Abstract: The invention relates to a method for producing low-odor n-butane by catalytic hydrogenation of a feed mixture. The aim of the invention is to provide such a method, wherein the feed material, in addition to n-butane, n-butene and up to 1 mass % formic acid and/or up to 1 mass % pentanals and/or up to 0.5 mass % pentanols, also comprises carbon monoxide. The aim is achieved by treating the feed mixture in the temperature range of 15 to 120° C. with an aqueous solution of an alkali metal or alkaline earth metal hydroxide in the concentration range of 0.5 to 30 mass % and subsequently subjecting the feed mixture to the catalytic hydrogenation.
Type:
Grant
Filed:
May 21, 2010
Date of Patent:
September 30, 2014
Assignee:
Evonik Degussa GmbH
Inventors:
Hans-Gerd Lueken, Alfred Kaizik, Markus Winterberg, Wilfried Bueschken, Dirk Fridag
Abstract: In a process for decontaminating radioactively polluted lubricant oil, (a) the lubricant oil to be decontaminated is mechanically filtered, (b) an acid solution of the salts of the elements, the radionuclides of which are to be removed, is added, and (c) a dose of a precipitating agent that cooperates with the elements, the radionuclides of which are to be removed, producing a salt of low solubility, is added, (d) the acid salt solution is intimately mixed with the lubricant oil after step (b), (e) the depositing aqueous phase is discharged after step (b), before step (c), (f) additional intimate mixing is carried out after the dosed admixture of step (c), and (g) finally the precipitation products are separated by centrifugation from the lubricant oil.
Abstract: There is provided a process for reduction of the nitrogen content of shale oil. The process comprises contacting shale oil with a low acid strength solvent in a first extraction zone, followed by contacting the shale oil with a high acid strength solvent in a second extraction zone. A portion of the high acid strength solvent containing extracted nitrogen-containing and non-nitrogen-containing compounds is passed to the first extraction zone and diluted to form low acid strength solvent, and at least a portion of the non-nitrogen-containing compounds redissolve into the shale oil in contact with the low acid strength solvent and are recovered. Thus, oil recovery is maximized at high nitrogen removal.