Casting Of Film (e.g., Sheet, Tape, Etc.) Patents (Class 264/650)
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Patent number: 12076965Abstract: The present disclosure provides articles comprising a laminate material having a void volume of at least 40%, having a lattice structure comprising a plurality of interconnected struts forming polyhedrons in a series that extends in three dimensions, or both, where the laminate materials have an interface density of at least 2.0 interfaces/micrometer (?m). Also described are methods for forming the same.Type: GrantFiled: November 2, 2017Date of Patent: September 3, 2024Assignee: Modumetal, Inc.Inventor: Christina A. Lomasney
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Patent number: 11944451Abstract: Novel tools and techniques for assessing, predicting and/or estimating effectiveness of fluid resuscitation of a patient and/or an amount of fluid needed for effective resuscitation of the patient, in some cases, noninvasively.Type: GrantFiled: July 26, 2022Date of Patent: April 2, 2024Inventors: Isobel Jane Mulligan, Gregory Zlatko Grudic, Steven L. Moulton
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Patent number: 11858850Abstract: A high-strength zirconia-alumina composite ceramic substrate suitable for semiconductor devices has been invented. It is manufactured by a procedure starting with mixing powder formula of alumina, zirconia, and a self-made synthetic additive for ball milling in an organic solvent at room temperature. The resulting mixture is homogenously dispersed and is then subjected to the steps of slurry preparation, degassing, green embryo forming, punching, calculation, and sintering to yield the final composite ceramic substrate with an excellent mechanical property of three-point bending strength>600 MPa and superior thermoelectric properties of thermal conductivity>26 W/mK, insulation resistance>1014 ?·cm and surface leakage current (150° C.)<200 nA.Type: GrantFiled: July 14, 2020Date of Patent: January 2, 2024Assignee: LEATEC FINE CERAMICS CO., LTD.Inventors: Chih-Hung Chu, Jui-Kai Wang
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Patent number: 11719664Abstract: A multimodal sensor of high sensitivity and high selectivity using multifunctional three-dimensional nanostructure having electric and optical sensing ability and a method thereof are provided. The method includes forming multi-layered nanowires including a multifunctional material, transferring the nanowires to a plurality of layers onto a target substrate to form the three-dimensional nanostructure, heat-treating the three-dimensional nanostructure, and forming electrode layers at the three-dimensional nanostructure.Type: GrantFiled: August 27, 2019Date of Patent: August 8, 2023Assignee: Korea Advanced Institute of Science and TechnologyInventors: Yeon Sik Jung, Hyeuk Jin Han, Seunghee Cho, Gyurac Lee
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Patent number: 11614394Abstract: A method for estimating characteristics of a ceramic fired body, the method including: preparing a ceramic fired body by firing a formed green body; measuring a color of the ceramic fired body; and with use of a correlation between the color and at least one characteristic selected from a group consisting of a porosity, a pore diameter, and a thermal expansion coefficient previously determined for a ceramic fired body having a same composition as that of the ceramic fired body, estimating the at least one characteristic of the ceramic fired body from the color of the ceramic fired body, measured in the previous step.Type: GrantFiled: February 10, 2020Date of Patent: March 28, 2023Assignee: NGK Insulators, Ltd.Inventor: Daniel Yukichi Kitaguchi
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Patent number: 11564314Abstract: A sintered body includes a crystal grain containing silicon nitride, and a grain boundary phase. If dielectric losses of the sintered body are measured while applying an alternating voltage to the sintered body and continuously changing a frequency of the alternating voltage from 50 Hz to 1 MHz, an average value ?A of dielectric losses of the sintered body in a frequency band from 800 kHz to 1 MHz and an average value ?B of dielectric losses of the sintered body in a frequency band from 100 Hz to 200 Hz satisfy an expression |?A??B|?0.1.Type: GrantFiled: October 15, 2019Date of Patent: January 24, 2023Assignees: Kabushiki Kaisha Toshiba, Toshiba Materials Co., Ltd.Inventors: Jun Momma, Katsuyuki Aoki, Satoshi Takahashi
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Patent number: 11492294Abstract: A method includes molding a raw material powder containing a ceramic powder and a thermoplastic resin having a glass transition temperature higher than room temperature into a shape by isostatic pressing and in which a raw material powder slurry is prepared by adding the ceramic powder and the thermoplastic resin to a solvent so that the thermoplastic resin is 2% by weight or more and 40% by weight or less with respect to a total weight of the ceramic powder and the thermoplastic resin, a cast-molded body is to formed by wet-casting the raw material powder slurry into a shape, dried, and subjected to first-stage isostatic press molding at a temperature lower than the glass transition temperature of the thermoplastic resin, then this first-stage press-molded body is heated to the glass transition temperature of the thermoplastic resin or above, and warm isostatic press (WIP) molding is performed.Type: GrantFiled: May 10, 2019Date of Patent: November 8, 2022Assignee: SHIN-ETSU CHEMICAL CO., LTD.Inventors: Masanori Ikari, Takuto Matsumoto
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Patent number: 10981346Abstract: This document describes systems and processes for forming improved synthetic molded slabs suitable for use in living or working spaces (e.g., along a countertop, table, floor, or the like).Type: GrantFiled: March 21, 2019Date of Patent: April 20, 2021Assignee: Cambria Company LLCInventors: Jon Louis Grzeskowiak, II, Martin E. Davis
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Patent number: 10981293Abstract: This document describes systems and processes for forming synthetic molded slabs, which may be suitable for use in living or working spaces (e.g., along a countertop, table, floor, or the like).Type: GrantFiled: September 11, 2020Date of Patent: April 20, 2021Assignee: Cambria Company LLCInventors: Jon Louis Grzeskowiak, II, Martin E. Davis
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Patent number: 10773418Abstract: This document describes systems and processes for forming synthetic molded slabs, which may be suitable for use in living or working spaces (e.g., along a countertop, table, floor, or the like).Type: GrantFiled: March 21, 2019Date of Patent: September 15, 2020Assignee: Cambria Company LLCInventors: Jon Louis Grzeskowiak, II, Martin E. Davis
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Patent number: 10692653Abstract: The present disclosure provides a ceramic sintered body having a favorable dielectric constant. In some embodiments of the present disclosure, the ceramic sintered body includes a semiconductor ceramic phase dispersed in a dielectric ceramic phase, wherein the semiconductor ceramic phase and the dielectric ceramic phase jointly form a percolative composite, and a volume fraction of the semiconductor ceramic phase is close to and less than a percolation threshold.Type: GrantFiled: October 27, 2017Date of Patent: June 23, 2020Assignee: YAGEO CORPORATIONInventor: Masayuki Fujimoto
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Patent number: 9625335Abstract: A pressure measuring cell includes at least one ceramic measuring membrane body; and at least one ceramic platform, wherein the measuring membrane body is connected with the platform along an annular, peripheral joint. The joint is formed as a welded connection between the measuring membrane body and the platform, wherein the measuring membrane body has a pressure-dependently deformable measuring membrane. A pressure sensor includes a pressure measuring cell and a housing, wherein the pressure measuring cell is held by the housing, and wherein the pressure measuring cell closes a housing opening, through which the pressure measuring cell communicates with an environment of the housing. A seal is clamped between a sealing surface surrounding the opening of the housing and a sealing surface of the pressure measuring cell.Type: GrantFiled: February 10, 2012Date of Patent: April 18, 2017Assignee: ENDRESS + HAUSER GMBH + CO. KGInventors: Andrea Berlinger, Ulfert Drewes, Michael Philipps, Andreas Rossberg, Elke Schmidt
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Patent number: 9289923Abstract: This document describes systems and processes for forming synthetic molded slabs, which may be suitable for use in living or working spaces (e.g., along a countertop, table, floor, or the like).Type: GrantFiled: January 30, 2015Date of Patent: March 22, 2016Assignee: Cambria Company LLCInventors: Jon Louis Grzeskowiak, II, Martin E. Davis
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Publication number: 20150108697Abstract: A method for producing ferrite ceramic includes the steps of providing a ferrite powder; oven-drying the ferrite powder; adding organic additives into the oven-dried powder and mixing them to form a ferrite slurry; debubbling the ferrite slurry and then tape casting it into a green tape; heating the green tape in air to 300-500° C. for 5 h to remove the organic additives from the green tape; sintering the organic additives removed green tape at 900-1000° C. for 2-5 h to obtain ferrite ceramic.Type: ApplicationFiled: September 15, 2014Publication date: April 23, 2015Applicant: AAC TECHNOLOGIES PTE. LTD.Inventors: Shaohua Su, Jinhui Yu
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Patent number: 8894920Abstract: A method for making a thin, free-standing ceramic sheet may include drawing a carrier film proximate a casting head and across a casting bed of a tape caster at a rate from about 2 cm/min to about 500 cm/min. Depositing a thin film of ceramic slip less than about 150 ?m on the carrier film with the casting head. The ceramic slip may comprises a ceramic powder with an ultimate crystallite size of less than about 10 ?m dispersed in a fluid vehicle such that the ceramic slip has a ceramic solids fraction of greater than about 20% by volume. The deposited ceramic slip may be dried on the carrier film thereby forming a green ceramic sheet on the carrier film. After the green ceramic sheet is dried, the green ceramic sheet may be sintered.Type: GrantFiled: October 29, 2009Date of Patent: November 25, 2014Assignee: Corning IncorporatedInventors: Lanrik Kester, Thomas Dale Ketcham, Brian Scott Kirk, Dell Joseph St Julien
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Publication number: 20140342237Abstract: Disclosed are a separator for an electrochemical device substantially comprising inorganic particles to provide an excellent mechanical strength, an electrochemical device comprising the same, and a method of manufacturing the separator using a high internal phase emulsion (RIPE).Type: ApplicationFiled: July 31, 2014Publication date: November 20, 2014Inventors: Jin-Woo Kim, Joo-Sung Lee, Jong-Hun Kim
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Publication number: 20140328747Abstract: Provided is a zinc oxide sputtering target, which can effectively suppress the occurrence of break or crack in the target during sputtering to enable production of a zinc oxide transparent conductive film with high productivity. The zinc oxide sputtering target is composed of a zinc oxide sintered body comprising zinc oxide crystal grains, wherein the zinc oxide sputtering target has a sputter surface having a (100) crystal orientation degree of 50% or more.Type: ApplicationFiled: June 16, 2014Publication date: November 6, 2014Inventors: Jun YOSHIKAWA, Katsuhiro IMAI, Koichi KONDO
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Patent number: 8801935Abstract: A process for preparing a reverse osmosis membrane that includes: (A) providing a polyamine, a polyfunctional acid halide, and a flux increasing additive having the formula Z+B? where Z+ is an easily dissociable cation and B? is a beta-diketonate; (B) combining the polyamine, polyfunctional acid halide, and flux increasing additive on the surface of a porous support membrane; and (C) interfacially polymerizing the polyamine and the polyfunctional acid halide, and flux increasing additive on the surface of the porous support membrane to form a reverse osmosis membrane comprising (i) the porous support membrane and (ii) a discrimination layer comprising a polyamide. The reverse osmosis membrane is characterized by a flux that is greater than the flux of the same membrane prepared in the absence of the flux increasing additive.Type: GrantFiled: November 10, 2011Date of Patent: August 12, 2014Assignee: NanoH2O, Inc.Inventors: Jeffrey Alan Koehler, Christopher James Kurth
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Patent number: 8753558Abstract: A method of forming a shaped abrasive particle includes extruding a mixture into an opening in a screen within an application zone and translating the screen and belt to a release zone and separating the screen and belt to form a precursor shaped abrasive particle on the belt, wherein the screen and belt are separated at a release angle of at least about 15° and not greater than about 45°, wherein the release angle is defined as an angle between a surface of the screen and a surface of the belt.Type: GrantFiled: December 31, 2012Date of Patent: June 17, 2014Assignee: Saint-Gobain Ceramics & Plastics, Inc.Inventor: Michael D. Kavanaugh
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Publication number: 20140066287Abstract: A sintered aluminum nitride substrate having a thermal conductivity of about 60 W/m-K to about 150 W/m-K, a flexural strength of about 200 MPa to about 325 MPa, a volume resistivity of greater than 1010 Ohm cm, a density of at least about 95% of theoretical, optionally at least 97%, and a reflectance factor of at least about 60% substantially over the wavelength range of 360 nm to 820 nm. A low temperature process for sintering aluminum nitride includes providing an AlN sintering formulation of AlN powder and a sintering aid of yttria, calcia, and optionally added alumina, forming the AlN sintering formulation into a green body, and sintering the green body at a temperature of about 1675° C. to 1750° C.Type: ApplicationFiled: March 13, 2013Publication date: March 6, 2014Inventors: Jonathan H. HARRIS, Thomas NEMECEK, Robert TESCH
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Patent number: 8652378Abstract: The present invention relates to rapid dissolve thin film drug delivery compositions for the oral administration of active components. The active components are provided as taste-masked or controlled-release coated particles uniformly distributed throughout the film composition. The compositions may be formed by wet casting methods, where the film is cast and controllably dried, or alternatively by an extrusion method.Type: GrantFiled: March 29, 2013Date of Patent: February 18, 2014Assignee: MonoSol Rx LLCInventors: Robert K. Yang, Richard C. Fuisz, Garry L. Myers, Joseph M. Fuisz
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Patent number: 8636945Abstract: A method for producing crystalline particles including a mixing step of producing a mixed material containing a lead-containing material and an additional material containing lithium and boron and a first firing step of firing the mixed material at a predetermined firing temperature to form polyhedral crystalline particles. The crystalline particles are used to produce a crystallographically oriented ceramic by preparing a template layer having uniform crystal orientation in a predetermined direction by fixing the crystalline particles on a substrate, forming a shaped body including a matrix layer arranged on the template layer, the matrix layer being composed of a mixed material that contains a lead-containing material and an additional material containing lithium and boron, and firing the shaped body.Type: GrantFiled: June 29, 2010Date of Patent: January 28, 2014Assignee: NGK Insulators, Ltd.Inventors: Takaaki Koizumi, Takuya Katsuno, Hideki Shimizu
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Publication number: 20140007936Abstract: Provided are a method for patterning a mesoporous inorganic oxide film, the method including a step of forming a mesoporous inorganic oxide film using a composition containing inorganic oxide particles; and a step of forming a pattern on the mesoporous inorganic oxide film using an elastic stamp for pattern formation, and then calcining the mesoporous inorganic oxide, and an electronic device including a mesoporous inorganic oxide film that has been patterned by the patterning method.Type: ApplicationFiled: July 3, 2013Publication date: January 9, 2014Inventors: EUN KYOUNG KIM, JONG HAK KIM, JEONG HUN KIM, JONG KWAN KOH, JONG BEOM NA, CHI HYUN PARK
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Patent number: 8617456Abstract: This invention describes a novel type of materials named by the inventors as Interface-Defined nano-Laminates (IDnL), and a new method for fabricating these materials from ceramic, metallic, and other powders. The laminate layer thickness in IDnL is smaller than that of ordinary laminates, but greater than that of superlattices. IDnL are fundamentally different from ordinary laminates in that their properties are defined by interfaces, and not by the properties of the bulk materials comprising individual layers. In contrast to superlattice materials, IDnL can be made thermally stable, due to the wide selection of interface-defining materials, which allows judicial use of equilibrium phase diagrams, and the “entropic stabilization” approach discovered by the authors; and in addition IDnL can be manufactured inexpensively in bulk, industrial quantities and large sizes by the techniques revealed in this invention. The degree of interface coherency in an IDnLs can be varied to optimize material properties.Type: GrantFiled: December 29, 2010Date of Patent: December 31, 2013Assignee: The United States of America as represented by the Secretary of the Air ForceInventors: Alexander Pechenik, Wesley P. Hoffman
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Patent number: 8609017Abstract: Electronically tunable dielectric materials having favorable properties are disclosed. The electronically tunable materials include an electronically tunable dielectric phase such as barium strontium titanate in combination with at least two additional metal oxide phases. The additional metal oxide phases may include, for example, oxides of Mg, Si, Ca, Zr, Ti and Al. The electronically tunable materials may be provided in bulk, thin film and thick film forms for use in devices such as phased array antennas, tunable filters and the like. The materials are useful in many applications, including the area of radio frequency engineering and design.Type: GrantFiled: February 17, 2007Date of Patent: December 17, 2013Assignee: BlackBerry LimitedInventors: Louise C. Sengupta, Xubai Zhang, Luna H. Chiu
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Patent number: 8597567Abstract: A ceramic sheet is produced by a method in which inorganic particles including, as a main component, an oxide represented by general formula ABO3 and containing a volatile component are mixed such that the A/B ratio is 1.05 or more, the inorganic particles are formed into a self-supported planar shaped body with a thickness of 30 ?m or less, and the shaped body is fired, without an inactive layer or with an inactive layer which does not substantially react with the shaped body and is disposed adjacent to the shaped body, at a temperature-rising rate of 30° C./min or more in a temperature range which is equal to or higher than a temperature at which the volatile component is volatilized.Type: GrantFiled: November 4, 2009Date of Patent: December 3, 2013Assignee: NGK Insulators, Ltd.Inventors: Shohei Yokoyama, Nobuyuki Kobayashi, Tsutomu Nanataki
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Patent number: 8586493Abstract: A silicon nitride sintered body, wherein in a silicon nitride substrate consisting of crystal grains of ?-type silicon nitride and a grain boundary phase containing at least one type of rare earth element (RE), magnesium (Mg) and silicon (Si), the grain boundary phase consists of an amorphous phase and a MgSiN2 crystal phase. The X-ray diffraction peak intensity of any crystal plane of a crystal phase containing the rare earth element (RE) is less than 0.0005 times the sum of the diffraction peak intensities of (110), (200), (101), (210), (201), (310), (320) and (002) of the crystal grains of the ?-type silicon nitride; and the X-ray diffraction peak intensity of (121) of the MgSiN2 crystal phase is 0.0005 to 0.003 times the sum of the X-ray diffraction peak intensities of (110), (200), (101), (210), (201), (310), (320) and (002) of the crystal grains of the ?-type silicon nitride.Type: GrantFiled: July 3, 2009Date of Patent: November 19, 2013Assignee: Hitachi Metals, Ltd.Inventors: Youichirou Kaga, Junichi Watanabe
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Patent number: 8562899Abstract: Electronically tunable dielectric materials having favorable properties are disclosed. The electronically tunable materials include an electronically tunable dielectric phase such as barium strontium titanate in combination with at least two additional metal oxide phases. The additional metal oxide phases may include, for example, oxides of Mg, Si, Ca, Zr, Ti and Al. The electronically tunable materials may be provided in bulk, thin film and thick film forms for use in devices such as phased array antennas, tunable filters and the like. The materials are useful in many applications, including the area of radio frequency engineering and design.Type: GrantFiled: October 16, 2003Date of Patent: October 22, 2013Assignee: Blackberry LimitedInventors: Louise C. Sengupta, Xubai Zhang, Luna H. Chiu
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Patent number: 8501080Abstract: A method for producing a crystallographically oriented ceramic including a preparation step of preparing a template layer having uniform crystal orientation in a predetermined direction, a formation step of forming a shaped body including a matrix layer arranged on the template layer, the matrix layer being composed of a mixed material that contains a lead-containing material and an additional material containing lithium and boron, and a firing step of firing the shaped body formed in the formation step at a predetermined firing temperature. Furthermore, after the firing step, a post-annealing step of heating the shaped body to remove lithium and boron may be included.Type: GrantFiled: June 29, 2010Date of Patent: August 6, 2013Assignee: NGK Insulators, Ltd.Inventors: Takaaki Koizumi, Takuya Katsuno
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Patent number: 8496870Abstract: This invention relates to a method of making lead-free piezoelectric ceramic films. Specifically, the invention is directed to a method for fabricating lead-free piezoelectric free standing films having enhanced piezoelectric properties. The films may be used for a number of applications including incorporation in microelectronic devices such as energy harvesting devices and sensor technologies.Type: GrantFiled: June 12, 2012Date of Patent: July 30, 2013Assignee: Drexel UniversityInventors: Wei-Heng Shih, Wan Y. Shih, Huidong Li
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Publication number: 20120288626Abstract: A self-replicating monolayer system employing polymerization of monomers or nanoparticle ensembles on a defined template provides synthesis of two-dimensional single molecule polymers. Systems of self-replicating monolayers are used as templates for growth of inorganic colloids. A preferred embodiment employs SAM-based replication, wherein an initial monolayer is patterned and used as a template for self-assembly of a second monolayer by molecular recognition. The second monolayer is polymerized in place and the monolayers are separated to form a replicate. Both may then function as templates for monolayer assemblies. A generic self-replicating monomer unit comprises a polymerizable moiety attached by methylene repeats to a recognition element and an ending unit that will not interfere with the chosen recognition chemistry. The recognition element is self-complementary, unless two replicating monomers with compatible cross-linking chemistry are employed.Type: ApplicationFiled: July 23, 2012Publication date: November 15, 2012Applicant: MASSACHUSETTS INSTITUTE OF TECHNOLOGYInventors: Joseph M. Jacobson, David W. Mosley
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Patent number: 8304133Abstract: The invention provides a method for producing a polymer electrolyte membrane including (A) a membrane formation step of forming a membrane-form product of an ionic group-containing polymer electrolyte on a support, (B) an acid treatment step of exchanging the ionic group into an acid type by bringing the membrane into contact with an inorganic acid-containing acidic liquid, (C) an acid removal step of removing a free acid in the acid-treated membrane, and (D) a drying step of drying the acid-removed membrane, wherein the steps (B) to (D) are carried out without separating the membrane from the support.Type: GrantFiled: December 26, 2007Date of Patent: November 6, 2012Assignee: Toyo Boseki Kabushiki KaishaInventors: Kousuke Sasai, Hiroki Yamaguchi, Yoshimitsu Sakaguchi, Kouta Kitamura, Masahiro Yamashita
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Patent number: 8277713Abstract: An implantable analyte sensor including a sensing region for measuring the analyte and a non-sensing region for immobilizing the sensor body in the host. The sensor is implanted in a precisely dimensioned pocket to stabilize the analyte sensor in vivo and enable measurement of the concentration of the analyte in the host before and after formation of a foreign body capsule around the sensor. The sensor further provides a transmitter for RF transmission through the sensor body, electronic circuitry, and a power source optimized for long-term use in the miniaturized sensor body.Type: GrantFiled: May 3, 2004Date of Patent: October 2, 2012Assignee: DexCom, Inc.Inventors: James R. Petisce, Mark Brister, Mark Shults, James H. Brauker, Paul V. Neale
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Patent number: 8241569Abstract: This invention relates to lead-free piezoelectric ceramic films and a method of making thereof. Specifically, the invention is directed to a method for fabricating lead-free piezoelectric free standing films having enhanced piezoelectric properties. The films may be used for a number of applications including incorporation in microelectronic devices such as energy harvesting devices and sensor technologies.Type: GrantFiled: November 20, 2008Date of Patent: August 14, 2012Assignee: Drexel UniversityInventors: Wei-Heng Shih, Wan Y. Shih, Huidong Li
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Patent number: 8236226Abstract: Methods for changing the shape of a surface of an article are disclosed. The methods may include providing a liquid polymer precursor, casting the precursor against a first tool assembly, curing the precursor to form a shape memory polymer substrate, deforming one or more surfaces of the substrate, and mobilizing the shape memory polymer to shift the deformed surface of the substrate from a deformed shape to a pre-set shape.Type: GrantFiled: April 22, 2011Date of Patent: August 7, 2012Assignee: 3M Innovative Properties CompanyInventors: Audrey A. Sherman, William J Bryan, Robert K. Galkiewicz, Mieczyslaw H. Mazurek, James R. Starkey, Wendi J. Winkler, Haiyan Zhang, Jeffrey M. Olofson
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Patent number: 8211345Abstract: This invention provides an optical film having a reduced thickness and an increased width, which is free from bleedout with the elapse of time (during storage) in a continuous wound state, a method for manufacturing an optical film, and a polarizing plate using the optical film. The optical film is a plasticizer-containing optical film having an overall width of 1500 mm to 4000 mm produced by a solution casting method. The amount of the plasticizer present in the center portion in the surface side of the optical film is determined as value A by TOF-SIMS. The amount of the plasticizer present in the center portion in the back side is determined as value B by the TOF-SIMS. Value X is determined by formula 1 based on the values A and B. The amount of the plasticizer present in the end portion in the surface side of the optical film is determined as value A? by TOF-SIMS, and the amount of the plasticizer present in the end portion of the back side is determined as value B? by the TOF-SIMS.Type: GrantFiled: July 12, 2007Date of Patent: July 3, 2012Assignee: Konica Minolta Opto, Inc.Inventor: Masahiro Shibuya
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Publication number: 20120135215Abstract: A free-standing zeolite membrane and a zeolite membrane supported on a support structure are disclosed. The free-standing zeolite membrane is fabricated by mixing zeolite particles and an optional inorganic binder, forming a green body, and sintering the green body at a sufficiently low temperature so as to prevent damage to the gas selectivity properties of the zeolite particles. The supported composite zeolite membrane is fabricated by mixing a sacrificial binder, an optional inorganic binder, boehmite sol and zeolite particles to form a slurry. The slurry is then coated onto a porous support structure, dried and sintered at a sufficiently low temperature so as to prevent damage to the gas selective properties of the zeolite particles. In both membranes, the zeolite particles span the entire thickness of the membrane to provide a high selectivity path for the flow of gas to pass therethrough.Type: ApplicationFiled: November 30, 2010Publication date: May 31, 2012Applicant: GENERAL ELECTRIC COMPANYInventors: Kevin Paul McEvoy, Hrishikesh Keshavan, Anthony Yu-Chung Ku, Steven Mitchell Kuznicki, Weizhu An, Lan Wu, Paul Donald Swenson
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Patent number: 8119554Abstract: Shaped bodies having catalytic properties which can be obtained by a process comprising the steps: a) production of a shaped body by means of a powder-based rapid prototyping process, b) if appropriate, a heat treatment of the shaped body, c) if appropriate, application of at least one catalytically active component to the shaped body, d) if appropriate, a further heat treatment, where steps b), c) and/or d) can be carried out a number of times, are used as reactor internals in heterogeneously catalyzed chemical reactions.Type: GrantFiled: September 26, 2008Date of Patent: February 21, 2012Assignee: BASF SEInventors: Nawid Kashani-Shirazi, Veronika Wloka, Wolfgang Gerlinger, Andrea Schmidt, Kerstin Heinen, Wolfgang Kollenberg
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Publication number: 20110176277Abstract: Provided are a silicon nitride substrate made of a silicon nitride sintered body that is high in strength and thermal conductivity, a method of producing the silicon nitride substrate, and a silicon nitride circuit substrate and a semiconductor module that use the silicon nitride substrate. According to the silicon nitride sintered body, in a silicon nitride substrate consisting of crystal grains 11 of ?-type silicon nitride and a grain boundary phase containing at least one type of rare earth element (RE), magnesium (Mg) and silicon (Si), the grain boundary phase consists of an amorphous phase 12 and a MgSiN2 crystal phase 13; the X-ray diffraction peak intensity of any crystal plane of a crystal phase containing the rare earth element (RE) is less than 0.0005 times the sum of the diffraction peak intensities of (110), (200), (101), (210), (201), (310), (320) and (002) of the crystal grains of the ?-type silicon nitride; and the X-ray diffraction peak intensity of (121) of the MgSiN2 crystal phase 13 is 0.Type: ApplicationFiled: July 3, 2009Publication date: July 21, 2011Applicant: HITACHI METALS, LTD.Inventors: Youichirou Kaga, Junichi Watanabe
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Patent number: 7947213Abstract: According to one aspect of the present invention the fuel cell device includes an electrolyte sheet. The electrolyte sheet has a substantially non-porous body of a varied thickness, a relatively smooth surface and a more textured surface with multiple indentations therein, wherein the thickest part of the electrolyte sheet is at least 0.5 micrometers greater than the thinnest part of said electrolyte sheet. The side of the electrolyte sheet with a relatively smooth surface is subjected to the predominately tensile force and the other, more textured surface subjected to predominately compressive force. According to one embodiment, the fuel cell also includes one cathode disposed on the more textured side of said electrolyte sheet at least at least one anode disposed opposite the cathode on the relatively smooth side of aid electrolyte sheet. According to one embodiment, the relatively smooth side of the electrolyte sheet is the fuel facing side and the more textured side is the air-facing side.Type: GrantFiled: July 3, 2007Date of Patent: May 24, 2011Assignee: Corning IncorporatedInventors: Michael E. Badding, Jacqueline L. Brown, Sean M. Garner, Thomas D. Ketcham, Dell J. St. Julien
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Patent number: 7866487Abstract: The problem addressed by this invention is to provide an aromatic polyamide porous film excellent in the capability of being thinned and capable of easily exhibiting stable porosity properties even if it is used for a long period of time at high temperature. This invention can be achieved by an aromatic polyamide porous film that contains an aromatic polyamide as a main component and is such that when an atomic force microscope is used to measure a range of S ?m2 at least on one surface, the sectional area S(10) ?m2 obtained at a depth of 10 nm from the surface and the sectional area S(20) ?m2 obtained at a depth of 20 nm from the surface satisfy the following formulae simultaneously. 0.01?S(10)/S?0.Type: GrantFiled: November 29, 2005Date of Patent: January 11, 2011Assignee: Toray Industries, Inc.Inventors: Masanori Sueoka, Kenta Nishihara, Akimitsu Tsukuda
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Patent number: 7799267Abstract: The disclosed invention relates to a method of manufacture of transparent ceramics such as yttrium aluminum garnet by tape casting. The method entails forming a mixture of ceramic oxide, dispersant and organic solvent, milling the mixture to produce a first slurry, mixing the first slurry with an organic binder and a plasticizer to form a treated slurry, milling the treated slurry to produce milled slurry, tape casting the milled slurry to produce cast tape, drying the cast tape to produce dried tape, stacking portions of dried tape to form an assembly, compressing the assembly to produce a preform, heating the preform to produce a green preform, and sintering the green preform to produce transparent yttrium aluminum garnet. The method may be used to produce a unitary ceramic product having differing transparent sections as well as transparent ceramic product having a dopant gradient across a portion of the thickness of the product.Type: GrantFiled: September 11, 2008Date of Patent: September 21, 2010Assignee: The Penn State Research FoundationInventors: Gary L. Messing, Elizabeth R. Kupp, Sang-Ho Lee, Garnia Y. Juwondo, Adam J. Stevenson
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Patent number: 7794557Abstract: A precursor tape casting method is one in which chemical precursors are converted into a final chemical phase from green tapes to products. Because chemical precursors are employed rather than the final powder materials, sintering is not required to form the material. Lower annealing temperatures instead of high temperature sintering allow the formation of grains of about 1 to about 100 nanometers in the final material. In addition, when the final material is a magnetic/insulator composite, improved magnetic properties may be obtained.Type: GrantFiled: June 10, 2005Date of Patent: September 14, 2010Assignee: Inframat CorporationInventors: Shiqiang Hui, Yide Zhang, Danny Xiao, Mingzhong Wu
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Publication number: 20100194005Abstract: During the manufacture of slabs with a veined effect a liquid or powder colouring agent is deposited on the surface of a thin layer of starting mixture by means of at least one dispensing device (40) and the resultant mixture is supplied, falling freely, from one end of an extractor belt (30) forming the bottom of a mixture metering/distributor unit, following which the mixture is transferred, falling freely, onto a temporary moulding support (14). This results in the production of slabs provided with veining extending through the entire thickness of the slabs and also visible along the whole edge of the slab, even after it has been machined.Type: ApplicationFiled: July 4, 2008Publication date: August 5, 2010Inventor: Luca Toncelli
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Patent number: 7754115Abstract: A ceramo-ceramic dental prosthesis is made from a patient's negative mandibular impression, including at least one working cavity having an inner surface matching the lower surface of the prosthesis to be produced and left at least by one tooth primed by the dental surgeon to be prosthetized. The method of making the prosthesis includes a step of providing a single-unit wax model used for producing by precision casting a single-unit metal model on which is mounted, by the dental technician, a ceramic, the single-unit model having previously been coated with a stripping product to avoid the adherence of the ceramic on the metal single-unit model after the ceramic is cured on the single-unit metal model.Type: GrantFiled: March 31, 2006Date of Patent: July 13, 2010Inventor: Germinal Veyrat
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Patent number: 7730808Abstract: Ceramic blades and fabrication methods thereof. A ceramic blade comprises a ceramic body having two sides and an edge. A coating layer is applied on the two sides and the edge, wherein the ceramic body is formed using a scraper to create substantially flat surface and to prevent residual stress damage.Type: GrantFiled: June 10, 2005Date of Patent: June 8, 2010Assignee: Industrial Technology Research InstituteInventors: Kuo-Chuang Chiu, Ren-Der Jean, Chuan-Lung Lu
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Patent number: 7695559Abstract: A cement suspension includes the following, in relation to the cement material: water (22-35% by weight); acetic acid (1-10% by weight); plasticizer (up to 8% by weight); and dispersant agent (0-2% by weight), having an apparent viscosity of 0.5-2 Pa·s for the casting speed gradient. Pieces of cement that are prepared from the suspension and which can be used as electronic components are also disclosed.Type: GrantFiled: April 28, 2005Date of Patent: April 13, 2010Assignees: Centre National de la Recherche Scientifique (C.N.R.S.), Ecole Nationale Superieure de Ceramique Industrielle (ENSCI)Inventors: Thierry Chartier, Youssef El Hafiane, Agnes Smith, Jean-Pierre Bonnet
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Patent number: 7666268Abstract: A coating material, green sheet and the method capable of producing a green sheet without a pin hole, having enough strength to be peeled from a support body and excellent surface smoothness even when the green sheet is extremely thin, and being suitable to make an electronic device thin and multilayered, are provided. The present invention provides a green sheet coating material comprising a ceramic powder, a binder resin including a butyral based resin as a main component thereof, and a solvent. The solvent includes a first solvent having an SP value as a solubility parameter of 10 or larger and a second solvent having the SP value of 8 or larger but smaller than 10. The second solvent is included by 20 to 60 wt % and, preferably, 25 to 60 wt % with respect to 100 wt % of the solvent as the entire weight.Type: GrantFiled: August 26, 2004Date of Patent: February 23, 2010Assignee: TDK CorporationInventors: Hisashi Kobayashi, Shigeki Satou
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Patent number: 7655180Abstract: A method for controlling the shrinkage of ceramic formed bodies is provided, including performing a preliminary test to determine an average shrinkage of ceramic formed bodies made from test lots of a ceramic powder, and determining a linear correlation between the average shrinkage and measured amounts of the ground test lots removed from a ball mill during a specific milling time interval. A batch of the ceramic powder is then ground, an amount of the ground ceramic powder removed from the ball mill during the specific time interval is measured, and the linear correlation is used to estimate the shrinkage of a ceramic body made therefrom. The difference between a target shrinkage and the estimated shrinkage is determined, and one or more of the processing conditions used to form the ceramic body are changed to offset the difference.Type: GrantFiled: July 15, 2005Date of Patent: February 2, 2010Assignee: NGK Insulators, Ltd.Inventors: Yukihisa Takeuchi, Tsutomu Nanataki, Koichi Iwata, Katsuyuki Takeuchi, Takuji Kimura
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Patent number: 7595019Abstract: Method of making an electrochemical device for the recovery of oxygen from an oxygen-containing feed gas comprising (a) preparing a green electrochemical device by assembling a green electrolyte layer, a green anode layer in contact with the green electrolyte layer, a green cathode layer in contact with the green electrolyte layer, a green anode-side gas collection interconnect layer in contact with the green anode layer, and a green cathode-side feed gas distribution interconnect layer in contact with the green cathode layer; and (b) sintering-the green electrochemical device by heating to yield a sintered electrochemical device comprising a plurality of sintered layers including a sintered anode-side gas collection interconnect layer in contact with the anode layer and adapted to collect oxygen permeate gas, wherein each sintered layer is bonded to an adjacent sintered layer during sintering.Type: GrantFiled: March 1, 2005Date of Patent: September 29, 2009Assignee: Air Products and Chemicals, Inc.Inventors: Raymond Ashton Cutler, Kent Neal Hutchings, Merrill Anderson Wilson, Ronald Almy Hollis, Dale M. Taylor