Abstract: The present invention involves an improved process for the preparation of Indocyanine green of Formula (I) having high purity of about 99%, wherein the process comprises steps of reacting 1,1,2-trimethyl-1H-benzo[e]indole with 1,4-butane sulfone in boiling solvent to give 4-(1,1,2-trimethyl-1H-benzo[e]indolium-3-yl)butane-1-sulfonate. Followed by reacting 4-(1,1,2-trimethyl-1H-benzo[e]indolium-3-yl)butane-1-sulfonate of Formula (IV) and N-phenyl-N-((1E,3E,5E)-5-(phenylimino)penta-1,3-dienyl)acetamide of formula (V) in presence of sodium acetate and alcohol; and extracting the title compound formula (I) with an ester solvent.
Type:
Grant
Filed:
November 29, 2016
Date of Patent:
May 14, 2019
Assignee:
DISHMAN CARBOGEN AMCIS LIMITED
Inventors:
Janmejay Rajnikant Vyas, Himani Dhotre, Narasimha Sarma, Babulal R. Patel, Dinesh Kumar Sharma, Dilip N. Patel, Ashish A. Soni
Abstract: A crushing drying device includes an object-to-be-treated supply port from which an object is supplied into a main body, a crushing portion for crushing the object by hammers rotated on a drive shaft, and a classifying portion having a space for circulating the object to be treated at a position away from the crushing portion, the crushing portion has a dry gas supply port from which the heated air is supplied in a predetermined direction along an inner surface of the device main body, and the classifying portion has discharge portions from which the crushed object is discharged together with the heated air, and deviation plates for changing a flow of the object transferred to the classifying portion, so that the crushing drying device is one machine.
Abstract: A hydrocarbon sequestering product, a method to obtain the product, and a method and a facility to sequester hydrocarbons, wherein the product comprises an oleophilic filamentous material that gets in contact with a medium contaminated by one or more hydrocarbons with the purpose of sequestrating the hydrocarbon(s) present in the medium to free it from said hydrocarbons.
Abstract: A wide variety of end products may be manufactured from fibers or fiber pulp derived from feathers. Examples of such end products are paper and paper-like products, non-woven and woven fibers, insulation, filters, extrusions, and composite sheets and plates.
Type:
Grant
Filed:
June 6, 1995
Date of Patent:
January 6, 1998
Assignee:
The United States of America as represented by the Secretary of Agriculture
Inventors:
George Gassner, III, Walter Schmidt, Michael J. Line, Clayton Thomas, Rolland M. Waters
Abstract: This invention relates to a process for the treatment of insulating materials in the supple, fluffy state, such as down, wherein the fluff of the down is subjected to a physical treatment adapted to take the filaments of the fluff into a substantially radial position, giving the fluff its maximum volume in which it is stabilized by the superficial deposit of a resin. The apparatus for carrying out the process comprises a dehydration enclosure in the form of a rotating drum with inner blades, hot air inlet and upper evacuation. The invention is more particularly applicable to the treatment of down for filling duvets, sleeping bags or the like.