Simultaneously Burning, Vaporizing, Or Melting Of Embedded Element Or Core To Form Nonrandom Void Patents (Class 264/610)
  • Patent number: 7556755
    Abstract: A process for producing a ceramic molding having a three-dimensional network structure with a plurality of spherical cells and a plurality of through holes present in dividing walls between the spherical cells, includes: a step of obtaining an aggregate of coated particles in which a plurality of ceramic particles are attached to the surface of spherical synthetic resin particles; a step of arranging the aggregate of coated particles in closest packed form within a mold; a step of filling gaps in the aggregate of coated particles with a ceramic so as to give a shaped product; a step of releasing the shaped product from the mold; a step of thermally decomposing the spherical synthetic resin particles of the shaped product so as to form the spherical cells and form the plurality of through holes in dividing wall-forming sections that are present between adjacent spherical cells; and a step of sintering the ceramic particles and the ceramic so as to form the dividing walls.
    Type: Grant
    Filed: November 15, 2004
    Date of Patent: July 7, 2009
    Assignee: Honda Motor Co., Ltd.
    Inventors: Kazuo Shibata, Tadashi Ohya, Tsuyoshi Tanaka
  • Patent number: 7494557
    Abstract: A method of using sacrificial materials for fabricating internal cavities and channels in laminated dielectric structures, which can be used as dielectric substrates and package mounts for microelectronic and microfluidic devices. A sacrificial mandrel is placed in-between two or more sheets of a deformable dielectric material (e.g., unfired LTCC glass/ceramic dielectric), wherein the sacrificial mandrel is not inserted into a cutout made in any of the sheets. The stack of sheets is laminated together, which deforms the sheet or sheets around the sacrificial mandrel. After lamination, the mandrel is removed, (e.g., during LTCC burnout), thereby creating a hollow internal cavity in the monolithic ceramic structure.
    Type: Grant
    Filed: January 30, 2004
    Date of Patent: February 24, 2009
    Assignee: Sandia Corporation
    Inventor: Kenneth A. Peterson
  • Publication number: 20090035558
    Abstract: The sintered ceramic product comprises a granular material bound by a nitrogenous mold. According to the invention, at least one anti-dust agent selected among calcium and boron exists in a surface layer of the product, the mass ratio of all the anti-dust agents in the surface layer being greater than that measured underneath this layer. This product advantageously has a reduced ratio of non-adherent particles to its surface.
    Type: Application
    Filed: October 27, 2006
    Publication date: February 5, 2009
    Applicant: Saint-Gobain Centre De Recherches ET D'Etudes Europeen
    Inventors: Eric Jorge, Frederic Roulet, Jacques Schoennahl
  • Patent number: 7371299
    Abstract: A set of resin sheets includes a plurality of resin sheets. Each resin sheet is disposed in a site to be a surface recess or inner void in a ceramic green sheet to be laminated, and a plurality of such ceramic green sheets each with the resin sheet disposed therein are laminated and fired, whereupon the resin sheets are removed by thermal decomposition during the firing. In the set of resin sheets, the relation of Ta<Tb?Tc is satisfied wherein Ta (° C.) indicates an 80% weight reduction temperature of an uppermost resin sheet, Tb (° C.) indicates an 80% weight reduction temperature of a lowermost resin sheet, and Tc (° C.) indicates a 20% weight reduction temperature of a resin binder which is contained in the ceramic green sheets in which the green sheets are disposed.
    Type: Grant
    Filed: May 26, 2005
    Date of Patent: May 13, 2008
    Assignee: Kyocera Corporation
    Inventors: Hiroyuki Takase, Shinichi Suzuki, Yuuji Tanaka
  • Patent number: 7357976
    Abstract: The ceramic molded body of the present invention includes spherical cells of a spherical bubble plurally formed therein: in the ceramic molded body the spherical cells neighboring each other are communicated through communication porosities and form a three-dimensional network structure, and a ratio (Md/MD) of a median (Md) of inner diameters of the communication porosities to a median (MD) of inner diameters of the spherical cells is less than 0.5. In the ceramic molded body used for manufacturing a metal matrix composite, a metal is filled within the spherical cells and the communication porosities.
    Type: Grant
    Filed: April 15, 2005
    Date of Patent: April 15, 2008
    Assignee: Honda Motor Co., Ltd.
    Inventors: Satoshi Yamamura, Kazuo Shibata, Tadashi Ohya
  • Patent number: 7351364
    Abstract: A method of manufacturing a hybrid structure (100) having a layer of CMC material (28) defining an interior passageway (24) and a layer of ceramic insulating material (18) lining the passageway. The method includes the step of casting the insulating material to a first thickness required for effective casting but in excess of a desired second thickness for use of the hybrid structure. An inner mold (14) defining a net shape desired for the passageway remains in place after the casting step to mechanically support the insulating material during a machining process used to reduce the thickness of the insulating material from the as-cast first thickness to the desired second thickness. The inner mold also provides support as the CMC material is deposited onto the insulating material. The inner mold may include a fugitive material portion (20) to facilitate its removal after the CMC material is formed.
    Type: Grant
    Filed: January 29, 2004
    Date of Patent: April 1, 2008
    Assignee: Siemens Power Generation, Inc.
    Inventors: Jay A. Morrison, Gary B. Merrill, Steven James Vance, Michael A. Burke
  • Patent number: 7323133
    Abstract: A method for producing ceramic micromanufactured items comprises the following stages: a starting material constituting at least a micromanufactured item (1) is prepared and used to from the micromanufactured item (1); said starting material includes at least a pre-ceramic polymer, and the method further comprises a stage in which the inner structure of the starting material is modified, said structure being turned from a polymeric structure to a ceramic structure after the forming stage of said micromanufactured item (1).
    Type: Grant
    Filed: May 13, 2002
    Date of Patent: January 29, 2008
    Assignee: Gimac DI Maccagnan Giorgio
    Inventors: Giorgio Maccagnan, Paolo Colombo
  • Publication number: 20080006970
    Abstract: Various embodiments of polymer fibers comprising a high heat polymer and process for making the polymer fibers are provided. In one embodiment, synthetic polymer fibers comprise polyetherimide polymer that is substantially free of foreign particulate matter greater than about 100 microns in size. A process for producing polymer fiber includes melting polymer comprising polyetherimide to a melt temperature that ranges from about 180-500° C. to form a molten polymer; passing the polyetherimide that is substantially free of foreign particulate matter above about 100 microns in size, through a spinneret comprising a plurality of hole openings to produce a fiber bundle; and cooling the fiber bundle with a cooling medium having a temperature that ranges from about 0° C. to about 80° C.
    Type: Application
    Filed: July 10, 2006
    Publication date: January 10, 2008
    Applicant: General Electric Company
    Inventors: Irene Dris, Anne Marie Lak, Craig Wojcicki
  • Patent number: 7303704
    Abstract: The present invention discloses a method of manufacturing lightweight ceramics by mixing several raw materials such as a powdered glass material, a powdered alkali silicate, and a water-soluble polymer in a certain proportion to form a dry substrate, and then adding water to mold the substrate into a desired shape; after the water in the substrate is baked dry, heat the substrate until the ceramic is formed. The oxide and hydroxide in the alkali silicate are used to lower the softening point of the powdered glass material, and when the powdered glass material is in the semi fluid state, the air and crystal water brought by the alkali silicate will expand and form air bubbles due to the high temperature.
    Type: Grant
    Filed: March 17, 2003
    Date of Patent: December 4, 2007
    Inventors: Cheng-Tsung Chang, Ming-Kun Liu
  • Patent number: 7290586
    Abstract: A ceramic foam having pores in the range of 20 to 800 microns and 10 to 30 % of theoretical density is placed in a preheated mould and molten metal or plastics is drawn in to form a bicomposite structure.
    Type: Grant
    Filed: August 22, 2001
    Date of Patent: November 6, 2007
    Assignee: Dytech Corporation Limited
    Inventor: Rodney Martin Sambrook
  • Patent number: 7276202
    Abstract: The present invention forms screw-like projection at the entrance of ceramic bottle and enables air-tightening with plastic cork, formed with screw-like projection in its body. It guarantees air tightening of ceramic bottle, and does not use imported cork, which decreases the need to import. Moreover, increases productivity by automating the air-tightening process of plastic cork. The present invention can reduce cost of production, at the same time, increasing productivity, and it can be re-used multiple times after the air-tightening.
    Type: Grant
    Filed: April 8, 2003
    Date of Patent: October 2, 2007
    Inventor: Kwang-Ho Choi
  • Patent number: 7163653
    Abstract: The invention relates to a method for producing ceramic brake disks from a green body consisting of a sheet molding compound (SMC) having reinforcing fibers, and the ensuing pyrolysis and melt infiltration. The aim of the invention is to create a single-element green body comprising very complex inner cavities after pyrolysis. In order to achieve this, the method comprises the following steps: the green body (1) is produced from a sandwich consisting of SMC (2), a thermoplastic insert (4), and SMC (2) in one working step in a tool (5a, 5b), subjected to pressure and temperature; and the insert (4) fills the green body (1) over its entire surface and comprises openings (6) which are arranged in such a way that the upper and lower SMC layers (2) are interconnected, at least in parts.
    Type: Grant
    Filed: September 20, 2001
    Date of Patent: January 16, 2007
    Assignee: Menzolit Fibron GmbH
    Inventor: Gerd Ehnert
  • Patent number: 7141203
    Abstract: The present invention provides an all-ceramic diffuser assembly that includes a diffuser element formed of a porous ceramic material and a base formed of a non-porous ceramic material. The base includes a peripheral undercut shoulder portion that overlaps a perimeter edge of the diffuser element to sealingly connect the diffuser element to the base. A conduit is formed in a fitting portion of the base for directing a stream of gas or liquid that is capable of diffusing through the diffuser element into a chamber formed between an inner surface of the diffuser element and a floor portion of the base. The present invention also provides a method of forming the diffuser assembly.
    Type: Grant
    Filed: July 7, 2004
    Date of Patent: November 28, 2006
    Assignee: Filtros, Ltd.
    Inventors: Philip S. Way, Billy Ray Bragg
  • Patent number: 7105111
    Abstract: Process for producing hollow bodies comprising fibre-reinforced ceramic materials, where cores whose shape corresponds to that of the hollow spaces are produced in a first step, a green body is produced in a second step by introducing the abovementioned cores and a press moulding compound into a mould, where the press moulding compound comprises carbon fibres and/or carbon threads and pitch and/or resins, the green body is cured in a third step by heating under pressure, and then carbonised in a fourth step by heating in the absence of oxidants to form a C/C body, which latter can be infiltrated with liquid metal with retention of its shape in a fifth step, with at least partial formation of carbides, where the cores comprise a material which is non-meltable but undergoes at least sufficient shrinkage above the curing temperature of the shaping by pressing of the press moulding compound for the shrunken core to be able to be taken out from the carbonised body; hollow bodies produced by this process and also t
    Type: Grant
    Filed: September 26, 2002
    Date of Patent: September 12, 2006
    Assignee: SGL Carbon AG
    Inventors: Moritz Bauer, Michael Heine, Udo Gruber, Ronald Huener, Andreas Kienzle, Andreas Rahn, Rainer Zimmermann-Chopin
  • Patent number: 7083757
    Abstract: Semiconductor wire bonding tools used in the assembly and interconnection of integrated circuits (ICs) are micromolded from a mixture of ultrafine particulate materials mixed with an organic binder. Following extraction of the binder the green bonding tools are sintered during which they undergo isotropic, constant and accurately predetermined shrinkage. Hence semiconductor wire bonding tools can be produced with virtually no limit to miniaturization, thus allowing the fabrication of higher integrated semiconductor products.
    Type: Grant
    Filed: February 18, 2002
    Date of Patent: August 1, 2006
    Inventors: Romain L. Billiet, Hanh T. Nguyen
  • Patent number: 6998064
    Abstract: A thermochemically stable oxidic thermal insulating material presenting phase stability, which can be used advantageously as a thermal insulating layer on parts subjected to high thermal stress, such as turbine blades or such like. The thermal insulating material can be processed by plasma spraying and consists preferably of a magnetoplumbite phase whose preferred composition is MMeAl11O19, where M is La or Nd and where Me is chosen from among zinc, the alkaline earth metals, transition metals, and rare earths, preferably from magnesium, zinc, cobalt, manganese, iron, nickel and chromium.
    Type: Grant
    Filed: July 14, 2003
    Date of Patent: February 14, 2006
    Assignee: MTU Aero Engines GmbH
    Inventors: Rainer Gadow, Guenter Schaefer
  • Patent number: 6955777
    Abstract: A plate for use in mixing and testing materials in the pharmaceutical industry is formed by a method in which apertures in a set of greensheets are formed by a material removal process, at least some of the apertures being filled with a fugitive material that escapes during sintering.
    Type: Grant
    Filed: January 7, 2003
    Date of Patent: October 18, 2005
    Assignee: International Business Machines Corporation
    Inventors: Govindarajan Natarajan, Umar Ahmad, Raschid J. Bezama, James N. Humenik, John U. Knickerbocker, Rao V. Vallabhaneni
  • Publication number: 20040262801
    Abstract: A method of preparing a low-density material and precursor for forming a low-density material is provided. An aqueous mixture of inorganic primary component and a blowing agent is formed, the mixture is dried and optionally ground to form an expandable precursor. Such a precursor is then fired with activation of the blowing agent being controlled such that it is activated within a predetermined optimal temperature range. Control of the blowing agent can be accomplished via a variety of means including appropriate distribution throughout the precursor, addition of a control agent into the precursor, or modification of the firing conditions such as oxygen deficient or fuel rich environment, plasma heating etc.
    Type: Application
    Filed: February 25, 2004
    Publication date: December 30, 2004
    Inventors: Hamid Hojaji, Shannon Marie Labernik, Thinh Pham, Huagang Zhang
  • Publication number: 20040222571
    Abstract: An actively-cooled, fiber-reinforced ceramic matrix composite thrust chamber for liquid rocket propulsion systems is designed and produced with internal cooling channels. The monocoque tubular structure consists of an inner wall, which is fully integrated to an outer wall via radial coupling webs. Segmented annular void spaces between the inner wall, outer wall and adjoining radial webs form the internal trapezoidal-shaped cooling channel passages of the tubular heat exchanger. The manufacturing method enables producing any general tubular shell geometry ranging from simple cylindrical heat exchanger tubes to complex converging-diverging, Delaval-type nozzle structures with an annular array of internal cooling channels. The manufacturing method allows for transitioning the tubular shell structure from a two-dimensional circular geometry to a three-dimensional rectangular geometry.
    Type: Application
    Filed: June 14, 2004
    Publication date: November 11, 2004
    Inventor: Wayne S. Steffier
  • Patent number: 6811744
    Abstract: A method and apparatus for embedding features and controlling material composition in a three-dimensional structure (130) is disclosed. The invention enables the control of material characteristics, within a structure (130) made from a plurality of materials, directly from computer rendering of solid models of the components. The method uses stereolithography and solid model computer file formats to control a multi-axis head (480) in a directed material deposition process (123). Material feedstock (126, 127) is deposited onto a pre-heated substrate (19). Depositions (15) in a layer-by-layer pattern, defined by solid models (141, 146), create a three-dimensional article having complex geometric details. Thermal management of finished solid articles (250-302), not available through conventional processing techniques, is enabled by embedded voids (152) and/or composite materials (126, 127), which include dissimilar metals (210, 216).
    Type: Grant
    Filed: April 22, 2002
    Date of Patent: November 2, 2004
    Assignee: Optomec Design Company
    Inventors: David M. Keicher, James W. Love, Kevin J. Dullea, James L. Bullen, Pierrette H. Gorman, Mark E. Smith
  • Publication number: 20040195733
    Abstract: A method for producing ceramic micromanufactured items comprises the following stages: a starting material constituting at least a micromanufactured item (1) is prepared and used to from the micromanufactured item (1); said starting material includes at least a pre-ceramic polymer, and the method further comprises a stage in which the inner structure of the starting material is modified, said structure being turned from a polymeric structure to a ceramic structure after the forming stage of said micromanufactured item (1).
    Type: Application
    Filed: January 27, 2004
    Publication date: October 7, 2004
    Inventors: Giorgio Maccagnan, Paolo Colombo
  • Patent number: 6773479
    Abstract: A particulate filter for diesel engines comprises a metal shell or casing inside which is set a filtering body made of ceramic foam. The filtering body is made up of a plurality of separate elements made of ceramic foam and having a substantially plane and elongated shape, which are set about a longitudinal axis of the shell in such a way as to define, inside the shell, an inner chamber (B) set inside the array of filtering elements and at least one outer chamber (A) set outside the array. The said chambers respectively communicate with the intake pipe and with the outlet pipe, or vice versa, in such a way that, during use, the flow of the engine exhaust gases that traverses the shell passing from the intake pipe to the outlet pipe (or vice versa) is forced to traverse the aforesaid filtering elements, thus assuming a component of radial velocity with respect to the longitudinal axis of the shell.
    Type: Grant
    Filed: January 18, 2002
    Date of Patent: August 10, 2004
    Assignee: C.R.F. Societa Consortile per Azioni
    Inventors: Massimo Debenedetti, Gianmarco Boretto
  • Publication number: 20040129371
    Abstract: A plate for use in mixing and testing materials in the pharmaceutical industry is formed by a method in which apertures in a set of greensheets are formed by a material removal process, at least some of the apertures being filled with a fugitive material that escapes during sintering.
    Type: Application
    Filed: January 7, 2003
    Publication date: July 8, 2004
    Applicant: INTERNATIONAL BUSINESS MACHINES CORPORATION
    Inventors: Govindarajan Natarajan, Umar Ahmad, Raschid J. Bezama, James N. Humenik, John U. Knickerbocker, Rao V. Vallabhaneni
  • Patent number: 6733607
    Abstract: A method for forming a low temperature cofired ceramic (LTCC) device includes forming a channel in a first LTCC tape layer. A wax is inserted in the channel. The wax is of a type that burns out at a temperature below a sintering temperature of the first LTCC tape layer. At least a second LTCC tape layer is stacked on the first LTCC tape layer to form a stack. The stack is pressed sufficiently for the first and second layers to bond into a laminate. The laminate is fired at the sintering temperature to form a sintered ceramic structure from the first and second LTCC tape layers, so that all or substantially all of the wax is burned out from the channel.
    Type: Grant
    Filed: April 15, 2002
    Date of Patent: May 11, 2004
    Assignee: Harris Corporation
    Inventors: Brian R. Smith, Randy T. Pike, C. Michael Newton
  • Patent number: 6699428
    Abstract: A method of producing a ceramic body having a construction such that cells are plugged alternately at both end faces of a ceramic honeycomb structural body by filling a plugging slurry into predetermined cells at both end faces of a ceramic honeycomb formed body, having the steps of: filling a plugging material for mask into the cells to be opened at one end face of the ceramic honeycomb formed body; immersing the end face, to which the plugging material for mask is filled, into a plugging slurry; and drying and sintering the ceramic honeycomb formed body while the plugging material for mask is removed during a drying step or a sintering step.
    Type: Grant
    Filed: April 23, 2002
    Date of Patent: March 2, 2004
    Assignee: NGK Insulators, Ltd.
    Inventors: Hideaki Nishi, Eiji Ito, Yoshimasa Kondo
  • Publication number: 20030190275
    Abstract: The inner shape of the body part in a hollow ceramic molded article constituting a precursor of a discharge vessel is precisely controlled so as to make a large improvement in the function of a discharge vessel formed by baking the hollow ceramic molded article.
    Type: Application
    Filed: December 18, 2002
    Publication date: October 9, 2003
    Inventors: Sugio Miyazawa, Shinzo Hayashi, Masaru Doi
  • Patent number: 6627019
    Abstract: A ceramic matrix composite part having elongated cooling channels within the wall thereof is manufactured by inserting decomposable inserts within a woven ceramic fiber preform. The inserts are tows of continuous carbon fibers surrounded by a carbonaceous filler, and are inserted where the channels are desired. The preform, with the inserts in place, is disposed within a mold. A ceramic matrix material is added and the fiber preform is consolidated with the ceramic matrix material. The consolidated part is then heated to thermally decompose the inserts to create the elongated channels within the part. The inserts may be flexible and woven into the preform using an automated weaving loom, or they may have limited flexibility and be inserted by machine or by hand.
    Type: Grant
    Filed: December 18, 2000
    Date of Patent: September 30, 2003
    Inventors: David C. Jarmon, Xiaolan Hu, Steven Wayne Burd, Christopher Dale Jones, Stephen K. Kramer, Christopher L. Kogstrom, Nikolaos Napoli, Bruce Bond
  • Patent number: 6616782
    Abstract: A thermal shock-resistant ceramic article and a method of manufacturing the article include alternating layers of a first material (2) comprising a fusible, particulate ceramic composition and a second material (3), typically comprising a porous, pyrolyzable material. The layered structure increases the article's work of fracture and toughness, and may lead to improved thermal shock-resistance. The method advantageously uses a sheet, film or sleeve to prepare the article for firing. The composition, thickness, and porosity of the second material (3) will affect the desired properties. The method is particularly adapted for manufacturing cylindrical articles, including stopper rods, nozzles, and pouring tubes for the metal casting industry.
    Type: Grant
    Filed: April 5, 2002
    Date of Patent: September 9, 2003
    Assignee: Vesuvius Crucible Company
    Inventor: Eric Hanse
  • Patent number: 6596168
    Abstract: The invention relates to a filter element and its manufacture to be used in removal of liquid from solids containing material to be dried in a capillary suction dryer which filter element contains a ceramic microporous layer having the pore size under 5 micrometer and supported by a ceramic internal layer having recess areas for liquid flowing. The internal layer is made of at least one substrate which continuously surrounds at least one recess area and which ceramic internal layer is surrounded by at least one essentially continuous microporous surface layer.
    Type: Grant
    Filed: January 16, 2001
    Date of Patent: July 22, 2003
    Assignee: Outokumpu Oyj
    Inventors: Kerry Johnson, Olli Högnabba, Bjarne Ekberg
  • Patent number: 6554882
    Abstract: A rapid tooling method is provided for molding metal particles, ceramic particles or mixtures thereof directly from patterns comprising a meltable, soluble or decomposable substance and preferably formed by rapid prototyping technology, as well as particle compositions therefor. The method comprises mixing at least about 95% by weight sinterable metal particles, sinterable ceramic particles or mixtures thereof with at least about 0.5 wt. % to about 5.0 wt. % binder to form a powder mixture; casting the mixture around a pattern; applying pressure sufficient to compact the mixture to form a preform; removing the pattern; and heating the preform at a sintering temperature sufficient to sinter the particles and form a molded article.
    Type: Grant
    Filed: May 26, 1998
    Date of Patent: April 29, 2003
    Assignee: Drexel University
    Inventors: Gongyao Zhou, Zongyan He
  • Patent number: 6544365
    Abstract: A method of producing a laminated ceramic electronic component results in an increased thickness of an internal electrode, reduced delamination, and produces a laminated ceramic electronic component having outstanding reliability. The method of producing a laminated ceramic electronic component includes the step of forming a green sheet supported on a carrier film and having an internal electrode paste layer configured to pass through the green sheet from the upper surface to the lower surface thereof, and a ceramic paste layer, the two layers being provided with a space therebetween, and the step of repeating the step of press-bonding the laminate of the green sheet and the carrier film, and separating the carrier film to obtain a ceramic laminate, pressing the ceramic laminate in the thickness direction, and then firing the laminate to obtain a ceramic sintered body.
    Type: Grant
    Filed: January 12, 2001
    Date of Patent: April 8, 2003
    Assignee: Murata Manufacturing Co., Ltd.
    Inventors: Hiromichi Tokuda, Tsuyoshi Tatsukawa
  • Patent number: 6524522
    Abstract: The present invention relates to the extrusion freeform fabrication of low cost, in situ, metallic foam components having oriented microstructures and improved mechanical properties such as energy absorption and specific stiffness. The present invention relates to the freeform fabrication of metallic foams to form parts having complex geometry that demonstrate superior mechanical properties and energy absorbing capacity.
    Type: Grant
    Filed: March 7, 2002
    Date of Patent: February 25, 2003
    Assignee: Advanced Ceramics Research, Inc.
    Inventors: K. Ranji Vaidyanathan, John L. Lombardi, Joseph Walish, Ronald A. Cipriani
  • Publication number: 20020149128
    Abstract: A method of making a permeable fiber-reinforced ceramic body comprising mixing an organic particulate with silica fiber, alumina fiber, alumina borosilicate fiber, a dispersant, and water to produce a slurry of fibrous ceramic material. The slurry is then placed within a mold and vaccuum pressure is applied thereto to substantially remove the water to form a fibrous ceramic body. The fibrous ceramic body is then dried and sintered to a temperature sufficient to bond the ceramic material together to form a porous ceramic article. Simultaneously, the fibrous ceramic body is heated to a temperature sufficient to generally burn off the organic particulate to create voids interconnecting the pores to form a permeable fiber reinforced porous ceramic article.
    Type: Application
    Filed: April 13, 2001
    Publication date: October 17, 2002
    Inventor: Robert A. DiChiara
  • Publication number: 20020043735
    Abstract: A method for producing a silicon nitride filter, which comprises heat-treating in nitrogen a green body comprising from 35 to 90 mass % of silicon nitride particles having an average particle diameter of from 1 to 30 &mgr;m, from 5 to 60 mass % of a pore-forming agent and from 0.
    Type: Application
    Filed: October 12, 2001
    Publication date: April 18, 2002
    Applicant: Asahi Glass Company, Limited
    Inventor: Naomichi Miyakawa
  • Patent number: 6355211
    Abstract: A method for producing high performance components by the consolidation of powdered materials under conditions of hot isostatic pressure. The method uses the inclusion of reactive materials mixed into pressure-transmitting mold materials and into the powder to be consolidated to contribute to in-situ materials modification including purification, chemical transformation, and reinforcement. The method also uses encapsulation of the mold in a sealed container to retain the mold material in position, and to exclude air and contaminants.
    Type: Grant
    Filed: February 7, 2000
    Date of Patent: March 12, 2002
    Inventor: Xiaodi Huang
  • Publication number: 20020005605
    Abstract: A method of removing a core from a CMC component in which the core was used to form an internal cavity. According to one embodiment of the invention, the core is removed from a fully densified CMC component by heating the component and core to a temperature at which the core deteriorates but below a temperature at which the component would melt or otherwise be damaged. According to a second embodiment of this invention, the component is only partially densified, and then impregnated with a coating material that is resistant to a leaching compound capable of removing the core. The core can then be removed using the leaching compound without damage to the internal surfaces of the component defined by the core when the component was fabricated.
    Type: Application
    Filed: August 6, 2001
    Publication date: January 17, 2002
    Inventors: Thomas J. Dunyak, James D. Steibel, David R. Chang, Peggy E. Jones
  • Patent number: 6328834
    Abstract: A process for producing bodies made of fiber-reinforced composites from fiber-reinforced precursor bodies having a porous carbon matrix, in particular from C/C bodies, includes (1) mixing fibers, fiber bundles or fiber agglomerates based on carbon, nitrogen, boron and/or silicon with at least one carbonizable binder to give a pressing composition, and (2) pressing the pressing composition to form a green body. At least one metal- or silicon-containing core is added to the green body. The green body is subsequently pyrolysed to convert the binder or binders into a porous carbon matrix, and the resulting fiber-reinforced precursor body is infiltrated with molten metal or silicon from the metal- or silicon-containing core.
    Type: Grant
    Filed: August 2, 1999
    Date of Patent: December 11, 2001
    Assignee: DaimlerChrysler AG
    Inventors: Kolja Rebstock, Karl-Heinz Roess
  • Patent number: 6319437
    Abstract: A powder injection molding and infiltration process. A powder of a skeleton material having a relatively high melting point is mixed with a composite binder to form a mold mixture. The composite binder is comprised of at least two binder materials. The mold mixture is molded into a desired shape in a mold device to produce a molded part. The composite binder is then removed to produce voids in the molded part and the voids are filled by infiltrating an infiltrant comprised of an infiltrant material having a relatively low melting point to produce a composite molded part. In a preferred embodiment the skeleton material is TiB2 and the infiltrant material is aluminum and the composite binder is comprised of a plastic and a wax. In this embodiment the wax portion of the composite binder is removed using a solvent and the plastic is removed during the infiltration step. The resulting composite part has a TiB2 skeleton with voids substantially filled with aluminum.
    Type: Grant
    Filed: February 16, 1999
    Date of Patent: November 20, 2001
    Assignee: Hi-Z Technology, Inc.
    Inventors: Norbert B. Elsner, Stanley Zalkind, Ian Sidney R. Clark, Fred Leavitt
  • Publication number: 20010033893
    Abstract: Composition for preparing water-repellent coatings on optical substrates, comprising a porous, electrically conductive molding and an organosilicon compound, obtainable by mixing an electrically conductive or semiconductive support material with a binder and subjecting the mixture to compression molding to form a compression molding, sintering the compression molding at preferably 1100 to 1500° C. in air to form a porous molding, impregnating the molding with the organosilicon compound, and ageing the impregnated molding by storage in air for at least 3 days.
    Type: Application
    Filed: June 28, 2001
    Publication date: October 25, 2001
    Inventors: Uwe Anthes, Reiner Dombrowski
  • Publication number: 20010016353
    Abstract: The present invention relates to hard tissue scaffolds comprising a resorbable ceramic, and their method of production. Specifically, this invention relates to novel scaffolds, formed via a replication technique, and useful as biological replacements for hard tissue.
    Type: Application
    Filed: March 28, 2001
    Publication date: August 23, 2001
    Inventors: Victor F. Janas, Kevor Shane TenHuisen
  • Patent number: 6254998
    Abstract: A method for making foam structures suitable for use as mechanical energy absorbers, structural members, filters, catalyst carriers or the like. A composite rod comprising an outer shell and an inner core is formed of respective mixtures of powders. The mixture for the outer shell comprises a sinterable powdered structural material such as ceramics, metals, intermetallics, and a powdered binder such as paraffin, wax or polymer. The inner core comprises a powdered channel-forming filler material such as melamine or polymers, or soluble inorganic compounds or a metal that can differentially be removed from the structural material of the shell. The composite rod may be formed by extrusion. The composite rod is sectioned into a plurality of composite rod segments of predetermined length and a plurality of these segments is assembled in randomly oriented relationship to one another. The assemblage of rod segments is then consolidated, and the binder and filler are then removed, as by heating.
    Type: Grant
    Filed: February 2, 2000
    Date of Patent: July 3, 2001
    Assignee: Materials and Electrochemical Research (MER) Corporation
    Inventor: Lev J. Tuchinsky
  • Patent number: 6248289
    Abstract: A method for molding relatively complex and large shapes by a co-injection molding process which results in a significantly less expensive and lighter molded product. The process steps include first injection molding a thermoplastic material highly densified with ceramic or stainless steel particulate material to form a shell structure having a homogeneous dispersion of the ceramic or stainless steel material within its matrix and then injecting a significantly less expensive material into the core of the preformed thermoplastic/ceramic or stainless steel structure and thereafter sintering the resulting molded structure. The resultant structure is a hollow shell of highly densified ceramic or stainless steel.
    Type: Grant
    Filed: June 23, 2000
    Date of Patent: June 19, 2001
    Assignee: Xerox Corporation
    Inventor: Jay lee Schneider
  • Patent number: 6248434
    Abstract: The invention concerns a composite body consisting of a hard metal, cermet or ceramic substrate body and at least one layer of a mechanically resistant material, a ceramic substance, a diamond-like layer, amorphous carbon and/or hexagonal boron nitride. The invention also concerns a method of producing this composite body, wherein, when the green compact has been dewaxed, with its pores still open and whilst it continues to be heated as from a temperature of between 600° C. and 1100° C., it is acted upon by sublimable solids and/or reaction gases which are necessary for coating purposes. The temperature of the green compact is then further increased and the latter is fully compressed by sintering, before one or more layers of the above-mentioned type is/are applied.
    Type: Grant
    Filed: June 3, 1999
    Date of Patent: June 19, 2001
    Assignee: Widia GmbH
    Inventors: Klaus Rödiger, Hartmut Westphal, Klaus Dreyer, Thorsten Gerdes, Monika Willert-Porada
  • Patent number: 6231707
    Abstract: In the formation of multilayer ceramic substrates, greensheets are utilized which have the same pattern and number of vias punched in each greensheet. Then, selected vias may be filled with metallic paste to form the internal connections of the multilayer ceramic substrate. The remaining vias may be filled with a fugitive material or left totally unfilled. Also disclosed is the multilayer ceramic substrate produced by this method.
    Type: Grant
    Filed: September 22, 1998
    Date of Patent: May 15, 2001
    Assignee: International Business Machines Corporation
    Inventors: Dinesh Gupta, L. Wynn Herron, John U. Knickerbocker, David C. Long, Jawahar P. Nayak, Robert A. Rita
  • Patent number: 6210625
    Abstract: The invention is a method of making a novel spherical form of granulated products that can be effectively used in various product forms in drug, fertilizer, foodstuff, feed, agricultural chemical, catalyst, ceramics, powder metallurgy, detergent, plastic, and bio-material fields, for instance, as catalysts, lightweight materials, sound-insulating materials, microcapsules, and lightweight aggregates. To obtain a granulated product which is a spherical solid shell having a spherical space therein, a polymer having high water absorption properties is swollen by the absorption of water therein, and then brought in contact with a powder to form a powder layer all over the surface of the swollen polymer particle. This spherical particle is then dried and fired if necessary.
    Type: Grant
    Filed: March 29, 1999
    Date of Patent: April 3, 2001
    Assignee: Mikuni Corporation
    Inventors: Mitsuhiro Matsushita, Shinpei Inamura
  • Patent number: 6197246
    Abstract: A plasma generating electrode device including a substrate 31 made of a dense ceramic, and an electrode 55 buried in said substrate 31, wherein said electrode 55 is isolated from a setting face of said substrate 31, and plasma is generated over said substrate. It is preferable that the minimum thickness of an electromagnetic wave permeation layer 37 is not less than 0.1 mm, the average thickness of the electromagnetic wave permeation layer is not less than 0.5 mm, the electrode 55 is a planar electrode made of a metal bulk, and the electrode is a monolithic sinter free from a joint face. This structure can be applied to an electric dust collector, an electromagnetic shield device or an electrostatic chuck. These can be preferably installed inside a semiconductor production unit using a halogen-based corrosive gas.
    Type: Grant
    Filed: March 2, 2000
    Date of Patent: March 6, 2001
    Assignee: NGK Insulators, Ltd.
    Inventors: Yusuke Niori, Koichi Umemoto, Ryusuke Ushikoshi
  • Patent number: 6183578
    Abstract: A method for assembling an ultrasonic transducer, first produces a plurality of plates of piezoelectric material. Then the plates are bonded together through use of a polymeric matrix comprising a polymer and intermixed particles having determined dimensional parameters, the particles acting to separate the plates by predetermined distances that are dependent upon the determined dimensional parameters. Preferred particles are polystyrene spheres. A second embodiment produces a plurality of strips of green piezoelectric ceramic material, each strip including a layer of a fugitive material. The strips are then placed in a stack and the stack is fired to convert the green piezoelectric ceramic material into densified ceramic plates. The firing acts to drive off said second fugitive material and to leave voids. The voids are then backfilled with a polymeric material to create a unified structure.
    Type: Grant
    Filed: April 21, 1999
    Date of Patent: February 6, 2001
    Assignee: Penn State Research Foundation
    Inventors: Timothy A. Ritter, Eugene R. Gerber, Kirk Shung, Thomas R. Shrout
  • Patent number: 6165409
    Abstract: The invention concerns a transfer element for transferring molten steel between an upstream container such as a tundish and a downstream vessel such as a continuous casting mold. this element is comprised of a body (4) that delimits a steel entrance zone, a channel (6) and a steel exit zone (9). It has at least one divider (16) in its exit zone (9) for dividing the steel flux into at least two jets. The divider is comprised of two parts of complementary form (19) solid with the body (4), located opposite each other and separated by an interstice (18).
    Type: Grant
    Filed: June 7, 1999
    Date of Patent: December 26, 2000
    Assignee: Vesuvius Crucible Company
    Inventors: Pascal Dubois, Eric Hanse
  • Patent number: 6126888
    Abstract: A method for making very strong gas mantles and other ceramic structures, and the resulting products, are provided. According to the method, an organic or composite structure is first pyrolyzed in the absence of oxygen to remove hydrogen, oxygen and nitrogen, leaving a porous carbon or composite structure, which is then impregnated with a metal compound-containing solution or slurry which is later fired in the presence of an oxidizing atmosphere to produce a refractory metal oxide which has about the same shape as the precursor carbon or composite structure. Due to minimal shrinkage of the mostly carbon or composite precursor, the resulting mantles and other ceramic structures have few defects in the fibers and great strength.
    Type: Grant
    Filed: January 8, 1999
    Date of Patent: October 3, 2000
    Assignee: Quantum Group Inc.
    Inventor: Mark K. Goldstein
  • Patent number: 6113836
    Abstract: A female mold (2, 12, 22, 32, 42, 52, 62) having a desirable pattern is formed on a substrate (1, 11, 21, 31, 41, 51, 61). Next, ceramic material (3, 13, 23, 33, 43, 53, 63) is filled in spaces in the female mold. Thereafter, the female mold is removed by heating the entire substrate, whereby a desirable thick film pattern can be finely and easily formed. The inorganic paste material comprising inorganic liquid vehicle containing water glass as main ingredient and powdery solid dispersed in the inorganic liquid vehicle is used as the ceramic material. The volume change of the inorganic paste material is small during the drying and calcinating processes, thus the inorganic paste material is prevented from being broken.
    Type: Grant
    Filed: June 22, 1998
    Date of Patent: September 5, 2000
    Assignee: Dai Nippon Insatsu Kabushiki Kaisha
    Inventors: Yorihiko Sakai, Norikatsu Ono, Norikazu Mineo, Takeshi Matsumoto, Hideaki Fujii