Vacuum Patents (Class 196/114)
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Patent number: 11097203Abstract: A system to treat and desalinate wastewater using a low energy ejector desalination system (LEEDS), which employs a static liquid-gas ejector and maximum heat integration in the water treatment system.Type: GrantFiled: March 10, 2020Date of Patent: August 24, 2021Assignee: BECHTEL HYDROCARBON TECHNOLOGY SOLUTIONS, INC.Inventors: Jorge T. Aguinaldo, Joseph P. Kanzleiter, Saurabh Tonapi, Mukesh K. Shah
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Patent number: 11027215Abstract: Vacuum distillation apparatus and methods are provided. In an embodiment, an apparatus is provided that includes an evaporation chamber having a bottom flow rate control (FRC) surface that is curved to provide multiple flow rates to a solution as it flows across the bottom surface. The apparatus also includes a wiper that is curved to match the curve of the bottom FRC surface and wipes the bottom FRC surface to distribute the solution. A heater heats the bottom FRC surface to evaporate one or more components from the moving solution.Type: GrantFiled: April 1, 2019Date of Patent: June 8, 2021Inventors: Paul Simon, Craig Marion, Tina Asher Marion
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Patent number: 10746477Abstract: Systems and methods for degassing and charging phase-change thermal devices are disclosed. In one embodiment, a system includes a flask, a first shut-off valve fluidly coupled to an outlet of the flask, and a first valve fluidly coupled to the first shut-off valve by a fluid line. The system further includes a second valve fluidly coupled to the first valve, wherein the second valve is operable to be fluidly coupled to the phase-change thermal device, a second shut-off valve fluidly coupled to the second valve, a third valve fluidly coupled to the first valve, a vacuum pump fluidly coupled to the third valve, and a fluid injection device fluidly coupled to the fluid line between the first valve and the first shut-off valve. The fluid injection device draws the working fluid from the flask and injects a desired amount into the phase-change thermal device.Type: GrantFiled: October 7, 2016Date of Patent: August 18, 2020Assignee: Toyota Motor Engineering & Manufacturing North America, Inc.Inventors: Feng Zhou, Yanghe Liu, Ercan Mehmet Dede, Shailesh N. Joshi
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Patent number: 10655070Abstract: Process for reclaiming useful products from a waste oil, comprising a thermal separation step performed in a vessel at conditions, of temperature and pressure, allowing to substantially avoid cracking of the waste oil and to assure the separation of said heated waste oil into a first heavy oil fraction and into a second light oil fraction having, in comparison with the waste oil, a low content in solids and/or in other contaminants that are different from water and from inert gas.Type: GrantFiled: February 13, 2013Date of Patent: May 19, 2020Inventors: Lucie B. Wheeler, Louis Bertrand
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Patent number: 10358507Abstract: The present invention is directed to a process for separating hydrocarbons from a solution comprising a polymer. The process comprises the steps of: (A) withdrawing a solution stream comprising the polymer from a first vessel; (B) passing the solution stream into a flash vessel; (C) spraying the solution stream into droplets in the first flash vessel thereby establishing a stream of droplets within the flash vessel. The solution forms a downwards falling film within the flash vessel.Type: GrantFiled: March 24, 2016Date of Patent: July 23, 2019Assignee: BOREALIS AGInventors: Mohammad Al-Haj Ali, Vasileios Kanellopoulos, Apostolos Krallis, Henry Sleijster, Samuli Zitting
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Patent number: 9999843Abstract: An apparatus, system and method are provided for controlling fluid flow through a vacuum chamber of a dehydration system, the vacuum chamber having a temperature sensing device operative to measure a temperature of a fluid in the vacuum chamber. A temperature difference between a temperature setpoint for the fluid and the measured temperature of the fluid is determined, and fluid is recirculated through the vacuum chamber while the temperature difference is greater than a predetermined temperature difference. While the temperature difference is less than the predetermined temperature difference, the fluid is recirculated through the vacuum chamber for a predetermined time period, and upon the predetermined time period expiring inhibiting recirculation of the fluid through the vacuum chamber.Type: GrantFiled: May 13, 2014Date of Patent: June 19, 2018Assignee: Parker-Hannifin CorporationInventor: John A. Trott
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Patent number: 9719214Abstract: A liquid asphalt heating and mixing system having a double helix heat exchanger positioned within a liquid asphalt storage vessel and being connected to a fluid heater and circulator to feed hot oil through said heat exchanger for heating liquid asphalt within the storage vessel. An eductor mixer is centrally aligned longitudinally with the heat exchanger with an intake end positioned interiorly of the heat exchanger and a discharge end directed away from the heat exchanger. A liquid asphalt pump is connected to the eductor mixer and to the storage vessel to pump liquid asphalt from the storage vessel, through the eductor mixer and back to the storage vessel.Type: GrantFiled: February 28, 2015Date of Patent: August 1, 2017Assignee: MAXAM EQUIPMENT, INC.Inventor: Lonnie D Greene
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Patent number: 8986536Abstract: The present invention provides a method and an apparatus for recovery of spent lubricating oil. The evaporation of hydrocarbon fractions from spent lubricating oil is carried out in three steps. The first step is at approximately 150-1030 mbar and between 70-240° C. in which is greater than 99% water, greater than 99% of ethylene glycol and greater than 50% of hydrocarbon molecules with normal boiling point up to 310° C. are evaporated from spent oil. The second step is operated at 6-30 mbar and 200-2900 C in which predominantly gasoil and light vacuum gasoil fractions are evaporated. The third step is operated at 250-320° C. and 0.5-15 mbar in which mainly heavy vacuum gasoil (boiling range of 425 to 570° C. on ASTM D-1160 test) is evaporated from spent oil.Type: GrantFiled: November 8, 2010Date of Patent: March 24, 2015Inventor: Rohit Joshi
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Patent number: 8945398Abstract: A water recovery process for a steam assisted gravity drainage system for a heavy oil recovery facility, the process comprising a flash drum and a flash drum heat exchanger/condenser, wherein the water recovery process receives hot water produced by a facility at a temperature above the water atmospheric boiling point and cools it to a temperature below the water atmospheric boiling point before transferring it to the remaining section of the water recovery process.Type: GrantFiled: March 29, 2011Date of Patent: February 3, 2015Assignee: 1nSite Technologies, Ltd.Inventor: Kenneth James
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Patent number: 8784648Abstract: A method is provided for producing vacuum in a vacuum oil-stock distillation column and includes pumping a gas-vapor medium out of a column by an ejector into a condenser; feeding a gas mixture and a high-pressure gas into a second gas-gas ejector from which the vapor-gas mixture is fed into a second condenser. A condensate is directed from the condensers into a separator in which the condensate is separated into a water-containing condensate and a hydrocarbon-containing condensate. The hydrocarbon-containing condensate is removed while the water-containing condensate is fed into a steam generator in which heat is supplied to the water-containing condensate from a hot distillate removed from the vacuum column and steam is produced from the water-containing condensate, the steam is fed as a high-pressure gas into the gas-gas ejectors. A plant for carrying out the method is also provided.Type: GrantFiled: June 24, 2009Date of Patent: July 22, 2014Inventor: Valery Grigorievich Tsegelsky
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Patent number: 8771474Abstract: A crude treatment system includes a primary and second distillation tower for treating crude containing corrosive material. The primary distillation tower fractionates first crude into a target fraction. The secondary distillation tower fractionates second crude having a corrosive material content greater than that of the first crude into a light fraction and a remaining heavy fraction. Corrosive material in the light fraction is insufficient to corrode the primary distillation tower. A light fraction supply line supplies the light fraction from the secondary distillation tower to the primary distillation tower for treatment. The secondary distillation tower and the supply line are made from a corrosion resistant material.Type: GrantFiled: November 29, 2010Date of Patent: July 8, 2014Assignee: JGC CorporationInventor: Naoaki Sawai
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Patent number: 8771478Abstract: A modular distillation apparatus including at least one heat exchanger that preheats contaminated liquids: a heater that heats the contaminated liquid from the heat exchanger; an evaporator condenser adapted o boil the contaminated liquid coming out of the heater to produce water vapor and contaminant concentrate, and condenser the water vapor into distilled water; a vacuum chamber capable of operating at below atmospheric pressure, the vacuum chamber housing the evaporator condenser and including at least one partition to separate the distilled water from the contaminate concentrate; a vapor compressor operably associated with the vacuum chamber to receive water vapor from the evaporator condenser in the vacuum chamber and pump the water vapor at pressure back through the evaporator condenser, wherein the heat exchanger recovers sensible heat from outgoing condensed distilled water and contaminant concentrate recycled from the vacuum chamber.Type: GrantFiled: April 24, 2008Date of Patent: July 8, 2014Assignee: Equus Environmental Ltd.Inventor: Dudley Edgar James Ward
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Patent number: 8722949Abstract: Systems and methods for coal liquefaction are provided. According to one embodiment, coal is introduced into a plasma furnace. A plasma energy field is generated within the plasma furnace by causing an electrical discharge between a pair of arc rods located within the plasma furnace and positioned above the coal. Hydrocarbons contained within the coal are separated from the coal by causing the plasma energy field to penetrate the coal and heat the coal to a temperature sufficient to liquefy the hydrocarbons by focusing and drawing the plasma energy field through the coal with a magnetic field created proximate to the coal. The liquefied hydrocarbons are then captured.Type: GrantFiled: October 29, 2013Date of Patent: May 13, 2014Assignee: Green Technology LLCInventors: John Lee Horning, Jan H. Matthias, Nigel Moriarty, John Stuart Lehde
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Patent number: 8597470Abstract: Systems and methods for extracting recoverable materials from source materials are provided. According to one embodiment, a plasma furnace includes an open-faced tray, a pair of arc rods, Faraday coils and a smooth interior surface. The open-faced tray carries tar sands from one end of the plasma furnace to another. The arc rods are disposed above the open-faced tray and are operable to generate a plasma energy field for vaporizing bitumen contained within the tar sands. The Faraday coils are positioned underneath the open-faced tray to create a magnetic field proximate to the tar sands and cause the plasma energy field to penetrate and heat the tar sands to a temperature sufficient to release a bond between the bitumen and the tar sands by focusing and drawing the plasma energy field through the tar sands. Vaporized bitumen condenses on the smooth interior surface from which it is collected.Type: GrantFiled: September 25, 2012Date of Patent: December 3, 2013Assignee: Green Technology LLCInventors: John Lee Horning, Jan H. Matthias, Nigel Moriarty, John Stuart Lehde
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Publication number: 20130158309Abstract: The invention provides a process and system for the depolymerisation of hydrocarbon-containing material for producing diesel oil and/or heating oil comprising a reactor adapted to exceed temperature operation of 390 degrees Celsius and provided with a plant specific exothermal heat source. In a preferred embodiment, raw materials enter the reactor in a liquid or viscous state by pre-heating and introducing it under pressure to the specially adapted reactor where further heating of the raw material takes place under vacuum.Type: ApplicationFiled: April 26, 2011Publication date: June 20, 2013Applicant: REGENERATIVE SCIENCES PATENTS LIMITEDInventors: Esther Spolzer, Walter Nutter, Rory Hughes
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Patent number: 8343316Abstract: A vacuum dehydrator for processing an oil containing entrained contaminants such as water, air, and particulates comprises a tower enclosing upper and lower chambers. A random packing is contained in the upper chamber. The oil is preheated to a temperature above the boiling point of water and is introduced into the upper chamber for downward flow through the random packing into the lower chamber. Entrained air and water is retained as water vapor in the upper chamber, and particulates are retained in the random packing. Heated ambient air is introduced into the lower chamber for upward flow through the random packing into the upper chamber, and the upper chamber is cooled to condense the water vapor. Oil and condensed water are pumped respectively from the lower and upper chambers.Type: GrantFiled: November 10, 2009Date of Patent: January 1, 2013Assignee: Siemens Industry, Inc.Inventors: Mortimer Daniel Williams, John G. Donnelly, Eric M. Laliberte, J. Rafael Lazo, Juan Alejandro Segrelles Sacristan, Anselmo Garcia Gracia
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Patent number: 8337672Abstract: The invention relates to the oil processing industry and can be used for producing vacuum in a vacuum petroleum distillation column. The inventive method involves pumping out a vapor-gas medium from the column by of a gas-gas ejector in such a way that a vapor-gas mixture is formed at the entry thereof and supplying said mixture to a condenser for producing a gas mixture and a vapor phase condensate. The gas mixture is supplied from the condenser to a liquid-gas jet apparatus and the condensate is delivered to an additional separator. A hydrocarbon-containing condensate is removed from the additional separator for the intended use thereof and a water-containing condensate is fed to a steam generator for producing steam by supplying heat of a hot distillate evacuated from the vacuum column. The thus obtained steam is used in the gas-gas ejector as a high-pressure gas.Type: GrantFiled: November 6, 2008Date of Patent: December 25, 2012Inventor: Valery Grigorievich Tsegelsky
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Publication number: 20110259795Abstract: A process of recovering base oil from lubrication oil that contains contaminants therein, the process comprises the steps of: (i) extracting a light diesel fraction from the lubrication oil; and (ii) distilling the lubricating oil under vacuum conditions after said extracting step (i) to obtain a base oil that is substantially free of said contaminants.Type: ApplicationFiled: November 2, 2009Publication date: October 27, 2011Applicant: ANNDA ENERGY PTE LTD.Inventors: Yingsui Yin, Ming Feng, Thiam Seng Lee, Disong Zhang
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Patent number: 7981253Abstract: An improved de-entrainment device for use in distillation towers, especially vacuum distillation towers used for fractionating petroleum atmospheric resids is in the form of a baffle which is to be located in the portion of the tower below the feed zone and at the top of the flash zone. The baffle is in the form of an apertured plate above the stripping zone and in its preferred form comprises number of radial fins or blades, resembling a static fan with openings between the fins to permit vapors from the lower portions of the tower to pass upwards through the baffle with a minimal pressure drop. The fins of the baffle are preferably oriented at an angle between 30° and 60° away from the incoming feed so that the incoming feed stream skims over the top edges of the fins.Type: GrantFiled: January 26, 2007Date of Patent: July 19, 2011Assignee: ExxonMobil Research & Engineering CompanyInventors: Arun K. Sharma, Theodore Sideropoulos, Rutton D. Patel, Brian D. Albert, Alvin U. Chen
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Patent number: 7718033Abstract: A one step method and system for producing nanofluids by a particle-source evaporation and deposition of the evaporant into a base fluid. The base fluid such (i.e. ethylene glycol) is placed in a rotating cylindrical drum having an adjustable heater-boat-evaporator and heat exchanger-cooler apparatus. As the drum rotates, a thin liquid layer is formed on the inside surface of the drum. A heater-boat-evaporator having an evaporant material (particle-source) placed within its boat evaporator is adjustably positioned near a portion of the rotating thin liquid layer, the evaporant material being heated thereby evaporating a portion of the evaporant material, the evaporated material absorbed by the liquid film to form nanofluid.Type: GrantFiled: July 12, 2006Date of Patent: May 18, 2010Assignee: The United States of America as represented by the United States Department of EnergyInventors: Milivoje Kostic, Mihajlo Golubovic, John R. Hull, Stephen U. S. Choi
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Patent number: 7588664Abstract: A vacuum column for oil distillation incorporates a thickened plate that has a layer of erosion-resistant material that is thicker than the corrosion-resistant thickness of an adjacent column section. Use of thickened, explosive- or roll-bonded clad plates may provide better service than either conventional plug-welded liners or conventional shell plates with weld overlays.Type: GrantFiled: July 27, 2005Date of Patent: September 15, 2009Assignee: Chicago Bridge & Iron CompanyInventors: Fahim E. Shadid, Alan W. Green
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Patent number: 7431803Abstract: A flash/separation vessel for treating hydrocarbon feedstock containing resid to provide a liquid phase and a vapor phase has: (A) an inlet for introducing hydrocarbon feedstock; (B) an inlet for adding heated vaporous diluent to the vessel to dilute the vapor phase; (C) a flash/separation vessel overhead outlet for removing the vapor phase as overhead; and (D) a flash/separation vessel liquid outlet for removing liquid phase as bottoms from the vessel.Type: GrantFiled: October 16, 2006Date of Patent: October 7, 2008Assignee: ExxonMobil Chemical Patents Inc.Inventor: Richard C. Stell
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Patent number: 7429312Abstract: The present group of inventions relates to processing of multi-component liquid mixtures (MCLM) employing reforming process, preferably for vacuum distillation of hydrocarbon mixtures and in petroleum refining and chemical industries. The inventions include the method for processing of multi-component liquid mixtures. The method of MCLM separation includes pressure feeding of a hydrocarbon liquid mixture to an a liquid-gas jet device nozzle which discharges to a vacuum chamber of liquid-gas jet device. A counter pressure jointly with the liquid-gas jet device forms a pressure surge in the vacuum chamber. The counter pressure is 0.4 to 0.7 of the magnitude of the feed pressure generated by the pump. The plant for MCLM processing includes a feed pump, a head delivery main, a discharge main, control instrumentation and a vacuum-generating device including a vacuum chamber, a liquid-gas jet device with a nozzle in the front end wall of the vacuum chamber.Type: GrantFiled: December 27, 2002Date of Patent: September 30, 2008Assignee: Energy Savings Technologies Financial Industrial Group LLCInventors: Yuriy Pavlovich Skakunov, Chamil Khakimovich Iskhakov, Sergey Vladimirovich Tishkin
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Patent number: 7267747Abstract: A vacuum distillation system and method utilizing a low capacity vacuum producing ejector operated in parallel with a primary ejector during the Winter months enables significant reduction in the absolute pressure of a vacuum distillation column. Operation of a vacuum distillation tower at lower absolute pressures results in increased yield of desirable vacuum distillation products.Type: GrantFiled: March 26, 2003Date of Patent: September 11, 2007Assignee: Chevron U.S.A. Inc.Inventor: Thomas Hugh Musial
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Patent number: 6740205Abstract: Incoming wastewater is preheated in a heat exchanger before delivery to a flash chamber through an orifice for flashing into water vapor rising into an upper section of the flash chamber which also has a bottom section into which liquid waste oil or other contaminants settles. Rise of such water vapor into the upper chamber section is induced by a vacuum established therein by a vacuum pump withdrawing the water vapor in a superheated and compressed condition for cooling within a condenser from which the incoming wastewater is delivered to a heat exchanger for preheating. The water vapor during rise into the upper section of the flash chamber is filtered to extract contaminates therefrom while liquefied water vapor thereafter formed therein is collected before the remaining water vapor is cooled into the condensate for collection within a distillate tank from which it is withdrawn for overboard discharge after being monitored for oil content.Type: GrantFiled: November 30, 2000Date of Patent: May 25, 2004Assignee: The United States of America as represented by the Secretary of the NavyInventor: Henry J. Molintas
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Patent number: 6605208Abstract: A process and apparatus are disclosed that relate generally to a process for reducing harmful or unwanted emissions during the production of asphalt, such as blue smoke. The process includes the introduction of a pump around of the wax oil fraction for re-introduction into the vacuum tower. Additional desirable features include stripping trays below the wax oil collection tray and the feed zone. The result is to produce an asphalt product that creates less blue smoke in the hot mix plant. Another desirable feature is that a product can be created that meets Performance Grade specifications with the addition of polymers or other additives.Type: GrantFiled: November 2, 2001Date of Patent: August 12, 2003Inventors: Kenneth Hucker, Sanford P. Brass
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Patent number: 6582564Abstract: A distillation apparatus includes a column body; a partition for dividing the interior of the column body; a first distillation section composed of an enriching section and an exhaust section; a second distillation section composed of an enriching section formed above an upper end of the first distillation section, and an exhaust section located adjacent to the enriching section of the first distillation section; a third distillation section composed of an enriching section located adjacent to the exhaust section of the first distillation section, and an exhaust section formed below a lower end of the first distillation section; a condenser; a negative pressure generation system for generating a negative pressure to thereby withdraw vent gas; a gas cooler for cooling the vent gas; a first discharge system disposed at the side of the column body and adapted to discharge liquid rich in a medium-boiling-point component formed from a high-melting-point material; and a second discharge system disposed at the bottoType: GrantFiled: March 21, 2001Date of Patent: June 24, 2003Assignee: Sumitomo Heavy Industries, Ltd.Inventors: Katsunori Tamura, Yoichi Harada
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Patent number: 6457563Abstract: An arrangement in a circulation lubrication system include a lubricating oil tank, pressure pipe lines for supplying oil to parts to be lubricated, return pipe lines for returning the oil from the parts to be lubricated to the oil tank, and a mechanism configured to pump oil into the pressure pipe lines and maintaining a desired state of lubrication. The mechanism configured to pump the oil into the pressure pipe lines may include a circulation lubrication pump and a suction duct through which the lubricating oil flows out of a lubricating oil tank, an underpressure tank coupled to the suction duct leading off from the lubricating oil tank, to the suction side of the circulation lubrication pump. The underpressure tank is a tank which allows the water contained in the oil to evaporate. To prevent cavitation of the circulation lubrication pump, the underpressure tank is placed substantially higher than the lubricating oil tank.Type: GrantFiled: December 10, 1999Date of Patent: October 1, 2002Assignee: Safematic OyInventors: Kari Ahlbom, Ari Airaksinen, Kari Antila, Jari Rinkinen, Arto Alfthan
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Publication number: 20020053531Abstract: A process and apparatus are disclosed that relate generally to a process for reducing harmful or unwanted emissions during the production of asphalt, such as blue smoke. The process includes the introduction of a pump around of the wax oil fraction for re-introduction into the vacuum tower. Additional desirable features include stripping trays below the wax oil collection tray and the feed zone. The result is to produce an asphalt product that creates less blue smoke in the hot mix plant. Another desirable feature is that a product can be created that meets Performance Grade specifications with the addition of polymers or other additives.Type: ApplicationFiled: November 2, 2001Publication date: May 9, 2002Inventors: Kenneth Hucker, Sanford P. Brass
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Publication number: 20020036158Abstract: A method for separating used oil in a simple batch process into usable fractions. A pretreatment step involves forming a mixture of the used oil and specified pretreatment chemicals. A reduced pressure is maintained throughout the process along with mixing of the formed mixture. Heat is applied at a predetermined rate corresponding to vaporization and recovery of usable fractions of aqueous, light hydrocarbons, base oil, and a pumpable residual. Each distillate fraction is removed as a vapor, condensed and collected. Undesirable cracking is avoided by maintaining a reduced pressure and avoiding rapid or localized heating within the mixture by mixing during the distillation process. The resulting aqueous and light fractions can be reused in the process or otherwise used. The pumpable residual can also be sold as a high quality asphalt extender. The recovered base oil fraction may be sold as a diesel fuel extender, lubricant, catalytic cracker feed stock, or #4 fuel oil for stationary power generators.Type: ApplicationFiled: August 6, 2001Publication date: March 28, 2002Inventor: Douglas P. Austin
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Patent number: 6350351Abstract: A plant for the vacuum distillation of liquids has a vacuum rectification column and a vacuum-producing device based on a liquid-gas jet apparatus. The plant is furnished additionally with a jet pump. A nozzle of the jet pump is connected to a pipeline for bleeding a liquid fraction from the column, an evacuated medium inlet of the jet pump is connected to an outlet of the liquid-gas jet apparatus and an outlet of the jet pump is connected to a separator of the vacuum-producing device. The plant provides more effective vacuum distillation of liquids.Type: GrantFiled: October 12, 1999Date of Patent: February 26, 2002Inventors: Serguei A. Popov, Mikhail V. Akimov
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Patent number: 6348134Abstract: The invention pertains to the field of oil refining and the petrochemical industry. The proposed plant for the distillation of a liquid has a vacuum rectification column with pipes for feed of a stock product and for bleeding of a gas-vapor phase and at least one liquid fraction; and a vacuum-producing device composed of a liquid-gas jet apparatus, a separator, a pump and a condenser. The gas intake of the liquid-gas jet apparatus is connected to the pipeline for bleeding of a gas-vapor phase, the liquid intake of the jet apparatus is connected to the discharge side of the pump and the outlet of the jet apparatus is connected to the condenser's intake. The intake of the separator is connected to the condenser's outlet, the liquid outlet of the separator is connected to the suction side of the pump and the gas outlet of the separator is connected to consumers of compressed gas.Type: GrantFiled: October 14, 1998Date of Patent: February 19, 2002Inventor: Serguei A. Popov
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Patent number: 6346173Abstract: The invention essentially relates to a method for vacuum distillation of liquids that includes feeding a polar liquid into a vacuum-producing liquid-gas jet apparatus as a motive liquid if evacuation of a nonpolar gas-vapor medium is to be effected. Further, the method includes condensing the nonpolar gas-vapor medium, forming a gas-liquid mixture, disengaging a gaseous phase from the mixture, forming a liquid emulsion containing the polar liquid and a nonpolar condensate, separating the emulsion into continuous layers, withdrawing the nonpolar condensate and recycling the polar liquid by pumping it back into the liquid-gas jet apparatus. A nonpolar liquid is to be used as the motive liquid of the liquid-gas jet apparatus if evacuation of a polar gas-vapor medium is required. There is another variant of the method applicable when an evacuated gas-vapor medium contains both polar and nonpolar components.Type: GrantFiled: April 6, 2001Date of Patent: February 12, 2002Inventors: Serguei A. Popov, Evgueni D. Petroukhine
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Patent number: 6280578Abstract: Essence of the invention is a: a liquid, whose saturated vapour pressure is not less than the pressure at the top of a rectification column, is delivered into the nozzle of a liquid-gas jet apparatus as a motive liquid; the pressure maintained in a separator represents from 1.1 to 160 times the pressure of a vapor phase at the inlet of the liquid-gas jet apparatus; condensation of easy-condensable components of the vapor phase in the motive liquid and forming of a liquid-vapor mixture take place after mixing of the vapor phase with the motive liquid; the liquid-vapor mixture is separated in the separator into a compressed gaseous component and a liquid medium. The introduced method results in an increase in efficiency of a pumping-ejector system for the distillation of a liquid product.Type: GrantFiled: December 21, 1998Date of Patent: August 28, 2001Inventor: Serguei A. Popov
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Patent number: 6277247Abstract: The invention pertains to the field of the petrochemical industry. The invention essentially relates to a system and method that includes feeding of a liquid having molecular weight more than 100 (in atomic mass units) into a nozzle of an ejector as a motive liquid, and delivery of a mixed medium from the ejector into a shaped reservoir, where flow velocity is reduced and static pressure is boosted. The outlet of the ejector is connected to the inlet of the shaped reservoir, the inlet of a separator is connected to the outlet of the shaped reservoir. The introduced method and the system for its embodiment ensure a more efficient operation.Type: GrantFiled: December 21, 1998Date of Patent: August 21, 2001Inventor: Serguei A. Popov
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Patent number: 6224716Abstract: A system for dehydrating lubricating and hydraulic fluids includes a heating circuit and circuitry for creating a vacuum. The heating circuitry introduces a stream of heated fluid into a vacuum chamber in which a partial vacuum is drawn by the vacuum circuit. Aqueous components of the fluid stream are flashed in the vacuum chamber by virtue of the elevated temperature and reduced pressure. Dehydrated fluid is then collected and evacuated from the vacuum chamber. Vapor from the vacuum chamber, including the aqueous components of the fluid stream are collected, condensed and separately evacuated. The heating circuit limits surface temperature of a heating element in a closed-loop manner to avoid degradation of the fluid. The fluid stream is introduced into the vacuum chamber or is recirculated through the heating circuit to maintain a desired level of fluid temperature in a closed-loop manner.Type: GrantFiled: March 18, 1998Date of Patent: May 1, 2001Assignee: Oilquip, Inc.Inventor: Perry D. Yoder
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Patent number: 6086721Abstract: A vacuum-creating apparatus of the unit is provided with a pump and a separator, wherein the pump is connected at its inlet to the separator, a jet device is made as a liquid-gas device and is connected at its outlet, by means of a pressure main, to the separator and at its liquid input to an output of the pump, wherein the longitudinal axis of the jet device is positioned vertically, the permissible deviation from the vertical axis being .+-.15.degree., an outlet cross section of a liquid supply nozzle of the jet device is positioned at a height of from 5 m to 35 m above an inlet to the separator and an outlet section of the pressure main is positioned below the level of the liquid in the separator to form a hydraulic seal.Type: GrantFiled: June 16, 1998Date of Patent: July 11, 2000Inventor: Valery Grigorievich Tsegelsky
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Patent number: 5980694Abstract: An installation for cleaning oil-polluted water, in particular at oil and gas production plants, is provided with a distillation column having a polluted water feed and at least one contact packing above which the outlet of the polluted water feed is located, a vapor discharge, a clean water outlet and a measuring device for the analysis of the water from the clean water outlet.Type: GrantFiled: July 25, 1997Date of Patent: November 9, 1999Assignee: EMSYS Separation Technology B.V.Inventors: Adrianus P. Apeldoorn, Jachebus W. Bos, Johannes J. Dozy, Johannes J. Elling, Leonardus C. Gordijn, Pieter Ottens, Wayne S. Penny, Cornelis Spel, Aatje J. Spel-van der Linde, Tom M. Vader, Theodorus J. De Wit
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Patent number: 5980698Abstract: A method for vacuum distillation includes separation of a liquid product delivered to a reservoir under vacuum into a vapour-gaseous phase and at least one liquid fraction, withdrawal of the vapour-gaseous phase from the reservoir using a vacuum-creating device, and subsequent separation of the vapour-gaseous phase into gas and a liquid phase by condensing performed directly in the vacumm-creating device. A portion of the liquid phase is used as a fluid working medium in the vacuum-creating device.An equipment for vacuum distillation includes a reservoir under vacuum conditions equipped with mains and a vacuum-creating device, which has an ejector, a separator and a pump, interconnected by mains.Type: GrantFiled: January 7, 1997Date of Patent: November 9, 1999Assignee: Valery Grigorievich TsegelskyInventors: Alexandr Alexeevich Abrosimov, Alexandr Mikhailovich Kochemasov, Ivan Alexandrovich Kochergin, Valery Grigorievich Tsegelsky
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Patent number: 5843384Abstract: The invention concerns a plant for purifying spent oil, including apparatus for dehydration, preferably by atmospheric distillation, directly followed by vacuum distillation producing a residue and at least one distilled oil fraction. The vacuum residue directly undergoes solvent extraction and the clarified oil obtained and the distilled oil fraction(s) undergo finishing hydrotreatment.Type: GrantFiled: January 3, 1997Date of Patent: December 1, 1998Assignee: Institut Francais du PetroleInventors: Marcel Aussillous, Patrick Briot, Pierre-Henri Bigeard, Alain Billon
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Patent number: 5820748Abstract: Gasses, water and solvents, major contaminants in used lubricating oils, can be removed from used lubricating oils at mild temperature conditions under vacuum. Apparatus in which the removal can take place includes a hollow vacuum separator vessel with a spray nozzle to spray an ultra fine spray of warm, used lubricating oil onto an angularly disposed thin film separator plate. In conjunction with the plate is a cooling device within the vacuum chamber. Cleaned oil can be passed from the bottom back into a holding tank, while water and solvents are drained out into a separate tank for safe disposal.Type: GrantFiled: April 25, 1997Date of Patent: October 13, 1998Inventor: Tajwar Shadikhan
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Patent number: 5814207Abstract: A method and apparatus for re-refining used oil, in which the used oil is processed in at least one cyclonic vacuum evaporator comprising a void evaporation chamber (4) into which feedstock is tangentially injected, and in which a fraction of the feedstock is condensed in a spray condenser (7) communicating with the evaporation chamber (4).Type: GrantFiled: June 7, 1996Date of Patent: September 29, 1998Assignee: Enprotec International Group N.V.Inventor: Kalevi John Kenton
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Patent number: 5628901Abstract: A single vessel with no moving parts is constructed to perform the functions of coalescing, vacuum dehydration, and thin film evaporation.Type: GrantFiled: April 30, 1993Date of Patent: May 13, 1997Assignee: Castrol Industrial North America Inc.Inventors: William L. Lawrence, Robert D. Coyle
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Patent number: 5597451Abstract: A thermal decomposition apparatus for plastics wherein plastics are melted and thermally decomposed, and the resulting decomposition gas is cooled for condensation and recovered in the form of a thermal decomposition oil. The apparatus comprises a thermal decomposition reactor for melting and thermally decomposing the plastics therein, an extraneous matter discharge duct having one end opened in a melt of plastics within the reactor, an extraneous matter collecting container connected to the other end of the discharge duct, and an aspirator for aspirating extraneous matter within the reactor together with the melt through the discharge duct into the container.Type: GrantFiled: June 15, 1995Date of Patent: January 28, 1997Assignee: Hitachi Zosen CorporationInventors: Kenichi Nagai, Kenji Yasuda, Toshio Hama, Yoshitoshi Sekiguchi, Toshio Tachibana, Osamu Nakanishi, Tadashi Moriyama
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Patent number: 5584969Abstract: A thermal decomposition apparatus for plastics wherein plastics are melted and thermally decomposed, and the resulting decomposition gas is cooled for condensation and recovered in the form of a thermal decomposition oil. The apparatus comprises a thermal decomposition reactor for melting and thermally decomposing the plastics therein, an extraneous matter discharge duct having one end opened in a melt of plastics within the reactor, an extraneous matter collecting container connected to the other end of the discharge duct, and an aspirator for aspirating extraneous matter within the reactor together with the melt through the discharge duct into the container.Type: GrantFiled: July 29, 1994Date of Patent: December 17, 1996Assignee: Hitachi Zosen CorporationInventors: Kenichi Nagai, Kenji Yasuda, Toshio Hama, Yoshitoshi Sekiguchi, Toshio Tachibana, Osamu Nakanishi, Tadashi Moriyama
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Patent number: 5167773Abstract: A distillation tower (1) has a plurality of liquid sidestream lines (5, 6, 7) and a multi-stage sidestream stripper (13) which includes a respective stripping section (14, 15, 16) for each sidestream line housed in a common, upright, cylindrical shell (28) which allows vapor to pass freely from each stage to the one above. Partial vaporization of each sidestream is achieved by applying a vacuum to the top of the stripper shell (point 21) and/or introducing strip gas at the bottom (point 20). Because the vapor passes serially through the stripping sections from the bottom of the stripper (13) to the top, the need to supply strip gas separately to the stripping sections and/or apply vacuum individually is avoided. The separation between the sidestream products is improved by including, in each stage, a rectification zone (22, 23, 24) positioned above the stripping section.Type: GrantFiled: January 16, 1990Date of Patent: December 1, 1992Assignee: Exxon Research and Engineering Co.Inventors: James D. Eagan, Adrianus Welmers
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Patent number: 5034103Abstract: A draw-off device is disclosed for a vacuum distillation column in which device a layer of gutters is provided. A secondary wall is arranged in the gutters creating a heat-insulating layer to reduce the condensation of vapor passing along the outer walls of the gutters.Type: GrantFiled: February 9, 1990Date of Patent: July 23, 1991Assignee: Shell Oil CompanyInventors: Johannes A. Hamer, Pieter van der Heijden, Pieter J. Hoek
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Patent number: 4995495Abstract: In attempting to upgrade crude oil to pipeline quality, it often proves necessary to treat the oil in more than one apparatus. A simple solution to the problem is to provide an apparatus including a flashing section coupled to a treating section in which the crude oil is desanded and dewatered. The flashing section heats the oil to a temperature in which water can exist only as a vapor, and the vapor thus generated is discharged through a demister.Type: GrantFiled: March 16, 1990Date of Patent: February 26, 1991Assignee: HTI Technology Canada Ltd.Inventor: Stephen V. Krynski
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Patent number: 4904347Abstract: A liquid product (4) leaving a furnace (2) is introduced into a series of cyclone separators (5, 6, 7). The liquid product to be vaporized is introduced tangentially into the top portion (5a, 6a, 7a) of each cyclone to place the product into contact with a side wall (5b, 6b, 7b) of the cyclone. A gaseous phase (11, 12, 13) formed in each cyclone is collected in the central zone (8, 9, 10) of the cyclone and is then introduced into a vacuum distillation column (3). The liquid phase obtained in each cyclone is collected at the bottom (5c, 6c, 7c) of the cyclone and then is introduced tangentially into the top (6a, 7a) of the following cyclone or, in the case of the last cyclone, is introduced directly into the vacuum distillation column (3). The side wall (5b, 6b, 7b) of each cyclone (5, 6, 7) is heated to a temperature near the maximum temperature allowable for avoiding all thermal deterioration of the product.Type: GrantFiled: December 17, 1987Date of Patent: February 27, 1990Assignees: Spie Batignolles, Electricite de FranceInventors: Pierre Cros, Christian Daumas
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Patent number: RE38366Abstract: A method and apparatus for re-refining used oil, in which the used oil is processed in at least one cyclonic vacuum evaporator comprising a void evaporation chamber (4) into which feedstock is tangentially injected, and in which a fraction of the feedstock is condensed in a spray condenser (7) communicating with the evaporation chamber (4).Type: GrantFiled: September 19, 2000Date of Patent: December 30, 2003Assignee: Avista Resources, Inc.Inventor: Kalevi John Kenton