Bostjancic, Dan Peterson, George R. Jones
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Patent number: 5472622Abstract: An improved salt basket for dewatering solids, particularly salts resulting from evaporation of industrial wastewaters. The salt basket system includes a pressurizable vessel having a screen floor situated above a bottom liquid collection head, an inlet for the brine/solids slurry from which solids are to be separated and dried, an inlet for air, an inlet for steam (the latter two inlets may be combined, where convenient), an inlet for solids free feed, and a drain outlet (these two may be combined where convenient into a combination feed/drain connection). Preferably, an automated system for introducing feed brine and for removing the solids product is provided. For safety, a pivotally attached lower door has a hydraulic failsafe closure mechanism and locking safety latches to prevent the door from inadvertently opening.Type: GrantFiled: April 20, 1993Date of Patent: December 5, 1995Assignee: Ionics, IncorporatedInventors: Robert L. Solomon, Ferris C. Standiford, Joseph Bostjancic, Dan Peterson, George R. Jones
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Patent number: 5423288Abstract: An apparatus for producing seed crystals in melts has a vertically oriented, closed vessel having a vessel base and having at least one inlet for the melt and having at least one outlet opening for the inoculated melt provided with seed crystals. A preferably annular region of the vessel wall is constructed as a cooling surface. In the interior of the vessel there is arranged a scraping unit which comprises a motor-driven rotating shaft which extends axially through the vessel as far as a point just short of the vessel base. At its end towards the vessel base, the shaft is provided with at least one scraping arm which, starting from the lower end of the shaft close to the vessel base, extends first in the direction towards the vessel wall and thence substantially parallel to the annular cooling surface and axially parallel to the drive shaft.Type: GrantFiled: February 24, 1994Date of Patent: June 13, 1995Assignee: Ciba-Geigy CorporationInventors: Ricardo Schneeberger, Hans Horisberger, Rudolf Buttiker
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Patent number: 5366716Abstract: Sulphur dioxide is separated from the flue gases of a cellulose pulp mill by absorbing it into a sodium sulphite solution. Sulphur dioxide is regenerated from the sodium bisulphite solution produced by an evaporation-crystallization method utilizing thermo-compressor evaporation technique. A lamella evaporator is utilized as the evaporator-crystallizer, the evaporator being divided into separate compartments for ease of cleaning the lamella surfaces. The recovered concentrated sulphur dioxide can be used wherever desired, for example for the production of chlorine dioxide.Type: GrantFiled: November 30, 1992Date of Patent: November 22, 1994Assignee: A. Ahlstrom CorporationInventor: Esko Mattelmaki
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Patent number: 5133807Abstract: A two-stage crystallization for the continuous production of sugar crystals from syrup comprises crystallizing the syrup in a first stage by subjecting the syrup to a sufficient heat of evaporation to produce a massecuite comprising water and a small content of dry material and having a low supersaturation coefficient, and subjecting the massecuite to flash evaporation of a certain volume of water and a notable increase in the supersaturation, and subsequently effectuating crystallization of the massecuite produced in the first stage by cooling in a second stage.Type: GrantFiled: April 17, 1991Date of Patent: July 28, 1992Assignee: FCBInventor: Jacques De Cremoux
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Patent number: 5122233Abstract: An apparatus including a device 1 for separating organic components from a process mixture, a vacuum evaporation device 4 for partially drying the mineral salts or mixtures thereof, a device 5 for thermal treatment of the partially dried mineral salts or mixtures thereof from the vacuum evaporation device 4, a condenser 7 for condensing the humid vapors from the vacuum evaporation device 4 and a device 9 for reverse osmosis treatment of the condensate as well as suitable conveying devices between the parts of the apparatus.Type: GrantFiled: April 23, 1990Date of Patent: June 16, 1992Inventor: Charles Zampieri
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Patent number: 5006204Abstract: An apparatus including an evaporator, a pre-crystallizer, a spray dryer and a fluid bed for drying whey and a rotating disc having a cone-shaped upper surface is provided for receiving partially dried whey from the spray dryer and delivering the whey to the fluid bed while permitting crystallization of the whey as it rests on the surface of the disc.Type: GrantFiled: October 31, 1988Date of Patent: April 9, 1991Assignee: A/S Niro AtomizerInventor: Jens P. Jensen
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Patent number: 4369091Abstract: A spray drying apparatus with a drying chamber (10) in which a liquid product is atomized by means of an atomizing wheel (11) and dried by means of warm drying gas or flue gas introduced through a tube (14) which is directed towards the bottom side of the atomizing wheel. In order to avoid adherence of particulate material present within the drying chamber (10) to the bottom side of the atomizing wheel (11) clearing or obstructing gas, preferably atmospheric air, is blown upwardly towards the bottom side of the atomizing wheel from a clearing gas inlet (18).Type: GrantFiled: January 22, 1981Date of Patent: January 18, 1983Assignee: A/S Niro AtomizerInventor: Peter E. Solver
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Patent number: 4352717Abstract: Apparatus for producing substantially spherical grain ferrite powder comprising a vertical cylindrical vessel in which a slurry of ferrite-forming powdered raw materials in alcohol is sprayed under applied pressure through a spray nozzle into a high temperature atmosphere of between 700.degree.-1500.degree. C. to allow the combustion of sprayed alcohol therein, thereby instantaneously producing spherical grain-ferrite powder. A hot air guide is provided along the inner surface of the wall of the vertical vessel extending upward in a spiral for providing a hot air current rising spirally upwardly within the vessel to provide a high temperature atmosphere above the spray nozzle.Type: GrantFiled: January 3, 1978Date of Patent: October 5, 1982Assignee: Dowa Mining Co., Ltd.Inventors: Yasuo Watanabe, Seizi Isoyama, Yoshikazu Yamamichi