Abstract: A process for the desalination and demineralization of solutions conmining acids and/or metal salts comprising a number of steps after introducing a solution to be treated. Initially, chemical agents are added to precipitate predetermined salts. Afterward clarification occurs. An inhibitor is then introduced for inhibiting further precipitation of the salts. The process proceeds by concentrating the salts in 5%-80% of tile flow of the solution to be treated into a supersaturated concentrate to form a concentrated fraction, the remaining fraction being a demineralized permeate. There is then removal of the effect of the precipitation inhibitor allowing precipitation of crystallizable supersaturated salts in the concentrate.

Abstract: There is provided water insoluble cross-linked polycarboxylic acid having at least two strands in a strand skeleton of the formula: ##STR1## wherein one carbonyl group of at least one maleoyl moiety thereof in each strand is covalently linked to a--HN.[(H).sub.p (CH).sub.2.(OH).sub.m ].NH-- moietyto provide the presence therein of at least one cross linked moiety of the formula: ##STR2## wherein R is hydrogen or lower alkylene or lower alkoxy of 1-4 carbon atoms, or phenyl, x and y are integers, z is an integer of 1-6, p is 0 or an integer up to z-1, m is 0 or an integer up to z, and w is an integer from 2-12. There is disclosed a method of making such polycarboxylic acid as well as methods of utilizing same to remove proteins from aqueous media containing same to provide a matrix. Methods are disclosed for recovering proteins from said matrix without denaturing them and methods for recovering the polycarboxylic acid from said matrix.

Abstract: Water to be utilized is reacted with soda ash and lime to produce a less corrosive and foulant water. Reaction sludges are fed to a desulfurization unit, where SO.sub.x, NO.sub.x and CO.sub.2 abatement occurs; other industrial waste sludges and/or waters and/or gases can also be utilized in such connection. FIG. 1 is one of the possible process schemes of present invention.

Abstract: A method and a system which enable simple and inexpensive removal of heavy metals from a heavy-metal-containing substance. In this method, a substance containing heavy metals and water are introduced into a mixing bath in proportions by weight of 1:3 to 1:6. A strong acid is added to the mixture, and the mixture is stirred while its pH is maintained at a pH lower than 4. As a result of stirring of the substance at a pH 4, heavy metals are extracted into the liquid as metal ions. The metal-ion-containing liquid is input to a heavy metal precipitation bath, and the pH of the liquid is increased to a pH higher than 10 by addition of alkali to the liquid. Gas bubbles of carbonic acid gas are input to the liquid from a lower portion of the heavy metal precipitation bath, and they are broken into a large quantity of small gas bubbles of carbonic acid gas by turbine blades. The large quantity of gas bubbles of carbonic acid are brought into contact with the metal-ion-containing liquid having a pH higher than 10.

Abstract: The present invention describes a process and an apparatus for treating sludge having both liquid and solid constituents. The sludge is first heated to a minimum optimum draining temperature. During heating, mechanical dewatering of the sludge occurs. In a preferred embodiment, a process is disclosed for treating waste paint sludge generated from a paint spraybooth, and heating is performed using microwave radiation. Liquid released from the paint sludge during dewatering can be recycled back to the spraybooth water, and vaporized exhaust generated during heating can either be condensed into liquid form and recycled, or incinerated and, preferably, sparged through untreated sludge to pre-heat it.

Abstract: A method and apparatus for treating waste liquids containing body fluids so as to prevent problems such as nosocomial infection due to such waste liquids containing body fluids discharged from patients under (surgical) operation or treatment, particularly those waste liquids containing blood or an irrigation liquid used to irrigate the body cavity of such patient. The method includes collecting a waste liquid containing body fluids into a container, separating the waste liquid into a supernatant liquor and a flocculate within the container, discharging the supernatant liquor from the container, and disposing of the flocculate remaining in the container together with the container.

Abstract: The present invention is directed to a continuous, portable dredging system that employs a series of screens and gravity separation devices with flocculation to remove sediments from the dredged slurry. The system produces a treated water stream having low solids content and a recovered solids product having a low water content.

Abstract: A process for filtering kaolin clay slurries in the presence of a filter aid which increases the percent solids in the filter cake, decreases the product solids in the waste filtrate, increases the rate of filtration, and yet does not interfere with redispersal of the filter cake after filtration. The process utilizes high molecular weight, highly anionic polyacrylic acid homopolymers or copolymers, or water soluble salts thereof, as filter aids for thickening and dewatering kaolin clay slurries. The flocculated clay may be redispersed after the separation process by normal means, such as the addition of low molecular weight anionic polymers with mixing.

Abstract: A method for recovering and separating precious and non-precious metals from waste streams, which removes, separates, and recovers such metals in a cost effective manner with more than 95% removal from waste streams and with minimal amounts of unprocessed solids and sludge remaining in the environment. Metals such as chromium, manganese, cobalt, nickel, copper, zinc, silver, gold, platinum, vanadium, sodium, potassium, beryllium, magnesium, calcium, barium, lead, aluminum, tin; and the like are removed and recovered from the waste streams with at least 95% removal and other metals and compounds, such as antimony, sulfur, and selenium are removed and recovered from waste streams with at least 50% removal. The method employs a unique complexing agent comprising a carbamate compound and an alkali metal hydroxide which facilitates the formation of the metals into ionic metal particles enabling them to be readily separated, removed and recovered.

Abstract: The invention relates to a solids and liquids effluent chemically enhanced treatment system comprising: (a) a pump for grinding solids and pumping ground solids and liquid effluent; (b) an inlet for introducing flocculant and coagulants into the solids and liquid effluent and mixing the flocculant with the solids and liquid effluent; (c) a mixing chamber having an inlet connected to an outlet of the pump, the mixing chamber having sufficient length to enable the flocculant and coagulants to fully mix with the solids and liquids effluent and form flocs which settle from the liquid effluent; (d) a settling chamber connected to an outlet of the mixing chamber, the settling chamber promoting laminar flow to the solids and liquid effluent and having sufficient length to enable the flocs in the liquid effluent to settle from the effluent; (e) a mechanical propulsion device for moving the solids and liquid effluent through the length of the settling chamber; and (f) a clarifier chamber connected to an outlet of the

Abstract: The instant invention provides a process for reducing chloride content from by-products generated during production of methylchlorosilanes, comprising, (a) hydrolyzing the by-products by combining the by-products with an aqueous medium, the aqueous medium optionally comprising a surfactant, at a pH of at least about 7 and at a temperature above about 0.degree. C. to yield a first phase comprising essentially solids and a second phase comprising an aqueous phase; (b) separating the first and second phase; and (c) oxidizing the solids from the first phase at a temperature of at least about 300.degree. C. for up to about 24 hours to yield a residue comprising less than about 1% by weight of chloride. The solids from the first phase may alternatively be reduced under a hydrogen flow, at a temperature of at least about 500.degree. C. for up to about 24 hours.

Abstract: A method and apparatus are provided for binding emulsified resin and tar substances in circulating water of a wet-cleaning and wet precipitation system for waste gas produced in the wood industry. Wood dust is metered into the circulating water and receives the emulsified substances adsorptively. The wood dust is removed from the water circulation path and sedimented.

Abstract: The invention relates to a method for separating ferrous ions from an iron-containing tinning electrolyte on the basis of methanesulfonic acid or phenolsulfonic acid, comprising the following steps:(a) providing a concentrated tin and iron-containing electrolyte containing 0.75 mols/l or more methanesulfonic acid phenolsulfonic acid(b) agitating and cooling the concentrated electrolyte to temperatures at which an insoluble Fe-salt preciptates(c) separating the insoluble precipitate to recover an electrolyte with a reduced iron concentration.and a recovery plant for tinning electrolytes on the basis of methanesulfonic acid or phenolsulfonic acid wherein this method is employed.

Abstract: A dewatering process in which a product comprising water and other materials is simultaneously subjected to compressive mechanical forces and electro-osmosis using a belt (12) having a plurality of connected spiral yarns and, at least in part, electrically conductive material thereon.

Abstract: To improve the separation of dispersedly precipitated sulfur from a washing solution used in the oxidative washing of hydrogen sulfide containing waste gases, the suspension is heated before filtration to about 45.degree. C. to 70.degree. C. Such heating causes the sulfur contained in the solution to coagulate into large flocks and form a mass of high purity sulfur which is largely non-thixotropic. This mass, often called a filter cake, can be washed and utilized in a large number of ways as a source of sulfur.

Abstract: According to the present invention, there is provided a method for nonbiologically treating an chlorinated organic compound contained in an environment polluted with the chlorinated organic compound, which comprises the step of introducing silicon into the environment to dechlorinate the chlorinated organic compound.

Abstract: Aqueous, homogeneous 20 to 60% solutions (L) of mixtures of(A) copolymers of(x) (meth)acrylic acidwith (y) maleic acid or maleic acid anhydride in the molar ratio (x)/(y)=0.7/1 to 7/1, with an average molecular weight M.sub.w in the range of from 500 to 500'000, as free acids and/or sodium saltsand (B) Nitrilotriacetic acid as free acid and/or sodium salt,in which the weight ratio (A)/(B) is in the range of from 1/1 to 1/10 at least 25% of the total carboxy groups are present as sodium salt and the pH of (L) is in the range of from 5 to 11, are suitable as adjuvants for the treatment of fibrous material, in particular as scouring agents for dyeings of hydrophilic fibrous material.

Abstract: Provided is a novel method and system for recovering aggregate fine size particles from a carrying medium. The method comprises:(a) introducing a feed containing particles to a sand screw, and separating the particles into separate groups of large and fine particles, the fine particles being present in a fine particle stream;(b) introducing the fine particle stream from the sand screw to one or more hydraulic centrifugal separators which overflow a fine particle stream and discharge a coarse particle stream;(c) introducing the overflow fine particle stream from the one or more hydraulic centrifugal separators to a thickening tank and removing precipitated material as an underflow stream from a lower portion of the thickening tank; and(d) introducing the underflow from the thickening tank to a filtering unit.

Abstract: The present invention provides a process for treating arsenic-containing waste water, comprising adding an oxidizing agent, if necessary, to arsenic-containing waste water to oxidize trivalent arsenic in the waste water into pentavalent arsenic; adding a calcium compound to adjust the pH to 12 or higher; separating it into solid and liquid (first solid/liquid separation); calcining the resulting sludge, while adding a ferric salt to the treated solution to adjust the pH to 6-9 after the solid/liquid separation; and separating it into solid and liquid (second solid/liquid separation). According to the present invention, it is possible to remove arsenic from waste water efficiently to yield treated water satisfying various tolerance limits under various regulations, while the arsenic-containing sludge separated from the waste water can become harmless in subsequent continuous steps.

Abstract: Method and apparatus are provided for separating coarse and ultrafine solids from a liquid stream to produce a substantially dry solids discharge and a clarified liquid. Apparatus is provided comprising a combination of a settling tank, a plurality of filter screens spaced along an endless link-chain conveyor, a screen vibrator and directed air streams. In operation, coarse solids settle preferentially to the tank bottom. Ultrafines solids remain in suspension. Relatively coarse filter screens are conveyed from a point outside the tank to traverse a prolonged path through the liquid. Ultrafine solids are captured on the screens, by filtering the liquid through an ever finer build-up of filter cake. The relatively large number of passes of the screens through the liquid provides effective filtering of suspended solids. Further, the screens dredge settled solids from the tank bottom.

Abstract: A system and method for disposing of vacuum degasser contaminants which includes adjusting the pH, in a reactor vessel, of a vacuum degasser underflow stream to precipitate lead and zinc into particulate matter. The solids are then concentrated in a thickener to produce an underflow stream that is communicated to a holding vessel to settle. The overflow from the thickener is filtered through a sand filter and discharged to meet applicable NPDES permit limits. Lime is added to the slurry in the holding vessel to further settle the solids, to aid in filtration, and to prevent leaching of lead from the filter cake during TCLP testing. An overlaying supernatant is decanted from the holding vessel and returned to the reactor vessel for further treatment. Limestone is added to the underflow stream. The resulting slurry is dewatered to produce a friable, non-hazardous filtrate cake and a filtrate. The filtrate is directed back to reactor vessel prior to discharge for further treatment.

Abstract: In the evaporation of process wastewater comprising a mixture of different types of wastewater, problems arise due to the formation of reaction products, so-called incrustations, which are difficult to separate. These incrustations clog up the evaporator, thus necessitating frequent stoppages for chemical and mechanical cleaning of the evaporator. The invention concerns an improved method for concentrating process wastewater by evaporation. In this method, one acid process flow and one alkaline process flow are evaporated alternately in one and the same evaporator. With this method, precipitates that are difficult to separate are dissolved in the evaporator during the respective evaporations. As a result, stoppages motivated by the need to clean the evaporator may be avoided to the utmost possible extent, while less and cheaper processing equipment is required.

Abstract: A process wastewater treatment plant, and a process relating thereto, which converts process wastewater generated in battery manufacturing and the like into clean process water and sodium sulfate salt by treating the process wastewater to remove impurities and contaminants, including debris, oil/grease, heavy metal oxides, lead and other heavy metals, suspended solids, bacteria, organic compounds, and/or gases, from the wastewater to produce a clean neutral sodium sulfate brine, subjecting the brine to heat to obtain distilled water and sodium sulfate salt, and purifying the distilled water by reverse osmosis for reuse as clear process water.

Abstract: A method for separating raw agricultural waste into a liquid portion and a nutrient enriched solids portion is disclosed. This method includes providing raw agricultural waste to be treated, adding to the raw agricultural waste an effective amount of a composition comprising a quaternized amino methylated polyacrylamide polymer for separating the raw agricultural waste into a mixture having a liquid portion and a nutrient solids portion, mixing the composition with the raw agricultural waste to facilitate the separation, and subjecting the mixture to at least one mechanical separation means for segregating the separated liquid portion from the separated nutrient solids portion. A method for transforming raw agricultural waste into a clarified liquid portion and a dewatered nutrient enriched solids portion is also provided.

Abstract: The present invention is to provide a method for treating sludge as a by-product of a process of tin electroplating a steel plate by means of a plating bath containing haloid ions, together with an equipment therefor. More specifically, by immersing the sludge in water prior to filtration, the residual sludge is subjected to alkali hydrolysis in the presence or absence of the ions of an alkali earth metal within a temperature range of 100.degree. to 400.degree. C., whereby cyanide compounds and fluoride compounds contained therein under environmental regulations are prepared into environmentally non-hazardous matters. By adjusting the filtrate to pH 7.5 to 10, the precipitate with the principal component of tin hydroxide is deposited to recover the tin components contained in the sludge. Furthermore, the recovered tin is refined into the metal tin, for recycling and use as the electrode by the plating.

Abstract: A method for recovering and separating precious and non-precious metals from waste streams, which removes, separates, and recovers such metals in a cost effective manner with more than 95% removal from waste streams and with minimal amounts of umprocessed solids and sludge remaining in the enviroment. Metals such as chromium, manganese, cobalt, nickel, copper, zinc, silver, gold, platinum, vanadium, sodium, potassium, beryllium, magnesium, calcium, barium, lead, aluminum, tin; and the like are removed and recovered from the waste streams with at least 95% removal and other metals and compounds, such as antimony, sulfur, and selenium are removed and recovered from waste streams with at least 50% removal. The method employs a unique complexing agent comprising a carbamate compound and an alkali metal hydroxide which facilitates the formation of the metals into ionic metal particles enabling them to be readily separated, removed and recovered.

Abstract: Apparatus for treating and dewatering of sludge taken from small-scale sewage treatment plants. The apparatus, which preferably is mounted on a vehicle, incorporates chamber-type units for dewatering, which can be connected by way of feed and return pipes, controllable valves, and pumps that can be switched on and off. A dewatering vessel with filter walls and separate sludge and filtrate chambers is connectable with a sludge chamber and a filtrate chamber, respectively, of a second dewatering vessel by way of joining pipes comprising at least one feeding pump and one controllable valve each, a radiation chamber arranged in the filtrate return pipe of one of the dewatering vessels, and a stone trap arranged in one other sludge feed pipe.

Abstract: Spent solutions from photographic processors are fed into a conduit (18) to which subsequently are added precipitating agents from a first source (22) and flocculating agents from a second source (28); so that, well grown or ripened clumps of flocculated solids are formed along the conduit before being emptied into a gravity collecting vessel and shipping container (38) from which clarified liquids are displaced by a mass (50) of accumulated flocculated solids, typically through a filter (58, 142, 150, 158, 162, 166, 220)for removal of any unsettled fines. Many of the clumps of flocculated solids become enlarged enough to individually extend across and substantially fill a cross-sectional area of the conduit. As a result, the enlarged clumps substantially block passage of and strain from the solution remaining fine particles which then adhere to the clumps.

Abstract: Water to be utilized is reacted with soda ash and lime to produce a less corrosive and foulant water. Reaction sludges are fed to a desulfurization unit, where SO.sub.x, NO.sub.x and CO.sub.2 abatement occurs; other industrial waste sludges and/or waters and/or gases can also be utilized in such connection. FIG. 1 is one of the possible process schemes of the present invention.

Abstract: The present invention in one embodiment, is a process that uses a chemical treatment to remove heavy metals from wastewater; heavy metals from wastewater containing oxygenated hydrocarbons; and arsenic, organic acids, and heavy metals from antifreeze solutions. In one aspect such a method includes adding an iron salt, to an antifreeze solution containing arsenic and heavy metals with adequate mixing for dispersion throughout the solution. Then, a base is added to increase the pH to a level from about 8 to 10. As the base is added, a precipitate with contaminates forms and is then removed by standard filtration techniques. The arsenic, organic acids, and heavy metals co-precipitate with the iron and are removed by filtration. The process may either be a batch process or a continuous process. In one aspect the wastewater is generated by a process according to the present invention for purifying contaminated soil or sediment.

Abstract: A method and apparatus for the removal of total cyanide from aqueous solution. The method includes the steps of placing the aqueous solution into a reaction tank, adding lime, ferrous sulfate, and acid to the solution in the reaction tank and agitating the resultant mixture for a reaction time of about one hour. The agitated mixture is transferred from the reaction tank to a clarifier tank and polyelectrolyte solution is added to induce iron-cyanide complex precipitate coagulation. The apparatus includes a reaction tank to hold the aqueous solution and a lime slurry tank, ferrous sulfate tank and acid tank in flow communication with the reaction tank. A pH control assembly controls the flow of acid from the acid tank into the reaction tank and a reaction tank agitation assembly extends into the interior of the reaction tank. The clarifier feed conduit extends between the reaction tank and a clarifier tank.

Abstract: Hydrophobic organic substances are separated from aqueous industrial effluent containing said hydrophobic organic substances and hydrophilic organic substances by adding to the effluent at substantially neutral pH a salt of a metal having an insoluble hydroxide thereby forming an hydroxide sludge entraining said hydrophobic, oxidizable organic substances, and separating the sludge from the treated effluent containing the hydrophilic organic substances. The invention has particular application to the removal of toxic hydrophobic, oxidizable organic substances from aqueous industrial effluent and their subsequent destruction by oxidation, especially ozonation, of the separated sludge, thereby reducing the oxygen demand compared with oxidation of the entire effluent to reduce said toxic substances to their discharge consent level.

Abstract: An improved partial oxidation, gasification process using low grade hydrocarbon feedstock involving the steps of gasification, waste heat recovery and carbon removal under formation of a soot water slurry containing the unburned carbon and ash. The soot water slurry is filtered to form a filtercake of carbon and ash, which cake is removed from the process. A direct once-through, partial oxidation process is thereby established, avoiding the recycle of unburned carbon and ash. The method also comprises filtration of the soot-ash slurries containing 0.5-3% unburned carbon and 0.1-2% ash having appreciable amounts of Fe, Ni and V. The slurry is cooled to a temperature below 80.degree. C. and filtered while confined between movable closed belts maintaining a constant pressure against the shrinking mass of carbon/ash particles until the moisture content is reduced to below 80% by weight.

Abstract: A wastewater treatment system wherein wastewater and air are passed into a mixing zone where the mixture is sprayed with water. The treated wastewater in the mixing zone is passed into a quiescent zone where light sludge is passed to the top of the quiescent zone and heavy sludge is passed to the bottom of the quiescent zone, the treated wastewater being disposed between the light sludge and the heavy sludge and the treated wastewater being passed from the quiescent zone into a discharge zone where the treated wastewater is discharged therefrom. The heavy sludge is discharged from the quiescent zone at predetermined discharge times and at predetermined intervals. The light sludge is passed from the quiescent zone into a light sludge bin where the light sludge is discharged therefrom for predetermined discharge time at predetermined discharge intervals. The heavy sludge and/or the light sludge then is passed into a drying system for drying the light sludge and the heavy sludge.

Abstract: Method to prevent the exhaustion of acid copper plating baths (12) and to treat sewage or sludges (20) containing copper in an ionic form so as to recover metallic copper (39), the method including the addition (11) of a compound which keeps the concentration of iron below a critical value (for instance, 60 grs/lt. ), the compound causing precipitation of iron in the form of ferrous sulphate and thus preventing the co-deposition of crystals of ferrous sulphate and copper sulphate with a possible incorporation of organic impurities such as stearates (35) present in the acid copper plating baths (12).

Abstract: Dry, free flowing solids, suitable for handling, transportation and/or disposal are produced from messy biologically treated sludges. In the process, the sludge feed is pressurized and heated, then flashed, in order to vaporize a portion of the water; the residual liquid, containing the solids and sometimes heavy metals, is contacted with a chelating agent, if needed, and a flocculating agent over a brief reaction period in order to precipitate a concentrated solid precipitate; and the precipitate is separated from the residual liquid water.

Abstract: A method is disclosed for remediating ponds and other water sites containing sludge and other waste materials by a dredging and dewatering process which is economical and efficient, uses relatively low cost equipment and provides for high remediation rates. The preferred process dredges the site to produce a sludge which is screened to remove oversize material. The screened sludge is then thickened and the thickened sludge dredged and fed as a uniform thickened sludge mixture to a filter press to dewater the sludge producing a final sludge product having a high solids content. A coagulant is preferably added to the sludge and a polymer and/or coagulant added to the thickened sludge filter press feed.

Abstract: Secondary sludge produced in the papermaking process is dewatered by adding a material capable of absorbing water together with dry fibers to the secondary sludge, and mixing the secondary sludge with the dried fibers to produce a modified secondary sludge which has sufficient structure and low enough moisture that it may be further dewatered by mechanical means. The preferred fiber adding materials are those readily produced in the papermaking process, particularly dry primary sludge, dried fines and bark and fly ash from boilers.

Abstract: A method is disclosed for separating a substance from a liquid medium. The method comprises combining the liquid medium containing the substance with magnetic particles under conditions for non-specific chemical binding of the magnetic particles. Thereafter, the medium is subjected to a magnetic field gradient to separate the particles from the medium. The preferred non-specific binding is achieved as the result of charge interactions between the particles usually by means of a polyionic reagent. The method of the invention has particular application to the separation of cells and microorganisms from aqueous suspensions and also to the determination of an analyte in a sample suspected of containing the analyte. The analyte is a member of a specific binding pair (sbp). The sample is combined in an assay medium with magnetic particles and a sbp member complementary to the analyte.

Abstract: A method for the re-treatment of residue generated in the course of removing fluorine from waste water.The method comprises the step of: drying the residues consisting of rare earth fluorides, which are generated in the course of treating the waste water with a rare earth compound to remove fluorine ions from the waste water; mingling the rare earth fluorides with a sodium hydroxide solid; heat treating the rare earth fluorides at temperatures ranging from approximately 320.degree. to approximately 450 .degree. C. for times ranging from approximately 0.5 to approximately 5 hours; and applying wash and dry to the heat-treated resultant, in due order.The invention pertains to the reuse of rare earth elements used in the treatment of fluorine. Products obtained by carrying out the method contain rare earth hydroxides, which are useful as materials for glass abrasive or for treating fluorine, catalysts, and other materials for the fields of using a variety of rare earth.

Abstract: Dispersions of finely divided high molecular weight polyacrylamide particles are formed and treated with a caustic material to hydrolyze the polymer without undesirable side chain reactions to form high molecular weight anionic acrylamide polymers. A preferred technique for forming these products comprises the formation of a stabilized water-in-oil emulsion of aqueous acrylamide monomer, polymerizing the monomer, reacting the polymer emulsion thus formed with a hydrolysis agent and inverting the resultant hydrolyzed polymers into solution. These materials are useful in a variety of industrial applications for removing particulates from effluent streams.

Abstract: Potassium permanganate is added to paper mill wastewater streams at an elevated temperature to remove color compounds from the effluent streams. The potassium permanganate causes the formation of flocculant particles which are precipitated out of the stream. This precipitate is then treated with acid to cause resolubilization.

Abstract: A titanium oxide hydrolysate slurry prepared by the sulfate process is treated with either an alkali metal hydroxide or an alkali metal carbonate to solubilize the sulfur bound to the titanium at a temperature of from 60.degree. C. to 120.degree. C. and the slurry is treated with an organic acid to remove the alkali metal compounds present. This process produces titanium oxide hydrolysate of high purity.

Abstract: A method of decontaminating the surface of a body carrying radioactive contaminants which comprises treating the surface with a decontaminant comprising a solution of tetrafluoroboric acid HBF.sub.4, treating the resultant liquor comprising decontaminant and dissolved species removed from the body surface with a first chemical agent which on reacting with dissolved species yields insoluble compounds and regenerated decontaminant solution, and characterized in that the regenerated decontaminant solution is further treated to cause removal of the first chemical agent from the decontaminant solution.

Abstract: A process and apparatus for treating culture medium with a dilute acid such as nitric acid, are disclosed. In a preferred embodiment, nitric acid is sprayed on to a floating oily layer of hydrophobic materials at the surface of a stilled culture rich in aerobic bacteria, which materials can obstruct oxygen take up. The nitric acid surface treats the protective hydrophobic third phase, increasing its surface viscosity and the undesired lipid or oily materials to be readily removed mechanically. Oxygen take up and thence microorganismic growth are promoted. Quite small quantities of dilute acid are effective and leave no toxic residue. An optional embodiment entrains nitrogen dioxide in the aeration gases to form nitric acid in situ for surface treatment of thin oily films occluding bubbles in the culture broth.

Abstract: A dispersant, such as sodium silicate, is added to the process water of the hot water extraction process which recovers bitumen from oil sands. The dispersant disperses the ultrafine (less than 300 nm) particles, to reduce the formation of flocs and sludge in the tailings pond. The volume of the pond is such that the retention time of process water is sufficiently short (less than 6 weeks when using sodium silicate) to avoid reforming flocs from the dispersed ultrafines. The ultrafines content in the process water builds up as the water is repeatedly recycled from the pond to the extraction process. The ultrafines content stabilizes at a steady state concentration as some ultrafines are continuously removed from the process water when the tailings are delivered onto the "beach" of the pond and become trapped in the sand.

Abstract: Lead oxide is used for neutralizing the sulfuric acid wastewater received from washing charged (formed) electrodes during lead battery production. The neutralization product, including lead sulfate and excess lead oxide, is returned directly to production of the active mass paste. The mother liquor, after a possible use as cleaning water, is subjected to another neutralization with lead oxide, separate from the wastewater received from the electrode washing procedure in view of its possible content of impurities. The resulting lead sulfate is sent to a metal-processing facility for recycling. The neutral mother liquor, after the removal of lead residues by conventional precipitation methods and filtration, is discharged as treated water.

Abstract: An oil or gas well cleaning method includes inserting tubing, such as a coiled tubing, into a well bore, for example, into a production pipe in a well bore. A cleaning fluid containing a flocculant is passed into the well and the flocculant in the cleaning fluid is mixed with solid particles in the well bore to flocculate the particles. The cleaning fluid and the flocculated particles are then removed from the well. In one embodiment, the cleaning fluid containing the flocculant is discharged from the lower end of the tubing into the well, and the cleaning fluid with the flocculated particles is removed from the well via the production pipe. Alternatively, the cleaning fluid containing the flocculant may be introduced into the well through the production pipe, and the cleaning fluid with the flocculated particles may be removed via the tubing. The flocculant may also serve as a friction reducer to reduce friction between the cleaning fluid, the solids, the production pipe, and the tubing.

Abstract: A system for removing hydrocarbons from solid materials. Contaminated solids are combined with a solvent (preferably terpene based) to produce a mixture. The mixture is washed with water to generate a purified solid product (which is removed from the system) and a drainage product. The drainage product is separated into a first fraction (consisting mostly of contaminated solvent) and a second fraction (containing solids and water). The first fraction is separated into a third fraction (consisting mostly of contaminated solvent) and a fourth fraction (containing residual solids and water). The fourth fraction is combined with the second fraction to produce a sludge which is separated into a fifth fraction (containing water which is ultimately reused) and a sixth fraction (containing solids). The third fraction is then separated into a seventh fraction (consisting of recovered solvent which is ultimately reused) and an eighth fraction (containing hydrocarbon waste).

Abstract: A process for separating the components of an emulsion. The process comprises, adjusting the pH of the emulsion to 4 less, adding a coagulant to the emulsion, forming a substantially uniform dispersion of inert particulate carrier in the emulsion adding a polyelectrolyte flocculent either during or after the step of forming the substantially uniform dispersion of inert particulate carrier in the emulsion to form floccs of the inert particulate carrier, the dispersed liquid phase, and the contaminants, allowing the floccs to settle, and separating the relatively clarified continuous liquid phase from the settled floccs.