Chemical Reaction Produces Filler Material In Situ Patents (Class 228/198)
  • Patent number: 11973002
    Abstract: A composite substrate includes, in this order: a ceramic plate; a metal layer containing at least one selected from the group consisting of aluminum and an aluminum alloy; and a thermal sprayed layer containing at least one selected from the group consisting of copper and a copper alloy, and an intermetallic compound containing copper and aluminum as constituent elements is scattered between the metal layer and the thermal sprayed layer.
    Type: Grant
    Filed: November 12, 2020
    Date of Patent: April 30, 2024
    Assignee: Denka Company Limited
    Inventors: Atsushi Sakai, Masaya Yumiba, Kentaro Nakayama, Yoshitaka Taniguchi
  • Patent number: 11578410
    Abstract: A method for depositing a metal-based coating on a particulate substrate, including: i) preparing a mixture comprising the particulate substrate, a powder comprising a coating metal oxide of one or more of Ti, Al, Zn, Sn, In, Sb, Ag, Co, V, Ni, Cr, Mn, Fe, Cu, Pt, Pd, Ta, Zr, Nb, Rh, Ru, Mo, Os, Re and W, a reducing agent powder of Al metal or Al alloy, and a powder of aluminium chloride; and ii) mixing and heating the mixture to form a coating on the particulate substrate, to produce a coated substrate product.
    Type: Grant
    Filed: November 16, 2018
    Date of Patent: February 14, 2023
    Assignee: D-BLOCK COATING PTY LTD.
    Inventors: Jawad Haidar, Sabaratnasingham Gnanarajan
  • Patent number: 11285568
    Abstract: Various embodiments include a solder preform for establishing a diffusion solder connection comprising: a microstructure including a solder material and a metallic material; a first joining surface for a first joining partner and a second joining surface for a second joining partner; and a diffusion zone comprising an intermetallic compound of at least some of the solder material and at least some of the metallic material. The first joining surface and the second joining surface include at least some solder material.
    Type: Grant
    Filed: April 23, 2018
    Date of Patent: March 29, 2022
    Assignee: SIEMENS AKTIENGESELLSCHAFT
    Inventors: Jörg Strogies, Klaus Wilke, Christian Schellenberg
  • Patent number: 10240222
    Abstract: A method of joining a first metal workpiece substrate and a second metal workpiece substrate by way of reaction metallurgical joining involves passing a pulsating DC electrical current through the metal workpiece substrates and a reaction material disposed between confronting faying surfaces of the workpiece substrates. The electrical current comprises a plurality of current pulses that generally increase in applied current level.
    Type: Grant
    Filed: July 1, 2015
    Date of Patent: March 26, 2019
    Assignee: GM GLOBAL TECHNOLOGY OPERATIONS LLC
    Inventors: James G. Schroth, Thomas A. Perry
  • Patent number: 10176958
    Abstract: The present invention is an electrode material constituting a movable electrode of a thermal fuse, having a five-layer clad structure including a core material layer, an intermediate layer formed on the both sides of the core material layer, and a surface layer formed on the intermediate layer, wherein the core material layer includes Cu, the intermediate layer includes an Ag—Cu-based alloy, the surface layer includes an Ag—CuO-based oxide-dispersed strengthened alloy, and the ratio of the thickness of the intermediate layer to the thickness of the surface layer (intermediate layer/surface layer) is 0.2 or more and 1.0 or less. This electrode material can be manufactured by partially internally oxidizing a three-layer clad material in which plate materials made of an Ag—Cu-based alloy are clad-jointed to both sides of the plate material made of Cu.
    Type: Grant
    Filed: April 26, 2013
    Date of Patent: January 8, 2019
    Assignee: TANAKA KIKINZOKU KOGYO K.K.
    Inventors: Osamu Sakaguchi, Michiya Takahashi, Shinya Adachi
  • Publication number: 20150099316
    Abstract: A method of forming a metal bonding layer includes forming first and second bonding metal layers on one surfaces of first and second bonding objects, respectively. The second bonding object is disposed on the first bonding object such that the first bonding metal layer and the second bonding metal layer face each other. A eutectic metal bonding layer is formed through a reaction between the first and second bonding metal layers. At least one of the first bonding metal layer and the second bonding metal layer includes an oxidation prevention layer formed on an upper surface thereof. The oxidation prevention layer is formed of a metal having an oxidation reactivity lower than an oxidation reactivity of the bonding metal layer on the upper surface which the oxidation prevention layer is disposed.
    Type: Application
    Filed: December 12, 2014
    Publication date: April 9, 2015
    Inventors: Yung Ho RYU, Seung Woo CHOI, Tae Hun KIM, Gyeong Seon PARK, Jong Hoon LIM, Sung Joon KIM, Myong Soo CHO
  • Publication number: 20150021377
    Abstract: A method of forge welding includes placing at least two components for welding together, adjacent each other and with an exothermic flux mixture placed between the components. The exothermic flux mixture is heated to initiate an exothermic reaction and the faying surfaces of the two components are pressed together. The components being welded may be tubular, in particular pipes. Apparatus for the method of forge welding and exothermic flux mixtures for the method of forge welding are also provided.
    Type: Application
    Filed: February 22, 2013
    Publication date: January 22, 2015
    Applicant: TUBEFUSE APPLICATIONS B.V.
    Inventors: Wayne RUDD, Hu Chun YI, Jeremy Joseph ITEN
  • Patent number: 8893361
    Abstract: A method and apparatus for joining a first workpiece and a second workpiece. A layer of exothermic material is placed between the first workpiece and the second workpiece. A plurality of currents is applied to the layer of exothermic material in a plurality of locations and substantially at the same time such that an exothermic reaction occurs in the layer of exothermic material.
    Type: Grant
    Filed: March 13, 2012
    Date of Patent: November 25, 2014
    Assignee: The Boeing Company
    Inventor: Fong Shi
  • Publication number: 20140273318
    Abstract: A method of forming a metal bonding layer includes forming a first bonding metal layer and a second bonding metal layer on surfaces of first and second bonding target objects, respectively. The second bonding target object is disposed on the first bonding target object to allow the first and second bonding metal layers to face each other. A eutectic metal bonding layer is formed through a reaction between the first and second bonding metal layers. At least one of the first and second bonding metal layers includes a reaction delaying layer formed of a metal for delaying the reaction between the first and second bonding metal layers.
    Type: Application
    Filed: March 12, 2014
    Publication date: September 18, 2014
    Applicant: SAMSUNG ELECTRONICS CO., LTD.
    Inventors: Yung Ho RYU, Jong Hoon LIM, Sung Joon KIM, Tae Hun KIM, Gyeong Seon PARK, Myong Soo CHO
  • Publication number: 20140248505
    Abstract: Laminated composite (10) comprising at least one electronic substrate (11) and an arrangement of layers (20, 30) made up of at least a first layer (20) of a first metal and/or a first metal alloy and of a second layer (30) of a second metal and/or a second metal alloy adjacent to this first layer (20), wherein the melting temperatures of the first and second layers are different, and wherein, after a thermal treatment of the arrangement of layers (20, 30), a region with at least one intermetallic phase (40) is formed between the first layer and the second layer, wherein the first layer (20) or the second layer (30) is formed by a reaction solder which consists of a mixture of a basic solder with an AgX, CuX or NiX alloy, wherein the component X of the AgX, CuX or NiX alloy is selected from the group consisting of B, Mg, Al, Si, Ca, Se, Ti, V, Cr, Mn, Fe, Co, Ni, Cu, Zn, Ga, Ge, Y, Zr, Nb, Mo, Ag, In, Sn, Sb, Ba, Hf, Ta, W, Au, Bi, La, Ce, Pr, Nd, Gd, Dy, Sm, Er, Tb, Eu, Ho, Tm, Yb and Lu and wherein the melti
    Type: Application
    Filed: September 21, 2012
    Publication date: September 4, 2014
    Inventors: Thomas Kalich, Christiane Frueh, Franz Wetzl, Bernd Hohenberger, Rainer Holz, Andreas Fix, Michael Guyenot, Andrea Feiock, Michael Guenther, Martin Rittner
  • Publication number: 20140212320
    Abstract: The present invention provides a process of initiating a self-propagating reaction with a coherent radiation source, which comprises mixing the chemical reactants, and contacting the chemical reactants by the coherent radiation, more specifically, the coherent radiation source may be a laser.
    Type: Application
    Filed: January 30, 2014
    Publication date: July 31, 2014
    Applicant: Colorado School of Mines
    Inventor: Reed Ayers
  • Patent number: 8590768
    Abstract: Copper metal or metal alloy workpieces and/or aluminum metal or metal alloy workpieces are joined in a solid state weld by use of a reactive material placed, in a suitable form, at the joining surfaces. Joining surfaces of the workpieces are pressed against the interposed reactive material and heated. The reactive material alloys or reacts with the workpiece surfaces consuming some of the surface material in forming a liquid-containing reaction product comprising a low melting liquid that removes oxide films and other surface impediments to a welded bond across the interface. Further pressure is applied to expel the reaction product and to join the workpiece surfaces in a solid state weld bond.
    Type: Grant
    Filed: June 14, 2010
    Date of Patent: November 26, 2013
    Assignee: GM Global Technology Operations LLC
    Inventors: David R. Sigler, James G. Schroth
  • Publication number: 20130292168
    Abstract: The invention relates to a starter material for a sintering compound, said starter material comprising particles which at least proportionally contain an organic metal compound and/or a precious metal oxide, the organic metal compound and/or the precious metal oxide being converted during heat treatment of the starter material into the elemental metal and/or precious metal. The invention is characterized in that the particles have a coating containing a reducing agent by means of which the organic metal compound and/or precious metal oxide is reduced to the elemental metal and/or precious metal at a temperature below the sintering temperature of the elemental metal and/or precious metal.
    Type: Application
    Filed: September 23, 2011
    Publication date: November 7, 2013
    Applicant: ROBERT BOSCH GMBH
    Inventors: Daniel Wolde-Giorgis, Andrea Feiock
  • Patent number: 8523045
    Abstract: Copper conductor members or other copper-base workpieces are welded using a suitable copper alloy material that is reactive with the joining surfaces of the copper members. The reactive metal material may be applied as a thin metal strip between assembled facing joining surfaces. The members are pressed together against the reactive material and heated. The combined pressure and heat enable the reactive material to react with facing workpiece material, to liquefy and remove oxides or the like that might inhibit the formation of a welded interface. The liquid, containing original reactive metal and byproducts, is squeezed from the interface of the workpieces to enable the formation of a solid-state weld between them without melting of un-reacted workpiece copper material.
    Type: Grant
    Filed: February 15, 2012
    Date of Patent: September 3, 2013
    Assignee: GM Global Technology Operations LLC
    Inventors: Thomas A. Perry, James G. Schroth, David R. Sigler
  • Publication number: 20130168144
    Abstract: The present invention relates to a method for manufacturing a printed circuit board, which includes: preparing a base substrate with an electrode pad; providing a conductive material having a predetermined height; disposing the conductive material on the electrode pad; and forming a conductive post on the electrode pad by bonding the electrode pad and the conductive material, and can achieve a fine pitch and easily implement a conductive post with a high aspect ratio.
    Type: Application
    Filed: December 17, 2012
    Publication date: July 4, 2013
    Applicant: Samsung Electro-Mechanics Co., Ltd.
    Inventor: Samsung Electro-Mechanics Co., Ltd.
  • Publication number: 20130105560
    Abstract: A new anchoring mechanism for the mold-crucible set to the tube, to which the cable is to be welded is described, and the inclusion and use of some bushings which are inserted between the cable and the mold.
    Type: Application
    Filed: September 24, 2012
    Publication date: May 2, 2013
    Applicant: KLK ELECTRO MATERIALES, S.A.
    Inventor: KLK ELECTRO MATERIALES, S.A.
  • Publication number: 20120273557
    Abstract: Copper conductor members or other copper-base workpieces are welded using a suitable copper alloy material that is reactive with the joining surfaces of the copper members. The reactive metal material may be applied as a thin metal strip between assembled facing joining surfaces. The members are pressed together against the reactive material and heated. The combined pressure and heat enable the reactive material to react with facing workpiece material, to liquefy and remove oxides or the like that might inhibit the formation of a welded interface. The liquid, containing original reactive metal and byproducts, is squeezed from the interface of the workpieces to enable the formation of a solid-state weld between them without melting of un-reacted workpiece copper material.
    Type: Application
    Filed: February 15, 2012
    Publication date: November 1, 2012
    Applicant: GM GLOBAL TECHNOLOGY OPERATIONS LLC
    Inventors: Thomas A. Perry, James G. Schroth, David R. Sigler
  • Publication number: 20120261459
    Abstract: A method of metalworking a substrate (10) previously strengthened in a gas heat treatment to form precipitates throughout an entire volume of the substrate (10), where the precipitates have an active chemical element incorporated during the gas heat treatment. The method includes: melting a portion of the substrate (10) during a full penetration metalworking process to form a molten portion (12); generating a metalworking atmosphere (22) having a supply of an active chemical element in a gas state during the metalworking process; exposing the molten portion (12) to the metalworking atmosphere (22); and cooling the molten portion (12) while maintaining exposure to the metalworking atmosphere (22) to form a solidified portion (36) comprising precipitates comprising the active chemical element, where the precipitates are present throughout an entire volume of the solidified portion (36), and thereby re-strengthen the entire volume of the solidified portion (36).
    Type: Application
    Filed: April 12, 2011
    Publication date: October 18, 2012
    Inventor: Gerald J. Bruck
  • Patent number: 8227536
    Abstract: A solder paste comprising a solder alloy powder and a flux. The volumetric expansion at the time of melting of the solder alloy is at most 0.5%. The flux contains a bisphenol A epoxy resin and a curing agent selected from a carboxylic anhydride and a dicarboxylic acid. The solder paste can be used in applications suitable for high-temperature solders. The solder alloy has an alloy composition comprising, in mass percent, 70-98% of Bi, a total of 0-0.5% of at least one substance selected from Ag, Cu, Sb, In, Zn, Ni, Cr, Fe, Mo, P, Ge, and Ga, and a remainder of Sn.
    Type: Grant
    Filed: August 11, 2006
    Date of Patent: July 24, 2012
    Assignees: Senju Metal Industry Co., Ltd., Murata Manufacturing Co., Ltd.
    Inventors: Shizuharu Watanabe, Hidekiyo Takaoka, Kosuke Nakano, Masafumi Seino, Ko Inaba
  • Publication number: 20120184446
    Abstract: A process produces a connecting structure between two superconductors, in particular magnesium diboride superconductors embodied as a superconducting core wire surrounded by normally conducting metal. A substance which reduces the melting point of magnesium is admixed to a substance mixture including magnesium and boron, and the exposed ends of the core wires are brought into contact with the substance mixture, which is caused to react in situ at a reaction temperature corresponding to the lower melting point to give magnesium diboride.
    Type: Application
    Filed: September 29, 2010
    Publication date: July 19, 2012
    Applicant: Siemens Aktiengesellschaft
    Inventors: Antje Drechsler, Wilfried Goldacker, Marijn Pieter Oomen, Jacob Johan Rabbers, Sonja Schlachter
  • Patent number: 8186568
    Abstract: A process for assembling two parts of an integrated electronic circuit has two successive steps. During a first step, the two circuit parts are made into a single unit by molecular bonding, realized on respective application surfaces of the two parts. During a second step, electrical connections are formed from connection portions already present in the application surfaces of the two circuit parts. The connections formed extend across the bonding interface, and are compatible with a high reliability and a high level of integration of the circuit.
    Type: Grant
    Filed: February 21, 2008
    Date of Patent: May 29, 2012
    Assignee: STMicroelectronics (Crolles 2) SAS
    Inventors: Philippe Coronel, Perceval Coudrain, Pascale Mazoyer
  • Publication number: 20120061454
    Abstract: An exothermic reaction mixture for joining metallic components includes at least one transition metal oxide and, as fuel, a mixture of aluminium and calcium suicide, wherein the molar ratio of aluminium to calcium suicide is from 16:1 to 0.25:1. Methods of preparing the exothermic reaction mixtures and for using them in welding applications are also described.
    Type: Application
    Filed: October 23, 2009
    Publication date: March 15, 2012
    Applicant: TUBEFUSE APPLICATIONS B.V.
    Inventors: Wayne Rudd, Allison Rudd, Diane Hopper, Hu Chun Yi
  • Publication number: 20120055979
    Abstract: A weld ignition system includes a wireless receiver that wirelessly receives a weld ignition activation signal. The weld ignition system further includes igniter that ignites a weld ignition material in response to the wireless receiver wirelessly receiving the weld ignition activation signal. The ignited weld ignition material initiates exothermic based welding of a weld material.
    Type: Application
    Filed: April 23, 2010
    Publication date: March 8, 2012
    Inventor: Fady Ameer Alghusain
  • Publication number: 20120045628
    Abstract: A method is described for producing a micromechanical component. The method includes providing a first substrate, providing a second substrate, developing a projecting patterned element on the second substrate, and connecting the first and the second substrate via the projecting patterned element. The method provides that the connecting of the first and the second substrate includes eutectic bonding. Also described is a micromechanical component, in which a first and a second substrate are connected to each other.
    Type: Application
    Filed: April 7, 2010
    Publication date: February 23, 2012
    Inventors: Julian Gonska, Heribert Weber
  • Patent number: 8074869
    Abstract: A reactive foil is used to assemble the components of rock bit cutters and to affix cutting elements to rock bit bodies. A small pulse of localized energy ignites the foil in a fraction of a second to deliver the necessary amount of heat energy to flow solder or braze and form a strong, true metallic joint. The reaction in the foil may be activated using optical, electrical, or thermal sources.
    Type: Grant
    Filed: November 14, 2007
    Date of Patent: December 13, 2011
    Assignee: Baker Hughes Incorporated
    Inventors: Nicholas J. Lyons, Nathan David Ames
  • Publication number: 20110198391
    Abstract: An assembly is disclosed for exothermic welding comprising a mold which is formed of a material which withstands exothermic welding temperatures and includes a weld cavity therein for positioning at least two members which are to be exothermically welded together, and an ignition cavity communicating with the weld cavity. The mold is capable of accommodating any one of several exothermic welding procedures which may involve either a flint igniter or the use of an electrical igniter which is readily accommodated by the mold in the performance of several of the procedures. The electrical igniter is formed of a pair of flat, longitudinally extending conductor strips with a sheet of insulation laminated therebetween, a filament adjacent one end of the strips, and one or more positioning tabs adjacent one end of the strips. A cartridge is also provided which contains the weld metal and the electrical igniter and which may be positioned in the ignition cavity of the mold.
    Type: Application
    Filed: April 21, 2011
    Publication date: August 18, 2011
    Applicant: Harger, Inc.
    Inventors: Curtis R. Stidham, Mark S. Harger
  • Publication number: 20110097161
    Abstract: Fluidizable potassium fluorozincate which is very suitable for dry fluxing applications can be prepared from a diluted potassium base selected from the group consisting of KOH, KHCO3 and K2CO3, ZnO and HF. The cumulative volume of the particles has an X10 value of equal to or greater than 1.5 microns, preferably, equal to or greater than 2 microns. It is very suitable for pneumatic transport for aluminum brazing.
    Type: Application
    Filed: June 18, 2009
    Publication date: April 28, 2011
    Applicant: SOLVAY FLUOR GMBH
    Inventors: Andreas Becker, Placido Garcia-Juan
  • Publication number: 20110031301
    Abstract: A method for joining components to be used in an electrical generator. First and second components are provided. The first and second components are preheated and a reactive bonding material is disposed between and in contact with the first and second components. The reactive bonding material includes a first material, which is a brazing material, and a second material that is capable of melting the first material upon an initiation of an exothermic reaction in the second material. An exothermic reaction is initiated in the second material to effect a release of thermal energy from the second material to melt the first material. Upon a cooling and solidification of the first material, the first material creates a bond between a first surface of the first component and a second surface of the second component to join the first and second components together.
    Type: Application
    Filed: August 6, 2009
    Publication date: February 10, 2011
    Inventors: David S. Segletes, William F. Jones
  • Publication number: 20100316885
    Abstract: The present invention relates to an assembly method by reactive brazing of a first metallic element such as an end cover plate of a vacuum cartridge with a second element such as the cylindrical body of said cartridge, said second element comprising an ion-covalent oxide at least at the surface by means of an alloy called added alloy designed to constitute a liquid brazing alloy designed to wet the two respectively metallic and ion-covalent oxide surfaces to be assembled of the above-mentioned two elements, said brazing alloy containing titanium and said metallic element containing nickel.
    Type: Application
    Filed: June 9, 2010
    Publication date: December 16, 2010
    Applicant: SCHNEIDER ELECTRIC INDUSTRIES SAS
    Inventors: Marie-Francoise Devismes, Dominique Mazzucchi, Hans Schellekens, Olga Kozlova
  • Publication number: 20100258537
    Abstract: Aluminum alloy workpieces and/or magnesium alloy workpieces are joined in a solid state weld by use of a reactive material placed, in a suitable form, at the joining surfaces. Joining surfaces of the workpieces are pressed against the interposed reactive material and heated. The reactive material alloys or reacts with the workpiece surfaces consuming some of the surface material in forming a reaction product comprising a low melting liquid that removes oxide films and other surface impediments to a welded bond across the interface. Further pressure is applied to expel the reaction product and to join the workpiece surfaces in a solid state weld bond.
    Type: Application
    Filed: April 9, 2009
    Publication date: October 14, 2010
    Applicant: GM GLOBAL TECHNOLOGY OPERATIONS, INC.
    Inventors: David R. Sigler, James G. Schroth, Xiaohong Q. Gayden, Yen-Lung Chen
  • Publication number: 20100243715
    Abstract: This invention relates to a thermite welding process for joining sections of a railway line in situ, the process including the preliminary step of mounting a suitable welding mould about the aligned sections of railway line to be welded together and sealing the mould to prevent run out; mounting a vibration means on the railway line at a suitable distance from the mould and operating it at a suitable frequency; heating the sections of railway line to a desired temperature; igniting an ignitor means and allowing it to drop into the mould to react with molten steel in the mould and fill a weld area about and between the sections of railway line in the mould; and when solidified, to vibrate the railway line for a further period of time until stress relieving of the cast weld area has occurred.
    Type: Application
    Filed: November 21, 2008
    Publication date: September 30, 2010
    Inventor: Brent Felix Jury
  • Patent number: 7771547
    Abstract: Methods are disclosed for producing in-situ composite solders having a particulate intermetallic phase homogeneously distributed throughout the solder matrix. An eutectic solder is mixed with the components of the intermetallic phase, melted and rapidly cooled to form the desired solder. In-situ composite solder alloys formed by the disclosed method provide greater solder joint strength and fatigue resistance.
    Type: Grant
    Filed: December 8, 2003
    Date of Patent: August 10, 2010
    Assignee: Board of Trustees Operating Michigan State University
    Inventors: Thomas R. Bieler, Karatholuvu N. Subramanian, Sunglak Choi
  • Publication number: 20100135812
    Abstract: A gas turbine airfoil is disclosed. The gas turbine airfoil includes a root section, a separate extension section attached to the root section, and a joint disposed between the root section and the extension section, the joint including at least one of a mechanical interlock and a metallurgical bond.
    Type: Application
    Filed: January 11, 2007
    Publication date: June 3, 2010
    Inventors: Ronald Ralph Cairo, Arthur Samuel Peck
  • Publication number: 20100127047
    Abstract: A method of inhibiting a formation of palladium-nickel-tin (Pd—Ni—Sn) intermetallic in solder joints is described as follows. Firstly, a solder alloy is provided. Then, at least one of a trace of copper and a trace of zinc is doped into the solder alloy. Afterward, the solder alloy is disposed on the Pd-bearing surface finish, such as a Pd/Ni bi-layer or a Au/Pd/Ni tri-layer. Next, the solder alloy is soldered with the surface finish as solder joints. During the soldering, the Cu and Zn will incorporate into the soldering reaction, forming copper-palladium-nickel-tin intermetallic and zinc-palladium-nickel-tin intermetallic, replacing the Pd—Ni—Sn respectively. Consequently, the addition of Cu and/or Zn into solders will inhibit the undesirable Pd—Ni—Sn intermetallic to form in the solder joints.
    Type: Application
    Filed: January 13, 2009
    Publication date: May 27, 2010
    Applicant: Yuan Ze University
    Inventors: Cheng-En Ho, Wei-Hsiang Wu, Cheng-Shiuan Lin
  • Publication number: 20100035072
    Abstract: A solder paste comprising a solder alloy powder and a flux. The volumetric expansion at the time of melting of the solder alloy is at most 0.5%. The flux contains a bisphenol A epoxy resin and a curing agent selected from a carboxylic anhydride and a dicarboxylic acid. The solder paste can be used in applications suitable for high-temperature solders. The solder alloy has an alloy composition comprising, in mass percent, 70-98% of Bi, a total of 0-0.5% of at least one substance selected from Ag, Cu, Sb, In, Zn, Ni, Cr, Fe, Mo, P, Ge, and Ga, and a remainder of Sn.
    Type: Application
    Filed: August 11, 2006
    Publication date: February 11, 2010
    Inventors: Shizuharu Watanabe, Hidekiyo Takaoka, Kosuke Nakano, Masafumi Seino, Ko Inaba
  • Publication number: 20100015463
    Abstract: One embodiment of the invention includes first particles comprising an intermetallic compound comprising titanium and aluminum; second particles comprising aluminum; and third particles comprising titanium.
    Type: Application
    Filed: December 21, 2007
    Publication date: January 21, 2010
    Inventor: June Sang Siak
  • Publication number: 20090242615
    Abstract: This invention is directed to a process for joining materials comprising providing an assembly comprising at least one material layer; at least one metal heat source; and at least one solder layer, each solder layer disposed between each metallic heat source and each material layer; placing the assembly in a controlled atmosphere; and initiating a chemical reaction in the metal heat source so as to enable the solder to join the material layer.
    Type: Application
    Filed: June 3, 2009
    Publication date: October 1, 2009
    Inventors: Neeraj Saxena, Kevin McKeigue
  • Publication number: 20090188969
    Abstract: A solid weld-metal-producing material is formed by agglomerating weld metal material powder. An igniter may be integrally formed in or on the agglomerated weld metal material. In addition to typical components of a weld metal material mixture, such as a reductant metal and a transition metal oxide, the agglomerated weld metal mixture may include a binder material, such as sodium silicate. In addition to functioning as a binder to help hold the agglomerated weld metal material together, the binder material may aid in the exothermic reaction that occurs when the weld metal material is ignited. The agglomerated weld metal material may be made by mixing together a reductant metal powder, a transition metal oxide powder, and possibly a binder solution. A slurry of the components may be pressed together, for example, using a die and a ram, and then may be dried.
    Type: Application
    Filed: April 8, 2009
    Publication date: July 30, 2009
    Inventors: Glenn T Siracki, John J. Gregel, Dale R. Boling, Frank J. Fitzgerald, George F. Kub, JR., Andrew W. Weisel, Johannes L.L.A van den Broek, Timothy P. Sepelak
  • Publication number: 20090186195
    Abstract: A process and apparatus for the reactive multilayer joining of components utilizing a print screen metallization technique to bond difficult-to-wet materials and temperature sensitive materials to produce joined products.
    Type: Application
    Filed: March 11, 2009
    Publication date: July 23, 2009
    Applicant: REACTIVE NANOTECHNOLOGIES, INC.
    Inventors: Ronald L. Spraker, Greg Caswell, Timothy P. Weihs
  • Publication number: 20090173626
    Abstract: A method for joining component bodies of material over bonding regions of large dimensions by disposing a plurality of substantially contiguous sheets of reactive composite materials between the bodies and adjacent sheets of fusible material. The contiguous sheets of the reactive composite material are operatively connected by an ignitable bridging material so that an igniting reaction in one sheet will cause an igniting reaction in the other. An application of uniform pressure and an ignition of one or more of the contiguous sheets of reactive composite material causes an exothermic thermal reaction to propagate through the bonding region, fusing any adjacent sheets of fusible material and forming a bond between the component bodies.
    Type: Application
    Filed: April 14, 2008
    Publication date: July 9, 2009
    Inventors: Alan Duckham, Jesse E. Newson, Michael V. Brown, Timothy Ryan Rude, Omar M. Knio, Ellen M. Heian, Jai S. Subramanian, Timothy P. Weihs, Yuping Lin, Jonathan Levin, Gary Catig
  • Publication number: 20090134206
    Abstract: For production of an electrically conductive or thermally conductive connection for contacting two elements, an elemental metal, in particular silver, is formed from a metal compound, in particular a silver compound, between the contact surfaces. In this production, the processing temperature for the use of a silver solder can be decreased below 240° C. and the processing pressure can be reduced to normal pressure. A contacting paste for this purpose contains a metal compound, in particular a silver compound, which decomposes below 400° C. while forming elemental silver. As a result, a metal is generated in situ from a chemical compound for producing a contact, which is usable above the temperature necessary for its production.
    Type: Application
    Filed: September 25, 2008
    Publication date: May 28, 2009
    Applicant: W. C. Heraeus GmbH
    Inventors: Wolfgang SCHMITT, Tanja DICKEL, Katja STENGER
  • Publication number: 20090032572
    Abstract: A reactive foil is used to join rock bit components such as leg sections, hardfacing, and cutter elements to the rolling cone earth-boring bit body. A small pulse of localized energy ignites the foil in a fraction of second to deliver the necessary amount of heat energy to reflow solder or braze and form a strong, true metallic joint. The reaction in the foil may be activated using optical, electrical, or thermal sources.
    Type: Application
    Filed: August 3, 2007
    Publication date: February 5, 2009
    Inventors: Andy Oxfdord, Mathews George, Curtis A. Proske
  • Publication number: 20080110962
    Abstract: This invention is directed to a process for joining materials comprising providing an assembly comprising at least one material layer; at least one metal heat source; and at least one solder layer, each solder layer disposed between each metallic heat source and each material layer; placing the assembly in a controlled atmosphere; and initiating a chemical reaction in the metal heat source so as to enable the solder to join the material layer.
    Type: Application
    Filed: July 23, 2007
    Publication date: May 15, 2008
    Inventors: Neeraj Saxena, Kevin McKeigue
  • Patent number: 6820795
    Abstract: A method for producing a joined body comprising a supporting member made of a ceramic material for supporting a semiconductor wafer, a metal member and a joining layer for joining the supporting and metal members is provided. A first metal film is formed on a joining surface of the supporting member. A second metal film is formed on a joining surface of the metal member. A metal adhesive is placed between the first and second films to provide an assembly. The assembly is then heated at a temperature not higher than a melting point of the metal adhesive while the assembly is subjected to isostatic pressing, so that the supporting and metal members are joined by diffusion joining.
    Type: Grant
    Filed: September 3, 2002
    Date of Patent: November 23, 2004
    Assignee: NGK Insulators, Ltd.
    Inventor: Tomoyuki Fujii
  • Patent number: 6534194
    Abstract: In accordance with the invention a reactive multilayer foil is fabricated by providing an assembly (stack or multilayer) of reactive layers, inserting the assembly into a jacket, deforming the jacketed assembly to reduce its cross sectional area, flattening the jacketed assembly into a sheet, and then removing the jacket. Advantageously, the assembly is wound into a cylinder before insertion into the jacket, and the jacketed assembly is cooled to a temperature below 100° C. during deforming. The resulting multilayer foil is advantageous as a freestanding reactive foil for use in bonding, ignition or propulsion.
    Type: Grant
    Filed: May 1, 2001
    Date of Patent: March 18, 2003
    Assignee: Johns Hopkins University
    Inventors: Timothy P. Weihs, Michael Reiss
  • Patent number: 6316125
    Abstract: The invention provides a new and improved process and exothermic reaction mixture for producing molten weld metal. The molten weld metal is used in joining one metallic piece with at least one other metallic piece. The process and exothermic reaction mixture have distinct advantages over the prior art. These advantages include a higher filler metal yield, an increased tensile strength, and a higher quality corrosion resistant weld. These advantages are accomplished by a process wherein a reactant mixture is provided which has a reducing agent, a metallic compound, and at least two filler metals that at least in part do not chemically react with the metallic compound, one of which is aluminum. The metallic compound subsequently forms, with the reducing agent, having a high heat of formation which provides an exothermic reaction with sufficient heat to melt the filler metals.
    Type: Grant
    Filed: April 1, 1999
    Date of Patent: November 13, 2001
    Assignee: Erico International Corporation
    Inventors: Nicolae Gaman, Harrie van den Nieuwelaar
  • Patent number: 6199751
    Abstract: A technique of forming a metallurgical bond between pads on two surfaces is provided. A metal coating placed on each surface includes a first metal base layer and a second metal surface layer. The first and second metals include a low melting point constituent. A first ratio of the two metals forms a liquid phase with a second ratio of the two metals forming a solid phase. The volume of the base layer metal exceeds the volume necessary to form the solid phase between the base metal and the surface metal. Conductive metal particles are provided having a core metal and a coating metal dispersed in an uncured polymer material, at a volume fraction above the percolation threshold. The core metal and the coating metal together include a low melting point constituent. At a first ratio the components form a liquid phase and at a second ratio the two components form a solid phase.
    Type: Grant
    Filed: March 23, 2000
    Date of Patent: March 13, 2001
    Assignee: International Business Machines Corporation
    Inventors: Michael A. Gaynes, Kostas I. Papathomas, Giana M. Phelan, Charles G. Woychik
  • Patent number: 6089444
    Abstract: Process for bonding a copper substrate to a tungsten substrate by providing a thin metallic adhesion promoting film bonded to a tungsten substrate and a functionally graded material (FGM) interlayer bonding the thin metallic adhesion promoting film to the copper substrate. The FGM interlayer is formed by sintering a stack of individual copper and tungsten powder blend layers having progressively higher copper content/tungsten content, by volume, ratio values in successive powder blend layers in a lineal direction extending from the tungsten substrate towards the copper substrate. The resulting copper to tungsten joint well accommodates the difference in the coefficient of thermal expansion of the materials.
    Type: Grant
    Filed: September 2, 1997
    Date of Patent: July 18, 2000
    Assignee: McDonnell Douglas Corporation
    Inventors: Kevin T. Slattery, Daniel E. Driemeyer, John W. Davis
  • Patent number: 6066219
    Abstract: The invention relates to a novel ceramic substrate with at least one layer essentially of aluminum nitride which is provided on at least one surface side with an intermediate or auxiliary layer which contains aluminum oxide and which has a thickness in the range of 0.5-10 microns, and to a process for its production.
    Type: Grant
    Filed: February 3, 1997
    Date of Patent: May 23, 2000
    Assignee: Curamik Electronics GmbH
    Inventors: Jurgen Schulz-Harder, Karsten Schmidt, Karl Exel
  • Patent number: 5988488
    Abstract: Process for bonding a copper substrate to a tungsten substrate by providing a thin metallic adhesion promoting film bonded to a tungsten substrate and a functionally graded material (FGM) interlayer bonding the thin metallic adhesion promoting film to the copper substrate. The FGM interlayer is formed by thermal plasma spraying mixtures of copper powder and tungsten powder in a varied blending ratio such that the blending ratio of the copper powder and the tungsten powder that is fed to a plasma torch is intermittently adjusted to provide progressively higher copper content/tungsten content, by volume, ratio values in the interlayer in a lineal direction extending from the tungsten substrate towards the copper substrate. The resulting copper to tungsten joint well accommodates the difference in the coefficient of thermal expansion of the materials.
    Type: Grant
    Filed: September 2, 1997
    Date of Patent: November 23, 1999
    Assignee: McDonnell Douglas Corporation
    Inventors: Kevin T. Slattery, Daniel E. Driemeyer