Removal And/or Separation Of Portion Of Recirculating Fluid Patents (Class 162/43)
  • Patent number: 10151063
    Abstract: The invention is related to a method for the preparation of kraft pulp with increased pulping yield from lignin-containing cellulosic material using polysulfide cooking liquor. In order to obtain a cost efficient system both in aspects of investment costs but also in aspects of heat economy of operating the process is most of the total charge of alkali charged as heated polysulfide liquor to an first atmospheric vessel, wherein the hot polysulfide liquor flashes off steam providing most if not all of the necessary steaming effect for the cellulose material. The polysulfide liquor is then allowed to impregnate the cellulose material at a temperature closer to cooking temperature but still so low that essentially no delignification occurs in impregnation vessel, as the H-factor in impregnation vessel is kept within 1-20.
    Type: Grant
    Filed: August 26, 2014
    Date of Patent: December 11, 2018
    Assignee: Valmet AB
    Inventors: Stefan Antonsson, Krister Olsson
  • Patent number: 8475627
    Abstract: A process of treating a lignocellulosic material includes a pre-extraction step in which hemicellulose is extracted from the lignocellulosic material. In one embodiment, the pre-extraction step involves contacting the lignocellulosic material with an aqueous solution under conditions that release acidic material from the lignocellulosic material into the aqueous solution, and the aqueous solution includes a basic material that at least partly neutralizes the acidic material so that the aqueous solution at the end of the pre-extraction step has a pH within a range of from 4.5 to 11. The process also includes a pulping step, after the pre-extraction step, in which the lignocellulosic material is separated into pulp. The process further includes an adsorption step, after the pulping step, in which hemicellulose is adsorbed on the pulp.
    Type: Grant
    Filed: May 16, 2011
    Date of Patent: July 2, 2013
    Assignees: University of Maine System Board of Trustees, International Paper Company
    Inventors: Adriaan Reinhard Pieter van Heiningen, Sung-Hoon Yoon, Haixuan Zou, Jianer Jiang, Gopal C. Goyal
  • Patent number: 8317975
    Abstract: An omnibus process of pulping and bleaching lignocellulosic materials in which a charge of a lignocellulosic material is biopulped and/or water extracted prior to pulping and bleaching. The lignocellulosic material may be mechanically pulped and bleached in the presence of an enzyme that breaks lignin-carbohydrate complexes. The aqueous extract in embodiments including a water extract step is separated into acetic acid and hemicellulose sugar aqueous solutions.
    Type: Grant
    Filed: April 27, 2006
    Date of Patent: November 27, 2012
    Assignee: The Research Foundation of the State University of New York
    Inventors: Thomas E. Amidon, Raymond Francis, Gary M. Scott, Jeremy Bartholomew, Bandaru V. Ramarao, Christopher D. Wood
  • Patent number: 8197639
    Abstract: The system and method reduce the liquid/wood ratio at the top of a vapor phase digester in a continuous digester plant. Chips that are to be cooked in the vapor phase digester are fed as a mixture of chips and liquid at a liquid/wood ratio that exceeds 8:1 in a transfer line to an inverted top separator arranged at the top of the vapor phase digester. The top separator feeds the chips upwardly. More than 50% of the liquid content of the mixture of chips and liquid is withdrawn in the top separator and the remaining liquid is fed out from the top separator to the top of the vapor phase digester. A pile of chips and a liquid volume are established at the top, wherein the pile of chips is disposed above the liquid surface of the liquid volume.
    Type: Grant
    Filed: February 19, 2008
    Date of Patent: June 12, 2012
    Assignee: METSO PAPER Sweden AB
    Inventor: Vidar Snekkenes
  • Patent number: 8157955
    Abstract: A system for collecting ligno-cellulosic biomass over a large area to enable the commercial refining of biomass from 2,500 to in excess of 50,000 tons of biomass per day to produce ethanol or other products. The biomass is collected at a series of collection points and then transported through a network of conduit “loops” interconnecting each of the collection points and the central refining plant. The water used to transport the biomass, as a slurry, is recovered and sequentially recycled in the same pipeline system to push the biomass slurry around the system in a “loop.” The outgoing and return legs of each loop optionally are located adjacent each other.
    Type: Grant
    Filed: February 4, 2011
    Date of Patent: April 17, 2012
    Assignee: Iogen Energy Corporation
    Inventor: Patrick J. Foody, Sr.
  • Patent number: 8080128
    Abstract: Disclosed is a method for increasing the concentration of xylose in lignocellulosic hydrolysate. The method includes the step of extruding lignocellulosic material and mixing the lignocellulosic material with diluted acid and the step of conducting hot-water extraction on the mixture. Hence, the concentration of the xylose in the lignocellulosic hydrolysate can achieve a high concentration of 60 g/L, and the yield of the xylose can reach to 90%.
    Type: Grant
    Filed: December 31, 2009
    Date of Patent: December 20, 2011
    Assignee: Atomic Energy Council - Institute of Nuclear Research
    Inventors: Wen-Hua Chen, Sheng-Shieh Chen, Wen-Song Hwang, Lee-Chung Men, Jia-Baau Wang
  • Patent number: 8057635
    Abstract: A system for collecting ligno-cellulosic biomass over a large area to enable the commercial refining of biomass from 2,500 to in excess of 50,000 tons of biomass per day to produce ethanol or other products. The biomass is collected at a series of collection points and then transported through a network of conduit “loops” interconnecting each of the collection points and the central refining plant. The water used to transport the biomass, as a slurry, is recovered and sequentially recycled in the same pipeline system to push the biomass slurry around the system in a “loop”.
    Type: Grant
    Filed: June 28, 2007
    Date of Patent: November 15, 2011
    Assignee: Iogen Energy Corporation
    Inventor: Patrick Foody, Sr.
  • Patent number: 7943009
    Abstract: A process of treating a lignocellulosic material includes a pre-extraction step in which hemicellulose is extracted from the lignocellulosic material. In one embodiment, the pre-extraction step involves contacting the lignocellulosic material with an aqueous solution under conditions that release acidic material from the lignocellulosic material into the aqueous solution, and the aqueous solution includes a basic material that at least partly neutralizes the acidic material so that the aqueous solution at the end of the pre-extraction step has a pH within a range of from 4.5 to 11. The process also includes a pulping step, after the pre-extraction step, in which the lignocellulosic material is separated into pulp. The process further includes an adsorption step, after the pulping step, in which hemicellulose is adsorbed on the pulp.
    Type: Grant
    Filed: December 30, 2009
    Date of Patent: May 17, 2011
    Assignees: University of Maine System Board of Trustees, International Paper Company
    Inventors: Adriaan Reinhard Pieter van Heiningen, Sung-Hoon Yoon, Haixuan Zou, Jianer Jiang, Gopal C. Goyal
  • Patent number: 7854847
    Abstract: Systems and methods for purifying wood pulp by caustic-borate extraction. The systems and method include a method for recovering both the caustic and borate compounds from the resultant hemicaustic effluent, so that they may be recycled and re-used. Efficient recovery of these components is enabled by a nanofiltration system that has one or more alkali-resistant nanofiltration membranes.
    Type: Grant
    Filed: November 9, 2006
    Date of Patent: December 21, 2010
    Assignee: Rayonier TRS Holdings Inc.
    Inventor: Jian Li
  • Patent number: 7842161
    Abstract: A process of treating a lignocellulosic material includes a pre-extraction step in which hemicellulose is extracted from the lignocellulosic material. Then, in a solvent pulping step, the lignocellulosic material is separated into pulp by contacting the lignocellulosic material with a cooking liquor comprising a solvent. In one embodiment, the solvent has a boiling point of at least about 150° C. In another embodiment, the cooking liquor comprises a mixture of solvent and water.
    Type: Grant
    Filed: December 26, 2007
    Date of Patent: November 30, 2010
    Assignees: The University of Maine System Board of Trustees, International Paper
    Inventors: Adriaan Reinhard Pieter van Heiningen, Sung-Hoon Yoon, Haixuan Zou, Jianer Jiang, Gopal C. Goyal
  • Patent number: 7824521
    Abstract: A process of treating a lignocellulosic material includes a pre-extraction step in which hemicellulose is extracted from the lignocellulosic material. In one embodiment, the pre-extraction step involves contacting the lignocellulosic material with an aqueous solution under conditions that release acidic material from the lignocellulosic material into the aqueous solution, and the aqueous solution includes a basic material that at least partly neutralizes the acidic material so that the aqueous solution at the end of the pre-extraction step has a pH within a range of from 4.5 to 11. The process also includes a pulping step, after the pre-extraction step, in which the lignocellulosic material is separated into pulp. The process further includes an adsorption step, after the pulping step, in which hemicellulose is adsorbed on the pulp.
    Type: Grant
    Filed: December 18, 2006
    Date of Patent: November 2, 2010
    Assignees: University of Maine System Board of Trustees, International Paper Company
    Inventors: Adriaan Reinhard Pieter van Heiningen, Sung-Hoon Yoon, Haixuan Zou, Jianer Jiang, Gopal C. Goyal
  • Patent number: 7604711
    Abstract: Method and apparatus for batch displacement digester systems to increase tank farm vessel temperatures for more efficient delignification rates by mitigating the formation of flow channels in the chip bed, minimizing the vertical temperature gradient in the digester and segregation of returning liquors to the tank farm from the digester.
    Type: Grant
    Filed: March 7, 2006
    Date of Patent: October 20, 2009
    Inventor: Craig A. Bianchini
  • Patent number: 7374637
    Abstract: The method is for bleaching cellulose pulp in a bleach line that has at least two bleaching steps. The filtrate distribution is led up through the bleaching line counter-currently to the flow of cellulose pulp established in the bleaching line. A single joint main conduit is used for the bleaching steps. Wash filtrates obtained from the wash steps, used after or before the bleaching step, are led in conduits to branch locations on the main conduit that are positioned downstream of the branch location for drawing off of wash and/or dilution liquor for the wash step in question. All branch points in the joint main conduit are in fluid communication with one another along the main conduit.
    Type: Grant
    Filed: November 16, 2005
    Date of Patent: May 20, 2008
    Assignee: GL&V Management Hungary kft
    Inventors: Vidar Snekkenes, Lennart Gustavsson
  • Patent number: 7364640
    Abstract: A process for removing silica from nonwood plant materials involving both chemical and mechanical action is described. The silica-rich epidermal cells are liberated mechanically by a pre-pulping and low-consistency refining step and subsequently removed from the pulp via the filtrate of a thickening step. Amorphous silica is liberated chemically by using an alkaline dilution source in the pulper, then removed from the pulp via the filtrate of a thickening step and a dewatering step. The silica is then removed from the filtrate by adjusting the pH, followed by a separation step. The desilicated fibrous material may then be chemically or mechanically pulped and bleached using known processes. The silica removed from the nonwood plant material may then be used as a feedstock for other applications.
    Type: Grant
    Filed: September 7, 2004
    Date of Patent: April 29, 2008
    Assignee: Alberta Research Council Inc.
    Inventors: Wade Chute, Sofia Vichnevsky
  • Patent number: 7297225
    Abstract: A process for high temperature peroxide bleaching of pulp in which pulp is retained at high temperature and pressure to increase bleaching activity but in which the pulp is cooled prior to discharge from the pressure vessel below the flash point thereby resulting in lower energy, nonviolent discharge. Through the use of a heat exchanger, the cooling of the pulp can be performed using recycled filtrate containing residual peroxide, which encourages further bleaching during atmospheric retention. The heat exchanger is also used to heat a water stream, which can be used earlier in the pulping process, resulting in cost savings because energy within the system is retained to a greater degree.
    Type: Grant
    Filed: June 22, 2004
    Date of Patent: November 20, 2007
    Assignee: Georgia-Pacific Consumer Products LP
    Inventors: Hazen Charles Thomas, Wayne F. Winkler, Jeffrey A. Lee
  • Patent number: 7217338
    Abstract: The process is for continuously cooking chemical pulp in a digester system consisting of at least one vessel for impregnating and cooking comprising an inlet into which a mixture of chips and process liquid is fed. The chips are impregnated at a predetermined impregnation temperature, Timp, and cooked at a predetermined cooking temperature, Tcook, after which dissolved pulp is fed out at the outlet of the digester system. The process liquid which is continually extracted is retained outside the digester system during a dwell time, t, of at least 30 min, without any heating above 140°, and thereafter returned to the digester system to a position which is substantially at the same level as the extraction, or downstream thereof, and thereby constitute part of the process liquid in the subsequent treatment zone. The process results in improved tear strength, beatability, bleachability and reduced color reversion, and increased yield across the digester.
    Type: Grant
    Filed: December 4, 2002
    Date of Patent: May 15, 2007
    Assignee: Kvaerner Pulping AB
    Inventors: Catrin Gustavsson, Mikael Lindstrom, Krister Olsson, Vidar Snekkenes
  • Patent number: 6942754
    Abstract: Xylooligosaccharide is produced from a lignocellulose pulp by enzyme-treating a lignocellulose pulp with hemicellulase, filtering the resultant reaction mixture to separate a liquid fraction from the enzyme-treated pulp, subjecting the separated liquid fraction to a permeation treatment through a separation membrane to separate a non-permeated fraction containing xylooligosaccharide-lignin complex with an increased concentration from a permeated fraction, collecting the non-permeated fraction, and separating and recovering xylooligosaccharide from the collected non-permeated fraction.
    Type: Grant
    Filed: April 22, 2002
    Date of Patent: September 13, 2005
    Assignee: Oji Paper Co., Ltd.
    Inventors: Yoshiya Izumi, Jun Sugiura, Hitoshi Kagawa, Naoya Azumi
  • Patent number: 6866748
    Abstract: The present invention provides a process for preparing polysulfide. More particularly, the process of the present invention allows one to prepare the amount of polysulfide needed using clarified white liquor, and to be used when and where it is needed during the cooking process. The process comprises reacting alkaline digesting liquor after clarification with a catalytic amount of a transition metal oxide catalyst, most preferably manganese dioxide. The reaction is conducted at a temperature of 98° C. or less, and is conducted for a short period of time, e.g., less than five minutes, with no oxygen gas or air being introduced with the catalyst and the main flow of clarified liquor.
    Type: Grant
    Filed: June 6, 2002
    Date of Patent: March 15, 2005
    Assignee: American Air Liquide, Inc.
    Inventors: Meenakshi V. Sundaram, Sebastien Corbeil, Michel Epiney
  • Patent number: 6824646
    Abstract: Lignocellulose pulp is bleached by bleaching a pulp in aqueous alkali solution with oxygen and treating the pulp with a hemicellulase, while a liquid fraction delivered from the enzyme treatment step is separated from the hemicellulase treated reaction mixture, and subjected to a penetration treatment through a separation membrane, for example, reverse osmosis membrane, to separate a permeated fraction from a non-permeated fraction; the permeated fraction is fed to the alkali-oxygen bleaching (oxygen delignification) step and is used as a liquid medium of the bleaching system.
    Type: Grant
    Filed: April 22, 2002
    Date of Patent: November 30, 2004
    Assignee: OJI Paper Co., Ltd.
    Inventors: Yoshiya Izumi, Jun Sugiura, Hitoshi Kagawa, Naoya Azumi
  • Patent number: 6746568
    Abstract: A method in bleaching of pulp is described, in which the pulp is subjected to a peroxide bleaching step, whereupon the pulp is washed and the washing liquid from the washing is separated from the pulp in the form of a filtrate. The method is characterised in that the filtrate is treated with an aluminium compound, such as aluminium sulphate or polyaluminium sulphate, for precipitation of interfering substances, such as oxygen-demanding organic material and metals, that the precipitated material is removed from the filtrate, that the aluminium content of the filtrate after precipitation of interfering substances is adjusted to at most 20 ppm, and that the filtrate is then recirculated to the peroxide bleaching step. By the method, a reduced consumption of hydrogen peroxide in the peroxide bleaching step is achieved.
    Type: Grant
    Filed: September 15, 2000
    Date of Patent: June 8, 2004
    Assignee: Kemira Kemi AB
    Inventors: Hans Terelius, Anette Olsson, Margareta Nilsson, Jessica Svensson, Christos Rampotas
  • Publication number: 20040099386
    Abstract: Separation of dissolved and colloidal high molecular weight organic by-products from liquors or filtrates in a cellulosic pulping process to improve the overall efficiency of the process.
    Type: Application
    Filed: November 20, 2003
    Publication date: May 27, 2004
    Inventor: Craig A. Bianchini
  • Patent number: 6723205
    Abstract: The invention relates to a degassing centrifugal apparatus such as a pump having energy recovery means and to a process for degassing a fluid. The apparatus has a rotatable hollow rotor connected to a fluid inlet at one end and a liquid outlet at the opposite end. A gas exhaust is connected to the center of the apparatus. The apparatus has at its inlet end means for bringing a fluid to rotate on the inner wall of said rotor. The apparatus comprises a turbine at its outlet end recovering excess dynamic energy from the rotating fluid. The apparatus is especially useful for centrifugal degassing of backwater in the production of paper or board machine.
    Type: Grant
    Filed: April 17, 2002
    Date of Patent: April 20, 2004
    Assignee: FOM Technology Oy AB
    Inventor: Paul Meinander
  • Patent number: 6715307
    Abstract: A sub-condenser 4 is disposed in a within-vehicle-compartment air passage P1, so that the sub-condenser is permitted to receive heat from a heater core 21.
    Type: Grant
    Filed: January 22, 2002
    Date of Patent: April 6, 2004
    Assignee: Calsonic Kansei Corporation
    Inventors: Jun Hatakeyama, Satoshi Ogihara
  • Patent number: 6544384
    Abstract: The strength properties of chemical cellulose pulp (particularly kraft pulp) are improved by substituting a cold impregnation soak for conventional impregnation procedures. After steaming, wood chips are soaked in an alkaline liquid at a temperature of about 80-110° C. (preferably 80-100° C., or 90-105° C.) for between one-half-72 hours (typically about 2-4 hours) at a pressure of about 0-15 bar (preferably about 1-5 bar), to dissolve at least about 8% of the wood (preferably about 10-20%) and at least about 15% of the lignin. The alkaline liquid used preferably contains sulfide (e.g. black liquor, green liquor, white liquor, or mixtures thereof), but almost any alkaline liquid having an alkali concentration of about 1.0 mole of NaOH/liter or less (typically about 0.75 m/l or less) is suitable. The wood chips are then raised to a cooking temperature of about 145-180° C. and cooked to produce the cellulose chemical pulp.
    Type: Grant
    Filed: October 15, 2001
    Date of Patent: April 8, 2003
    Assignee: Andritz Inc.
    Inventors: Kaj O. Henricson, Aki Hannu Vilpponen, Hannu Olavi Ramark, Auvo Kimmo Kettunen, C. Bertil Stromberg
  • Patent number: 6461473
    Abstract: A process for washing pulp including a dilution step, an extraction step and a subsequent displacement step. The process further includes the steps of: diluting the pulp; passing the diluted pulp to the extraction step; developing a first filtrate from the extraction step; passing the pulp from the extraction step to the displacement step; developing a second filtrate from the displacement step; segregating the first and second filtrates; providing the second filtrate to the dilution step; providing a determined minimum volume of the first filtrate needed for the dilution step; and eliminating the remaining volume of the first filtrate from further use in the washing of the pulp.
    Type: Grant
    Filed: September 23, 1998
    Date of Patent: October 8, 2002
    Assignees: Andritz Oy, GL&V Management Hungary Kft
    Inventors: Harri Qvintus, Pekka Tervola
  • Publication number: 20020129911
    Abstract: A continuous digester configuration and process for continuously cooking and digesting cellulosic material and producing cellulosic pulp is disclosed. The digester configuration comprises a plurality of jump-stage recirculations located along the length of a continuous digester vessel, wherein each of the jump-stage recirculations moves extracted liquor from one elevation of the digester vessel and re-introduces the liquor at a higher elevation in the vessel to maintain an internal liquor downflow substantially throughout the entire digester vessel. The process for continuously cooking and digesting cellulosic material comprises maintaining an internal concurrent liquor downflow substantially throughout the continuous digester vessel, wherein the internal liquor downflow does not exceed 400 gallons per ton of b.d. wood feed.
    Type: Application
    Filed: October 16, 2001
    Publication date: September 19, 2002
    Inventors: Bruno S. Marcoccia, James Robert Prough, Louis O. Torregrossa
  • Patent number: 6451172
    Abstract: A drainer for a feed system for a cellulose digester has a substantially open and hollow inlet (devoid of a spiral flow imparter or a like flow restriction) and a substantially annular screen within an elongated housing having a flow direction between the housing inlet and outlet. The screen is slotted and the slots are at an angle &agr; between 5-90° with respect to the flow direction, so as to minimize passage of cellulose material through the slots, or clogging of the slots.
    Type: Grant
    Filed: May 18, 2000
    Date of Patent: September 17, 2002
    Assignee: Andritz Inc.
    Inventors: Mark D. Barrett, J. Robert Prough, C. Bertil Stromberg
  • Publication number: 20020079071
    Abstract: The invention relates to a process for continuous cooking of wood chips at elevated pressure and temperature in a vertical digester (1) for production of chemically dissolved pulp.
    Type: Application
    Filed: September 28, 2001
    Publication date: June 27, 2002
    Applicant: Kvaerner Pulping AB;
    Inventors: Vidar Snekkenes, Lennart Gustavsson, Sven-Erik Olsson
  • Publication number: 20020079070
    Abstract: The invention relates to a process for continuous cooking of wood chips at elevated pressure and temperature in a vertical digester (1) for production of chemically dissolved pulp.
    Type: Application
    Filed: September 28, 2001
    Publication date: June 27, 2002
    Applicant: Kvaerner Pulping AB
    Inventors: Vidar Snekkenes, Lennart Gustavsson, Sven-Erik Olsson
  • Publication number: 20020069986
    Abstract: A system and method for improved filtrate addition in a continuous digester is disclosed. The system comprises a blow dilution header/nozzle assembly located in the blow dilution zone of the digester. The header/nozzle assembly comprises (i) a plurality of nozzles for introducing and distributing filtrate into the blow dilution zone, and (ii) a plurality of measurement and control devices for monitoring and controlling filtrate flow through the plurality of nozzles. The method comprises (a) introducing and distributing filtrate through a plurality of nozzles of a blow dilution header/nozzle assembly in the blow dilution zone of the continuous digester; and (b) measuring and controlling the filtrate flow through each nozzle of the plurality of nozzles.
    Type: Application
    Filed: June 12, 2001
    Publication date: June 13, 2002
    Inventors: Bruno S. Marcoccia, James Robert Prough
  • Patent number: 6350348
    Abstract: A method of cooking pulp in an alkaline batch process (using one or more batch digesters) improves pulp bleachability. The wood material is supplied to the digester; the cellulosic material is pre-treated in the digester with a first liquor, the first liquor is displaced by a second liquor, the displaced first liquor is led to a further treatment, the cellulose material is treated with the second liquor, and the cooked pulp is removed from the digester. The second liquor is displaced as two consecutive parts, i.e. as strong black liquor and weak black liquor, and after cooling in a heat exchanger the strong black liquor thus obtained is fed into the digester as the first liquor in a subsequent batch (in the same, or a different, batch digester).
    Type: Grant
    Filed: July 19, 1999
    Date of Patent: February 26, 2002
    Assignee: Andritz-Ahlstrom Oy
    Inventors: Kaj Henricson, Auvo Kettunen, Hannu Ramark
  • Patent number: 6346167
    Abstract: Kraft pulp of increased strength and bleachability may be produced with decreased consumption of effective alkali, and at a lower H factor, by keeping the dissolved organic material (DOM) concentration low substantially through the entire kraft cook, including by extracting high DOM liquid from at least one part of a continuous digester and replacing it with much lower level DOM liquid. Existing pulp mills having two-vessel hydraulic, one-vessel hydraulic, or other systems may be retrofit to provide for extractions and additions of low DOM dilution liquor (including substantially DOM-free white liquor). Also, commercial size batch digesters (8 tons per day of pulp or more) can be operated with low DOM liquor to produce increased strength pulp. Using dilution with low DOM liquor also results in reduced H factor and effective alkali consumption, and increased bleachability.
    Type: Grant
    Filed: January 19, 2001
    Date of Patent: February 12, 2002
    Assignee: Andritz-Ahlstrom Inc.
    Inventors: Bruno S. Marcoccia, J. Robert Prough, Richard O. Laakso, Joseph R. Phillips, Rolf C. Ryham, Jan T. Richardsen, R. Fred Chasse
  • Patent number: 6332950
    Abstract: A method in connection with the pretreatment of comminuted fibrous material intended for chemical cellulose pulp production. The fibrous material is fed through a low pressure system that has a gas phase part followed by a liquid phase part. The liquid phase part includes a low pressure circulation where a circulating liquid is withdrawn from the fibrous material and recirculated back to the fibrous material in an upstream position. The fibrous material is sluiced into a high pressure system that has a liquid phase transfer part operatively connected to a digester. A hot process liquid and/or the circulating liquid are evaporatively cooled by being allowed to flash within the low pressure system.
    Type: Grant
    Filed: December 17, 1999
    Date of Patent: December 25, 2001
    Assignee: Kaverner Pulping AB
    Inventors: Vidar Snekkenes, Lennart Gustavsson
  • Publication number: 20010037865
    Abstract: A new and improved way of continuously cooking fiber material, wherein temperatures and alkaline levels are controlled to be maintained within specific levels in different zones of the digesting process in order to optimize chemical consumption and heat-economy and at the same time achieve very good pulp properties. The digesting process includes a top separator that separates the transport liquid from the fiber material and permits the fiber material to be exposed to the cooking liquid.
    Type: Application
    Filed: December 14, 2000
    Publication date: November 8, 2001
    Applicant: Kvaerner Pulping AB
    Inventors: Vidar Snekkenes, Johan Engstrom, Sven-Erik Ohlsson, Per Nystrom, Soren Soderqvist, Bjorn Karlsson
  • Publication number: 20010023748
    Abstract: In the production of chemical pulp, such as kraft pulp, it is possible to reduce the amount of ancillary equipment, and/or the size of the continuous digester vessel, while achieving enhanced uniformity of treatment by avoiding “hang ups”. Instead of providing vertical counter-current flow of liquid and comminuted cellulosic fibrous material being treated in the lower half of the digester, the counter-current flow may be a cross flow, that is substantially horizontal (e.g. radial) while the flow of the chip column is vertical. Regardless of the configuration of the digester vessel, a single pump may be utilized for all of the recirculations, or only a few pumps for all of the recirculations.
    Type: Application
    Filed: May 31, 2001
    Publication date: September 27, 2001
    Applicant: Andritz-Ahlstrom Inc.
    Inventors: Bruno S. Marcoccia, C. Bertil Stromberg, Brian F. Greenwood
  • Patent number: 6280568
    Abstract: Kraft pulp of increased strength and bleachability may be produced with decreased consumption of effective alkali, and at a lower H factor, by keeping the dissolved organic material (DOM) concentration low substantially through the entire kraft cook, including by extracting high DOM liquid from at least one part of a continuous digester and replacing it with much lower level DOM liquid. Existing pulp mills having two-vessel hydraulic, one-vessel hydraulic, or other systems may be retrofit to provide for extractions and additions of low DOM dilution liquor (including substantially DOM-free white liquor). Also, commercial size batch digesters (8 tons per day of pulp or more) can be operated with low DOM liquor to produce increased strength pulp. Using dilution with low DOM liquor also results in reduced H factor and effective alkali consumption, and increased bleachability.
    Type: Grant
    Filed: August 15, 2000
    Date of Patent: August 28, 2001
    Assignee: Andritz-Ahlstrom Inc.
    Inventors: Bruno S. Marcoccia, J. Robert Prough, Richard O. Laakso, Joseph R. Phillips, Rolf C. Ryham, Jan T. Richardsen, R. Fred Chasse
  • Patent number: 6254723
    Abstract: In a single-vessel system for continuous cooking of kraft pulp, chips and liquor are conveyed from a high pressure feeder in a transfer line to a first end of a digester. A part of the liquor is separated from the chips that are withdrawn from an outlet defined in an upper part of the digester and conveyed in a return line to the high pressure feeder. A constituent flow of liquor is led from the return line and heated and fed via one or more inlets into the digester at a location that is downstream of the outlet for the return line.
    Type: Grant
    Filed: December 13, 1999
    Date of Patent: July 3, 2001
    Assignee: Kvaerner Pulping AB
    Inventors: Vidar Snekkenes, Lennart Gustavsson
  • Patent number: 6235151
    Abstract: Calcium carbonate scaling is inhibited in a multi-stage alkaline waste liquor evaporation plant in a chemical cellulose pulp mill having a bleaching plant. Calcium-containing effluent from the bleaching plant is treated together with alkaline waste liquor in the evaporation plant. A portion of the alkaline waste liquor of the evaporation plant is supplied to the bleaching effluent to increase the carbonate content of the effluent. Then the bleaching effluent is heated to 110-160° C. by direct contact with a heating medium (e.g. steam, or secondary vapor) and maintained in a retention tank for a period of about 1-20 minutes to reduce the amount of dissolved calcium in the effluent. Finally the heat-treated bleaching effluent is evaporated with the alkaline waste liquor in the evaporation plant, with minimized scaling.
    Type: Grant
    Filed: April 26, 1999
    Date of Patent: May 22, 2001
    Assignee: Andritz-Ahlstrom Oy
    Inventors: Olof Fagerlind, Heikki Jaakkola, Erkki Kiiskila
  • Patent number: 6159337
    Abstract: Kraft pulp of increased strength and bleachability may be produced with decreased consumption of effective alkali, and at a lower H factor, by keeping the dissolved organic material (DOM) concentration low substantially through the entire kraft cook, including by extracting high DOM liquid from at least one part of a continuous digester and replacing it wit much lower level DOM liquid. Existing pulp mills having two-vessel hydraulic, one-vessel hydraulic, or other systems may be retrofit to provide for extractions and additions of low DOM dilution liquor (including substantially DOM-free white liquor). Also, commercial size batch digesters (8 tons per day of pulp or more) can be operated with low DOM liquor to produce increased strength pulp. Using dilution with low DOM liquor also results in reduced H factor and effective alkali consumption, and increased bleachability.
    Type: Grant
    Filed: October 8, 1999
    Date of Patent: December 12, 2000
    Assignee: Andritz-Ahlstrom Inc.
    Inventors: Bruno S. Marcoccia, J. Robert Prough, Richard O. Laakso, Joseph R. Phillips, Rolf C. Ryham, Jan T. Richardsen, R. Fred Chasse
  • Patent number: 6132556
    Abstract: A method of controlling the pressure of a vertical continuous comminuted cellulosic fibrous material (wood chip) digester is provided using a pressure-control extraction in a zone relatively insensitive to changes in the flow rate of liquid introduction or removal. The method comprises controlling the pressure in the digester primarily (or substantially exclusively) by varying the flow rate of liquor extracted from the pressure-control extraction to maintain the pressure in the digester at a desired superatmospheric level while avoiding non-uniform, unstable material movement in the counter-current washing zone; and introducing dilution liquid into the digester at the at least one recirculation-dilution loop. The pressure-control extraction is preferably substantially the upper extraction in the digester. Substantially except during excessive over pressure and under pressure conditions the extraction flow from the main extraction is maintained substantially constant.
    Type: Grant
    Filed: September 4, 1998
    Date of Patent: October 17, 2000
    Assignee: Andritz-Ahlstrom Inc.
    Inventors: C. Bertil Stromberg, J Robert Prough, Bruno S. Marcoccia, Richard O. Laakso, Carl L. Luhrmann
  • Patent number: 6086712
    Abstract: Kraft pulp of increased strength and bleachability may be produced with decreased consumption of effective alkali, and at a lower H factor, by keeping the dissolved organic material (DOM) concentration low substantially through the entire kraft cook, including by extracting high DOM liquid from at least one part of a continuous digester and replacing it with much lower level DOM liquid. Existing pulp mills having two-vessel hydraulic, one-vessel hydraulic, or other systems may be retrofit to provide for extractions and additions of low DOM dilution liquor (including substantially DOM-free white liquor). Also, commercial size batch digesters (8 tons per day of pulp or more) can be operated with low DOM liquor to produce increased strength pulp. Using dilution with low DOM liquor also results in reduced H factor and effective alkali consumption, and increased bleachability.
    Type: Grant
    Filed: October 20, 1998
    Date of Patent: July 11, 2000
    Assignee: Ahlstrom Machinery Inc.
    Inventors: Bruno S. Marcoccia, J. Robert Prough, Richard O. Laakso, Joseph R. Phillips, Rolf C. Ryham, Jan T. Richardsen, R. Fred Chasse
  • Patent number: 6071375
    Abstract: A gas purged viewport for endpoint detection in a gas phase processing chamber is provided which prevents contamination of an optical monitoring window by use of a purge gas flow. The purge gas purges the viewport and prevents deposition of byproducts and contaminants on the window which will adversely effect endpoint detection. The gas purge viewport includes a prechamber between the optically transparent window and the process chamber. The purge gas is passed through the prechamber and into the processing chamber to purge the window. The gas purge system may also be used to purge other parts such as sensors.
    Type: Grant
    Filed: December 31, 1997
    Date of Patent: June 6, 2000
    Assignee: Lam Research Corporation
    Inventors: Anthony L. Chen, John Holland
  • Patent number: 5849150
    Abstract: Kraft pulp of increased strength and bleachability may be produced with decreased consumption of effective alkali, and at a lower H factor, by keeping the dissolved organic material (DOM) concentration low substantially through the entire kraft cook, including by extracting high DOM liquid from at least one part of a continuous digester and replacing it with much lower level DOM liquid. Existing pulp mills having two-vessel hydraulic, one-vessel hydraulic, or other systems may be retrofit to provide for extractions and additions of low DOM dilution liquor (including substantially DOM-free white liquor). Also, commercial size batch digesters (8 tons per day of pulp or more) can be operated with low DOM liquor to produce increased strength pulp. Using dilution with low DOM liquor also results in reduced H factor and effective alkali consumption, and increased bleachability.
    Type: Grant
    Filed: December 30, 1996
    Date of Patent: December 15, 1998
    Assignee: Ahlstrom Machinery Inc.
    Inventors: Bruno S. Marcoccia, J. Robert Prough, Richard O. Laakso, Joseph R. Phillips, Rolf C. Ryham, Jan T. Richardsen, R. Fred Chasse
  • Patent number: 5849151
    Abstract: Digester systems for producing paper pulp from comminuted cellulosic fibrous material take into account the level of dissolved organic materials (DOM), such as lignin, hemi-cellulose, and cellulose, maintaining the DOM level at about 100 g/l throughout the cook (particularly kraft cook). In order to make sure there is sufficient liquid to slurry the material in the feed system of a two vessel system, some liquid is withdrawn from the circulation conduits between the digester and impregnation vessel, cooled, and fed to the feed system. In a vapor phase digester, the level of liquid at the top of the digester is more precisely controlled by circulating some of the withdrawn liquid from a circulatory loop of the digester to the level tank associated with the feed system. An in-line drainer may be provided in the feed system between a make-up liquor pump and a liquid inlet conduit leading to the top of an impregnation vessel.
    Type: Grant
    Filed: May 27, 1997
    Date of Patent: December 15, 1998
    Assignee: Ahlstrom Machinery Inc.
    Inventors: Bruno S. Marcoccia, J. Robert Prough, Richard O. Laakso, R. Fred Chasse
  • Patent number: 5788813
    Abstract: A method and apparatus for treating green liquor from a sulphate pulp mill enhances the clarification of the green liquor and may easily be integrated into existing pulp mills. A first portion of the green liquor from the sulphate pulp mill is clarified in a clarifier to produce a clarified green liquor and a dregs-containing green liquor. The dregs-containing green liquor is filtered in a green liquor filter to produce filtrate and dregs. The filtrate is combined) with the clarified green liquor to produce a first combined stream; and the dregs are filtered in a dregs filter. A second portion of green liquor from the sulphate pulp mill is combined with the dregs-containing green liquor to produce a second combined stream, and the second combined stream is introduced into the green liquor filter. The dregs from step (b) are washed prior to filtering the dregs, the green liquor filter and washer comprising a single structure.
    Type: Grant
    Filed: September 11, 1996
    Date of Patent: August 4, 1998
    Assignee: Ahlstrom Machinery Oy
    Inventors: Holger Engdahl, Martti Pokkinen, Pekka Tormikoski
  • Patent number: 5741399
    Abstract: In a pulp washing method which employs a dilution stage, followed by an extraction stage, and followed, in turn by a dilution stage, filtrates from the extraction stage and the displacement stage are segregated so that at least a part of the filtrate from the extraction stage may be removed from the pulp washing.
    Type: Grant
    Filed: June 24, 1996
    Date of Patent: April 21, 1998
    Assignee: Beloit Technologies, Inc.
    Inventor: John S. Antkowiak
  • Patent number: 5716496
    Abstract: A method and an apparatus are provided for controlling crystallization (and thus preventing harmful fouling of heat transfer surfaces) during the treatment of black liquor. The black liquor is concentrated to a high dry solids content (at least about 70%, e.g. about 75-90%) in a falling film crystallizing apparatus (e.g. falling film evaporator). A part of the liquor flowing from the heat transfer surfaces and collected in a retention vessel (e.g. an interior volume of the evaporator) is recirculated to the heat exchange surfaces and a part of the liquor is discharged for further treatment (e.g. combustion in a recovery boiler). A part of the black liquor in the recirculation system is returned directly to the retention vessel in order to facilitate mixing and thus to bring about, in the retention vessel, crystallization of inorganic salts of the black liquor that is as complete as possible.
    Type: Grant
    Filed: July 10, 1995
    Date of Patent: February 10, 1998
    Assignee: Ahlstrom Machinery Oy
    Inventor: Erik Agren
  • Patent number: 5679217
    Abstract: Provided is a method and apparatus which decreases a liquor--to--wood ratio at the top of a continuous digester while increasing a liquor--to--wood ratio in the upstream pre-impregnation vessel. A substantially wood-chip free liquor portion is drawn from the top of the digester through a heater to the bottom of the pre-impregnation vessel through a return conduit. A stream is drawn off the return conduit, upstream of the heater, for transfer to the top of the vessel without mixing with wool chips.
    Type: Grant
    Filed: February 3, 1995
    Date of Patent: October 21, 1997
    Assignee: Kvaerner Pulping AB
    Inventors: Peter Outzen, Staffan Berg, Alf Aspvik
  • Patent number: 5674359
    Abstract: The pretreatment of cellulosic fibrous material is adjusted to improve pulp strength. The cellulosic material is initially pretreated with a low temperature alkaline liquid (e.g. 80.degree.-110.degree. C.), and then with a higher temperature (but still below cooking temperature), higher alkali concentration liquor. Only then is the material--which has alkali which has completely penetrated the cellulose fiber walls--subjected to cooking with white liquor at a temperature of about 150.degree.-180.degree. C. Green, white, or black liquor can be used in the first impregnation zone, while white liquor (with polysulfide addition) is preferably used in the second zone.
    Type: Grant
    Filed: February 8, 1995
    Date of Patent: October 7, 1997
    Assignee: Ahlstrom Machinery Inc.
    Inventors: R. Fred Chasse, Bruno S. Marcoccia, Kaj O. Henricson
  • Patent number: 5620562
    Abstract: Kraft pulp of increased strength and bleachability may be produced with decreased consumption of effective alkali, and at a lower H factor, by keeping the dissolved organic material (DOM) concentration low substantially through the entire kraft cook, including by extracting high DOM liquid from at least one part of a continuous digester and replacing it with much lower level DOM liquid. Existing pulp mills having two-vessel hydraulic, one-vessel hydraulic, or other systems may be retrofit to provide for extractions and additions of low DOM dilution liquor (including substantially DOM-free white liquor). Also, commercial size batch digesters (8 tons per day of pulp or more) can be operated with low DOM liquor to produce increased strength pulp. Using dilution with low DOM liquor also results in reduced H factor and effective alkali consumption, and increased bleachability.
    Type: Grant
    Filed: April 3, 1996
    Date of Patent: April 15, 1997
    Assignee: Ahlstrom Machinery Inc.
    Inventors: Bruno S. Marcoccia, J. Robert Prough, Richard O. Laakso, Joseph R. Phillips, Rolf C. Ryham, Jan T. Richardsen, R. Fred Chasse