Producing Fiber Containing Article Or Fiber Patents (Class 264/640)
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Patent number: 6740286Abstract: Methods for consolidation and densification of fibrous monolith composite structures are provided. Consolidation and densification of two- and three-dimensional fibrous monolith components having complex geometries can be achieved by pressureless sintering. The fibrous monolith composites are formed from filaments having at least a first material composition generally surrounded by a second material composition. The composites are sintered in an inert gas or nitrogen gas at a pressure of no more than about 30 psi to provide consolidated and densified fibrous monolith composites.Type: GrantFiled: December 4, 2001Date of Patent: May 25, 2004Assignee: Advanced Ceramics Research, Inc.Inventors: Manish P. Sutaria, Mark J. Rigali, Ronald A. Cipriani, Gregory J. Artz, Anthony C. Mulligan
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Publication number: 20040097155Abstract: New nonwoven fibrous webs are taught which comprise a collected mass of a) directly formed fibers disposed within the web in a C-shaped cross-sectional configuration and b) staple fibers having a crimp of at least 15% dispersed among the directly formed fibers in an amount of at least 5% the weight of the directly formed fibers. The web is lofty but free of macrovoids. Preferably, the web has a filling ratio of at least 50 and a light transmittance variation of about 2% or less. Typically, fibers within the web are bonded together at points of fiber intersection, preferably with autogenous bonds, to provide a compression-resistant matrix. The webs are especially useful as acoustic and thermal insulation.Type: ApplicationFiled: November 15, 2002Publication date: May 20, 2004Applicant: 3M Innovative Properties CompanyInventors: David A. Olson, Jonathan H. Alexander, Michael R. Berrigan
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Publication number: 20040087431Abstract: The present invention relates to a method for producing silicon oxycarbide fibers by pyrolysis of preceramic precursors.Type: ApplicationFiled: October 14, 2003Publication date: May 6, 2004Applicant: UNIVERSITA DEGLE STUDI DI TRENTOInventors: Gian Domenico Soraru, Sandra Dire, Alberto Berlinghieri
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Patent number: 6716782Abstract: A porous ceramic fiber insulating material and method of making a material having a combination of silica (SiO2) and alumina (Al2O3) fibers, and boron-containing powders is the topic of the new invention. The insulative material is composed of about 60 wt % to about 80 wt % silica fibers, about 20 wt % to about 40 wt % alumina fibers, and about 0.1 wt % to about 1.0 wt % boron-containing powders. A specific boron-containing powder used for this invention is boron carbide powder which provide boron-containing by-products, which aid in fusion and sintering of the silica and alumina fibers. The material is produced by forming an aqueous slurry, blending and chopping the fibers via a shear mixer, orienting the fibers in the in-plane direction, draining water from the fibers, pressing the fibers into a billet, heating the fibers to remove residual water, and firing the billet to fuse the fibers of the material. After sintering, bulk density of the new insulation material ranges from 6 to 20 lb/ft3.Type: GrantFiled: August 16, 2002Date of Patent: April 6, 2004Assignee: The Boeing CompanyInventors: Vann Heng, Karrie Ann Hinkle, Mary Ann Santos
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Patent number: 6716376Abstract: The invention relates to a process for producing a fiber composite material containing fibers with a high hot strength, in particular based on carbon, silicon, boron and/or nitrogen, a pressing compound being produced from fibers, a binder and, if appropriate, fillers and/or additives, which is then pressed in a press mold to form a green body. Various pressing compounds are produced, which contain fibers of different qualities and/or in different proportions, and the press mold is filled with the various pressing compounds in a number of successive steps. The invention also relates to a fiber composite material of this nature.Type: GrantFiled: November 1, 2000Date of Patent: April 6, 2004Assignee: DaimlerChrysler AGInventors: Tilmann Haug, Kolja Rebstock, Christian Schwarz
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Publication number: 20040005835Abstract: An elastic strand laminate, and a method of making an elastic strand laminate. The elastic strand laminate includes a plurality of self-adhering elastic strands made up of an elastomeric adhesive composition. The self-adhering elastic strands can be laminated to one or more facing sheets using conventional hot melt equipment.Type: ApplicationFiled: December 26, 2002Publication date: January 8, 2004Inventors: Peiguang Zhou, Cristian M. Neculescu
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Patent number: 6630029Abstract: In a method of coating a CMC fiber, the fiber is passed through a reaction zone along a path substantially parallel to a longitudinal axis of the zone, a flow of fiber coating reactant is passed though the reaction zone, at least a portion of the flow of reactant is disrupted from a path substantially parallel to the fiber path to create a mixing flow adjacent the fiber. A coating reactor includes a reactor chamber to accommodate a fiber passing along a path substantially parallel to a longitudinal axis of the chamber and a flow of fiber coating reactant. The reactor chamber further includes a flow disrupter located within the reactor chamber to disrupt at least a portion of the flow of reactant from a path substantially parallel to the fiber path to create a mixing flow adjacent the fiber.Type: GrantFiled: December 4, 2000Date of Patent: October 7, 2003Assignee: General Electric CompanyInventor: Milivoj Konstantin Brun
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Patent number: 6627019Abstract: A ceramic matrix composite part having elongated cooling channels within the wall thereof is manufactured by inserting decomposable inserts within a woven ceramic fiber preform. The inserts are tows of continuous carbon fibers surrounded by a carbonaceous filler, and are inserted where the channels are desired. The preform, with the inserts in place, is disposed within a mold. A ceramic matrix material is added and the fiber preform is consolidated with the ceramic matrix material. The consolidated part is then heated to thermally decompose the inserts to create the elongated channels within the part. The inserts may be flexible and woven into the preform using an automated weaving loom, or they may have limited flexibility and be inserted by machine or by hand.Type: GrantFiled: December 18, 2000Date of Patent: September 30, 2003Inventors: David C. Jarmon, Xiaolan Hu, Steven Wayne Burd, Christopher Dale Jones, Stephen K. Kramer, Christopher L. Kogstrom, Nikolaos Napoli, Bruce Bond
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Patent number: 6613255Abstract: A method of making a permeable fiber-reinforced ceramic body comprising mixing an organic particulate with silica fiber, alumina fiber, alumina borosilicate fiber, a dispersant, and water to produce a slurry of fibrous ceramic material. The slurry is then placed within a mold and vaccuum pressure is applied thereto to substantially remove the water to form a fibrous ceramic body. The fibrous ceramic body is then dried and sintered to a temperature sufficient to bond the ceramic material together to form a porous ceramic article. Simultaneously, the fibrous ceramic body is heated to a temperature sufficient to generally burn off the organic particulate to create voids interconnecting the pores to form a permeable fiber reinforced porous ceramic article.Type: GrantFiled: April 13, 2001Date of Patent: September 2, 2003Assignee: The Boeing CompanyInventor: Robert A. DiChiara, Jr.
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Publication number: 20030160350Abstract: A process for producing a continuous alumina fiber blanket by heat treating an alumina fiber precursor formed from a spinning solution containing an aluminum compound, by using a specific high-temperature furnace capable of high-temperature heat treatment. According to this process, a continuous sheet (W) of alumina fiber precursor formed from a spinning solution containing an aluminum compound is supplied continuously into a high-temperature furnace and subjected to heat treatment while being conveyed in one direction by plural conveying mechanisms (2, 3) disposed in said high-temperature furnace. In this operation, the speed of said conveying mechanisms is reduced progressively in the direction of conveyance in correspondence to the rate of heat shrinkage of the continuous sheet (W) of alumina fiber precursor, thereby to lessen fiber crush in the alumina fiber precursor and obtain a continuous alumina fiber blanket with uniform thickness and high bulk density as well as high strength.Type: ApplicationFiled: January 23, 2003Publication date: August 28, 2003Inventors: Mamoru Shoji, Norio Ikeda, Toshiaki Sasaki
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Patent number: 6602369Abstract: The present invention relates to a process for producing a laminated sheet comprising an alumina fiber precursor, which process comprises spinning out an alumina fiber precursor from a solution mainly comprising an aluminum compound, falling and stacking said alumina fiber precursor on the surface of an accumulator to form a thin lamina sheet of alumina fiber precursor, continuously pulling out said lamina sheet from the accumulator, transferring the resultant lamina sheet to a folding device, and folding the sheet by a predetermined width while stacking the folded sheet and continuously moving the stacking sheet in the direction orthogonal to the folding direction.Type: GrantFiled: July 6, 1999Date of Patent: August 5, 2003Assignee: Mitsubishi Chemical CorporationInventors: Mamoru Shoji, Norio Ikeda, Toshiaki Sasaki
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Publication number: 20030137084Abstract: SiC fiber-reinforced SiC-matrix composite has the structure that SiC filaments are inserted into SiC matrix formed as a pyrolysis product of polyvinyl-silane (PVS) infiltrated into openings of said SiC filaments. PVS as a polymeric SiC precursor has structural units (a) and (b) at an a/b ratio of 1. A SiC fiber preform is impregnated with PVS slurry in an open or vacuum atmosphere, preheated at 300-400° C. in an inert gas atmosphere to moderate PVS to a viscous or semi-cured state, and then pyrolyzed in an argon atmosphere under application of a unidirectional pressure. A product is SiC fiber-reinforced SiC-matrix composite excellent in mechanical strength and high-temperature property with high density. The SiC composite is further densified by infiltration of PVS slurry suspending fine SiC particles therein or by repetition of impregnation with sole PVS and pressure-less pyrolysis after the pressurized pyrolysis.Type: ApplicationFiled: October 25, 2002Publication date: July 24, 2003Applicant: Japan Science and Technology CorporationInventors: Akira Kohyama, Masaki Kotani, Yutai Katoh
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Publication number: 20030132558Abstract: A method for preparing a refractory carbide component includes the steps of providing a carbon rich polymer precursor to silicon carbide and excess carbon, determining an amount of excess carbon in the carbon rich polymer precursor, combining the carbon rich polymer precursor with a selected amount of refractory metal to form a precursor/metal mixture, the selected amount being selected so as to provide stoichiometrically equivalent amounts of the excess carbon and the refractory metal, forming the mixture into a preform of a propulsion component, and heating the preform so as to thermally degrade the carbon rich polymer precursor to produce the silicon carbide and the excess carbon, the excess carbon and the refractory metal reacting to form refractory metal carbide and provide the refractory carbide component.Type: ApplicationFiled: July 16, 2001Publication date: July 17, 2003Inventors: Wayde R. Schmidt, Donald C. Giedt
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Patent number: 6571858Abstract: A method of manufacturing a preform for compounding use which, is to be impregnated with a molten metal to be compounded with a matrix material, is provided. The method includes the step of mixing short fibers, ceramic particles and a binder material together to make a mixture. The average of lengths of the short fibers is 100 to 200 &mgr;m while the volumetric percentage of the short fibers is 1 to 7%. The content of the binder material in the mixture is 0.3 to 5.0 mass %. The method includes also the steps of forming the mixture so as to have a predetermined shape, and sintering the mixture at a temperature of 1000 to 1150° C. to form the preform. Thus, it is restrained that the preform is deformed or an un-reinforced region is formed in the compounded portion.Type: GrantFiled: September 20, 2001Date of Patent: June 3, 2003Assignee: Mazda Motor CorporationInventor: Makoto Fujita
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Patent number: 6558782Abstract: Flexible graphite article of manufacture made by compressing a mixture of expanded graphite particle and a fluoro-resin including ethylene-tetrafluoroethylene (ETFE) copolymers after additional heat treatment. An article of manufacture of a gasket material made shows enhanced mechanical properties especially after oil immersion and reduced leakage.Type: GrantFiled: April 18, 2000Date of Patent: May 6, 2003Assignee: SGL Technic, Inc.Inventors: Anatoliy S. Bakman, Akira Kubo
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Publication number: 20030057612Abstract: A process for producing a SiC ceramic microtube, comprising the steps of oxidizing the surface of an organosilicon polymer to become infusible by exposure to an ionizing radiation, extracting the uncrosslinked central portion of the fiber with an organic solvent to make a hollow silicon polymer fiber, and firing it in an inert gas so that it acquires a ceramic nature.Type: ApplicationFiled: September 11, 2002Publication date: March 27, 2003Applicant: Japan Atomic Energy Research instituteInventors: Masaki Sugimoto, Akira Idesaki, Kiyohito Okamura
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Patent number: 6524979Abstract: There is described a fiber-reinforced material composed of a sheetlike textile material and a thermoset resin with a fiber content of from 30 to 70% by weight, at least 30% of the fiber being synthetic fiber. The thermoset resin is preferably a phenolic resin which contains up to 25% by weight of a fluoropolymer. The sheetlike textile material is preferably 100% synthetic fiber, in particular polyacrylonitrile fiber. There are also described a prepeg formed from the textile material and the thermosetting resin and the process for producing these articles and the use of the material for producing construction elements, in particular for hydraulic systems, by application of mechanical shaping processes.Type: GrantFiled: March 8, 1999Date of Patent: February 25, 2003Assignee: Hoechst AG & Reitex Hydraulik GmbHInventors: Georg Michael Lorenz, Elke Gebauer, Ulrich Schuster, Manfred Tschacher, Burgnard Schönrogge
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Patent number: 6511727Abstract: Flat strip lamella for reinforcing weight-carrying or weight-transferring building components. It has a composite structure consisting of a plurality of pliant or loose-flex supporting fibers (26) aligned parallel to each other, and a binding matrix (28) which connects the supporting fibers to each other so that they are shear-resistant, and is fastenable by means of an adhesive (16) by its broad side to the surface of the building component (12) that is to be reinforced. So that the flat strip lamella, to which the binding matrix gives rigid elastic form, can also be bent over corner edges of a building component (12), the invention proposes that the binding matrix (28) be removed, in at least an intermediary area (30), by uncovering the supporting fibers (26), and that the uncovered supporting fibers be subjected to a liquid or pasty thermosetting plastic, in order to stabilize the bent-over condition.Type: GrantFiled: July 16, 1999Date of Patent: January 28, 2003Assignee: Sika AG, vormals Kaspar Winkler & Co.Inventors: Alexander Bleibler, Ernesto Schümperli, Werner Steiner
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Patent number: 6503441Abstract: A method for producing shaped articles of ceramic composites provides a high degree of dimensional tolerance to these articles. A fiber preform is disposed on a surface of a stable formed support, a surface of which is formed with a plurality of indentations, such as grooves, slots, or channels. Precursors of ceramic matrix materials are provided to the fiber preform to infiltrate from both sides of the fiber preform. The infiltration is conducted under vacuum at a temperature not much greater than a melting point of the precursors. The melt-infiltrated composite article substantially retains its dimension and shape throughout the fabrication process.Type: GrantFiled: May 30, 2001Date of Patent: January 7, 2003Assignee: General Electric CompanyInventors: Gregory Scot Corman, Milivoj Konstantin Brun, Henry Charles McGuigan
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Publication number: 20020180120Abstract: A method for producing shaped articles of ceramic composites provides a high degree of dimensional tolerance to these articles. A fiber preform is disposed on a surface of a stable formed support, a surface of which is formed with a plurality of indentations, such as grooves, slots, or channels. Precursors of ceramic matrix materials are provided to the fiber preform to infiltrate from both sides of the fiber preform. The infiltration is conducted under vacuum at a temperature not much greater than a melting point of the precursors. The melt-infiltrated composite article substantially retains its dimension and shape throughout the fabrication process.Type: ApplicationFiled: May 30, 2001Publication date: December 5, 2002Inventors: Gregory Scot Corman, Milivoj Konstantine Brun, Henry Charles McGuigan
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Patent number: 6447893Abstract: A fiber-composite material (7) is comprised of a yarn aggregate (6) in which yam (2A, 2B) including at least a bundle (3) of carbon fiber and a carbon component other than carbon fiber is three-dimensionally combined and integrally formed without separation from each other; and a matrix made of Si—SiC-based materials (4A, 4B, 5A, 5B) filled between the yarn (2A, 2B) adjacent to each other within the yarn aggregate (6).Type: GrantFiled: June 30, 1999Date of Patent: September 10, 2002Assignees: NGK Insulators, Ltd., Across Co., Ltd.Inventors: Shigeru Hanzawa, Takao Nakagawa
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Publication number: 20020079604Abstract: Ceramic oxide pre-forms comprising substantially continuous, alpha alumina fibers, and methods for making the same. The ceramic oxide pre-forms are useful, for example, as in making metal matrix composites reinforced with substantially continuous, alpha alumina fibers.Type: ApplicationFiled: September 27, 2001Publication date: June 27, 2002Inventors: Sarah J. Davis, Scott R. Holloway, William J. Satzer, John D. Skildum, Larry R. Visser, Ernest R. Waite
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Publication number: 20020079623Abstract: This invention pertains to a method of forming a fiber-reinforced ceramic matrix composite comprising: (a) impregnating a ceramic fiber coated with at least one layer binary coating comprised of boron nitride and silicon nitride wherein the silicon nitride is applied over the boron nitride with a preceramic composition comprising a curable preceramic polymer; (b) forming the impregnated fibers into a desired shape; (c) curing the formed impregnated fibers; (d) heating the cured impregnated fibers of (c) to a temperature of at least 1000° C. in an inert atmosphere for a time effective to convert the preceramic polymer to a ceramic.Type: ApplicationFiled: December 18, 2001Publication date: June 27, 2002Inventor: Daniel Ralph Petrak
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Patent number: 6395220Abstract: Carbon fiber bundles may be dispersed into substantially single mono-filaments in pitch by stirring a mixture of fibers and pitch at a temperature at which the pitch has a viscosity of about 0.1 to about 5 poise. The resulting fiber pitch binder contains about 0.5 to about 10.0 wt. % carbon fibers substantially dispersed as substantially single mono-filaments which are randomly oriented which may then be used directly as a binder for producing carbon bodies, for example, graphite electrodes, pinstock or specialty graphite articles. This unique binder using an economical amount of carbon fibers has the capacity to increase the strength and reduce the coefficients of thermal expansion of the resulting carbon products in more than one direction due to the random orientation of the carbon fibers.Type: GrantFiled: November 2, 1999Date of Patent: May 28, 2002Assignee: UCAR Carbon Technology CorporationInventors: Irwin C. Lewis, Terrence A. Pirro
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Publication number: 20020056946Abstract: Polycarbosilane is mixed with 5-35 wt % of polyvinylsilane to prepare a silicon-base polymer blend which is impregnated in silicon carbide fibers or fabrics to form a preceramic molding body which is exposed to an ionizing radiation to be rendered curing and then fired in an inert gas to produce a composite in which the silicon carbide matrix is reinforced with the silicon carbide fibers.Type: ApplicationFiled: September 19, 2001Publication date: May 16, 2002Inventors: Masaki Sugimoto, Yosuke Morita, Kiyohito Okamura, Masayoshi Itoh
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Patent number: 6368663Abstract: There is disclosed a hybrid treatment into which CVI treatment and PIP treatment are combined. A dense matrix is formed around a ceramic fiber by the CVI treatment, and a gap in the matrix is infiltrated/filled well with the matrix by the PIP treatment, so that hermetic properties are enhanced. Moreover, when a volume ratio of the matrix by the CVI treatment in the total matrix is set to about 5% or more, about 80% or less, fine cracks are present in the matrix by the PIP treatment, so that a binding force of the ceramic fiber is weakened, and Young's modulus can be reduced. As a result, a thermal stress is alleviated and a resistance to thermal shock is enhanced.Type: GrantFiled: June 29, 1999Date of Patent: April 9, 2002Assignee: Ishikawajima-Harima Heavy Industries Co., LtdInventors: Takeshi Nakamura, Hiroshige Murata, Shoju Masaki
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Patent number: 6365092Abstract: A shaped sintered fibrous porous body exhibits a structure with a three-dimensional corrugated or undulating shape and porosity.Type: GrantFiled: June 23, 1999Date of Patent: April 2, 2002Assignee: ABB Lummus Global, Inc.Inventors: Stefan Backa, Rebei Bel Fdhila, Markku Rissanen
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Patent number: 6314858Abstract: An integrated, layered armor structure having multiple layers which alternate in their exhibited characteristics between extremely hard and ductile. The extremely hard layers of the armor structure are designed to shatter an impacting projectile, or pieces thereof, and to fracture in such a way as to dissipate at least a portion of the kinetic energy associated with the projectile pieces and to disperse the projectile pieces and hard layer fragments over a wide area. The ductile layers of the armor structure are designed to yield under the force of impinging projectile pieces and hard layer fragments from an adjacent hard layer. This yielding dissipates at least a portion of the remaining kinetic energy of these pieces and fragments. Pieces and fragments not possessing sufficient kinetic energy to tear through the ductile layer are trapped therein and so stopped.Type: GrantFiled: July 15, 1999Date of Patent: November 13, 2001Assignee: Northrop Grumman CorporationInventors: Thomas Edward Strasser, Steven Donald Atmur
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Patent number: 6294125Abstract: A method for changing the dielectric properties of a polymer impregnated and pyrolyzed ceramic matrix composite (polymer impregnated and pyrolyzed ceramic matrix composite) is disclosed. The polymer impregnated and pyrolyzed ceramic matrix composite can be used in aircraft and turbine engines. polymer impregnated and pyrolyzed ceramic matrix composite comprises a ceramic matrix, a reinforcing fiber, and at least 1 additive used to change dielectric properties (dielectric constant and loss factor). The additive can be a low dielectric constant material having a dielectric constant in the range of 1 to 7.5. The low dielectric constant material can be an oxide such as silica or aluminosilicate or a non-oxide such as silicon nitride, boron nitride, or silicon carbide. The low dielectric constant material can be incorporated in the ceramic matrix as a filler.Type: GrantFiled: December 23, 1998Date of Patent: September 25, 2001Assignee: Dow Corning CorporationInventors: Todd Jeffery Bridgewater, Daniel Ralph Petrak, Andrew Szweda
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Patent number: 6261509Abstract: A process for producing polycrystalline silicon carbide by heating an amorphous ceramic fiber that contains silicon and carbon in an environment containing boron oxide vapor. The boron oxide vapor is produced in situ by the reaction of a boron containing material such as boron carbide and an oxidizing agent such as carbon dioxide, and the amount of boron oxide vapor can be controlled by varying the amount and rate of addition of the oxidizing agent.Type: GrantFiled: April 3, 2000Date of Patent: July 17, 2001Assignee: Dow Corning CorporationInventors: Thomas Duncan Barnard, Jonathan Lipowitz, Kimmai Thi Nguyen
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Patent number: 6254998Abstract: A method for making foam structures suitable for use as mechanical energy absorbers, structural members, filters, catalyst carriers or the like. A composite rod comprising an outer shell and an inner core is formed of respective mixtures of powders. The mixture for the outer shell comprises a sinterable powdered structural material such as ceramics, metals, intermetallics, and a powdered binder such as paraffin, wax or polymer. The inner core comprises a powdered channel-forming filler material such as melamine or polymers, or soluble inorganic compounds or a metal that can differentially be removed from the structural material of the shell. The composite rod may be formed by extrusion. The composite rod is sectioned into a plurality of composite rod segments of predetermined length and a plurality of these segments is assembled in randomly oriented relationship to one another. The assemblage of rod segments is then consolidated, and the binder and filler are then removed, as by heating.Type: GrantFiled: February 2, 2000Date of Patent: July 3, 2001Assignee: Materials and Electrochemical Research (MER) CorporationInventor: Lev J. Tuchinsky
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Patent number: 6248269Abstract: A process for manufacturing a brake lining made of a fiber-reinforced ceramic C/SiC material includes (1) producing a carbon fiber body having at least one of a defined volume of pores and capillaries; (2) infiltrating the carbon fiber body with at least one of carbon or a carbon precursor; (3) pressing the infiltrated carbon fiber body, thereby forming a green compact; (4) pyrolyzing the green compact, thereby forming a porous C/C body; (5) adjusting at least one of a pore and a capillary volume of the porous C/C body to maximally approximately 60% by volume; and (6) infiltrating the C/C body with liquid silicon so that carbon, at least in an area of pores and capillaries which is close to the surface, becomes silicon carbide.Type: GrantFiled: December 29, 1999Date of Patent: June 19, 2001Assignee: DaimlerChrysler AGInventors: Gerd Dietrich, Gerhard Gross, Tilmann Haug, Kolja Rebstock
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Patent number: 6245283Abstract: A fiber-bond type ceramic material 4 is produced by using as raw material fibers 1 inorganic fibers of Si—M—C—O synthesized by melt spinning polycarbosilane, then infusibilizing the produced threads, and firing the set threads, forming from the raw material fibers a woven fabric 2 having all the fibers thereof extended perpendicularly or obliquely relative to the direction of compression during the course of a hot-press fabrication at a weaving step 12, heat-treating the woven fabric in the air, thereby preparing a woven fabric of oxidized fibers 3 provided with an oxide layer on the surface thereof at an oxidizing step 14, and subjecting the woven fabric of oxidized fibers to a hot-press fabrication while compressing the fabric in the direction of the compression thereby causing the oxide layers on the surface to adhere fast to each other and form a matrix at a hot-press step 16.Type: GrantFiled: September 24, 1998Date of Patent: June 12, 2001Assignees: Ishikawajima-Harima Heavy Industries, Ube Industries, Ltd., Shikibo, Ltd.Inventors: Shouju Masaki, Takemi Yamamura, Tetsurou Hirokawa, Takeshi Tanamura
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Patent number: 6231792Abstract: A porous composite product comprised of a network of fibers is produced by forming an unsintered preformed network of fibers and a gasifiable structure forming agent, followed by gasification of the structure forming agent prior to sintering of the fibers at appropriate junction points. The preferred structure forming agent is a cellulosic material.Type: GrantFiled: August 7, 1998Date of Patent: May 15, 2001Assignee: ABB Lummus Global Inc.Inventors: Rudolf A. Overbeek, Ali M. Khonsari, Yung-Feng Chang, Lawrence L. Murrell, Bruce J. Tatarchuk, Michael W. Meffert
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Patent number: 6228293Abstract: A process for producing a body having a porous matrix of at least one recrystallized ceramic material, or for producing a similar fiber-reinforced body, includes shaping a raw material batch which contains a raw material powder and then sintering. A raw material powder is used which has grain size distribution of a fine grain fraction of an average grain size of at most approximately 2 &mgr;m and a coarse grain fraction of an average grain size of approximately 1.5 &mgr;m to approximately 30 &mgr;m, and the sintering process is carried out at a temperature of at most approximately 1,800° C. Because of the selected grain sizes and grain size distributions, the sintering process can be carried out at lower temperatures. In particular, reinforcing fibers can be worked in which can withstand higher sintering temperatures. By defining the grain size of the powder, a porosity can also be set which permits a good impregnating with organic and/or inorganic substances.Type: GrantFiled: August 24, 1998Date of Patent: May 8, 2001Assignee: DaimlerChrysler AGInventors: Jochen Kriegsmann, Rolf Meistring, Nicole Neumann, Reinhard Nixdorf
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Patent number: 6206992Abstract: A fibrous ceramics fabrication method using a room extrusion process and a fibrous monolithic ceramics fabrication method using thereof is disclosed. The method includes the steps of obtaining a extrusion-purpose slurry by evenly mixing a hydrophilic cellulose bonding agent 3 to 7 and a hydrophilic organic plasticizer 5 to 20 for improving a formation property by softening the cellulose bonding agent with a distilled water 45 to 55, with regard to a weight percent 100 of a ceramic powders selected from a group of silicon nitride, silicon carbide and alumina, carrying out a room temperature extrusion from the extrusion-purpose slurry, and coating the fiber by passing through a mixedly dispersed coating-purpose slurry a ceramic powders 20 to 45 selected from a group of boron nitride and graphite, an organic dispersant 0.Type: GrantFiled: November 4, 1998Date of Patent: March 27, 2001Assignee: Agency for Defense DevelopmentInventors: Yong-Kee Baek, Do-Kyung Kim, Shi-Woo Lee, Jong-Gyu Paik
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Patent number: 6187254Abstract: The present invention relates to a method for sintering of a silicon nitride based material using gas pressure sintering technique. It has been found that using a sintering atmosphere containing nitrogen and 0.1-10 vol-% carbon monoxide a cutting tool material is obtained with improved properties, particularly increased edge toughness, when machining heat resistant alloys.Type: GrantFiled: January 15, 1999Date of Patent: February 13, 2001Assignee: Sandvik ABInventors: Marianne Collin, Marian Mikus
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Patent number: 6183852Abstract: A fibrous ceramic mat is molded from a slurry of ceramic fibers and/or ceramic microparticles and/or a metal. The mat is impregnated with a sol prior to drying. A catalyst for the sol is introduced into the mat to cause the sol to gel. The sol-gel binder forms bonds so that the mat is dimensionally stabilized. The mat is dried to produce the desired ceramic insulation that has preferably a consistent microstructure and a fully gelled sol-gel binder through its entire thickness. If we use a metal, it corrodes (i.e., oxidizes) or otherwise reacts to form a refractory binder that augments the sol and reduces the need to infuse sol incrementally to achieve strength. Using metal powder significantly reduces the cost of manufacture.Type: GrantFiled: March 11, 1994Date of Patent: February 6, 2001Assignee: The Boeing CompanyInventors: Michael E. Rorabaugh, Darryl F. Garrigus, Juris Verzemnieks
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Patent number: 6153291Abstract: A method of fiber preparation for discontinuous fiber-reinforced ceramic matrix composite and a coated discontinuous fiber prepared by this method. The method includes immersing a fiber spool in a resin and drip drying the fiber spool until any excess resin is removed. Next, the damp fiber is cut or chopped and heated to the green-state cure temperature of the resin. After the resin has cured, the product is a coated discontinuous fiber whereby the inner fiber filament bundle is held together by a cured resin shell and the individual filaments are held together by the resin.Type: GrantFiled: October 13, 1998Date of Patent: November 28, 2000Assignee: Northrop Grumman CorporationInventor: Thomas Edward Strasser
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Patent number: 6136237Abstract: A method for fabricating a fiber-reinforced ceramic matrix composite (FRCMC) part includes the steps of forming a blank from FRCMC material such that the blank has a dimension approximating a desired finished dimension for the part measuring the dimension of the blank in an unloaded condition, applying a load to the blank and then removing the load so as to cause permanent strain of the blank, measuring the dimension of the blank after the load has been applied and then removed, and comparing the measured dimension after loading to the previously measured dimension. In a preferred embodiment of the invention, if the dimension after loading differs from the dimension previously measured, the loading and measuring steps are repeated. After each loading cycle, the blank is measured and the measured dimension is compared to that previously measured after the prior loading cycle.Type: GrantFiled: April 13, 1999Date of Patent: October 24, 2000Assignee: The Boeing CompanyInventors: Andreas Straub, Jerry Brockmeyer, Eric Krieg
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Patent number: 6132856Abstract: A highly heat-resistant sintered SiC fiber bonded material free of a decrease in strength and less breakable at an ultra-high temperature over 1,400.degree. C., comprising inorganic fibers which are composed mainly of a sintered SiC crystal, contain at least one kind of metal atoms selected from the class consisting of metal atoms of the 2A, 3A and 3B groups of the periodic table and are bonded nearly in the close-packed structure and 1 to 50 nm boundary layers composed mainly of carbon which are present at the interface of fibers, the less breakable highly heat-resistant sintered SiC fiber-bonded material having a density of at least 2.7 g/cm.sup.3 and an elastic modulus of at least 200 GPa, and a process for the production thereof.Type: GrantFiled: July 17, 1998Date of Patent: October 17, 2000Assignee: Ube Industries, Ltd.Inventors: Toshihiro Ishikawa, Shinji Kajii, Kenji Matsunaga, Toshihiko Hogami
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Patent number: 6129887Abstract: A process for producing polycrystalline silicon carbide includes heating an amorphous ceramic fiber that contains silicon and carbon in an environment containing boron oxide vapor. The boron oxide vapor is produced in situ by the reaction of a boron containing material such as boron carbide and an oxidizing agent such as carbon dioxide, and the amount of boron oxide vapor can be controlled by varying the amount and rate of addition of the oxidizing agent.Type: GrantFiled: August 26, 1998Date of Patent: October 10, 2000Assignee: Dow Corning CorporationInventors: Thomas Duncan Barnard, Jonathan Lipowitz, Kimmai Thi Nguyen
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Patent number: 6103178Abstract: The present invention relates to a method for the formation of amorphous boron silicon oxycarbide fibers and crystalline boron-doped silicon carbide fibers wherein the method comprises preparing a blend of a siloxane resin and a carborane-siloxane oligomer, forming the blend into green fibers, and then curing and pyrolyzing the fibers.Type: GrantFiled: February 2, 1999Date of Patent: August 15, 2000Assignee: Dow Corning CorporationInventors: Duane Ray Bujalski, Kai Su
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Patent number: 6083619Abstract: An inorganic material comprising an aerogel, a process for its preparation, and its use. The invention relates to a composite material comprising from 10 to 95% by volume of aerogel particles whose particle diameter is less than 0.5 mm and a phyllosilicate as inorganic matrix material.Type: GrantFiled: May 21, 1997Date of Patent: July 4, 2000Assignee: Hoechst AktiengesellschaftInventors: Dierk Frank, Andreas Zimmermann, Helmut Stuhler
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Patent number: 6080475Abstract: A composite material comprising aerogel, a process for its preparation, and its use. The invention relates to a composite material comprising from 10 to 95% by volume of aerogel particles and at least one inorganic binder, a process for its preparation, and its use.Type: GrantFiled: August 13, 1997Date of Patent: June 27, 2000Assignee: Hoechst AktiengesellschaftInventors: Dierk Frank, Andreas Zimmermann, Helmut Stuhler
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Patent number: 6077600Abstract: A pollutant-reducing catalytic converter for an internal combustion engine. The catalytic converter is of ceramic and operates at higher temperatures for increased efficiency. A ceramic foam is used as the substrate for the catalyst. The foam is an open-celled foam and the substrate is deposited on the walls of the cells. Thus, there is a maximum area of catalyst with a minimum amount of catalyst required. The catalytic converter can be placed in the engine compartment adjacent the engine for maximum efficiency without causing temperature problems within the engine compartment.Type: GrantFiled: July 7, 1998Date of Patent: June 20, 2000Assignee: Grumman CorporationInventors: Steven Donald Atmur, Thomas Edward Strasser
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Patent number: 6056907Abstract: A debonding layer is formed on fibers such as silicon carbide fibers by fing a thin film of a metal such as nickel or iron on the silicon carbide fibers and then annealing at a temperature of about 350-550.degree. C. to form a debond layer of a metal silicide and carbon. These fibers having the debond coating can be added to composite forming materials and the mixture treated to form a consolidated composite. A one heating-step method to form a consolidated composite involves inserting the silicon carbide fibers with just the initial metal film coating into the composite forming materials and then heating the mixture to form the debond coating in situ on the fibers and to form the consolidated composite. Preferred heating techniques include high temperature annealing, hot-pressing, or hot isostatic pressing (HIP).Type: GrantFiled: March 31, 1997Date of Patent: May 2, 2000Assignee: The United States of America as represented by the Secretary of the NavyInventors: Richard K. Everett, Alan S. Edelstein, John H. Perepezko
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Patent number: 6054094Abstract: A method for the manufacture of a ceramic composite fiber in which a second phase is dispersed within a matrix fiber, wherein the matrix consists of a substance selected from alumina, zirconia, mullite, YAG, silica, magnesia, nitrides, carbides, metals, alloys, and polymers; the second phase consists of a substance selected from zirconia, mullite, YAG, other oxides, and metals; and the composite fiber can be produced by synthesizing a fiber from a precursor solution containing the substance of the matrix, and the second phase starting solution dispersed through the solution, and then heating the fiber.Type: GrantFiled: December 22, 1997Date of Patent: April 25, 2000Assignees: Japan as represented by Director General of Agency of Industrial Science and Technology, Fine Ceramics Research AssociationInventors: Atsuya Towata, Mutsuo Sando, Koichi Niihara
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Patent number: 6039823Abstract: The graphitized composite article of the present invention is formed by embedding carbon fiber felt in a matrix of a carbon filler; a thermosetting resin and a solvent; curing the composite article; then, carbonizing and graphitizing the cured composite article to form the graphitized composite article for use as a separator plate capable of substantially inhibiting mixing of hydrogen and oxygen and/or the loss of electrolyte within a fuel cell stack. The graphitized composite article may be a graphitized laminate.Type: GrantFiled: March 9, 1998Date of Patent: March 21, 2000Assignee: International Fuel CellsInventors: Albert P. Grasso, Ronald G. Martin, Robert P. Roche
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Patent number: 6026568Abstract: An internal combustion engine of either two-cycle or four-cycle construction including a block having at least one cylinder bore therein having sidewalls carrying a liner of a structural fiber reinforced ceramic matrix composite material disposed in sealed fiber reinforced sliding relationship within the cylinder bore, and a cylinder head sealing atop end of the cylinder bore to form a closed combustion chamber in combination with the piston. The cylinder head also has the structural fiber reinforced ceramic matrix composite material disposed on an inner surface thereof facing the combustion chamber. The preferred engine is a two-cycle engine having an externally scavenged intake system and an oil sump lubricating system thereby eliminating the need to separately mix or inject lubricating oil. Higher operating temperatures and closer tolerances allow higher fuel efficiency and less pollutant production.Type: GrantFiled: November 1, 1997Date of Patent: February 22, 2000Assignee: Northrop GrummanInventors: Steven Donald Atmur, Thomas Edward Strasser, Philip Shacter, Michael James Hagen