Hydration And/or Gelatinization Patents (Class 162/187)
  • Patent number: 11879213
    Abstract: The present invention relates to a high-strength fibre composition comprising fibres up to 7 mm long with a viscosity of between 10 and 20 cP. The fibres present in said composition are distributed according to the length thereof, thereby guaranteeing high strength. The fibre composition according to the invention can also be redispersible. The use of the fibre composition according to the invention and an article comprising said composition are also disclosed.
    Type: Grant
    Filed: December 10, 2019
    Date of Patent: January 23, 2024
    Assignee: SUZANO S.A.
    Inventors: Elenice Pereira Maia, Fábio Carucci Figliolino
  • Patent number: 11814794
    Abstract: A cellulose fiber molded product having improved tensile elastic modulus and a method for manufacturing the molded product is provided. The cellulose fiber molded product contains cellulose fibers as the main component, in which the cellulose fibers contain pulp and defibrated fibers, and the defibrated fibers contain microfibrillated cellulose. The method for manufacturing the molded product includes preparing a cellulose fiber slurry using the pulp and the defibrated fibers, forming wet paper from the cellulose fiber slurry, and dehydrating, pressurizing, and heating the wet paper. The defibrated fibers include microfibrillated cellulose, or microfibrillated cellulose and cellulose nanofibers.
    Type: Grant
    Filed: September 18, 2019
    Date of Patent: November 14, 2023
    Assignee: Daio Paper Corporation
    Inventors: Takaaki Imai, Takahiro Miyoshi, Junya Okawa
  • Patent number: 11674006
    Abstract: Mineral wool insulation products are provided. The mineral wool insulation includes a plurality of mineral wool fibers and a wax emulsion applied to the mineral wool fibers. The wax emulsion imparts excellent water resistance and thermal performance properties to the mineral wool insulation.
    Type: Grant
    Filed: September 18, 2019
    Date of Patent: June 13, 2023
    Assignee: Owens Corning Intellectual Capital, LLC
    Inventors: Scott W. Schweiger, Christopher A. Stoneburg
  • Patent number: 11131062
    Abstract: The invention relates to a method for producing paper, board or the like. The method comprises obtaining a thick stock comprising cellulose fibres, forming a fibrous web and drying of drying the fibrous web. A strength agent system, which comprises at least one synthetic or natural polymer, or their mixture, and microfibrillated parenchymal cellulose material originating from non-wood sources, is added to the thick stock. The invention relates also to paper or board produced by the method.
    Type: Grant
    Filed: July 16, 2020
    Date of Patent: September 28, 2021
    Assignee: Kemira Oyj
    Inventors: Kaisa Karisalmi, Tom Lundin, Mikko Virtanen, Antti Laukkanen, Jason McKee
  • Patent number: 10858618
    Abstract: A detergent composition and processes for making and using same. A detergent composition that includes cellulose fibers to improve the deposition and/or retention of encapsulated benefit agent onto fabrics.
    Type: Grant
    Filed: October 2, 2017
    Date of Patent: December 8, 2020
    Assignee: The Procter & Gamble Company
    Inventors: Susana Fernandez-Prieto, Pieter Jan Maria Saveyn, Johan Smets
  • Patent number: 9816230
    Abstract: The present invention is a hydrated, nanocellulose nonwoven sheet and method for manufacturing the nanocellulose sheet having dermatologically active ingredients. The sheet is formed through a high pressure or vacuum filtration process from a dilute suspension. This suspension, which contains the nanocellulose, may also contain dermatologically active ingredients. The dermatologically active ingredients are incorporated into the unwoven sheet. The dilute suspension may contain binding agents that improve the strength of the nonwoven nanocellulose sheet. These binding agents can also be cross-linked after the formation of the sheet by applying other chemical agents or treating the sheet after formation.
    Type: Grant
    Filed: December 31, 2015
    Date of Patent: November 14, 2017
    Assignee: Innovatech Engineering, LLC
    Inventors: David Haldane, Joshua Kearney, Jesyca Turner, Raghuram Dhumpa
  • Patent number: 9266968
    Abstract: An advantageous and effective process for obtaining carboxymethyl cellulose (CMC) from agro-industrial residues, comprising the steps of a) Preparing the raw material, wherein the raw material is washed, dried, grounded and washed again; b) a pumping step, wherein the product obtained from the step a) is reacted with sodium hydroxide; c) a synthesis step, wherein consists in grounding the pulp; adding a solution of isopropanol and distilled water under stirring at room temperature; adding NaOH aqueous solution up to the alkalization of the mixture; adding monochloroacetic acid in isopropanol; filtrating; suspending in methanol solution and neutralizing with acetic acid. The CMC obtained from the process can be employed in a several industrial processes.
    Type: Grant
    Filed: May 9, 2013
    Date of Patent: February 23, 2016
    Assignees: VALE S.A., UNIVERSIDADE FEDERAL DO ESPIRITO SANTO
    Inventors: Leonidio Stegmiller, Jose Antonino Alves e Silva Reis, Reinaldo Walmir De Jesus, Liliane Durans de Moraes Costa, Antonio Alberto Ribeiro Fernandes, Erica Dutra Albuquerque, Jeferson da Silva Correa, Mauricio Kuster Cunha, Marlon Christian Marianelli Bastos, Patricia Machado Bueno Fernandes, Poliana Belisário Zorzal
  • Patent number: 8945346
    Abstract: Described herein is nanocellulose produced by introducing a mixture of cellulose based fiber raw material and water through a refining gap, having a width smaller than 0.1 mm. In the refining gap, the fiber raw material is subjected to processing forces varying in the direction of introducing said mixture, by means of refining zones provided in the gap one after each other in the feeding direction, whereby the refining surfaces differ in surface patterning and/or surface roughness. The mixture of fiber raw material and water is guided past the refining surfaces in the feeding direction to different locations in the refining zone by by-pass channels provided in the stator. The width of the refining gap is maintained by the combined effect of the feeding pressure of the mixture of fiber raw material and water fed into the refining gap and the axial force of the rotor.
    Type: Grant
    Filed: December 30, 2011
    Date of Patent: February 3, 2015
    Assignee: Upm-Kymmene Corporation
    Inventors: Tomas Bjoerkqvist, Timo Koskinen, Markus Nuopponen, Annikki Vehniaeinen, Sirkka Gustafsson
  • Patent number: 8906198
    Abstract: A method for producing micro fibrillated cellulosic material from pulp where multiple passes through a medium consistency refiner are made either singularly or in combination with low consistency refiners and high consistency refiners.
    Type: Grant
    Filed: October 10, 2013
    Date of Patent: December 9, 2014
    Assignee: Andritz Inc.
    Inventors: Marc Sabourin, Antti Luukkonen
  • Patent number: 7625463
    Abstract: A method for making a fibrous composite, comprising blending a carboxyalkyl cellulose and a galactomannan polymer or a glucomannan polymer in water to provide an aqueous solution; treating the aqueous solution with a first crosslinking agent to provide a gel; drying the gel to provide a solid; comminuting the solid to provide a plurality of particles; combining at least a portion of the plurality of particles with an aqueous suspension comprising cellulose treated with a galactomannan polymer or a glucomannan polymer, and optionally a second crosslinking agent, to provide a mixture; and mixing the mixture with a water-miscible solvent to provide a fibrous composite.
    Type: Grant
    Filed: October 2, 2006
    Date of Patent: December 1, 2009
    Assignee: Weyerhaeuser NR Company
    Inventors: S. Ananda Weerawarna, Su Bing
  • Patent number: 7381294
    Abstract: A method for producing a microfibrillated cellulose, which comprises subjecting a slurry containing a pulp having a solids concentration of 1 to 6 wt % to the treatment with a disc refiner repeatedly ten times or more, to thereby prepare a microfibrillated cellulose having a number average fiber length or 0.2 mm or less and an amount of water hold of 10 mL/g or more, the amount representing the volume of water capable of being held by a unit weight of the cellulose fiber. The method allows the production of a microfibrillated cellulose having high quality with stability and with good efficiency.
    Type: Grant
    Filed: July 15, 2003
    Date of Patent: June 3, 2008
    Assignee: Japan Absorbent Technology Institute
    Inventors: Migaku Suzuki, Yutaka Hattori
  • Patent number: 7226526
    Abstract: The invention relates to a starch and fiber mixture, and the application of a starch and fiber mixture in paper manufacturing. The starch and fiber mixture is applied to a paper mat, after the paper mat is formed. The starch and fiber mixture may be obtained by the selective filtering of white water from the papermaking process, particularly by use of a pressure screen.
    Type: Grant
    Filed: November 22, 2005
    Date of Patent: June 5, 2007
    Assignee: Corn Products International, Inc.
    Inventors: Philip Strong, Brian Edward Ireland, John Gregory Kinney
  • Patent number: 7056460
    Abstract: A process for making an improved gypsum/wood fiber board is described. Products resulting from the process are also described. The process comprises adding a diisocyanate, specifically methylenediphenyldiisocyanate (MDI) to an aqueous slurry of calcium sulfate material and cellulosic fibers, where the MDI is added as an emulsion stable in the conditions in which the slurry is maintained. The process further includes passing the MDI containing slurry onto a flat porous forming surface to form a filter cake; removing a substantial portion of the water from the filter cake through the porous surface; pressing the filter cake to form a board and remove additional water; and drying the board to remove the remaining free water.
    Type: Grant
    Filed: January 14, 2003
    Date of Patent: June 6, 2006
    Assignee: United States Gypsum Company
    Inventor: Mark Englert
  • Patent number: 7011729
    Abstract: The invention relates to a starch and fiber mixture, and the application of a starch and fiber mixture in paper manufacturing. The starch and fiber mixture is applied to a paper mat, after the paper mat is formed. The starch and fiber mixture may be obtained by the selective filtering of white water from the papermaking process, particularly by use of a pressure screen.
    Type: Grant
    Filed: November 12, 2003
    Date of Patent: March 14, 2006
    Assignee: Corn Products International, Inc.
    Inventors: Philip Strong, Brian Edward Ireland, John Gregory Kinney
  • Patent number: 6946058
    Abstract: A process and product of making a tissue product is provided. For example, the method can comprise (a) providing a first papermaking furnish containing refined softwood fibers; (b) providing a second papermaking furnish containing hardwood fibers; (c) incorporating the first and second papermaking furnishes into a tissue web such that the tissue web has a hardwood layer and a softwood layer; (d) contacting the tissue web with a drying surface so that the hardwood layer is disposed adjacent thereto; and (e) removing the tissue web from the drying surface with a creping blade at a creping pocket angle of less than about 82 degrees.
    Type: Grant
    Filed: May 23, 2002
    Date of Patent: September 20, 2005
    Assignee: Kimberly-Clark Worldwide, Inc.
    Inventor: Sheng-hsin Hu
  • Patent number: 6630056
    Abstract: An intensely colored transparent and/or translucent paper has chroma c and brightness L, as measured by a Hunterlab instrument, which measures the Cartesian coordinates a, b, L of a point P of color and its polar coordinates H and c. The paper is such that the ratio of c to L is higher than 30%, preferably higher than 50%. The paper contains a colorant in the stock, preferably 5 to 10% by weight of liquid coloring agent in relation to the weight of the finished paper. The colorant is a coloring agent which fixes directly in the cellulose. The paper is suitable for printing and/or writing.
    Type: Grant
    Filed: December 13, 1999
    Date of Patent: October 7, 2003
    Assignees: Thibierge & Comar, Arjo Wigging Fine Papers Limited
    Inventors: Emeric Thibierge, Jean-Francois Loeillot, James Christopher Body, Robert Graham Bracewell
  • Patent number: 6623848
    Abstract: The invention relates to absorvents for water and aqueous liquids, which are vased on water-swell-able, yet water-insoluble polymers wherein cyclodextrin or cyclodextrin derivatives and zeolites high in silicon have been incorporated ionically, covalently and/or as a result of mechanical inclusion.
    Type: Grant
    Filed: February 14, 2002
    Date of Patent: September 23, 2003
    Assignee: Stockhausen GmbH & Co. KG
    Inventors: Helmut Brehm, Jorg Harren, Jorg Issberner, Richard Mertens
  • Patent number: 6312669
    Abstract: The invention concerns buccodental formulation characterized in that it comprises at least a thickening agent comprising cellulose nanofibrils, said cellulose nanofibrils being substantially amorphous, having a crystallinity index not more than 50%. The invention also concerns said cellulose nanofibrils as thickening agent and/or flavour enhancer in buccodental formulations.
    Type: Grant
    Filed: May 16, 2000
    Date of Patent: November 6, 2001
    Assignee: Rhodia Chimie
    Inventors: Robert Cantiani, Claudie Willemin
  • Patent number: 6183596
    Abstract: A super microfibrillated cellulose having an arithmetic average fiber length of 0.05 to 0.1 mm, a water retention value of at least 350%, a rate of the number of fibers not longer than 0.25 mm of at least 95% based on the total number of the fibers as calculated by adding up, and an axial ratio of the fibers of at least 50. The super microfibrillated cellulose is produced by passing a slurry of a previously beaten pulp through a rubbing apparatus having two or more grinders which are arranged so that they can be rub together to microfibrillate the pulp to obtain microfibrillated cellulose and further super microfibrillate the obtained microfibrillated cellulose with a high-pressure homogenizer to obtain the super microfibrillated cellulose. A coated paper produced with a coating material containing the super microfibrillated cellulose, and a tinted paper produced from a paper stock containing the super microfibrillated cellulose as a carrier carrying a dye or pigment are also provided.
    Type: Grant
    Filed: July 1, 1997
    Date of Patent: February 6, 2001
    Assignee: Tokushu Paper Mfg. Co., Ltd.
    Inventors: Yuji Matsuda, Mariko Hirose, Katsuhiko Ueno
  • Patent number: 5964983
    Abstract: A microfibrillated cellulose containing at least around 80% of primary walls and loaded with carboxylic acids, and a method for preparing same, in particular from sugar beet pulp, wherein the pulp is hydrolysed at a moderate temperature of 60-100.degree. C.; at least one extraction of the cellulose material is performed using a base having a concentration of less than 9 wt. %; and the cellulose residue is homogenised by mixing, grinding or any high mechanical shear processing, whereafter the cell suspension is fed through a small-diameter aperture, and the suspension is subjected to a pressure drop of at least 20 MPa and high-speed sheer action followed by a high-speed deceleration impact. The cellulose is remarkable in that a suspension thereof can easily be recreated after it has been dehydrated.
    Type: Grant
    Filed: July 16, 1997
    Date of Patent: October 12, 1999
    Assignee: General Sucriere
    Inventors: Elisabeth Dinand, Henri Chanzy, Michel R. Vignon, Alain Maureaux, Isabelle Vincent
  • Patent number: 5817262
    Abstract: A process is described for making a gypsum board having improved water resistance. The resulting gypsum board products are also described. The process comprises adding an aqueous siloxane emulsion to an aqueous slurry of a calcium sulfate material and host particles, where the siloxane emulsion is stable under the condition in which the slurry is maintained. The process further includes passing said siloxane containing slurry onto a flat porous forming surface to form a filter cake; removing a substantial portion of the water from the filter cake through the porous surface; pressing the filter cake to form a board and remove additional water; and drying the board to remove the remaining free water and to cause the core of the board to reach a temperature sufficient to cure the siloxane.
    Type: Grant
    Filed: December 20, 1996
    Date of Patent: October 6, 1998
    Assignee: United States Gypsum Company
    Inventor: Mark H. Englert
  • Patent number: 4952278
    Abstract: A paper structure having both high opacity and improved tensile strength through the incorporation of expanded fiber and an opacifying mineral pigment, such as titanium dioxide, is disclosed. The addition of expanded fiber to the paper structure makes it possible to increase the opacity of the paper through the use of the conventional mineral pigments without adversely affecting the paper's tensile strength. These opacified paper structures are especially useful for producing high quality, strong, light weight printing and writing papers which require material pigments for enhanced opacity.
    Type: Grant
    Filed: June 2, 1989
    Date of Patent: August 28, 1990
    Assignee: The Procter & Gamble Cellulose Company
    Inventors: Paul E. Gregory, Kenneth D. Vinson
  • Patent number: 4761203
    Abstract: A process for making mechanically expanded fiber from fibrous material having a fibrillar ultrastructure. The expanded fiber is made by impacting the fibrous material with a plurality of fine media. Impacting by the fine media causes the fibers to expand from a fibrous form to a highly fibrillated form, wherein fibrils separate from, or become substantially disassociated from, the fibrous material ultrastructure. Cellulosic fibrous material is particularly applicable to the process. Cellulosic fibrous material is preferably impacted with fine media at least until the cellulose-containing phase of an aqueous slurry containing 0.5%, by weight, of cellulosic material will retain at least fifty percent of the initial volume of such cellulose-containing phase upon unagitated settling for a period of sixty minutes.
    Type: Grant
    Filed: December 29, 1986
    Date of Patent: August 2, 1988
    Assignee: The Buckeye Cellulose Corporation
    Inventor: Kenneth D. Vinson
  • Patent number: 4692211
    Abstract: High strength, cellulosic-gel-containing kraft paper is made by mechanically refining kraft papermaking pulp to a freeness of CSF 500-800, mixing the resulting refined pulp with from 1 to 10% hydrated cellulosic gel binder, running the resulting fluid mixture into a felted sheet and pressing and drying the sheet to form the kraft paper product.
    Type: Grant
    Filed: May 23, 1986
    Date of Patent: September 8, 1987
    Assignee: Eucatex S.A. Industria e Comercio of Sao Paulo
    Inventor: James R. Roberts
  • Patent number: 4483743
    Abstract: Microfibrillated celluloses having properties distinguishable from all previously known celluloses, are produced by passing a liquid suspension of cellulose through a small diameter orifice in which the suspension is subjected to a pressure drop of at least 3000 psig and a high velocity shearing action followed by a high velocity decelerating impact, and repeating the passage of said suspension through the orifice until the cellulose suspension becomes a substantially stable suspension. The process converts the cellulose into microfibrillated cellulose without substantial chemical change of the cellulose starting material.
    Type: Grant
    Filed: October 18, 1982
    Date of Patent: November 20, 1984
    Assignee: International Telephone and Telegraph Corporation
    Inventors: Albin F. Turbak, Fred W. Snyder, Karen R. Sandberg
  • Patent number: 4481076
    Abstract: Redispersible microfibrillated cellulose is prepared by the addition to a liquid dispersion of the microfibrillated cellulose, an additive compound capable of substantially inhibiting hydrogen bonding between the cellulose fibrils. The microfibrillated cellulose, upon drying, is characterized by having a viscosity when redispersed in water of at least 50% of the viscosity of an equivalent concentration of the original dispersion.
    Type: Grant
    Filed: March 28, 1983
    Date of Patent: November 6, 1984
    Assignee: International Telephone and Telegraph Corporation
    Inventor: Franklin W. Herrick
  • Patent number: 4481077
    Abstract: A process of preparing microfibrillated cellulose comprising adding to never-dried cellulosic pulp an additive compound capable of substantially inhibiting hydrogen bonding of the fibrils in the cellulose and then drying the pulp and additive. Microfibrillation of a suspension of the cellulosic pulp is carried out at considerably increased efficiency if the additive compound is present prior to drying the pulp. The resulting MFC product can be dried and redispersed without substantial loss of viscosity.
    Type: Grant
    Filed: March 28, 1983
    Date of Patent: November 6, 1984
    Assignee: International Telephone and Telegraph Corporation
    Inventor: Franklin W. Herrick
  • Patent number: 4448639
    Abstract: A paper cover sheet material for use in the production of gypsum wallboard, the paper cover sheet material having excellent drainage, porosity and drying properties, and a wallboard product produced therefrom, the paper cover sheet material being produced from fibers comprising a major proportion of cellulose fibers and a minor proportion of mineral fibers, the paper composition additionally comprising a cellulose gel, a latex binder and a flocculating agent, thereby enabling the mineral fibers to be dispersed in an aqueous slurry without materially fracturing the fibers, and retaining the shot present in the mineral fibers without permitting the shot to be released and thereby to contaminate the papermaking equipment. The excellent porosity, drying properties and drainage of the paper permit the gypsum wallboard formed with the paper to be readily set and dried with reduced heat energy requirements.
    Type: Grant
    Filed: June 24, 1982
    Date of Patent: May 15, 1984
    Assignee: United States Gypsum Company
    Inventor: William J. Long
  • Patent number: 4421583
    Abstract: A non-woven alginate fabric useful as a wound dressing is made by spreading a tow of calcium alginate filaments in a flow of water, overfeeding the spread filaments onto a water-pervious support so that the filaments cross over each other and drying the filaments so that the alginate filaments become bonded to each other at their points of contact where they cross over each other. The filaments used have preferably been stretched in an atmosphere of steam and water-washed but not dried and are preferably dried by suction on the water-pervious support.
    Type: Grant
    Filed: September 22, 1982
    Date of Patent: December 20, 1983
    Assignee: Courtaulds Limited
    Inventors: Fred C. Aldred, Charles R. Moseley
  • Patent number: 4411738
    Abstract: The production of hardboard by the wet press process is speeded up by the incorporation of finely divided fibers in an aqueous slurry of otherwise fast draining wood fibers and a thermosetting binder so that a barrier of said fine fibers is formed during hot pressing of the mat and steam pressure is built up in the mat. The high pressure permits a curing temperature of from about 300.degree. F. to about 350.degree. F. in the core of the mat and a concomitant acceleration of the cure of the binder.
    Type: Grant
    Filed: April 30, 1982
    Date of Patent: October 25, 1983
    Assignee: United States Gypsum Company
    Inventors: Bruce A. Wittrup, Kendall D. White, Jr.
  • Patent number: 4374702
    Abstract: Microfibrillated celluloses having properties distinguishable from all previously known celluloses, are produced by passing a liquid suspension of cellulose through a small diameter orifice in which the suspension is subjected to a pressure drop of at least 3000 psig and a high velocity shearing action followed by a high velocity decelerating impact, and repeating the passage of said suspension through the orifice until the cellulose suspension becomes a substantially stable suspension. The process converts the cellulose into microfibrillated cellulose without substantial chemical change of the cellulose starting material.
    Type: Grant
    Filed: October 22, 1981
    Date of Patent: February 22, 1983
    Assignee: International Telephone and Telegraph Corporation
    Inventors: Albin F. Turbak, Fred W. Snyder, Karen R. Sandberg
  • Patent number: 4309247
    Abstract: Filter media sheets comprising particulate retention aid consisting of cellulose pulp of +100 to -100 Canadian Standard Freeness, and method of making the same.
    Type: Grant
    Filed: February 21, 1980
    Date of Patent: January 5, 1982
    Assignee: AMF Incorporated
    Inventors: Kenneth C. Hou, Eugene A. Ostreicher
  • Patent number: 4087317
    Abstract: Cellulosic pulp is made in 85% yield by mechanically defiberizing lignocellulose in a steam atmosphere, mixing the resulting aqueous fibrous pulp with a lignocellulose-pulping quantity of finely divided lime, and digesting the pulp in the presence of the lime to a predetermined degree of pulp digestion. The resulting digested fiber can then be mechanically beated in aqueous medium until it is substantially converted to a hydrated cellulosic gel product.
    Type: Grant
    Filed: August 4, 1975
    Date of Patent: May 2, 1978
    Assignee: Eucatex S.A. Industria e Comercio
    Inventor: James R. Roberts
  • Patent number: 4077833
    Abstract: A fire resistant bauxite composition board comprises, in percent by weight, from 10 to 85% lignocellulose particles, from 65 to 20% bauxite particles, and from 5 to 25% binder, particularly a hydrated cellulosic gel binder. The bauxite, (aluminum oxide dihydrate), is characterized by containing a large amount of water of hydration, by stability below 200.degree. C., and by release of its water of hydration at above 200.degree. C. Accordingly, the bauxite-containing board is stable during its manufacture, storage and use. However, in a fire situation the substantial amount of released water of hydration materially supplements the inherent non-combustible character of the bauxite in increasing the fire resistance of the board.
    Type: Grant
    Filed: November 10, 1975
    Date of Patent: March 7, 1978
    Assignee: Eucatex S.A. Industria E Comercio
    Inventor: James R. Roberts
  • Patent number: 4051276
    Abstract: This invention relates to solutions of selected organo-metallic compounds ssolved in an organic solvent which are useful for deacidifying a cellulose fiber paper. The paper is treated by means well known in the art, such as dipping or spraying. The organo-metallic compounds useful in this invention are compounds which may be rapidly hydrolyzed to an alkaline material such as lower alkyl compounds of lithium, aluminum, magnesium, gallium, zinc, and mixtures of these compounds. The organic solvent is a liquid which will not react with the organo-metallic compound, dissolve inks, or cause discoloration of other materials usually found in and around printed matter. After the paper is impregnated with the solution the organo-metallic compound remaining on the paper is hydrolyzed to an alkaline material.
    Type: Grant
    Filed: February 23, 1976
    Date of Patent: September 27, 1977
    Assignee: The United States Government as represented by the Librarian of Congress
    Inventors: John C. Williams, George B. Kelly, Jr.
  • Patent number: 4043862
    Abstract: A fire resistant vermiculite composition board comprises, in percent by weight, from 40 to 90% heat expanded vermiculite particles; from 5 to 20% ceramic clay particles; from 10 to 30% hydrated cellulosic gel having a TAPPI drainage time of at least 900 seconds; from 1 to 20% defiberized wood; and from 1 to 20% starch. The vermiculite is in an incompletely expanded condition of a degree predetermined to permit its further expansion upon subsequent exposure to heat. This results in a corresponding expansion of the composition board of which it is a component when the board is exposed to fire, preventing the formation of cracks and insuring continued fire protecting coverage of the area across which the board is applied.
    Type: Grant
    Filed: July 21, 1975
    Date of Patent: August 23, 1977
    Assignee: Eucatex S. A. Industria E Gomercio
    Inventor: James R. Roberts
  • Patent number: 3969549
    Abstract: A method of deacidifying paper wherein the paper has a substantially cellulose fiber base or substrate by exposing the paper to the vapors of a volatile organometallic compound and subsequently decomposing said compound to a base or alkaline material in situ. The treated material is usually first dried in vacuo and exposed under anhydrous or nearly anhydrous conditions to the organic-metallic compound. The method has the advantage of being able to treat large quantities of material at any one time.
    Type: Grant
    Filed: December 24, 1974
    Date of Patent: July 13, 1976
    Assignee: The United States of America as represented by the Librarian of Congress
    Inventors: John C. Williams, George B. Kelly, Jr.