Abstract: The present invention describes a high speed, high precision electrochemical micromachining tool, chemical solution and method for the one sided through-mask micropatterning of conducting foils and films supported by insulating material. The tool of the present invention can include either a movable plate means allowing for the movement of the workpiece to and fro above the cathode assembly, or a movable cathode assembly means allowing for the movement of said cathode assembly to and fro beneath the workpiece. Said cathode assembly also consists of a nozzle assembly from which the electrolytic solution emerges as electrolytic shower and impinges upon the workpiece. Methods to resolve the problems related to the loss of electrical contact during the electrochemical micromachining process are also described.

Abstract: A water purifying apparatus of compact construction. The water purifying apparatus has a water channel for receiving water via an inflow passage and discharging water via an outflow passage. An electrically conductive filter is disposed in and fully occupies a portion of the water channel for purifying water flowing through the filter. A first electrode is electrically connected to the filter, and a second electrode, disposed in the filter, is electrically connected to the filter via water flowing through the filter. A battery supplies voltage between the first and second electrodes. A switch controls application of the voltage from the batteries to the first and second electrodes. A circuit board having a control circuit is disposed above the first electrode, the second electrode and the switch. The circuit board is electrically connected to the various electronic components.

Abstract: An improved plating tank having a tank separator which segregates the tank into an upper tank and a lower tank. A plating chamber attached to the tank separator encases a rack having one or more surfaces for supporting semiconductor wafers to be plated. A chamber passage formed of an inner surface of the chamber is connected between an opening in the tank separator and the upper tank to allow solution pumped from the lower tank to the upper tank to pass through the tank separator opening into the chamber passage and to flow over the anodes and the wafers.

Abstract: In an electropolishing or electrolytic etching apparatus the anode is separated from the cathode to prevent bubble transport to the anode and to produce a uniform current distribution at the anode by means of a solid nonconducting anode-cathode barrier. The anode extends into the top of the barrier and the cathode is outside the barrier. A virtual cathode hole formed in the bottom of the barrier below the level of the cathode permits current flow while preventing bubble transport. The anode is rotatable and oriented horizontally facing down. An extended anode is formed by mounting the workpiece in a holder which extends the electropolishing or etching area beyond the edge of the workpiece to reduce edge effects at the workpiece. A reference electrode controls cell voltage. Endpoint detection and current shut-off stop polishing. Spatially uniform polishing or etching can be rapidly performed.

Abstract: An autoelectrolytic hydrogen generator system constituted by one or a plurality of similar cells wherein a galvanic arrangement of magnesium and aluminum plates of sacrificial elements as anode; stainless steel as cathode and sea water as electrolyte, by its very nature is made to develop a voltage when connected in short circuit causing a current to flow within the system and hydrogen production of hydrogen in situ and on demand by the electrolytic action at one pole, the cathode, and additional hydrogen by the electrochemical reaction at the other pole, the anode. Surplus electric energy of the system applied to a optional electrolyzer will also be made to produce additional hydrogen at its two sacrificial aluminum electrodes.

Abstract: The process for the electrochemical separation of metal mixtures and metal alloys comprises the steps of dissolving the starting material in an elecrolyte, substituting the metals dissolved in the electrolytic solution in succession in accordance with their electrochemical potential by electrochemically less noble metals in each case and depositing them. The electrolytic solution containing the dissolved metals is passed continuously through several cells, connected to each other, in which the electrolytic solution is brought into contact with said less noble metals. Several of the metals dissolved can be substituted simultaneously by one or more electrochemically less noble metals. Metals that are deposited simultaneously together are separated electrolytically from each other, and metals which have again gone into solution are again substituted outside the electrolysis cells by said less noble metals and deposited.

Abstract: An apparatus for water purification, and in particular for electrical water purification in combination with a filtering apparatus for providing purified water for drinking and other application common in the home, farm or business. Metal, hydrogen and oxygen ions are introduced into water to be purified by carbon and copper electrodes. After ionizing the water to be purified, the water is then filtered in a filter tank which contains layers of various filtration media, including granular activated carbon.

Abstract: An apparatus for preparing and cleaning a machining liquid of an electroerosion machine comprises a filter, to which a concentrate flow is supplied from a concentrate tank and from which a permeate flow is drained off. Over a considerably extended time the quality of the machining liquid is maintained within a desired quality range, because the filter is constructed as a membrane filter and a disposal container having a fleece filter is provided to which is supplied at least part of the concentrate flow from the membrane filter and from which the partial flow filtered through the fleece filter is returned to the concentrate tank.

Abstract: An electrolytic cell of the type to which electrolyte is continuously charged and from which a product or products of electrolysis is or are continuously removed, the electrolytic cell being associated in close proximity with an item or items of apparatus in which electrolyte may be treated prior to charging to the electrolytic cell and/or in which a product or products of electrolysis may be treated after removal from the electrolytic cell. Also, a plurality of such electrolytic cells and items of apparatus. Electrolyte may be purified in the items of apparatus associated in close proximity with the electrolytic cells prior to charging to the cells, and the product streams from the cells may be treated in the items of apparatus prior to combining the product streams.

Abstract: An electrolytic treatment method and a unit in which such a method is practiced are provided wherein heavy metal hydrous oxides are precipitated and recovered from a dilute waste stream to render the waste stream suitable for discharge. The waste stream is passed into the cathode chamber of an anion exchange membrane delineated electrolytic cell and subjected to high current density electrolysis to promote the formation of regular, noncompressible metal hydrous oxide crystals. Fluoride ion is added to the precipitate-containing waste stream, the precipitate is filtered and the clarified liquid waste stream is split so that a portion is discharged and a portion is recycled into the metal ion-containing waste stream for further treatment.

Abstract: An apparatus for the production of sterilized and calcium-ion water includes: a housing structure; an electrolytic cell with electrical terminals and electrodes installed in the housing structure; a plurality of electromagnetic valves separately provided at a water-intake pipe and a water-drain pipe in communication with the electrolytic cell; a setting switch disposed in the housing structure and electrically coupled with the electrolytic cell for adjusting the current intensity of electrolysis therewith; a hydraulic-pressure switch provided at a water pressure pipe for the control of the water-level in the electrolytic cell; an ultraviolet sterilizing tank connected to the electrolytic cell for sterilizing the electrolyzed water; and a control circuit respectively coupled with the electrolytic cell, the electromagnetic valves and the setting and hydraulic switches; whereby, calcium-ion water can be effectively produced for drinking purposes.

Abstract: Liquid is clarified by passing it between spaced plates of a stack including two interleaved sets of plates, one set being connected to one direct current lead and the other set being connected to the other direct current lead. The liquid may flow through the spaces between the plates in a single direction in parallel paths or may flow in a serpentine path. Impurities removed from the liquid adhere to the plates and may be purged from the plates periodically by reversing the direction of flow of current between the plates. Impurities sloughed off the plates are trapped in a filter in the cell outlet.

Abstract: An electro-chemical machine supplies pulses to a spaced workpiece and electrode in a working tank through an electrolyte in order to finish the workpiece, while eliminating electrolytic products produced in a gap between the workpiece and electrode by supplying clean electrolyte to the gap. This machine includes: an electrolyte filtering apparatus for removing dirty electrolyte containing electrolytic products from the working tank and filtering it; an electrolyte supplying apparatus for intermittently supplying the filtered electrolyte to the gap through a supply hole formed in the electrode; and a power supply apparatus for supplying the pulses to the workpiece and electrode when the flow of electrolyte to the gap stops. Clean electrolyte can be supplied to the gap almost simultaneously with the removal of dirty electrolyte, and then the finishing work is started. A glossy mirror surface on the workpiece can be automatically obtained by repeating those operations.

Abstract: An anode used in electroplating is formed by a plurality of individual anode segments. The anode segments are arranged in predetermined patterns. The segments of certain patterns are selectively energized to establish an effective anode size that relates to the size of the article to be electroplated, thereby establishing an electrical field of uniform characteristics to transfer ions from the anode to the article at a uniform deposition rate over the whole surface of the article. By adjusting the effective size of the anode to correspond or relate to the size of the article, the non-uniform deposition rates associated with concentrated localized field are avoided, and the physical size of the electroplating apparatus can be reduced. An electrophoretic ion filter is also placed between the cathode and the article. This ion filter is preferably formed of a plastic porex material, such as porous polypropylene or polyethylene.

Abstract: An electrode is positioned with a predetermined gap between the electrode and a surface of a work in an electrolyte tank. Pulses are intermittently applied to the electrode. Electrolyte including residual products is discharged from the tank. The discharged electrolyte is cleaned by a filtering device to produce clean electrolyte. The clean electrolyte is supplied to the electrolyte tank for next machining.

Abstract: An electroplating system with improved water use efficiency and unique waste water treatment which enables operation without access to public sewers thereby permitting compliance with governmental regulations regarding disposal of waste water. Water use efficiency is achieved by means of limited use of overhead water sprays, multiple rinse tank backflow to the prior process tank and water evaporation from said process tanks. In addition, all waste water not returned to the prior process tank locally at each plating subassembly is transferred to an inplant sump for common evaporative treatment.

Abstract: A process is disclosed for purifying gases and liquids and/or for recovering particles contained or substances dissolved therein or for implementing other technological process procedures. Technological process procedures take place in exchangeable, mobile, individual vessels (1,2,3,4) chargeable with active known substances (for instance ion exchange resins) and/or provided with technological process assemblies (for instance mechanical filters), the vessels being mutually connected and forming a reaction column (7). The vessels (1,2,3,4) filled with the same or with different substances are passed by one medium or by several separate media partial streams (X,Y). In the case of several partial streams, the media partial streams (X,Y) always pass part of the vessels (1,2,3,4) or, after mixing, the resulting media mixture (X+Y) passes the other part of the vessels (1,2,3,4).

Abstract: The zero discharge spray system comprises a tank for collecting and storing inse water, a set of spray nozzles aligned within the tank, and a pump for both pumping used rinse water through the spray nozzles and/or to the plating bath as makeup for evaporation. A timer level control system maintains the plating bath level and the rinse tank level, and limits the nozzles spray time. The system also includes a fresh water spray for final rinse of plated parts. By using a controlled spray rinse system which reduces the amount of water added to the system so as not to exceed that lost by evaporation, no contaminated rinse water is discharged as waste.

Abstract: The invention is a device and method for electroplating a metal workpiece having axial symmetry, such as a circular workpiece. In this invention the workpiece, which is the cathode, is rotated inside an anode structure submerged in the plating solution. Part of the rotating cathode continuously moves through a region of intense current fluxes created by passing DC current between the anode and cathode. The rotating cathode stirs the plating solution, which speeds up the plating rate. At the same time, with only part of the cathode passing continuously through the intense current flux region, the deposition process is periodically slowed down and intensified.

Abstract: The invention resides in an apparatus for the decontamination of radioactivated metallic waste by the electrolytic oxidation-reduction with an aqueous nitric acid solution containing trivalent cerium ions, i.e. the step of converting the trivalent cerium ions into tetravalent cerium ions through electrolytic oxidation and the step of dissolving the surface layer of the radioactivated metallic waste by oxidizing it with the electrolytic solution now vested with the oxidative power of the freshly produced tetravalent cerium ions and, at the same time, effecting regeneration of the tetravalent cerium ions.

Abstract: An electroplating system with improved water use efficiency and unique waste water treatment which enables operation without access to public sewers thereby permitting compliance with governmental regulations regarding disposal of waste water. Water use efficiency is achieved by means of limited use of overhead water sprays, multiple rinse tank backflow to the prior process tank and water evaporation from said process tanks. In addition, all waste water not returned to the prior process tank locally at each plating subassembly is transferred to an inplant sump for common evaporative treatment.

Abstract: In an electrolytic reduction cell in which molten metal is produced by electrolysis of a molten electrolyte, less dense than the molten metal product, the molten product metal collects at the bottom of the cell. A filter is provided at this location and is constructed from a material which is resistant to attack by both the molten metal and molten electrolyte, and which is wetted by the molten metal, but not by the electrolyte. By correcting sizing of the passage or passages in the filter molten metal product can be drawn out of the cell without simultaneous withdrawal of molten electrolyte. In the case of a cell for the production of aluminium the filter is preferably constructed from titanium diboride.

Abstract: In an electrolytic reduction cell for the production of molten metal, particularly aluminium, by electrolysis of a less dense salt monolayer of ceramic shapes is located on the floor of the cell. Such shapes are formed of a ceramic material, wettable by molten aluminium, but not wettable by the cell electrolyte. The spacing between adjacent shapes and/or the apertures in individual shapes is selected such that interfaced surface forces prevent entry of electrolyte between the shapes. The shapes may be tiles, honeycombs, cylinders, tubes, balls etc. The product metal may be collected in a sump for periodic withdrawal from the cell or withdrawn continuously or at short intervals through a selective filter that permits passage of molten metal, but not of molten cell electrolyte, at low withdrawal rates.

Abstract: Water purification is accomplished in a swimming pool, spa or decorative pool body of water by adding salt in quantities sufficient to make the water slightly conductive and by circulating that water through the electric field between a pair of electrode plates where the dissociated ions of salt and water are converted to oxidizing agents capable of destroying organic matter and are converted to substances that can be removed in such a mechanical filtration system. That process results in economical and effective purification which is augmented in one form of the invention by the inclusion in the water circulation path of dissimilar metals which aid in the destruction of organic matter. The process is facilitated by the use of a special electrochemical processing unit in which the electrode dissociation is accomplished.