With Placement Of Tracer In Or About Well Patents (Class 250/259)
  • Patent number: 11492535
    Abstract: A method may include introducing a resin treatment fluid into a wellbore, the resin treatment fluid including a resin, a hardening agent, and a neutron contrasting agent; and allowing the resin treatment fluid to set to form a hardened mass.
    Type: Grant
    Filed: November 29, 2021
    Date of Patent: November 8, 2022
    Assignee: Halliburton Energy Services, Inc.
    Inventors: James Robert Benkley, Paul J. Jones, Samuel Lewis
  • Patent number: 11384622
    Abstract: A method of decontaminating naturally occurring radioactive material (NORM) from downhole equipment may include injecting a NORM dissolver into an isolated region of a wellbore in which NORM-contaminated production equipment is located; and removing the NORM contaminants from the production equipment. The method may also include recommencing production of hydrocarbons following the decontamination.
    Type: Grant
    Filed: April 20, 2017
    Date of Patent: July 12, 2022
    Assignee: CAMERON INTERNATIONAL CORPORATION
    Inventors: Mohammed Abdellatif, Mohamed AlMahdy, Henricus Fortuin
  • Patent number: 11274547
    Abstract: A tracer injection system can include a tracer solution, a pump configured to pump the tracer solution, a data transmitter associated with the tracer solution, a data receiver configured to receive tracer characteristic data from the data transmitter, and a pump controller that variably operates the pump, based at least in part on the tracer characteristic data received by the data receiver. A tracer injection method can include associating a data transmitter with a container and a tracer solution in the container, so that the data transmitter is transported with the container and the tracer solution, receiving from the data transmitter data indicative of a characteristic of the tracer solution, and pumping the tracer solution from the container at a flow rate based at least in part on the received data.
    Type: Grant
    Filed: August 29, 2018
    Date of Patent: March 15, 2022
    Assignee: Reservoir Metrics IP Holdings, LLC
    Inventor: Mitchell C. Smithson
  • Patent number: 10655445
    Abstract: A method for evaluating induced fractures in a wellbore includes obtaining a first set of data in a wellbore using a downhole logging tool. A first proppant is pumped into the wellbore, after the first set of data is captured. The first proppant includes a first tracer that is not radioactive. A second proppant is also pumped into the wellbore, after the first proppant is pumped into the wellbore. The second proppant includes a second tracer that is not radioactive, and the second tracer is different than the first tracer. A second set of data is obtained in the wellbore using the downhole tool after the first and second proppants are pumped into the wellbore. The first and second sets of data are compared.
    Type: Grant
    Filed: December 4, 2017
    Date of Patent: May 19, 2020
    Assignee: CARBO CERAMICS INC.
    Inventors: Jeremy Zhang, Harry D. Smith, Jr.
  • Patent number: 10344581
    Abstract: Methods for logging a well utilizing natural radioactivity originating from clay based particulates are disclosed. The methods can include utilizing a gravel pack slurry containing a liquid and gravel pack particles to hydraulically place the particles into a gravel pack zone of a borehole penetrating a subterranean formation and obtaining a post gravel pack data set by lowering into the borehole traversing the subterranean formation a gamma ray detector and detecting gamma rays resulting from a native radioactivity of the gravel pack particles. The methods can further include using the post gravel pack data set to determine a location of the gravel pack particles and correlating the location of the gravel-pack particles to a depth measurement of the borehole to determine the location, height, and/or percent fill of gravel-pack particles placed in the gravel pack zone of the borehole.
    Type: Grant
    Filed: May 6, 2016
    Date of Patent: July 9, 2019
    Assignee: CARBO CERAMICS INC.
    Inventors: Qianmei Zhang, Harry D. Smith, Jr.
  • Patent number: 10337317
    Abstract: A method for monitoring precipitation of a wax component in a hydrocarbon fluid stream i) using a labelled wax introduced in a fluid transport system at one in-flow point and measuring its absolute or relative concentration at one out-flow point is provided. A method for generating a labelled wax, and the use of a labelled wax is also provided.
    Type: Grant
    Filed: September 18, 2015
    Date of Patent: July 2, 2019
    Assignee: Institutt for Energiteknikk
    Inventors: Martin Foss, Tor Bjørnstad, Terje Sira
  • Patent number: 9976383
    Abstract: Disclosed are traceable polymeric additives that comprise a tagging material and methods of using the traceable polymeric additives in subterranean applications, such as cementing. An embodiment discloses a well treatment composition comprising a base fluid and a traceable polymeric additive comprising a polymer and a tagging material.
    Type: Grant
    Filed: January 23, 2017
    Date of Patent: May 22, 2018
    Assignee: Halliburton Energy Services, Inc.
    Inventors: Christopher Lynn Gordon, Craig Wayne Roddy, Jiten Chatterji
  • Patent number: 9593572
    Abstract: In one aspect, a wellbore system is disclosed for determining breach of cement section in the wellbore, wherein the system includes a cement section in the wellbore formed to prevent flow of fluids including hydrocarbons through the cement section, nonradioactive tracers that emit radioactive emission when activated by a radiation source, a radioactive source that generates radioactive particles to activate the nonradioactive tracers that have migrated through the cement to cause the nonradioactive tracers to emit radiation, a detector for detecting the radioactive emission from the nonradioactive tracer, and a processor that determines from the detected radioactive emission a fluid leak through the cement section.
    Type: Grant
    Filed: October 1, 2014
    Date of Patent: March 14, 2017
    Assignee: BAKER HUGHES INCORPORATED
    Inventors: Darin H. Duphorne, Rocco DiFoggio
  • Patent number: 9580637
    Abstract: Disclosed are traceable polymeric additives that comprise a tagging material and methods of using the traceable polymeric additives in subterranean applications, such as cementing. An embodiment discloses a method of well treatment comprising introducing a fluid comprising a traceable polymeric additive into a wellbore, wherein the traceable polymeric additive comprises a polymer and a tagging material.
    Type: Grant
    Filed: November 22, 2013
    Date of Patent: February 28, 2017
    Assignee: Haliburton Energy Services, Inc.
    Inventors: Christopher Lynn Gordon, Craig Wayne Roddy, Jiten Chatterji
  • Patent number: 9359886
    Abstract: This disclosure relates to systems and methods associated with a replenishable receptacle for tagger and/or tracer material in a wellbore. The system may include a receptacle configured to contain tracer material and release tracer material into fluid flowing in a wellbore responsive to the fluid flowing adjacent to the receptacle. The tracer material includes a distinctive element or chemical configured to facilitate determining information associated with movement of fluid in the wellbore. A rate of the release of the tracer material may be related to a rate of flow of the fluid in the wellbore. The receptacle may be further configured to be refilled with tracer material responsive to the tracer material contained by the receptacle being depleted. Refilling the receptacle may be performed via one or more of a wireline, a coiled tubing, a tractor, a robot, a work-string and/or tubing from a light intervention vessel, and/or other approaches.
    Type: Grant
    Filed: April 2, 2014
    Date of Patent: June 7, 2016
    Assignee: CHEVRON U.S.A. INC.
    Inventor: John Alasdair Cameron
  • Publication number: 20150130468
    Abstract: A fluid monitoring apparatus includes a housing and a tracer sensor attached to an exterior of the housing. The housing has at least one flow passage for a fluid sample and a port for the tracer sensor to monitor the fluid sample in the housing. In one example, the monitoring apparatus may include a plurality of tracer sensors attached to the housing, wherein the tracer sensors are interchangeably attached to the housing. In one embodiment, the monitoring apparatus may be attached to a first well for detecting the presence of a tracer in the first well, wherein the tracer is supplied from a second well.
    Type: Application
    Filed: October 17, 2014
    Publication date: May 14, 2015
    Inventors: Sean M. CHRISTIAN, Daniel Charles BOYDE
  • Publication number: 20150115144
    Abstract: In an embodiment, scintillator can have a Figure of Merit of 0.4 at a temperature greater than 120° C., a Figure of Merit of at least 0.05 at a temperature of at least 160° C., or both. In another embodiment, a scintillator can include a Br-containing or an I-containing elpasolite. Either scintillator can be used in a radiation detection apparatus that include a photosensor and a radiation detection apparatus. Such an apparatus can be used to detect and discriminate two different types of radiation over a wide range of temperatures. The radiation detection apparatus can be useful in drilling, well logging, or as a portal detector.
    Type: Application
    Filed: October 15, 2014
    Publication date: April 30, 2015
    Inventors: Kan Yang, Peter R. Menge, Julien Lejay, Vladimir Ouspenski
  • Publication number: 20150076335
    Abstract: An apparatus for detecting a gamma-ray includes: a gamma-ray detection material comprising a material transparent to light having a plurality of nano-crystallites where each nano-crystallite in the plurality has as periodic crystal structure with a diameter or dimension that is less than 1000 nm and includes (i) a heavy atom having an atomic number greater than or equal to 55 that emits an energetic electron upon interacting with an incoming gamma-ray and (ii) and an activator atom that provides for scintillation upon interacting with the energetic electron to emit light photons wherein the heavy atom and the activator atom have positions in the periodic crystal structure of each nano-crystallite in the plurality; and a photodetector optically coupled to the gamma-ray detection material and configured to detect the light photons emitted from the scintillation and to provide a signal correlated to the detected light photons.
    Type: Application
    Filed: September 12, 2014
    Publication date: March 19, 2015
    Applicant: BAKER HUGHES INCORPORATED
    Inventors: Maxim Vasilyev, Valery N. Khabashesku, Andrei Fedorov, Mikhail Korjik
  • Patent number: 8969793
    Abstract: Systems and methods for measuring neutron-induced activation gamma-rays in a subterranean formation are provided. In one example, a downhole tool for measuring neutron-induced activation gamma-rays may include a neutron source and a gamma-ray detector. The neutron source may emit neutrons according to a pulsing scheme that includes a delay between two pulses. The delay may be sufficient to allow substantially all neutron capture events due to the emitted neutrons to cease. The gamma-ray detector may be configured to detect activation gamma-rays produced when elements activated by the emitted neutrons decay to a non-radioactive state.
    Type: Grant
    Filed: June 26, 2009
    Date of Patent: March 3, 2015
    Assignee: Schlumberger Technology Corporation
    Inventors: Christian Stoller, Peter Wraight, Brad Roscoe
  • Patent number: 8927924
    Abstract: A leak detector (190) includes a sensor head (260), a light source (200) optically coupled to the sensor head and operable to generate excitation light. A detector (205) is optically coupled to the sensor head and operable to detect fluorescence light. A signal processing unit (210) is coupled to the detector and operable to signal a leak condition responsive to an intensity of the fluorescence light exceeding a threshold. A fluid-tight enclosure (235) encloses at least the light source, the detector, and the signal processing unit.
    Type: Grant
    Filed: March 6, 2009
    Date of Patent: January 6, 2015
    Assignee: FMC Technologies, Inc.
    Inventors: Daniel McStay, Laurie Costello, David Kane
  • Publication number: 20150001385
    Abstract: The fluid tracers according to the invention have the advantage of producing a memory effect fluorescent signal, that is to say a signal modified as a function of the physico-chemical conditions encountered in the medium through which the nanoparticles pass after injection into the geological underground area. The analysis of fluorescent signals in the fluids collected after diffusion makes it possible to deduce therefrom information on the characteristics of the oil reservoir.
    Type: Application
    Filed: June 22, 2012
    Publication date: January 1, 2015
    Applicant: TOTAL SA
    Inventors: Pascal Perriat, Nicolas Crowther, Matteo Martini, Olivier Tillement, Thomas Brichart, Nicolas Agenet
  • Patent number: 8921768
    Abstract: Logging systems and methods that employ nanosensors to obtain spectral measurements downhole. The nanosensors can be dispersed in borehole fluids (including cement slurries) that circulate, diffuse, or get injected in a borehole. Because the nanosensors have diameters on the order of 10 nm to 1000 nm, they readily penetrate into cracks, pores, and other voids where their carrier fluids can reach. The nanosensors transport light sources and recording media to measure spectra in these otherwise inaccessible regions. The nanosensors are then recovered and analyzed to reconstruct the measured spectra and determine relevant material characteristics. Among other things, spectral measurements can reveal the presence of certain elements and molecules in the formation and fluids, from which information scientists determine composition and phases of formation fluids and the formation itself.
    Type: Grant
    Filed: June 1, 2011
    Date of Patent: December 30, 2014
    Assignee: Halliburton Energy Services, Inc.
    Inventors: Christopher M. Jones, Michael T. Pelletier, Jing Shen, Marian L. Morys
  • Publication number: 20140299756
    Abstract: This disclosure relates to systems and methods associated with a replenishable receptacle for tagger and/or tracer material in a wellbore. The system may include a receptacle configured to contain tracer material and release tracer material into fluid flowing in a wellbore responsive to the fluid flowing adjacent to the receptacle, The tracer material includes a distinctive element or chemical configured to facilitate determining information associated with movement of fluid in the wellbore. A rate of the release of the tracer material may be related to a rate of flow of the fluid in the wellbore. The receptacle may be further configured to be refilled with tracer material responsive to the tracer material contained by the receptacle being depleted. Refilling the receptacle may be performed via one or more of a wireline, a coiled tubing, a tractor, a robot, a work-string and/or tubing from a light intervention vessel, and/or other approaches.
    Type: Application
    Filed: April 2, 2014
    Publication date: October 9, 2014
    Applicant: CHEVRON U.S.A. INC.
    Inventor: John Alasdair Cameron
  • Patent number: 8731888
    Abstract: Systems and methods which provide modeling or simulation of gamma ray (GR) tool response using a hybrid analytical and numerical technique are shown. Embodiments employ a GR tool simulation technique which provides gamma ray information simulated as a function of only the gamma particles which reach the detector without scattering. Embodiments utilize a discretization function to determine the gamma particles which would reach a point detector from each unit volume source of an investigation domain without scattering. Embodiments further utilize the foregoing discretization function with respect to a plurality of point detectors, wherein the particular number and configuration of point detectors are selected to relatively accurately simulate the results of a particular GR detector configuration, such as line detector or volume detector configurations.
    Type: Grant
    Filed: November 14, 2008
    Date of Patent: May 20, 2014
    Assignee: ExxonMobil Upstream Company
    Inventors: Hezhu Yin, Guo Pingjun, JinJuan Zhou
  • Patent number: 8674290
    Abstract: The present invention relates to novel methods for monitoring or tracing a job operation performed in a borehole, such as well boreholes traversing a geological formation. In one embodiment, the novel methods of the invention comprise the steps of: (a) disposing into the borehole a neutron absorber during the performance of the job operation; (b) logging the borehole with an instrument capable of measuring a neutron capture in and around the borehole after performance of the job operation; and (c) monitoring or tracing the job operation performed in the borehole by comparing the measured neutron capture with a baseline neutron capture in and around the borehole. The methods of the present invention pose small or no risk from a health safety and environment perspective and are useful for monitoring or tracing hydraulic fracturing, cementing operation in well boreholes, production logging or subsurface location of downhole collars, float shoes and other jewellry.
    Type: Grant
    Filed: September 16, 2010
    Date of Patent: March 18, 2014
    Inventors: Robert Michael Masnyk, Hermann Kramer
  • Publication number: 20140070084
    Abstract: The present invention relates to methods for monitoring or tracing a job operation performed in a borehole, such as well boreholes traversing a geological formation. In one embodiment, the methods of the invention include (a) disposing into the borehole, in alternate stages, a neutron absorber during the performance of the job operation; (b) logging the borehole with an instrument capable of measuring a neutron capture in and around the borehole after performance of the job operation; and (c) monitoring or tracing the job operation performed in the borehole by comparing the measured neutron capture with a baseline neutron capture in and around the borehole. The methods of the present invention pose small or no risk from a heath safety and environment perspective and are useful for monitoring or tracing hydraulic fracturing, cementing operation in well boreholes, production logging or subsurface location downhole collars, float shoes and other jewellery.
    Type: Application
    Filed: November 18, 2013
    Publication date: March 13, 2014
    Inventors: Robert Michael MASNYK, Hermann Kramer
  • Patent number: 8575548
    Abstract: A transport of plasmonic particles through a mineral formation is analyzed by flowing a plasmonic particles solution through an immobile phase (e.g., a mineral formation), determining an absorbance of the plasmonic particles solution subsequent to flowing the plasmonic particles solution through the immobile phase, comparing the determined absorbance of the plasmonic particles solution with an absorbance of the plasmonic particles solution determined previous to flowing the plasmonic particles solution through the immobile phase, and determining an absorbance of the plasmonic particles to the immobile phase as a function of the comparison. The plasmonic particles solution may be produced by dissolving or suspending plasmonic particles in a mobile phase. Flowing the plasmonic particles solution through the immobile phase may include injecting the plasmonic particles solution into the immobile phase, and then flushing the plasmonic particles solution through the immobile phase.
    Type: Grant
    Filed: June 2, 2011
    Date of Patent: November 5, 2013
    Assignee: William Marsh Rice University
    Inventors: Andrew R. Barron, Samuel J. Maguire-Boyle, Alvin White Orbaek
  • Publication number: 20130277543
    Abstract: The present invention relates an Integral analysis method of inter-well tracer tests, which integrates and performs continuous feedback to each of the major stage (design, operation and interpretation) allowing quantitative interpretation of these tests. It is presented as a tool to investigate the behavior of injection fluids for recovery of hydrocarbons, as well as for the dynamic characterization of reservoirs. The main advantage of this invention is that it allows a greater certainty in the tracer response and a marked improvement in the sensitivity and quantitative analysis of the test results, since the curves fit both with mathematical models and numerical models. Another outstanding attraction of this invention is the reduction in the costs of testing such applications.
    Type: Application
    Filed: March 28, 2013
    Publication date: October 24, 2013
    Inventor: Instituto Mexicano Del Petroleo
  • Patent number: 8555967
    Abstract: Disclosed are spacer fluids and methods of use in subterranean formations. Embodiments may include use of consolidating spacer fluids in displacement of drilling fluids from a well bore annulus. Embodiments may include determining the boundary between a cement composition and a consolidating spacer fluid based on presence of tagging material in the well bore.
    Type: Grant
    Filed: April 26, 2013
    Date of Patent: October 15, 2013
    Assignee: Halliburton Energy Services, Inc.
    Inventors: Jiten Chatterji, Ronnie G. Morgan, Craig W. Roddy, James R. Benkley, D. Chad Brenneis
  • Publication number: 20130256522
    Abstract: A pulsed neutron generator includes a sealed tube. a gas reservoir is disposed in the sealed tube and includes an electrically heatable filament disposed within a porous, sintered getter. The getter includes dispersed particles of a thermally reversible hydride-adsorptive material therein. The dispersed particles have deuterium and/or tritium adsorbed on them. A gas ionizer disposed in the sealed tube. A target is disposed in the sealed tube. The target includes adsorbed deuterium and/or tritium therein.
    Type: Application
    Filed: March 28, 2012
    Publication date: October 3, 2013
    Inventors: Luke T. Perkins, Dylan Leber
  • Patent number: 8502135
    Abstract: A method for estimating a parameter of interest of an earth formation having a fluid contained in pores of the earth formation, the method includes: conveying a carrier through a borehole penetrating the earth formation; irradiating the earth formation with neutrons from a neutron source disposed at the carrier; measuring radiation emitted from the earth formation resulting from the irradiating using at least one detector; calculating or determining a mathematical parameter from radiation measured by the at least one detector; predicting values of the mathematical parameter over a range of values of an earth formation property; and comparing the mathematical parameter to the predicted values to estimate the parameter of interest.
    Type: Grant
    Filed: March 24, 2011
    Date of Patent: August 6, 2013
    Assignee: Baker Hughes Incorporated
    Inventors: David M. Chace, Rafay Z. Ansari, Feyzi Inanc, W. Allen Gilchrist, Jr., Elton Frost, Jr.
  • Publication number: 20130168543
    Abstract: A transport of plasmonic particles through a mineral formation is analyzed by flowing a plasmonic particles solution through an immobile phase (e.g., a mineral formation), determining an absorbance of the plasmonic particles solution subsequent to flowing the plasmonic particles solution through the immobile phase, comparing the determined absorbance of the plasmonic particles solution with an absorbance of the plasmonic particles solution determined previous to flowing the plasmonic particles solution through the immobile phase, and determining an absorbance of the plasmonic particles to the immobile phase as a function of the comparison. The plasmonic particles solution may be produced by dissolving or suspending plasmonic particles in a mobile phase. Flowing the plasmonic particles solution through the immobile phase may include injecting the plasmonic particles solution into the immobile phase, and then flushing the plasmonic particles solution through the immobile phase.
    Type: Application
    Filed: June 2, 2011
    Publication date: July 4, 2013
    Applicant: WILLIAM MARSH RICE UNIVERSITY
    Inventors: Andrew R. Barron, Samuel J. Maguire-Boyle, Alvin W. Orbaek
  • Patent number: 8470936
    Abstract: A liquid epoxy resin composition for semiconductor encapsulation comprising: (A) at least one epoxy resin, (B) at least one curing accelerator and (C) at least one acid anhydride terminated polyamic acid. The liquid epoxy resin composition provides a cured material that has an excellent adhesiveness to a semiconductor chip surface and has an excellent moisture resistance.
    Type: Grant
    Filed: July 29, 2011
    Date of Patent: June 25, 2013
    Assignee: Namics Corporation
    Inventors: Pawel Czubarow, Osamu Suzuki, Toshiyuki Sato, Kazuyoshi Yamada, Kaori Matsumura
  • Patent number: 8283173
    Abstract: This invention relates to a process utilizing natural carbon-13 isotope for identification of early breakthrough of injection water in oil wells. All natural water sources are labeled by unique ratios of carbon isotopes (13C/12C). Following the requirements of the invention, the carbon isotope ratio for oil bearing formation water and for local aquifer water which is to be injected in to the oil reservoir rock is determined. The carbon isotope ratio of the produced water from the selected oil wells is then monitored periodically. When the carbon isotope ratio of the produced (oil well) water shows deviation from the formation water value and tends towards injection water value, then the early breakthrough phenomenon of injection water is identified. Thus the contrast in natural carbon isotope ratios of injection water, formation water and produced water from selected oil wells serve as tracer in the identification of “Early Breakthrough” phenomenon of injection water and its movement.
    Type: Grant
    Filed: December 3, 2007
    Date of Patent: October 9, 2012
    Assignee: Council of Scientific & Industrial Research
    Inventors: Balbir Singh Sukhija, Dontireddy Venkat Reddy, Pasupuleti Nagabhushanam, Dattatrey Jaiwant Patil, Syed Hussain
  • Publication number: 20120175511
    Abstract: The present invention relates to novel methods for monitoring or tracing a job operation performed in a borehole, such as well boreholes traversing a geological formation. In one embodiment, the novel methods of the invention comprise the steps of: (a) disposing into the borehole a neutron absorber during the performance of the job operation; (b) logging the borehole with an instrument capable of measuring a neutron capture in and around the borehole after performance of the job operation; and (c) monitoring or tracing the job operation performed in the borehole by comparing the measured neutron capture with a baseline neutron capture in and around the borehole. The methods of the present invention pose small or no risk from a health safety and environment perspective and are useful for monitoring or tracing hydraulic fracturing, cementing operation in well boreholes, production logging or subsurface location of downhole collars, float shoes and other jewellery.
    Type: Application
    Filed: September 16, 2010
    Publication date: July 12, 2012
    Inventors: Robert Michael Masnyk, Hermann Kramer
  • Patent number: 8141633
    Abstract: In one general implementation, a method for identifying fluids in a wellbore includes generating light in a visible spectrum from a light source in a production wellbore; generating light in an ultraviolet spectrum from the light source in the production wellbore; receiving a first fluid in the production wellbore from a subterranean zone; receiving a second fluid in the production wellbore from the subterranean zone; capturing at least one image of a combined flow of the first fluid and the second fluid in at least one of the visible spectrum and the ultraviolet spectrum with an optical receiver in the production wellbore; and distinguishing, at least in part through the image, the first fluid from the second fluid in either or both the visible and ultraviolet spectrums.
    Type: Grant
    Filed: March 25, 2009
    Date of Patent: March 27, 2012
    Assignee: Occidental Chemical Corporation
    Inventors: David W. Hampton, Robert C. Kramm
  • Patent number: 8119737
    Abstract: Disclosed is an adhesive composition which includes (a) an epoxy resin, (b) a curing agent and (c) a polymer compound incompatible with said epoxy resin, and further optionally includes (d) a filler and/or (e) a curing accelerator. Also disclosed are a process for producing an adhesive composition, including mixing (a) the epoxy resin and (b) the curing agent with (d) the filler, followed by mixing the resultant mixture with (c) the polymer compound incompatible with the epoxy resin; an adhesive film including the above-mentioned adhesive composition formed into a film; a substrate for mounting a semiconductor including a wiring board and the above-mentioned adhesive film disposed thereon on its side where chips are to be mounted; and a semiconductor device which includes the above-mentioned adhesive film or the substrate for mounting a semiconductor.
    Type: Grant
    Filed: April 12, 2011
    Date of Patent: February 21, 2012
    Assignee: Hitachi Chemical Company, Ltd.
    Inventors: Teiichi Inada, Keiji Sumiya, Takeo Tomiyama, Tetsurou Iwakura, Hiroyuki Kawakami, Masao Suzuki, Takayuki Matsuzaki, Youichi Hosokawa, Keiichi Hatakeyama, Yasushi Shimada, Yuuko Tanaka, Hiroyuki Kuriya
  • Publication number: 20110239754
    Abstract: A technique facilitates detection of water incursion in a hydrocarbon well. Well equipment is positioned in a wellbore with one or more downhole components or regions comprising a tracer material. The tracer material is released in the presence of water to indicate incursion of water at a specific location along the wellbore. A sensor system is employed to detect the released tracer material.
    Type: Application
    Filed: March 31, 2010
    Publication date: October 6, 2011
    Applicant: SCHLUMBERGER TECHNOLOGY CORPORATION
    Inventors: Stephen Dyer, Carlos Abad, Bruno Drochon
  • Publication number: 20110215234
    Abstract: Downhole deployable tools for measuring tracer concentrations are disclosed. According to one embodiment, an apparatus comprises a support cable configured to allow the apparatus to be lowered into and raised from a wellbore. A housing is attached to the support cable. The housing includes a detector window on the exterior of the housing. A detector system within the housing includes a detector that measures tracer concentrations. The detector is operably connected to the detector window to direct energy or particles from the detector window to the detector.
    Type: Application
    Filed: March 4, 2011
    Publication date: September 8, 2011
    Inventor: Peter E. Rose
  • Patent number: 7947779
    Abstract: Disclosed is an adhesive composition which includes (a) an epoxy resin, (b) a curing agent and (c) a polymer compound incompatible with said epoxy resin, and further optionally includes (d) a filler and/or (e) a curing accelerator. Also disclosed are a process for producing an adhesive composition, including mixing (a) the epoxy resin and (b) the curing agent with (d) the filler, followed by mixing the resultant mixture with (c) the polymer compound incompatible with the epoxy resin; an adhesive film including the above-mentioned adhesive composition formed into a film; a substrate for mounting a semiconductor including a wiring board and the above-mentioned adhesive film disposed thereon on its side where chips are to be mounted; and a semiconductor device which includes the above-mentioned adhesive film or the substrate for mounting a semiconductor.
    Type: Grant
    Filed: October 7, 2010
    Date of Patent: May 24, 2011
    Assignee: Hitachi Chemical Company, Ltd.
    Inventors: Teiichi Inada, Keiji Sumiya, Takeo Tomiyama, Tetsurou Iwakura, Hiroyuki Kawakami, Masao Suzuki, Takayuki Matsuzaki, Youichi Hosokawa, Keiichi Hatakeyama, Yasushi Shimada, Yuuko Tanaka, Hiroyuki Kuriya
  • Publication number: 20100006750
    Abstract: A tracer system comprising a tracer compound for a fluid system, the tracer compound comprising one or more polyether alcohol compounds. The one or more polyether alcohol compounds is arranged for being placed in contact with a first part of said fluid system. The one or more polyether alcohol compounds is truly monodisperse. The polyether alcohol compounds comprises one or more functional groups. The one or more truly monodisperse polyether alcohol compounds is arranged for being detected in a second part of the fluid system in fluid communication with said first part of said fluid system. The tracer compound is detectable in very low concentrations.
    Type: Application
    Filed: July 10, 2009
    Publication date: January 14, 2010
    Inventors: Kolbjorn ZAHLSEN, Lars Kilaas
  • Publication number: 20090139713
    Abstract: The invention relates to methods and apparatus for determining a downhole parameter in an underbalanced drilling environment which include: selectively activating a first fluid flowing from the formation through a wellbore while under balanced drilled; detecting the activated first fluid, and determining a depth at which said fluid enters the wellbore.
    Type: Application
    Filed: August 28, 2008
    Publication date: June 4, 2009
    Inventors: John Edwards, Christian Stoller, Peter Wraight, Roger Griffiths, Nicolas Renoux
  • Patent number: 7432499
    Abstract: The invention relates to methods and apparatus for determining a downhole parameter in an underbalanced drilling environment which include: selectively activating a first fluid flowing from the formation through a wellbore while under balanced drilled; detecting the activated first fluid; and determining a depth at which said fluid enters the wellbore.
    Type: Grant
    Filed: March 3, 2004
    Date of Patent: October 7, 2008
    Assignee: Schlumberger Technology Corporation
    Inventors: John Edwards, Christian Stoller, Peter Wraight, Roger Griffiths, Nicolas Renoux
  • Patent number: 7339160
    Abstract: The invention concerns an apparatus for analysing water chemistry. According to the invention, the apparatus is adapted to operate downhole and comprises a colouring agent supply device for supplying a colouring agent to a water sample, the colour of the water sample thus supplied being indicative of the water sample chemistry, and a colorimetric analyser arranged to determine the colour of the water sample.
    Type: Grant
    Filed: November 19, 2003
    Date of Patent: March 4, 2008
    Assignee: Schlumberger Technology Corporation
    Inventors: Bhavani Raghuraman, Anthony Robert Holmes Goodwin, Oliver Clinton Mullins, Philip Andrew Rabbito, Li Jiang, Timothy Gareth John Jones, Andrew Loris Kurkjian, Gale Hyslip Gustavson
  • Patent number: 7028773
    Abstract: Water-based mud filtrate concentration in a downhole fluid sample drawn from the borehole of an oil well is assessed. To measure water-based mud filtrate concentration, a water-based mud having a water-soluble fluorescent dye tracer is pumped into the borehole; sample fluid from a selected downhole location is pumped through a downhole flow line having a window; sample fluid flowing in an excitation region of the downhole flow line is illuminated through the window with fluorescence excitation light; and fluorescence emission from the excitation region is measured to produce a measured value. The measured value represents the fraction of water-based mud filtrate in the sample fluid. A calibration value is determined representing 100% water-based mud filtrate. A method for validating a sample of connate water as having an acceptably low WBM filtrate contamination tests for validation downhole, in real time.
    Type: Grant
    Filed: December 13, 2002
    Date of Patent: April 18, 2006
    Assignee: Schlumberger Technology Coporation
    Inventors: Go Fujisawa, Oliver C. Mullins, Chengli Dong, Andrew Kurkjian
  • Patent number: 6955217
    Abstract: A method and apparatus for determining whether a tubing conveyed perforating (TCP) gun has fired by detecting a change in characteristics of the flow of an oil well. A method and apparatus detects the presence of fluorescent tracer dye to determine whether or not a TCP gun has fired. The method and apparatus detects a change is capacitance, or fiber optic electrical properties to determine whether or not a TCP gun has fired. The method and apparatus detects the number of charges fired to determine whether or not all TCP guns have fired and also provides a method and apparatus for determining the contributions of injection wells to producing wells by introducing fluorescent tracers into injection wells and detecting the presence of the fluorescent tracers at production wells. A method and apparatus is provided for placing fluorescent dye particles in a gravel pack to sense when a gravel pack is deteriorating by detecting the tracer dye particles in the well flow.
    Type: Grant
    Filed: May 16, 2003
    Date of Patent: October 18, 2005
    Assignee: Baker Hughes Incorporated
    Inventors: John Clark, Jamie Oag
  • Patent number: 6881953
    Abstract: The claimed method of tracing drains starts with a comprehensive building survey in which all existing drains are numbered. A Master Blueprint and a Master Spreadsheet are created using information collected in the building survey. A tracer is used to determine the flow of storm water to and from the building's storm drains. A test location, consisting of a storm manhole or a sanitary manhole is then chosen and water is run continuously through this manhole. A non-toxic fluorescent tracer is added to the target sanitary drain and a sample of the water running through the test location is withdrawn. A fluorometer is used to detect the fluorescent signal of non-toxic fluorescent tracer in the sample of water withdrawn. This procedure is repeated until all test locations have been surveyed and the information recorded on the Master Blueprint and Master Spreadsheet. The information is used to replumb drains.
    Type: Grant
    Filed: September 28, 2001
    Date of Patent: April 19, 2005
    Assignee: Nalco Company
    Inventors: Michael J. Weiland, John E. Hoots
  • Patent number: 6670605
    Abstract: Disclosed is a formation fluid analysis module which utilizes a down-hole mass spectrometer to determine the molecular constituents of formation fluids, as distinguished from drilling contaminants, and to provide information about the physical and chemical properties of the sample.
    Type: Grant
    Filed: February 25, 2000
    Date of Patent: December 30, 2003
    Assignee: Halliburton Energy Services, Inc.
    Inventors: Bruce H. Storm, Jr., David P. Fries
  • Patent number: 6596998
    Abstract: A method for determining which of a plurality of detectors transmitted a signal, such as a signal related to neutron or gamma emissions, includes connecting each of the detectors to a single cable, such as an environmentally rugged cable. Signals are transmitted from each of the detectors over the single cable. The two ends of the cable are connected to two receivers. A different unique delay is introduced between receipt by the two receivers of a signal over the cable for each of the detectors. The receivers, which have a preamplifier, an amplifier and a discriminator, receive the signals from the two ends of the cable. A timing analyzer, such as a time-to-amplitude converter, measures a delay between one signal from one end and the other signal from the other end of the cable. A processor employs the amplitude of the signal output by the timing analyzer.
    Type: Grant
    Filed: July 31, 2000
    Date of Patent: July 22, 2003
    Assignee: Westinghouse Electric Company LLC
    Inventor: George G. Siedel
  • Patent number: 6564866
    Abstract: A method and apparatus detects the presence of a fluorescent tracer dye, a change in capacitance, or a change in fiber optic electrical properties to determine whether or not a TCP gun has fired. The method and apparatus detects the number of charges fired to determine whether or not all TCP guns have fired and also determines the contributions of injection wells to producing wells by introducing fluorescent tracers into injection wells and detecting the presence of the fluorescent tracers at production wells. The invention places fluorescent dye particles in a gravel pack to sense when a gravel pack is deteriorating by detecting the tracer dye particles in the well flow.
    Type: Grant
    Filed: December 27, 2000
    Date of Patent: May 20, 2003
    Assignee: Baker Hughes Incorporated
    Inventors: John Clark, Jamie Oag
  • Patent number: 6344331
    Abstract: A biphase immunoassay method is provided in which a water immiscible liquid is qualitatively or quantitatively measured by mixing a sample of the water immiscible liquid with an aqueous solution containing a specific binding partner of the analyte. Binding occurs at or across the interface between the respective liquids and the degree of association of the analyte with its binding partner is dependent upon the concentration ratio rather than absolute quantities. The degree of association may be determined and used to determine the presence and/or concentration of analyte in the sample.
    Type: Grant
    Filed: October 23, 1998
    Date of Patent: February 5, 2002
    Assignee: Molecular Light Technology Research Limited
    Inventors: Raymond Lathan Ball, Jeremy Paul Aston, Jennifer Cryer, Ian Weeks
  • Patent number: 5929437
    Abstract: Radioactive particles are provided for use in tracing the flow path in or near a well of fluids injected into the well. The particles include an element which can be made radioactive by bombardment with neutrons and a material to encapsulate the element. The encapsulant is preferably an organic polymer having a high softening temperature. The particles may be injected into a well in treating fluids and their location may be later determined by gamma ray logging of the well.
    Type: Grant
    Filed: May 20, 1997
    Date of Patent: July 27, 1999
    Assignee: Protechnics International, Inc.
    Inventors: Douglas W. Elliott, David L. Holcomb
  • Patent number: 5879946
    Abstract: A method for allowing authentification of a bulk liquid e.g. petrol or another mineral oil based product, comprises introducing into the liquid a small amount of a chemiluminescent substance. Samples for authentification are subjected to the conditions required to trigger the chemiluminescent reaction and monitored for chemiluminescent emission.
    Type: Grant
    Filed: April 28, 1997
    Date of Patent: March 9, 1999
    Assignee: Molecular Light Technology Limited
    Inventors: Ian Weeks, Sian Aerona Herbert
  • Patent number: 5783822
    Abstract: The present invention provides improved traceable well cement compositions and methods. The compositions are basically comprised of hydraulic cement, sufficient water to form a pumpable slurry and a normally non-radioactive tracer compound which becomes radioactive and emits detectible rays over a relatively short time period when exposed to neutrons. The methods of the invention relate to cementing a zone in a well and subsequently detecting the subterranean location of the cement composition therein. A traceable well cement composition of the invention is formed and introduced into a subterranean zone to be cemented. Neutrons are then emitted from a source in the well so that the tracer compound emits detectible rays, the rays are detected and the location of the cement composition in the well is determined.
    Type: Grant
    Filed: May 16, 1997
    Date of Patent: July 21, 1998
    Assignee: Halliburton Energy Services, Inc.
    Inventors: Ronnie J. Buchanan, Jiten Chatterji, James F. Heathman
  • Patent number: 5572021
    Abstract: Methods are provided for detecting the surface and/or subterranean locations of well treating fluids after the treating fluids have been introduced into wells and used for performing treatments therein. The methods of determining the subterranean locations of treating fluids basically comprise introducing a treating fluid into a well having a non-hazardous thermal neutron absorbing material combined therewith and performing a treatment in the well with the fluid. Fast neutrons from a source thereof are emitted in the well after the treatment whereby they interact with elements in the well and are thermalized. The thermal neutrons backscattered in the well are detected, and a count representing the detected thermal neutrons is generated. The subterranean locations of the treating fluid are determined by comparing the thermal neutron counts in the well before and after placement of the thermal neutron absorbing treating fluid therein.
    Type: Grant
    Filed: May 1, 1995
    Date of Patent: November 5, 1996
    Assignee: Halliburton Company
    Inventors: James F. Heathman, Robert F. Shelley, Jiten Chatterji