With Partitions Patents (Class 196/111)
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Patent number: 11298647Abstract: The packing has one or more thin-layer packing elements that are installed upright, the packing element having a main body portion with a planar liquid film formation surface, and one or more wall portions that are provided upright relative to the liquid film formation surface along a linear direction. The side surface of each wall portion has a curved portion at the base thereof connected to the liquid film formation surface, the curved portion curving so as to continue into the liquid film formation surface.Type: GrantFiled: January 24, 2019Date of Patent: April 12, 2022Assignees: IHI Corporation, University Public Corporation OsakaInventors: Yoshiyuki Iso, Ryosuke Ikeda, Shiko Nakamura, Kenji Katoh, Tatsuro Wakimoto
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Patent number: 11219840Abstract: The present disclosure relates to a dividing wall distillation column and a method for refining vinylidene dichloride by using the same and, more specifically, to a dividing wall distillation column capable of refining, in a high purity, vinylidene dichloride from a crude product; and a method for refining vinylidene dichloride by using the same. According to the dividing wall distillation column of the present disclosure and the method for refining vinylidene dichloride by using the same, vinylidene dichloride can be refined, in a high purity, from a crude product having a small amount of vinylidene dichloride and a large quantity of high boiling components, and energy consumption can be reduced more than that in conventional cases.Type: GrantFiled: September 14, 2018Date of Patent: January 11, 2022Assignee: HANWHA SOLUTIONS CORPORATIONInventors: Woo Youl Ahan, Shin Beom Lee
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Patent number: 11103804Abstract: A separation system includes a column including a stripping section proximal to a lower end of the column, a rectifying section proximal to an upper end of the column, and an intermediate section disposed between the stripping section and the rectifying section. The intermediate section includes first and second vertical sides separated by a vertical wall. The column includes a feed port to receive a material stream to be separated. The separation system further includes a reboiler in fluid communication with the column. The reboiler provides vapor to the stripping section. The separation system also includes a condenser in fluid communication with the column. The condenser provides liquid to the rectifying section, the condenser to provide a distillate effluent stream. The separation system further includes an active vapor control to control the relative vapor flow rate to the first and second sections.Type: GrantFiled: March 28, 2018Date of Patent: August 31, 2021Assignee: GTI SOLUTIONS INTERNATIONAL LLCInventor: Ian Buttridge
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Patent number: 11052324Abstract: Systems and methods are provided for improving process control of separation systems that include one or more dividing walls within a single column. It has been discovered that improved process control can be achieved by controlling the dividing wall columns based on energy balance instead of mass balance. The energy balancing can be performed in part based on controlling temperature at a plurality of locations on the feed side within a first divided portion of the column. Using energy balancing based on temperature control at a plurality of locations on the feed side can facilitate maintaining the operation of the dividing wall columns within a single region of phase space that can be suitably approximated by linear models. This can allow conventional process controllers to manage the manipulated and controlled variables. In addition to controlling the temperature at a plurality of locations on the feed side, a plurality of other characteristics can be used as manipulated or controlled variables.Type: GrantFiled: August 20, 2019Date of Patent: July 6, 2021Assignee: ExxonMobil Research & Engineering CompanyInventors: Robert Piszczek, Philippe D'Hooghe, David A. Hokanson, Erik Kluwen
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Patent number: 10933344Abstract: A high capacity and high efficiency co-current and cross-flow vapor-liquid contacting apparatus and process is useful in distillation columns and other vapor-liquid contacting processes. The apparatus is characterized by an arrangement of offset contacting modules in horizontal stages. The modules define a co-current contacting volume and in an exemplary configuration the modules include a liquid distributor and a demister. Half modules comprise downcomers against the shell of the vessel for transporting liquid to the subjacent stage.Type: GrantFiled: March 29, 2018Date of Patent: March 2, 2021Assignee: UOP LLCInventor: Zhanping Xu
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Patent number: 10012436Abstract: A multiple pass, parallel flow downcomer tray for a mass transfer column and method for liquid-vapor contacting in a mass transfer column is provided. The multiple pass, parallel flow downcomer tray has at least four mass transfer decks configured to provide contact between an ascending vapor passing upward through apertures on the tray surface and a traversing liquid on the tray surface. The tray further includes a central downcomers disposed near a central axis of the tray and two or more peripheral downcomers disposed near the edge of the tray and spaced apart from the central axis, wherein at least two of the four mass transfer decks are configured to discharge the traversing liquid into the peripheral downcomers and two of the four mass transfer decks are configured to discharge the traversing liquid into the central downcomer.Type: GrantFiled: October 30, 2015Date of Patent: July 3, 2018Assignee: PRAXAIR TECHNOLOGY, INC.Inventors: Guang X. Chen, Steven C. Brown, John P. Ricotta
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Patent number: 9902910Abstract: A method and apparatus a crude oil treating apparatus includes a treating section and a flashing section connected together by a pipe and a flashing valve. The method includes the steps of passing wet crude oil into the treating section; separating water from the wet crude oil in the treating section; obtaining partially dry crude oil; passing the partially dry crude oil via the pipe and the flashing valve to the flashing section of the apparatus; heating the partially dry crude oil upstream of the flashing section and downstream of the flashing valve by heat exchange with the water separated from the crude oil in the treating section; and obtaining dry crude oil from the flashing section.Type: GrantFiled: May 31, 2012Date of Patent: February 27, 2018Assignee: AKER PROCESS SYSTEMS ASInventor: Fatiha Akrour
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Patent number: 9803146Abstract: The present subject matter provides a process for hydrocarbon residue upgradation. The combination of the hydrocarbon residue along with aromatic rich hydrocarbons, catalysts and surfactants allow the operation of visbreaking unit at higher temperature while producing a stable bottom product.Type: GrantFiled: August 27, 2013Date of Patent: October 31, 2017Assignee: Hindustan Petroleum Corporation Ltd.Inventors: Pramod Kumar, Madan K. Kumar, Venkata Chalapathi Rao Peddy, Venkateswarlu Choudary Nettem, Sri Ganesh Gandham
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Patent number: 9770701Abstract: The invention relates to packed contact devices used in heat/mass exchange column apparatuses in which the processes of rectification, distillation, absorption, and extraction are run, and can be applied in the oil refining, petrochemical, chemical, gas-processing, and food-manufacturing industries. A contact device for carrying out heat/mass exchange and separation of phases in sectional cross-flow packed columns in gas/liquid and liquid/liquid systems comprises a plurality of identical contact elements assembled one upon another in one or more rows in blocks held together by spokes and vertical posts, with formation of walls in the column body that are restricted on horizontal end faces by horizontal segmental baffles conjugated in an arc with the column body; thereat, arranged between the walls are liquid distributors having a perforated part, an additional baffle, deflector plates, and vertical support plates. The space between the lower and upper walls is sealed by means of battens.Type: GrantFiled: October 20, 2015Date of Patent: September 26, 2017Inventor: Igor Anatol'evich Mnushkin
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Patent number: 8968524Abstract: The invention relates to a method producing a portioned column by forming a first segment and a third segment into arcuate segments, and attaching these arcuate segments to a second z-shaped segment to from two contiguous volumes with approximately semi-circular cross-sections that combine to form a partitioned, approximately cylindrical segment.Type: GrantFiled: July 10, 2009Date of Patent: March 3, 2015Assignee: L'Air Liquid Societe Anonyme pour l'Etude et l'Exploitation des Procedes Georges ClaudeInventors: Fabrice Del Corso, Golo Zick
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Patent number: 8877014Abstract: Split-shell fractionation columns and associated processes for separating aromatic hydrocarbons. A split-shell fractionation column includes a housing shell having a first height and a partition having a second height and disposed within the housing shell. The partition includes first and second vertically oriented baffles separated by a gap region, a seal plate connecting top ends of the baffles, a first input port formed to extend through the partition for the introduction of a gas into the gap region, and a first output port formed to extend outwardly from a bottom of the gap region and through the housing shell. The partition defines a first distillation zone and a second distillation zone within the housing shell.Type: GrantFiled: December 14, 2012Date of Patent: November 4, 2014Assignee: UOP LLCInventors: Jason T. Corradi, David William Ablin
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Patent number: 8852404Abstract: An improved apparatus strips HPNA's from hydroprocessed streams in a fractionation column having a split shell configuration. Only one vapor stripping feed is required to the split shell of the fractionation column. The resulting reduction in steam requirement provides a superior fractionation in the column.Type: GrantFiled: December 14, 2010Date of Patent: October 7, 2014Assignee: UOP LLCInventors: Richard K. Hoehn, Daniel J. Breitenfeldt
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Patent number: 8845864Abstract: Provided is a dividing wall distillation column. The dividing wall distillation column includes a main column having a dividing wall. The main column includes a pressure equalization unit for pressure equalization between a preliminary divisional section and a main divisional section which are divided by the dividing wall. The dividing wall distillation column has an effect of enabling easier operations due to the uniform pressure drop between the two divisional sections divided by the dividing wall.Type: GrantFiled: February 12, 2010Date of Patent: September 30, 2014Assignee: LG Chem, Ltd.Inventors: Sung Kyu Lee, Joon Ho Shin, Jong Ku Lee
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Patent number: 8771478Abstract: A modular distillation apparatus including at least one heat exchanger that preheats contaminated liquids: a heater that heats the contaminated liquid from the heat exchanger; an evaporator condenser adapted o boil the contaminated liquid coming out of the heater to produce water vapor and contaminant concentrate, and condenser the water vapor into distilled water; a vacuum chamber capable of operating at below atmospheric pressure, the vacuum chamber housing the evaporator condenser and including at least one partition to separate the distilled water from the contaminate concentrate; a vapor compressor operably associated with the vacuum chamber to receive water vapor from the evaporator condenser in the vacuum chamber and pump the water vapor at pressure back through the evaporator condenser, wherein the heat exchanger recovers sensible heat from outgoing condensed distilled water and contaminant concentrate recycled from the vacuum chamber.Type: GrantFiled: April 24, 2008Date of Patent: July 8, 2014Assignee: Equus Environmental Ltd.Inventor: Dudley Edgar James Ward
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Patent number: 8480860Abstract: A divided exchange column includes a shell column having a first longitudinal axis, a cylindrical wall spaced apart from and surrounding the first longitudinal axis and defining a first interior space, a first divided wall column having a second longitudinal axis substantially parallel to the first longitudinal axis, and a second divided wall column having a third longitudinal axis substantially parallel to the first and the second longitudinal axes, where the first divided wall column and the second divided wall column are positioned in the first interior space of the shell column.Type: GrantFiled: October 22, 2008Date of Patent: July 9, 2013Assignee: Air Products and Chemicals, Inc.Inventor: Kenneth William Kovak
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Patent number: 8137470Abstract: A crucible assembly for deposition and an inner plate used in the crucible assembly. The crucible assembly includes a main body having an inner space accommodating a deposition material and an opening arranged at an upper portion of the inner space, a cap having an aperture arranged at a top of the main body and combined with the main body and an inner plate arranged between the main body and the cap, the inner plate covering the opening of the main body, the crucible assembly including inner channels arranged to allow vapor of the deposition material from the inner space of the main body to be expelled to an outside of the aperture in the cap via a space arranged between an outer side surface of the inner plate and an inner side surface of the cap.Type: GrantFiled: December 29, 2008Date of Patent: March 20, 2012Assignee: Samsung Mobile Display Co., Ltd.Inventors: Kyung-Soo Min, Chang-Soon Ji
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Patent number: 8092655Abstract: A dividing wall column is described which includes the following segments: a) an upper column region (1), b) an enrichment section (2) of the feed section, c) a stripping section (4) of the feed section, d) an upper part (3) of the offtake section, e) a lower part (5) of the offtake section, f) an intermediate region (9) of the feed section, g) an intermediate region (10) of the offtake section and h) a lower column region (6). The dividing wall column has a dividing wall (7) is located vertically between the segments b) (2) and d) (3) and between the segments c) (4) and e) (5). The segments b) (2), d) (3), c) (4) and e) (5) have separation-active internals, Segment b (2) has a cross-sectional area Ab which is at least 10% smaller than the cross-sectional area Ad of segment d) (3), and segment c) has a cross-sectional area Ac which is at least 10% greater than the cross-sectional area Ae of segment e) (5).Type: GrantFiled: February 14, 2001Date of Patent: January 10, 2012Assignee: BASF AktiengesellschaftInventors: Wolfram Burst, Horst Hartmann, Gerd Kaibel, Guido Harms
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Publication number: 20110139604Abstract: A dividing wall column comprises the following segments: a) an upper column region (1), b) an enrichment section (2) of the feed section, c) a stripping section (4) of the feed section, d) an upper part (3) of the offtake section, e) a lower part (5) of the offtake section, f) an intermediate region (9) of the feed section, g) an intermediate region (10) of the offtake section and h) a lower column region (6). For the purposes of the present invention, it is essential that the dividing wall (7) is located vertically between the segments b) (2) and d) (3) and between the segments c) (4) and e) (5), the segments b) (2), d) (3), c) (4) and e) (5) have separation-active internals and the cross-sectional area Ab of the segment b) (2) is at least 10% smaller than the cross-sectional area Ad of segment d) (3), and the cross-sectional area Ac of the segment c) (4) is at least 10% greater than the cross-sectional area Ae of segment e) (5).Type: ApplicationFiled: February 14, 2001Publication date: June 16, 2011Inventors: Wolfram Burst, Horst Hartmann, Gerd Kaibel, Guido Harms
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Patent number: 7713386Abstract: The apparatus includes an alkylation unit connected to a first benzene recycle conduit, a feed conduit and an alkylation effluent conduit; a transalkylation unit connected to an polyalkylbenzene recycle conduit, a second benzene recycle conduit, and a transalkylation effluent conduit. A dividing wall distillation column is in fluid communication with the transalkylation effluent conduit, the alkylation effluent conduit, a product stream, a bottoms stream conduit and first and second benzene recycle conduits. A polyalkylbenzene fractionation column is connected to the bottoms stream conduit, the polyalkylbenzene recycle conduit and a heavy component conduit.Type: GrantFiled: May 23, 2007Date of Patent: May 11, 2010Assignee: UOP LLCInventors: Michael A. Schultz, Steven P. Lankton, Constante P. Tagamolila
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Patent number: 7714180Abstract: A process and apparatus for recovering product from reactor effluent of a reactor for a hydrocarbon feedstream is disclosed. An indigenous C4 stream is used as lean oil in a demethanizer, which facilitates significant cost and operational savings. C4 bottoms from a downstream depropanizer is used as lean oil recycle.Type: GrantFiled: August 16, 2007Date of Patent: May 11, 2010Assignee: ExxonMobil Chemical Patents Inc.Inventors: David J Duhon, John E Asplin
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Patent number: 7691239Abstract: A differential vapor pressure (DYP) cell is disposed in a divided wall column that receives a feed comprising a first, second, and third component. A separation section on the feed side of the divided wall column separates the feed in a vapor comprising the first and second component, and a liquid comprising the second and third component. The DYP cell is disposed in the divided wall column at a level below the point where the feed enters the column, and the DYP cell measures the concentration of the first component.Type: GrantFiled: December 4, 2002Date of Patent: April 6, 2010Assignee: Fluor Technologies CorporationInventors: Henry Kister, Walt Stupin
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Patent number: 7329330Abstract: A process for working up by distillation the crude products obtained in the process according to DE-A 196 07 954 and containing 1,6-hexanediol (HDO), 1,5-pentanediol (PDO) or caprolactone (CLO) in order to obtain the corresponding pure products, the working-up by distillation being carried out in each case in a dividing wall column (TK) in which a dividing wall (T) is arranged in the longitudinal direction of the column with formation of an upper common column region (1), a lower common column region (6), a feed section (2, 4) having a rectification section (2) and stripping section (4), and a take-off section (3, 5) having a stripping section (3) and rectification section (5), with feeding of the respective crude product HDO, PLO or CLO in the middle region of the feed section (2, 4) and removal of the high boiler fraction (C) from the bottom of the column, of the low boiler fraction (A) via the top of the column and of the medium boiler fraction (B) from the middle region of the take-off section (3, 5), orType: GrantFiled: January 8, 2002Date of Patent: February 12, 2008Assignee: Basf AktiengesellschaftInventors: Martin Gall, Gerd Kaibel, Thomas Krug, Harald Rust, Frank Stein
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Patent number: 7267746Abstract: A control apparatus and control method for controlling the separation in a dividing wall distillation column of at least two feeds into at least three products is disclosed. The apparatus uses a temperature measuring device to measure the temperature of fluid in the column, a controller, and a means for adjusting the temperature of fluid in the column. The temperature measuring device may be on either side of the dividing wall or above or below the dividing wall, and more than one such device may be used. The apparatus and method may be used in the production of alkylaromatic hydrocarbons by alkylating aromatic hydrocarbons with olefinic hydrocarbons.Type: GrantFiled: August 27, 2003Date of Patent: September 11, 2007Assignee: UOP LLCInventors: James W. Harris, Steven P. Rosenblum, Michael A. Schultz, Dennis E. O'Brien, Douglas G. Stewart
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Patent number: 7129387Abstract: An apparatus for recovering ethylene from a hydrocarbon feed stream, where the apparatus is a single distillation column pressure shell encasing an upper region and a lower region. The upper region houses an ethylene distributor rectifying section and the lower region houses a C2 distributor section and an ethylene distributor stripping section. Vapor passes from the lower region into the upper region, and liquid passes from the upper region to the lower region. The process for recovering the ethylene is also disclosed. The hydrocarbon feed stream is introduced into the C2 distributor section, and after a series of stripping and refluxing steps, distinct hydrocarbon products are recovered from the C2 distributor section, the ethylene distributor stripping section, and the ethylene distributor rectifying section, respectively.Type: GrantFiled: March 20, 2003Date of Patent: October 31, 2006Assignee: BP Corporation North America Inc.Inventors: Rian Reyneke, Michael J. Foral, Guang-Chung Lee
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Patent number: 7090748Abstract: A dividing-wall column having a dividing wall which is essentially disposed along the long direction of the column is proposed, which divides the column interior into a feed part, a take off part, an upper shared column part and a lower shared column part, with feed in whole or in part in the vaporous state of a mixture to be separated between the upper region of the feed part and the lower region of the feed part and/or side stream take off in whole or in part in the vaporous state between the upper region of the take off part and the lower region of the take off part, where if feed is in whole or in part in the vaporous state the cross-sectional area of the upper region of the feed part is increased by plane-parallel displacement of the dividing wall toward the upper region of the take off part, and/or if the side stream take off is in whole or in part in the vaporous state, the cross-sectional area of the lower region of the take off part is increased by displacement of the dividing wall toward the lower rType: GrantFiled: December 16, 2002Date of Patent: August 15, 2006Assignee: BASF AktiengesellschaftInventors: Gerd Kaibel, Christian Miller, Katrin Klass, Alois Kindler, Werner Aquila, Walter Dobler, Klaus Breuer, Achim Pommer, Thomas Dirnsteiner
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Patent number: 7001490Abstract: Crude ammonia is separated into a low boiler fraction, a high boiler fraction and an intermediate-boiling pure fraction by continuous fractional distillation in a distillation apparatus configured either as a dividing wall column or as a system of thermally coupled distillation columns. In the process of the present invention, the low boiler fraction is taken off at the top of the distillation apparatus. The intermediate-boiling pure fraction is obtained at a side offtake which is preferably provided with droplet precipitators. In addition, the gas loading of the distillation column is restricted so that the operating pressure is in the range from 2 to 30 bar and the F factor does not exceed 2.0 Pa0.5.Type: GrantFiled: January 24, 2001Date of Patent: February 21, 2006Assignee: BASF AktiengesellschaftInventors: Karl-Heinz Wostbrock, Gerd Kaibel, Christian Tragut, Gabriele Anken
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Patent number: 6793770Abstract: The invention concerns an evaporator, especially for the sugar industry, with at least two heat exchangers, into the top of which the medium to be concentrated is loaded and which are heated with steam with different compositions and/or different pressures in a cross stream, wherein the concentrated medium and the exhaust steam generated, after they come out of the heat exchanger, are carried off separately. To produce an evaporator that is simple and inexpensive in design, the invention proposes that the medium to be concentrated be loaded by a medium distribution common to all heat exchangers and the medium leaving the first heat exchanger go directly into the next heat exchanger. Only after the medium comes out of the second heat exchanger are the exhaust steam and the medium separated. The steam spaces in the heat exchanger separated from the exhaust steam space are separated from one another by a common dividing wall.Type: GrantFiled: November 6, 2000Date of Patent: September 21, 2004Assignee: Balcke-Durr Energietechnik GmbHInventors: Klaus Niepoth, Boris Morgenroth
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Patent number: 6770173Abstract: Partitions for columns for the separation of components or chemical reactions are assembled from plates or wall elements provided with plug and clamp connectors along respective edges and formed by strips so that the partitions can be easily and safely assembled and disassembled.Type: GrantFiled: September 28, 2000Date of Patent: August 3, 2004Assignee: Julius Montz GmbHInventors: Helmut Jansen, Jochen Leben, Thomas Rietfort, Egon Zich
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Publication number: 20040045804Abstract: A process for obtaining pure 1,3-butadiene from crude 1,3-butadiene by distillation is carried out in a dividing wall column in which a dividing wall is located in the longitudinal direction of the column to form an upper common column region, a lower common column region, a feed section and an offtake section.Type: ApplicationFiled: October 14, 2003Publication date: March 11, 2004Inventors: Gerd Bohner, Klaus Kindler, Melanie Pahl, Gerd Kaibel
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Publication number: 20040040829Abstract: A process for working up by distillation the crude products obtained in the process according to DE-A 196 07 954 and containing 1,6-hexanediol (HDO), 1,5-pentanediol (PDO) or caprolactone (CLO) in order to obtain the corresponding pure products, the working-up by distillation being carried out in each case in a dividing wall column (TK) in which a dividing wall (T) is arranged in the longitudinal direction of the column with formation of an upper common column region (1), a lower common column region (6), a feed section (2, 4) having a rectification section (2) and stripping section (4), and a take-off section (3, 5) having a stripping section (3) and rectification section (5), with feeding of the respective crude product HDO, PLO or CLO in the middle region of the feed section (2, 4) and removal of the high boiler fraction (C) from the bottom of the column, of the low boiler fraction (A) via the top of the column and of the medium boiler fraction (B) from the middle region of the take-off section (3, 5), orType: ApplicationFiled: June 25, 2003Publication date: March 4, 2004Inventors: Martin Gall, Gerd Kaibel, Thomas Krug, Harald Rust, Frank Stein
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Publication number: 20040026224Abstract: An object of the present invention is to provide a method for simulating a distillation apparatus having a coupling-type distillation column (10), the method speeding completion of simulation operation. The simulation for the distillation apparatus including a coupling-type distillation column (10) is performed by use of a simulation program for simulating a distillation apparatus including a main column (31) and a side column (32) in combination.Type: ApplicationFiled: April 28, 2003Publication date: February 12, 2004Inventors: Shizuo Midori, Yurie Ohkuma, Tamura Katsunori, Yoichi Harada
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Patent number: 6682633Abstract: A modular apparatus for fractional distillation and other forms of vapor-liquid contacting is presented. The apparatus performs cocurrent contacting of vapor and liquid in a number of identical structural units which are placed in horizontal layers in a column or other enclosure. The structural units, or modules, are horizontally spaced apart in each layer to provide spaces for the downcomers from the modules of the next higher layer. The downcomers deliver the liquid to one of two inclined contacting channels, with the contacting channels discharging the vapor and liquid into separation chambers at the top of the module. Vapor flows upward from the separation chambers to the contacting channel of the next higher module and liquid flows down through a single central downcomer to the next lower contacting channel.Type: GrantFiled: December 22, 2000Date of Patent: January 27, 2004Assignee: UOP LLCInventors: Zhanping Xu, Dennis H. Bielinski
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Publication number: 20030230476Abstract: Process for the purification of toluenediisocyanate from a crude distillation feed comprising toluenediisocyanate, an organic solvent and less than 2% by weight phosgene by separating the crude distillation feed in a dividing-wall distillation column into at least four product fractions P1-P4.Type: ApplicationFiled: June 9, 2003Publication date: December 18, 2003Inventors: Bill Brady, Friedhelm Steffens, Berthold Keggenhoff, Kai Verkerk, Gerhard Ruffert
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Patent number: 6645350Abstract: Problems generated by heat transfer through the vertical dividing wall of a trayed “dividing wall column” and into a downcomer of a tray are mitigated by providing a separate vertical isolation wall between the downcomer and dividing wall. The isolation wall forms one side of the downcomer and is spaced a short distance outward from the dividing wall to form an isolation volume which thermally insulates the downcomer from the dividing wall. The added wall is parallel to the dividing wall and supplants the dividing wall as a part of the downcomer. It eliminates a need to insulate the dividing wall.Type: GrantFiled: June 15, 2001Date of Patent: November 11, 2003Assignee: UOP LLCInventor: Paul C. Steacy
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Publication number: 20030183501Abstract: A distillation apparatus includes a column body; a partition for dividing the interior of the column body; a first distillation section composed of an enriching section and an exhaust section; a second distillation section composed of an enriching section formed above an upper end of the first distillation section, and an exhaust section located adjacent to the enriching section of the first distillation section; a third distillation section composed of an enriching section located adjacent to the exhaust section of the first distillation section, and an exhaust section formed below a lower end of the first distillation section; a condenser; a negative pressure generation system for generating a negative pressure to thereby withdraw vent gas; a gas cooler for cooling the vent gas; a first discharge system disposed at the side of the column body and adapted to discharge liquid rich in a medium-boiling-point component formed from a high-melting-point material; and a second discharge system disposed at the bottoType: ApplicationFiled: May 2, 2003Publication date: October 2, 2003Applicant: SUMITOMO HEAVY INDUSTRIES, LTD.Inventors: Katsunori Tamura, Yoichi Harada
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Publication number: 20030116420Abstract: A dividing-wall column having a dividing wall which is essentially disposed along the long direction of the column is proposed, which divides the column interior into a feed part, a take off part, an upper shared column part and a lower shared column part, with feed in whole or in part in the vaporous state of a mixture to be separated between the upper region of the feed part and the lower region of the feed part and/or side stream take off in whole or in part in the vaporous state between the upper region of the take off part and the lower region of the take off part, where if feed is in whole or in part in the vaporous state the cross-sectional area of the upper region of the feed part is increased by plane-parallel displacement of the dividing wall toward the upper region of the take off part, and/or if the side stream take off is in whole or in part in the vaporous state, the cross-sectional area of the lower region of the take off part is increased by displacement of the dividing wall toward the lower rType: ApplicationFiled: December 16, 2002Publication date: June 26, 2003Inventors: Gerd Kaibel, Christian Miller, Katrin Klass, Alois Kindler, Werner Aquila, Walter Dobler, Klaus Breuer, Achim Pommer, Thomas Dirnsteiner
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Patent number: 6582564Abstract: A distillation apparatus includes a column body; a partition for dividing the interior of the column body; a first distillation section composed of an enriching section and an exhaust section; a second distillation section composed of an enriching section formed above an upper end of the first distillation section, and an exhaust section located adjacent to the enriching section of the first distillation section; a third distillation section composed of an enriching section located adjacent to the exhaust section of the first distillation section, and an exhaust section formed below a lower end of the first distillation section; a condenser; a negative pressure generation system for generating a negative pressure to thereby withdraw vent gas; a gas cooler for cooling the vent gas; a first discharge system disposed at the side of the column body and adapted to discharge liquid rich in a medium-boiling-point component formed from a high-melting-point material; and a second discharge system disposed at the bottoType: GrantFiled: March 21, 2001Date of Patent: June 24, 2003Assignee: Sumitomo Heavy Industries, Ltd.Inventors: Katsunori Tamura, Yoichi Harada
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Patent number: 6558515Abstract: A control method and apparatus for regulating the rate of vapor flow in the two adjacent sections of a dividing wall fractional distillation column are presented. The liquid level on a tray at the top of each section is used to control the rate of vapor flow through the tray. The liquid level is controlled by measuring the pressure differential across the tray in each section and varying the flow of liquid to this tray in response to the differential.Type: GrantFiled: April 23, 2001Date of Patent: May 6, 2003Assignee: UOP LLCInventor: Paul C. Steacy
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Patent number: 6551465Abstract: The operation of the dividing wall section of a dividing wall column is controlled by a control apparatus comprising a ratio controller which divides the liquid flowing into the dividing wall section. The rate of return of overhead liquid to the column is set by monitoring the temperature in the top of the product dividing wall section and the sidecut product draw rate is set by monitoring a temperature in the bottom of the product dividing wall section.Type: GrantFiled: April 23, 2001Date of Patent: April 22, 2003Assignee: UOP LLCInventors: Charles P. Van Zile, James W. Harris
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Publication number: 20030047438Abstract: An object of the present invention is to reduce the number of instruments used in a distillation apparatus to thereby simplify control.Type: ApplicationFiled: October 25, 2002Publication date: March 13, 2003Applicant: SUMITOMO HEAVY INDUSTRIES, LTD.Inventors: Katsunori Tamura, Ken Nishiyama, Taizo Inoue, Keiji Yoshimoto, Noboru Okamoto, Minoru Nagashima
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Patent number: 6514387Abstract: The invention relates to a rectifying column for extractive distillation, comprising a column main section (204) and a raffinate section (205) above said main section, an evaporator (208) situated on the lower end of the column, an inlet (214) disposed between the main section of the column and the raffinate section and a solvent inlet (215) arranged on the top side of the raffinate section (205) for feeding an extracting agent. According to the invention, the main section (204) has two chambers (216, 217) connected in parallel. A stripping section (222) is disposed between the bottom of the column (221) and the main section (204), in which concentration of the extracting agent occurs from the top down. The bottom (221) is connected to the solvent inflow (215) by a device (223) for recycling the extracting agent.Type: GrantFiled: August 1, 2000Date of Patent: February 4, 2003Assignee: Krupp Uhde GmbHInventors: Gerd Emmrich, Bärbel Kolbe, Helmut Gehrke, Frank Ennenbach, Uwe Ranke
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Patent number: 6395138Abstract: This distributor (1) includes: a primary distributor (3) which delimits a closed volume provided with liquid predistribution openings (8) which open into the column; a device for feeding the primary distributor (3) with liquid under a pressure very much greater than the internal pressure of the column; and a secondary distributor (4) which occupies substantially the entire cross-section of the column, which includes a gas overhead in communication with the internal space of the column and which is subdivided by partitions (13, 17) into a plurality of compartments (16), each of which receives liquid originating from at least one of the said openings (8) of the primary distributor (3), this secondary distributor (4) having a bottom (9) provided with orifices (12) for fine distribution of the liquid over virtually the entire cross-section of the column, the number of these orifices being very much greater than the number of openings (8) of the primary distributor.Type: GrantFiled: May 17, 2000Date of Patent: May 28, 2002Assignee: L'Air Liquide, Societe Anonyme a Directoire et Conseil de Surveillance pour l'Etude et l'Exploitation des Procedes Georges ClaudeInventors: Bernard Darredeau, Jean-Yves Lehman
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Patent number: 6387222Abstract: A method of distillation for separating a material which is solid at ambient temperature from a lower boiling and lower melting point material, and the apparatus.Type: GrantFiled: March 30, 2000Date of Patent: May 14, 2002Assignee: BASF AktiengesellschaftInventors: Christian Tragut, Gerd Kaibel
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Patent number: 6365006Abstract: The present invention pertains to the alcohol processing industry and relates to a method that includes feeding a mixture into a distillation column which is fitted with contact devices for discharging the vapors through the top of said column. This method further includes boiling a bottom product and supplying the vapor thus formed back into the column. A part of the vapor to be processed using one of said contact devices is then fed back into the vapor flow or liquid flow towards one at least of said devices located upstream relative to the flow direction. In another or the same embodiment, a part of the vapor is fed back into the liquid flow under the level thereof and towards the same contact device in a place that is located upstream from its discharge relative to the flow direction of said vapor. The vapor feedback is preformed without complete condensation thereof.Type: GrantFiled: May 27, 1999Date of Patent: April 2, 2002Assignee: General Electric CompanyInventors: Valery J. Aristovich, Jury V. Aristovich, Andrey J. Sokolov, Elena V. Sokolova
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Publication number: 20020023830Abstract: A distillation apparatus includes a column body; a partition for dividing the interior of the column body; a first distillation section composed of an enriching section and an exhaust section; a second distillation section composed of an enriching section formed above an upper end of the first distillation section, and an exhaust section located adjacent to the enriching section of the first distillation section; a third distillation section composed of an enriching section located adjacent to the exhaust section of the first distillation section, and an exhaust section formed below a lower end of the first distillation section; a condenser; a negative pressure generation system for generating a negative pressure to thereby withdraw vent gas; a gas cooler for cooling the vent gas; a first discharge system disposed at the side of the column body and adapted to discharge liquid rich in a medium-boiling-point component formed from a high-melting-point material; and a second discharge system disposed at the bottoType: ApplicationFiled: March 21, 2001Publication date: February 28, 2002Applicant: SUMITOMO HEAVY INDUSTRIES, LTD.Inventors: Katsunori Tamura, Yoichi Harada
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Patent number: 6348137Abstract: An apparatus and a method for separating a liquid mixture by fractional distillation. The apparatus includes at least two chambers with a conduit from the lower portion of a chamber which contains liquid to the upper portion of an adjacent chamber, a source of pressurized vapor, and a conduit from the source of pressurized vapor to the lower portion of the chamber which contains liquid. Flow of the liquid from the chamber which contains liquid is effected by introducing pressurized vapor into the liquid, thereby reducing the density of the liquid, pumping the liquid into the upper portion of the adjacent chamber. The two or more chambers can be housed in a single circular vessel, where the chambers are separated by partitions radiating from the center of the cylindrical vessel to the wall of the vessel. The apparatus can have a reduced height compared to conventional distillation columns.Type: GrantFiled: January 7, 2000Date of Patent: February 19, 2002Assignee: IOR Energy Pty Ltd.Inventor: Arthur Nommensen
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Publication number: 20010052453Abstract: In a dividing wall column comprising as segmentsType: ApplicationFiled: May 3, 2001Publication date: December 20, 2001Inventors: Harald Rust, Gerd Kaibel
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Publication number: 20010010286Abstract: Crude ammonia is separated into a low boiler fraction, a high boiler fraction and an intermediate-boiling pure fraction by continuous fractional distillation in a distillation apparatus configured either as a dividing wall column or as a system of thermally coupled distillation columns. In the process of the present invention, the low boiler fraction is taken off at the top of the distillation apparatus. The intermediate-boiling pure fraction is obtained at a side offtake which is preferably provided with droplet precipitators. In addition, the gas loading of the distillation column is restricted so that the operating pressure is in the range from 2 to 30 bar and the F factor does not exceed 2.0 Pa0.5.Type: ApplicationFiled: January 24, 2001Publication date: August 2, 2001Inventors: Karl-Heinz Wostbrock, Gerd Kaibel, Christian Tragut, Gabriele Anken
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Patent number: 6165325Abstract: A vacuum vessel for continuous or semicontinuous treatment of fatty oils in connection with deodorization includes spaces through which the oil which is to be treated is brought to pass. The vessel also contains U-tubes used to heat or cool the oil and perforated pipes arranged at the bottom of the vessel. Through these pipes stripping gas is led into the oil. The vacuum vessel is connected to a vacuum source. According to the invention the vessel has the form of a container with a mainly rectangular bottom with partitions parallel to a long side of the container. These partitions delimit channels connected in series through which the oil passes. The bottom of a first channel as seen in the direction of flow is arranged on a higher level than the second channel seen in the direction of flow such that the oil is forced to pass through the vessel by gravity. The vacuum vessel has a low height in relation to the length of its sides.Type: GrantFiled: March 4, 1997Date of Patent: December 26, 2000Assignee: Alfa Laval ABInventors: Peter Sjoberg, Anders M.A. Hillstrom
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Patent number: 6077985Abstract: An integrated deethanizer and ethylene fractionation column and process for separating a feed stream comprising ethylene, ethane and C.sub.3+ is disclosed. A single shell houses a refluxed upper portion and a lower portion of the column. A generally vertical wall partitions the lower portion of the column into a deethanizer section and an ethylene stripper section. The upper column portion is used as the absorption section of the ethylene fractionator. The feed is supplied to an intermediate stage in the deethanizer, and the deethanizer is operated at a lower pressure (and correspondingly lower temperature) matching that of the ethylene fractionation. The design allows the use of one slightly larger column in place of the two large columns previously used for separate deethanization and ethylene fractionation.Type: GrantFiled: March 10, 1999Date of Patent: June 20, 2000Assignee: Kellogg Brown & Root, Inc.Inventor: Karl Stork