Composition Analysis Patents (Class 250/390.04)
  • Patent number: 7501624
    Abstract: A system for producing beams of high energy photons and neutrons and a method to use such beams to actively interrogate and detect concealed nuclear materials, radiological materials, and chemical explosives.
    Type: Grant
    Filed: June 11, 2007
    Date of Patent: March 10, 2009
    Assignee: Brookhaven Technology Group, Inc.
    Inventors: J. Paul Farrell, Vadim Dudnikov
  • Patent number: 7430479
    Abstract: The system and method provide security and cargo handling personnel a versatile tool to rapidly check cargo for hidden radiological materials, explosives, drugs, and chemical weapons material. Gamma ray emission is stimulated by a pulsed neutron source. The gamma ray signature is used to classify the material. Passive gamma ray analysis can be used to detect and identify radiological material. The method of determining the contents of a target includes irradiating a target; detecting at least one spectrum emitted from the target; performing a primary analysis to extract a first set of indicators; and performing a secondary analysis to decide the contents of the target. The primary analysis utilizes either a least squares analysis or principal component analysis. The secondary analysis utilizes a generalized likelihood ratio test or support vector machines.
    Type: Grant
    Filed: August 1, 2005
    Date of Patent: September 30, 2008
    Assignee: Science Applications International Corporation
    Inventors: Daniel Holslin, Giancarlo Borgonovi
  • Patent number: 7423273
    Abstract: In accordance with an embodiment, a method of examining contents of an object is disclosed comprising conducting a first examination of an object, checking for the presence of delayed neutrons if the first examination indicates that suspect material is present, and determining whether the object contains nuclear material based, at least in part, on the check. The first examination may comprise a manual examination and scanning of the object to form an image, for example. The first examination may also comprise scanning of the object at two different radiation energies, calculating a function of the energy detected at the two radiation energies, and determining whether the object at least potentially contains suspect material based, at least in part, on the comparison. Systems are also disclosed.
    Type: Grant
    Filed: February 28, 2005
    Date of Patent: September 9, 2008
    Assignee: Varian Medical Systems Technologies, Inc.
    Inventors: James E. Clayton, Paul Bjorkholm
  • Patent number: 7405409
    Abstract: A neutron elastic scattering detector device for non-invasively detecting the presence of at least one predetermined element of an object of interest. The detector device comprises a neutron source that simultaneously outputs, at a creation time, a neutron in a first direction and an associated baseline particle in a second direction. The first direction is opposite of the second direction. The neutron can impinge upon the predetermined element of the object of interest and scatter therefrom in a third direction. A baseline particle detector system detects the baseline particle and outputs a baseline signal characteristic thereof. A neutron detector system detects the neutron and outputs a scattering signal in characteristic thereof. The processing unit analyzes the baseline signal and the scattering signal to determine the presence of the predetermined element.
    Type: Grant
    Filed: February 17, 2006
    Date of Patent: July 29, 2008
    Assignee: The Regents of the University of Michigan
    Inventor: Kimberlee Jane Kearfott
  • Publication number: 20080175351
    Abstract: A method and a system for detecting the presence of special nuclear materials in a suspect container. The system and its method include irradiating the suspect container with a beam of neutrons, so as to induce a thermal fission in a portion of the special nuclear materials, detecting the gamma rays that are emitted from the fission products formed by the thermal fission, to produce a detector signal, comparing the detector signal with a threshold value to form a comparison, and detecting the presence of the special nuclear materials using the comparison.
    Type: Application
    Filed: October 12, 2007
    Publication date: July 24, 2008
    Applicant: THE REGENTS OF THE UNIVERSITY OF CALIFORNIA
    Inventors: Eric B. Norman, Stanley G. Prussin
  • Patent number: 7399976
    Abstract: Disclosed is a method of discriminating materials by employing fast neutron and continuous spectral X-ray and an equipment for the same. The method comprising the steps of: (a) transmitting a fast neutron beam produced by a fast neutron source and a continuous spectral X-ray beam produced by a continuous spectral X-ray source through inspected objects; (b) directly measuring the intensity of the transmitted X-rays and the intensity of the transmitted neutrons by a X-ray detector array and a neutron detector array respectively; and (c) identifying the materials of the inspected object by Z-dependency curves formed by the attenuation differences between the neutron beam and X-ray beam transmitted through different materials of the inspected object. This direct measurement of transmitted dual-ray technique has much more efficient than secondary radiations measurement such as neutron activation analysis, has much more material discrimination sensitivity than dual-energy x-ray technique.
    Type: Grant
    Filed: February 14, 2006
    Date of Patent: July 15, 2008
    Assignees: Tsinghua University, Nuctech Company Limited
    Inventors: Kejun Kang, Haifeng Hu, Yali Xie, Qitian Miao, Yigang Yang, Yuanjing Li, Zhiqiang Chen, Xuewu Wang
  • Publication number: 20080156997
    Abstract: A neutron elastic scattering detector device for non-invasively detecting the presence of at least one predetermined element of an object of interest. The detector device comprises a neutron source that simultaneously outputs, at a creation time, a neutron in a first direction and an associated baseline particle in a second direction. The first direction is opposite of the second direction. The neutron can impinge upon the predetermined element of the object of interest and scatter therefrom in a third direction. A baseline particle detector system detects the baseline particle and outputs a baseline signal characteristic thereof. A neutron detector system detects the neutron and outputs a scattering signal in characteristic thereof. The processing unit analyzes the baseline signal and the scattering signal to determine the presence of the predetermined element.
    Type: Application
    Filed: February 17, 2006
    Publication date: July 3, 2008
    Inventor: Kimberlee Jane Kearfott
  • Patent number: 7391031
    Abstract: A system for detecting a compound in a sample includes a neutron source, at least one gamma ray detector positioned proximate the sample, and a signal processor. The neutron source directs a neutron beam toward the sample. The gamma ray detector collects gamma rays emitted from the sample and the signal processor determines the compounds in the sample based on the gamma rays collected by the gamma ray detector. The compound is selected from the group consisting of peroxides and superoxides.
    Type: Grant
    Filed: December 19, 2006
    Date of Patent: June 24, 2008
    Assignee: Pratt & Whitney Rocketdyne, Inc.
    Inventors: Andrew J. Zillmer, Gregory A. Johnson
  • Publication number: 20080142722
    Abstract: A system for detecting a compound in a sample includes a neutron source, at least one gamma ray detector positioned proximate the sample, and a signal processor. The neutron source directs a neutron beam toward the sample. The gamma ray detector collects gamma rays emitted from the sample and the signal processor determines the compounds in the sample based on the gamma rays collected by the gamma ray detector. The compound is selected from the group consisting of peroxides and superoxides.
    Type: Application
    Filed: December 19, 2006
    Publication date: June 19, 2008
    Applicant: Pratt & Whitney Rocketdyne, Inc.
    Inventors: Andrew J. Zillmer, Gregory A. Johnson
  • Patent number: 7359480
    Abstract: A system for inspecting cargo for the presence of special nuclear material. The cargo is irradiated with neutrons. The neutrons produce fission products in the special nuclear material which generate gamma rays. The gamma rays are detecting indicating the presence of the special nuclear material.
    Type: Grant
    Filed: May 3, 2004
    Date of Patent: April 15, 2008
    Assignee: Lawrence Livermore National Security, LLC
    Inventors: Dennis R. Slaughter, Bertram A. Pohl, Arden D. Dougan, Adam Bernstein, Stanley G. Prussin, Eric B. Norman
  • Publication number: 20080017806
    Abstract: Apparatus and methods for effectively detecting and locating explosive substances within remote targets, including improvised explosive devices (IEDs). The detection apparatus includes a thermal neutron beam generator, a gamma ray detector, data collection modules and sensors, and a detection processing module. The thermal neutron beam generator includes a fast neutron source, a neutron moderator to slow the fast neutrons to thermal neutrons, and a rotatable neutron shield enclosing the generated thermal neutrons. The neutron shield has an aperture to form a thermal neutron beam directed at a remote target. If the remote target contains explosive substances, gamma rays radiate isotropically from the remote target when it is bombarded by the thermal neutrons. A portion of these gamma rays are intercepted and detected by the gamma ray detector, which is spaced apart from the thermal neutron source in order to minimize the neutron-irradiated air path seen by the detector, thereby reducing background noise.
    Type: Application
    Filed: July 18, 2006
    Publication date: January 24, 2008
    Inventor: Wayne B. Norris
  • Patent number: 7253414
    Abstract: Methods and apparatus for continuous real-time measurement of bulk material using gamma irradiation. A multi-energy gamma attenuation device monitors bulk material flow and produces a spectrum that is compared to a baseline spectrum to produce a relative weight/impurity/component ratio. A sample analysis, in combination with measurement of the relative weight/impurity/component ratio of the sample, allows for determination of the coefficients for determining the absolute weight/impurity/component values of the bulk material.
    Type: Grant
    Filed: June 24, 2004
    Date of Patent: August 7, 2007
    Assignee: Energy Technologies, Inc.
    Inventors: Peter M. Osucha, David K. Swindell, Jack R. Lee
  • Patent number: 7214948
    Abstract: A high measuring resolution along with a large irradiation surface and a high beam intensity are required for structural analysis of material according to the small angle neutron scattering measuring technique. However, with known diaphragm collimators, the necessary beam divergence cannot be reached without an unacceptable loss of intensity. The inventive neutron optical component (1) comprises a plurality of successively arranged pinhole diaphragms embodied as grating diaphragms (7), each grating diaphragm (7) comprising a plurality of diaphragm apertures (14). In this way, the neutron beam is divided into individual beams which are each improved in terms of the convergence thereof. Furthermore, the channels defined by the course of the grating diaphragms (7) by means of respectively identically positioned diaphragm apertures (14) are narrowed according to the convergence cone provided by the structure of the measuring instrument.
    Type: Grant
    Filed: August 25, 2003
    Date of Patent: May 8, 2007
    Assignee: Hahn-Meitner-Institut Berlin GmbH.
    Inventors: Ferenc Mezei, Daniel Clemens, Lounis Mokrani
  • Patent number: 7151447
    Abstract: A method for identifying at least one threat to the homeland security. Each threat is either hidden inside at least one cargo container before transit, or is placed inside at least one cargo container while in transit. Each threat while interacting with its surrounding generates a unique threat signature. The method comprises the following steps: (A) detecting at least one threat signature; and (B) processing each detected threat signature to determine a likelihood of at least one threat to become a threat to the homeland security.
    Type: Grant
    Filed: August 31, 2004
    Date of Patent: December 19, 2006
    Assignee: Erudite Holding LLC
    Inventors: Paul H. Willms, James H. Stanley
  • Patent number: 7061604
    Abstract: A structural member of a mortar projectile is inspected. The structural member is a composite structure having a thermoplastic matrix with a filler of steel balls. The composite structure has a central cavity into which is placed a strobe light. Surrounding the composite structure is a detection arrangement having a detection medium of photographic film. When the strobe light is activated the film is exposed and developed to obtain an image indicative of the distribution of the steel balls in the matrix. The image is analyzed to determine if the structural member is acceptable.
    Type: Grant
    Filed: February 11, 2004
    Date of Patent: June 13, 2006
    Assignee: The United States of America as represented by the Secretary of the Army
    Inventors: Robert Charles Beam, John B. Niles, Drew Diedalis
  • Patent number: 6720552
    Abstract: A magnet for use with a neutron scattering apparatus. The neutron scattering apparatus provides an incident beam of neutrons to a sample under analysis. The magnet has first and second body portions of high conductivity material and has a mid-plane portion there between in which the sample under analysis is positioned. The first and second body portions of the coil are electrically connected to each other via the mid-plane portion of the coil between the body portions of the coil. The conductive mid-plane portion has a split that allows neutron scattering through large angles.
    Type: Grant
    Filed: October 17, 2002
    Date of Patent: April 13, 2004
    Assignee: FSU Research Foundation, Inc.
    Inventors: Mark D. Bird, Iain R. Dixon, Yehia Eyssa, Andrei Gavrilin, Scott Gundluch
  • Patent number: 6707047
    Abstract: A non-destructive method for quantifying the hydrogen content or a hydrogen-bearing constituent in a material is based on the principle of moderating neutron spectroscopy. This technique is particularly suited for analyzing materials containing the high scattering/capture cross-section element of hydrogen. The method involves exposing a neutron moderator to a beam of radiation comprising neutrons and measuring thermal neutron intensities at a plurality of locations in the moderator. These measured intensities reflect the energy distribution of the beam of radiation incident upon the moderator. Thus, by measuring these intensities with the material present, and comparing these intensities to a model, to those of a composition standard(s), or combinations thereof, the hydrogen content of the material is quantified. Furthermore, the hydrogen-bearing constituent of the material is quantified by knowing or estimating the chemical or molecular structure of the material.
    Type: Grant
    Filed: April 17, 2003
    Date of Patent: March 16, 2004
    Assignee: Battelle Memorial Institute
    Inventors: Richard A. Craig, Mary Bliss
  • Patent number: 6693281
    Abstract: Methods and apparatus involving neutron resonance radiography are used to map the elemental composition of an object. Sets of neutrons having energies within particular energy bands are directed through an object to be imaged. The attenuation of the neutrons passed through the object is detected, and that data can be used to detect explosives, weapons, drugs and other contraband.
    Type: Grant
    Filed: December 31, 2001
    Date of Patent: February 17, 2004
    Assignee: Massachusetts Institute of Technology
    Inventors: Gongyin Chen, Richard C. Lanza
  • Publication number: 20030178573
    Abstract: A non-destructive method for quantifying the hydrogen content or a hydrogen-bearing constituent in a material is disclosed. The method is based on the principle of moderating neutron spectroscopy which is particularly suited for analyzing materials containing the high scattering/capture cross-section element of hydrogen. The method comprises the steps of exposing a neutron moderator to a beam of radiation comprising neutrons and measuring thermal neutron intensities at a plurality of locations in the moderator. These measured intensities reflect the energy distribution of the beam of radiation incident upon the moderator. Thus, by measuring these intensities with the material present, and comparing these intensities to a model, to those of a composition standard(s), or combinations thereof, the hydrogen content of the material is quantified. Furthermore, the hydrogen-bearing constituent of the material is quantified by knowing or estimating the chemical or molecular structure of the material.
    Type: Application
    Filed: April 17, 2003
    Publication date: September 25, 2003
    Inventors: Richard A. Craig, Mary Bliss
  • Patent number: 6603122
    Abstract: A neutron detection system for detection of contaminants contained within a bulk material during recycling includes at least one neutron generator for neutron bombardment of the bulk material, and at least one gamma ray detector for detection of gamma rays emitted by contaminants within the bulk material. A structure for analyzing gamma ray data is communicably connected to the gamma ray detector, the structure for analyzing gamma ray data adapted. The identity and concentration of contaminants in a bulk material can also be determined. By scanning the neutron beam, discrete locations within the bulk material having contaminants can be identified.
    Type: Grant
    Filed: May 24, 2001
    Date of Patent: August 5, 2003
    Assignee: UT-Battelle, LLC
    Inventor: Rusi Taleyarkhan
  • Publication number: 20030127590
    Abstract: A magnet for use with a neutron scattering apparatus. The neutron scattering apparatus provides an incident beam of neutrons to a sample under analysis. The magnet has first and second body portions of high conductivity material and has a mid-plane portion there between in which the sample under analysis is positioned. The first and second body portions of the coil are electrically connected to each other via the mid-plane portion of the coil between the body portions of the coil. The conductive mid-plane portion has a split that allows neutron scattering through large angles.
    Type: Application
    Filed: October 17, 2002
    Publication date: July 10, 2003
    Applicant: FSU Research Foundation, Inc.
    Inventors: Mark D. Bird, Iain R. Dixon, Yehia Eyssa, Andrei Gavrilin, Scott Gundluch
  • Patent number: 6580079
    Abstract: A non-destructive method for quantifying the hydrogen content or a hydrogen-bearing constituent in a material. Moderating neutron spectroscopy is particularly suited for analyzing materials containing the high scattering/capture cross-section element of hydrogen. A neutron moderator is exposed to a beam of neutron radiation and the thermal neutron intensities at a number of locations in the moderator are then measured. The measured intensities reflect the energy distribution of the radiation beam incident upon the moderator. By measuring intensities with the material present and comparing the intensities to a model, or to those of a composition standard(s), the hydrogen content of the material is quantified. The hydrogen-bearing constituent of the material may be further quantified by knowing or estimating the chemical or molecular structure of the material.
    Type: Grant
    Filed: September 6, 2000
    Date of Patent: June 17, 2003
    Assignee: Battelle Memorial Institute
    Inventors: Richard A. Craig, Mary Bliss
  • Patent number: 6563898
    Abstract: The present invention relates to a method and portable apparatus which is used to detect substances, such as explosives and drugs, by neutron irradiation. The apparatus has a portable neutron generating probe and corresponding controllers and data collection computers. The probe emits neutrons in order to interrogate an object. The probe also contains gamma ray detectors for the collection of gamma rays from fast neutron, thermal neutron and neutron activation reactions. Data collected from these detectors is sent to the computer for data de-convolution then object identification in order to determine whether the object being interrogated contains explosives or illicit contraband.
    Type: Grant
    Filed: September 30, 1999
    Date of Patent: May 13, 2003
    Assignee: Western Kentucky University
    Inventors: George Vourvopoulos, Sandor Sudar
  • Publication number: 20020171042
    Abstract: Methods and apparatus involving neutron resonance radiography are used to map the elemental composition of an object. Sets of neutrons having energies within particular energy bands are directed through an object to be imaged. The attenuation of the neutrons passed through the object is detected, and that data can be used to detect explosives, weapons, drugs and other contraband.
    Type: Application
    Filed: December 31, 2001
    Publication date: November 21, 2002
    Inventors: Gongyin Chen, Richard C. Lanza
  • Patent number: 6388260
    Abstract: Crystals of lithium tetraborate or alpha-barium borate had been found to be neutron detecting materials. The crystals are prepared using known crystal growing techniques, wherein the process does not include the common practice of using a fluxing agent, such as sodium oxide or sodium fluoride, to reduce the melting temperature of the crystalline compound. Crystals prepared by this method can be sliced into thin single or polycrystalline wafers, or ground to a powder and prepared as a sintered compact or a print paste, and then configured with appropriate electronic hardware, in order to function as neutron detectors.
    Type: Grant
    Filed: March 6, 2000
    Date of Patent: May 14, 2002
    Assignee: Sandia Corporation
    Inventors: F. Patrick Doty, Ilya Zwieback, Warren Ruderman
  • Patent number: 6314152
    Abstract: A technique for determining percent body fat using neutron inelastic scattering is disclosed. It relies on a correlation between a carbon-oxygen ratio in the body and the percent body fat with corrections made for a level of patient hydration in the lean tissue. The animal body is irradiated with neutrons having sufficient energy to inelastically scatter off carbon and oxygen. The resulting gamma rays are detected and counted, and the level of hydration is measured. The ratio of the detected gamma rays and hydration are then related to a proportion of fat in the animal body. This technique provides accuracy approaching that achieved with hydrodensitometry with only small radiation doses between 5 and 20 millirem, but without any requirements for immersion.
    Type: Grant
    Filed: September 16, 1997
    Date of Patent: November 6, 2001
    Assignee: Trustees of Tufts College
    Inventor: Joseph J. Kehayias
  • Patent number: 6205195
    Abstract: This invention provides coded aperture imaging apparatus and methods for the detection and imaging of radiation which results from nuclear interrogation of a target object. The apparatus includes: 1) a radiation detector for detecting at least a portion of the radiation emitted by the object in response to nuclear excitation and for producing detection signals responsive to the radiation; 2) a coded aperture disposed between the detector and the object such that emitted radiation is detected by the detector after passage through the coded aperture; and 3) a data processor for characterizing the object based upon the detection signals from the detector and upon the configuration of the coded aperture.
    Type: Grant
    Filed: February 26, 1999
    Date of Patent: March 20, 2001
    Assignee: Massachusetts Institute of Technology
    Inventor: Richard C. Lanza