Producing Metal Oxide Containing Product Patents (Class 264/681)
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Patent number: 7597866Abstract: The present invention provides a lutetium oxide sinter to which yttrium is added in an amount of 100 mass ppm to 7000 mass ppm, whose average particle size is from 0.7 to 20 ?m, and with which there is no precipitation of a hetero phase containing yttrium at the grain boundary.Type: GrantFiled: September 28, 2004Date of Patent: October 6, 2009Assignee: Konoshima Chemical Co., Ltd.Inventors: Shunsuke Hosokawa, Hideki Yagi, Takagimi Yanagitani
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Patent number: 7585486Abstract: The present invention relates to high-purity niobium monoxide powder (NbO) produced by a process of combining a mixture of higher niobium oxides and niobium metal powder or granules; heating and reacting the compacted mixture under controlled atmosphere to achieve temperature greater than about 1945° C., at which temperature the NbO is liquid; solidifying the liquid NbO to form a body of material; and fragmenting the body to form NbO particles suitable for application as capacitor anodes. The NbO product is unusually pure in composition and crystallography, and can be used for capacitors and for other electronic applications. The method of production of the NbO is robust, does not require high-purity feedstock, and can reclaim value from waste streams associated with the processing of NbO electronic components. The method of production also can be used to make high-purity NbO2 and mixtures of niobium metal/niobium monoxide and niobium monoxide/niobium dioxide.Type: GrantFiled: May 24, 2007Date of Patent: September 8, 2009Assignee: Reading Alloys, Inc.Inventors: Charles A. Motchenbacher, James W. Robison, Brian J. Higgins, Thomas J. Fonville
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Publication number: 20090218735Abstract: The present invention relates to producing ceramic targets, which serves as a material source for magnetron, electron-beam, ion-beam and other film applying methods in micro-, opto-, nano-electronics. The aim of the proposed invention is to reduce the doping level of ceramics by non-controllable impurities, to increase a ceramic density and to improve performance characteristics of ceramic targets. In the method for synthesizing the ceramics doped by a low-melting metal consisting in that a mixture of components is pressed and sintered; as a doping additive, the mixture of components contains a low-melting metal and the surface of the main component particles is covered and moistened prior to pressing by the doping metal layer by grinding the mixture of the components. The grinding can be carried out at a melting temperature of the low-melting metal.Type: ApplicationFiled: August 16, 2005Publication date: September 3, 2009Applicant: OTKRYTOE AKTSYONERNOE OBSHCHESTVO "POLEMA"Inventors: Aslan Khajimuratovich Abduev, Abil Shamsudinovich Asvarov, Akhmed Kadievich Akhmedov, Ibragimkhan Kamilovich Kamilov
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Publication number: 20090221416Abstract: In one aspect, a molding compound for producing a refractory lining, especially for a combustion chamber of a stationary gas turbine is provided. The molding compound comprises, in weight percent, more than approximately 50% of aluminum oxide and, in weight percent, less than approximately 50% of aluminum silicate.Type: ApplicationFiled: June 30, 2006Publication date: September 3, 2009Inventors: Holger Grote, Wolfgang Kollenberg, Dieter Nikolay, Marc Tertilt
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Publication number: 20090211903Abstract: Disclosed are an indium (In) zinc (Zn) oxide based sputtering target, a method of manufacturing the same, and an In Zn oxide based thin film deposited using the In Zn oxide based sputtering target. The In Zn oxide based sputtering target has a composition of (MO2)x(In2O3)y(ZnO)z, in which x:y is about 1:0.01 to 1:1, y:z is about 1:0.1 to 1:10, and M is at least one metal selected from a group consisting of hafnium (Hf), zirconium (Zr), and titanium (Ti).Type: ApplicationFiled: February 25, 2009Publication date: August 27, 2009Inventors: Yoon-Gyu LEE, Jin-Ho LEE, Yil-Hwan YOU, Ju-Ok PARK
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Publication number: 20090215609Abstract: The inventive sintered product is produced from an initial feedstock having a zirconium content ranging from 75 to 99% and the following average chemical weight composition, in percentage by weight, based on oxides: 60 %=ZrO2+HfO2=75%, 27%=SiO2=34%, 0.2=TiO2=1.5 %, 0.3<Y2O3=3.5 %, other oxides:=1%, to give a total of 100%. Said product can be used for glassworks.Type: ApplicationFiled: March 31, 2006Publication date: August 27, 2009Applicant: SAINT GOBAIN CENTRE DE RECHERCHES ET D'ETUDES EUROPEENInventors: Michel Gaubil, Yves Boussant-Roux, Charles McGarry, Isabelle Cabodi, Olivier Citti
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ZINC OXIDE BASED SPUTTERING TARGET, METHOD OF MANUFACTURING THE SAME, AND ZINC OXIDE BASED THIN FILM
Publication number: 20090211904Abstract: Disclosed are a zinc (Zn) oxide based sputtering target, a method of manufacturing the same, and a Zn oxide based thin film deposited using the Zn oxide based sputtering target. The Zn oxide based sputtering target has a composition of InxHoyO3(ZnO)T, in which x+y=2, x:y is about 1:0.001 to 1:1, and T is about 0.1 to 5.Type: ApplicationFiled: February 26, 2009Publication date: August 27, 2009Inventors: Yoon-Gyu Lee, Jin-Ho Lee, Yil-Hwan You, Ju-Ok Park -
Patent number: 7576035Abstract: A pillar-shaped honeycomb structure has a plurality of cells longitudinally placed in parallel with one another with a wall portion therebetween, wherein the honeycomb structure mainly includes inorganic fibers which form the honeycomb structure without lamination interfaces.Type: GrantFiled: April 7, 2008Date of Patent: August 18, 2009Assignee: Ibiden Co., Ltd.Inventors: Kazushige Ohno, Tomokazu Oya
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Publication number: 20090183995Abstract: A ceramic material (20, 20A, 20B, 20C, 20C?, 20D, 20E, 20E1, 20E2, 20E3, 20E4, 20F) comprises a structural mass made of at least one refractory compound selected from refractory borides, aluminides and oxycompounds, and combinations thereof. This structural mass has an open microporosity that is impregnated with colloidal and/or polymeric particles of iron oxide and/or a precursor of iron oxide. These particles promote wetting of the structural mass by molten aluminum and/or form upon heat treatment a sintered barrier against oxygen diffusion through the structural mass. The ceramic material can be used on cathodes (15), carbon or metal-based anodes (5,5,?), sidewalls (16) and other parts (26) of aluminum electrowinning cells, on electrodes (15A) of arc furnaces, and on stirrers (10) or vessels (45) of aluminum purification apparatus.Type: ApplicationFiled: January 7, 2005Publication date: July 23, 2009Inventors: Thinh T. Nguyen, Vittorio De Nora
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Publication number: 20090160108Abstract: The present invention relates to refractory articles in general having improved surface properties. The objective of the invention is to propose an improvement of the refractory articles comprised of a fused silica matrix which will overcome the some of the defects while keeping the excellent known properties of the fused silica matrix. This objective is reached when a sintered ceramic phase is present in the porosity of at least a portion of at least a surface of the matrix. The present invention also relates to a process for producing such an article.Type: ApplicationFiled: May 14, 2007Publication date: June 25, 2009Applicant: VESUVIUS CRUCIBLE COMPANYInventors: Nathalie Niveau, Gilbert Rancoule
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Publication number: 20090148772Abstract: The present invention provides a lithium-containing composite oxide for a positive electrode for a lithium secondary battery, which has a large volume capacity density and high safety, and excellent durability for charge and discharge cycles and charge and discharge rate property, and its production method. The lithium-containing composite oxide is represented by the general formula LipNxMyOzFa (where N is at least one element selected from the group consisting of Co, Mn and Ni, M is at least one element selected from the group consisting of Al, Sn, alkaline earth metal elements and transition metal elements other than Co, Mn and Ni, 0.9?p?1.2, 0.965?x<2.00, 0<y?0.035, 1.9?z?4.2, and 0?a?0.Type: ApplicationFiled: February 10, 2009Publication date: June 11, 2009Applicant: AGC Seimi Chemical Co., Ltd.Inventors: Takeshi KAWASATO, Kazushige Horichi, Megumi Uchida, Takuya Mihara, Naoshi Saito
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Publication number: 20090139877Abstract: Disclosed herein is a composition for use in a NOx electrode comprising: Tb(1-x)Ln(x)E(1-y)Q(y1)X(y2)Z(y3)O3 wherein Ln is a lanthanoid or a combination of lanthanoids, E is a metal selected from chromium, iron, and a combination thereof, Q is an element selected from magnesium, calcium, strontium, and a combination thereof, X is an element selected from boron, lead, phosphorus, germanium, and a combination thereof, Z is an element selected from barium, silicon, aluminum, and a combination thereof, x is from 0 to about 0.5, y is from about 0.05 to about 0.8, and y1, y2, y3 are independently from 0 to about 0.8, with the proviso that y=y1+y2+y3, and y2+y3 is greater than 0. Also disclosed are a method of making it, electrodes and sensors comprising it, and a method of detecting NOx.Type: ApplicationFiled: November 30, 2007Publication date: June 4, 2009Inventors: Da Yu Wang, Sheng Yao, Elizabeth Briggs, Raymond L. Bloink, David D. Cabush
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Publication number: 20090114886Abstract: A fired material including at least one metal atom selected from indium, zinc and tin, at least one alkali metal atom selected from cesium, potassium and lithium, and an oxygen atom, wherein the atomic ratio (alkali metal atom)/(metal atom+alkali metal atom) is 0.1 to 80 at. %.Type: ApplicationFiled: November 17, 2006Publication date: May 7, 2009Inventors: Shigekazu Tomai, Satoshi Umeno
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Patent number: 7521389Abstract: A precursor composition for the production of granulated ceramic material, particularly for ceramic proppants, comprises 20 to 55% by weight of magnesium orthosilicate, 20 to 35% by weight of MgO, and 2.5 to 11% by weight of Fe2O3. The resulting lightweight proppant material shows high mechanical strength. To further decrease the specific density of the proppant, the formation of small pores can be increased by adding 0.3 to 2.4% carbon as a gas-forming agent.Type: GrantFiled: June 29, 2007Date of Patent: April 21, 2009Assignee: Ilem Research and Development EstablishmentInventors: Sergey Shmotev, Sergey Pliner
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Nanocrystalline sintered bodies made from alpha aluminum oxide method for production and use thereof
Publication number: 20090098365Abstract: Nanocrystalline sintered bodies, and a method of making same, said sintered bodies based on a 95 to 100% content of alpha-aluminum oxide by weight, a Vickers hardness greater than or equal to 17.5 GPa, and a crystal structure where the average primary crystal size of the alpha-aluminum oxide is less than or equal to 100 nanometers.Type: ApplicationFiled: July 12, 2006Publication date: April 16, 2009Applicant: Center for Abrasives and Refractories Research & Developement C.A.R.R.D. GmbHInventor: Paul Moeltgen -
Publication number: 20090081100Abstract: After synthesizing particles by liquid phase synthesis, the solution is substituted without drying these particles, and here, a solution comprising a grain boundary phase composition consisting of at least one or more types selected from a group consisting of Al2O3, yttrium oxide, silicon oxide, yttrium-silicon complex oxide, aluminum-silicon complex oxide, and a compound having a garnet structure with a lower melting point than the aforementioned particles, or a solution comprising a precipitate is introduced. Microparticles are adjusted by allowing adhesion and growth of the solution comprising a composition of grain boundary phase or the solution comprising a precipitate on the surface of the particles; these microparticles are allowed to align in 3-dimensions in solution and are formed into a molded body, and this molded body is sintered.Type: ApplicationFiled: March 29, 2006Publication date: March 26, 2009Applicant: FUJIFILM CORPORATIONInventors: Masayuki Suzuki, Tomotake Ikada
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Patent number: 7504351Abstract: Provided are an ITO sputtering target wherein the number of particles having a grain diameter of 100 nm or greater exposed in the ITO sputtering target as a result of royal water etching or sputter etching is 1 particle/?m2, and an ITO sputtering target having a density of 7.12 g/cm3 or greater capable of improving the sputtering performance, in particular inhibiting the generation of arcing, suppressing the generation of defects in the ITO film caused by such arcing, and thereby effectively inhibiting the deterioration of the ITO film.Type: GrantFiled: August 4, 2004Date of Patent: March 17, 2009Assignee: Nippon Mining & Metals Co., Ltd.Inventor: Toshiya Kurihara
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Publication number: 20090066221Abstract: A conversion element (3) comprising a ceramic material (31) with a multiplicity of pores (32) provided for at least the partial absorption of at least one primary radiation (52) and for transforming the primary radiation (52) into at least one secondary radiation (53), wherein the conversion element (3) has a density greater than or equal to 97% of the theoretical solid-state density of the ceramic material (31), and the pores (32) in the conversion element (3) have a diameter substantially between 200 nm and 5000 nm.Type: ApplicationFiled: March 13, 2007Publication date: March 12, 2009Applicant: KONINKLIJKE PHILIPS ELECTRONICS N.V.Inventors: Peter Schmidt, Hans-Helmut Bechtel, Wolfgang Busselt, Baby-Seriyati Schreinemacher
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Patent number: 7481963Abstract: A method for reducing the loss of magnesium during the sintering of aluminum oxide articles, such as ceramic discharge vessels for lighting applications. Magnesium oxide is added to aluminum oxide articles to control grain growth during sintering, but the sintering causes magnesium loss from the article. In order to address this problem, one or more aluminum oxide articles that are enriched in magnesium oxide are added to the sintering furnace to stem the loss of magnesium oxide in the remaining articles. The enriched aluminum oxide article is made by soaking a porous aluminum oxide article in an aqueous solution of magnesium nitrate and heating the porous article to convert the magnesium nitrate to magnesium oxide. The enriched articles may then be added in one or several locations to the sintering furnace, where the magnesium from the enriched articles is released to suppress the magnesium loss.Type: GrantFiled: June 28, 2005Date of Patent: January 27, 2009Assignee: Osram Sylvania Inc.Inventors: Jeffrey T. Neil, Victor E. Perez, Timothy J. Horton
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Patent number: 7431808Abstract: An electrically conductive titanium dioxide sputter target with an electrical resistivity of less than 5 ?-cm, which contains as an additive at least one doping agent or a mixture of doping agents in an amount of less than 5 mole %. The doping agent or agents are selected from the group including indium oxide, zinc oxide, bismuth oxide, aluminum oxide, gallium oxide, antimony oxide, and zirconium oxide. This treatment renders the titanium dioxide sputter target suitable for use in a direct-current sputtering process without any negative effects on the properties of the coating.Type: GrantFiled: August 19, 2002Date of Patent: October 7, 2008Assignee: W.C. Heraeus GmbH & Co., KGInventors: Markus Schultheis, Christoph Simons, Martin Weigert
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Patent number: 7429350Abstract: The invention relates to a composite target in the form of a bar made of ceramic powders and designed to be evaporated under an electron beam, the target comprising zirconia and at least one zirconia stabilizer. In characteristic manner, said target is wherein said zirconia stabilizer is at a molar content lying in the range 2% to 30% and wherein said zirconia is formed by more than 90% of a monoclinic phase. The invention is applicable to fabricating a ceramic thermal barrier of low thermal conductivity and high thermomechanical strength formed by evaporation under an electron beam.Type: GrantFiled: December 10, 2007Date of Patent: September 30, 2008Assignees: SNECMA, SNECMA ServicesInventors: Bertrand Saint-Ramond, Andre Malie, Christophe Chaput, Isabelle Porte, Cyrille Delage
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Publication number: 20080233406Abstract: A translucent ceramic having a high linear transmittance and a high refractive index, substantially not causing double refraction, and exhibiting a high anomalous dispersion has a pyrochlore compound represented by the general formula AxByOw (wherein 1.00?x/y?1.10 and w represents a positive number maintaining electroneutrality) as a main component. The main component has a cubic crystal system. Preferably, the A site comprises a trivalent metallic element, and the B site comprises a tetravalent metallic element. More preferably, A is at least one of La, Y, Gd, Yb, and Lu, and B is of at least one of Ti, Sn, Zr, and Hf. The translucent ceramic is useful as a material of, for example, an objective lens used in an optical pickup.Type: ApplicationFiled: May 9, 2008Publication date: September 25, 2008Applicant: MURATA MANUFACTURING CO., LTD.Inventor: Takeshi Hayashi
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Publication number: 20080224366Abstract: A composite material includes polyimide material, a particulate metal oxide dispersed in the polyimide material in an amount between about 0.1 wt % and about 20.0 wt %, and a carbonaceous material dispersed in the polyimide material in an amount between about 0.0 wt % and about 45.0 wt %.Type: ApplicationFiled: December 31, 2007Publication date: September 18, 2008Applicant: SAINT-GOBAIN PERFORMANCE PLASTICS CORPORATIONInventors: Gwo S. Swei, Ilya L. Rushkin, David Worth House, Pawel Czubarow
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Publication number: 20080226894Abstract: There is provided an yttrium oxide-containing material with excellent mechanical characteristics. The yttrium oxide-containing material becomes strong by adding silicon carbide (SiC) and yttrium fluoride (YF3) to yttrium oxide (Y2O3), and yield, handling, reliability can be improved accordingly when this strengthened yttrium oxide-containing material is applied to components of semiconductor manufacturing equipment.Type: ApplicationFiled: March 7, 2008Publication date: September 18, 2008Applicants: NGK INSULATORS, LTD., NAGAOKA UNIVERSITY OF TECHNOLOGYInventors: Yoshimasa KOBAYASHI, Yuji Katsuda, Hiroaki Sakai, Koichi Niihara, Tadachika Nakayama
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Patent number: 7425284Abstract: The purpose of the invention is a process for making a solid part designed to form all or part of an anode for the production of aluminium by fused bath electrolysis, containing a cermet formed from at least one metallic oxide such as a mixed oxide with spinel structure, and at least one metallic phase, in which a mixed oxide is used containing a metal R in the form of a cation in its chemical structure, the said metal R being fully or partly reducible by a reduction operation during the manufacturing process, so as to form all or part of the said metallic phase. This process can provide a cermet with a uniform distribution of fine metallic particles.Type: GrantFiled: October 5, 2004Date of Patent: September 16, 2008Assignee: Aluminum PechineyInventors: Philippe Tailhades, Abel Rousset, Armand Gabriel, Véronique Laurent, Valérie Baco-Carles, Airy-Pierre Lamaze
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Patent number: 7332695Abstract: A carbon heating element having an arbitrary specific resistance and an arbitrary shape which are arbitrary necessary as a heating element, and a method of producing the same. The carbon heating element is obtained by uniformly dispersing one or at least two metal or metalloid compounds into a composition having shapability and showing a high yield of a carbon residue after firing, shaping the dispersed material-containing mixture thus obtained, and firing the shaped material under a nonoxidizing atmosphere.Type: GrantFiled: August 27, 2003Date of Patent: February 19, 2008Assignee: Mitsubishi Pencil Co., Ltd.Inventors: Yoshihisa Suda, Osamu Shimizu
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Patent number: 7303722Abstract: The present invention relates to a method of making a sintered body comprising one or more hard constituents in a binder phase by injection molding or extrusion. According to the invention, the binder system comprises 30-70 wt % poly(ethylene-co-vinylacetate) and balance (Polyethylene)-blend-(Poly(oxy-1,2-ethanediyl), .alpha.-hydro-.omega.-hydroxy)-based wax. The solids loading of the feedstock, ?, is 0.51<?<0.53, calculated using the equation: ? = ? f - ? b ? s - ? b where ?s is the density of the material as sintered, ?b is the density of the binder system and ?f is the density of the feedstock, measured with a helium pycnometer. Debinding is performed by heating in a furnace in flowing hydrogen atmosphere.Type: GrantFiled: August 25, 2004Date of Patent: December 4, 2007Assignee: Seco Tools ABInventors: Johnny Bruhn, Evert Löwdin, Tomas Rostwall
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Patent number: 7253129Abstract: A rare earth garnet sintered compact which is produced by subjecting a rare earth garnet powder such as YAG to a pre-sintering, sintering the pre-sintered product by HIP, and annealing the sintered product at 1100° C. to 1600° C. in a whole oxygen atmosphere under a whole pressure of 4.5 MPa or more, and has an average crystallite diameter of 0.9 to 9 ?m, an optical loss coefficient of 0.002 cm?1 or less and a strain of a transmitted wave of 0.05 ? cm?1 or less.Type: GrantFiled: January 27, 2003Date of Patent: August 7, 2007Assignee: Konoshima Chemical Co., Ltd.Inventors: Yanagitani Takagimi, Yagi Hideki
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Patent number: 7169198Abstract: The invention relates to a method for the production of a sintered, microcrystalline ?-Al2O3-based shaped body, which are used, for example, as abrasive bodies, wherein an ?-Al2O3 powder is used as starting material, said powder having an average particle diameter of <2 ?m, and processed with at least one binder and a solvent with the purpose of obtaining an extrudable material that is subsequently extruded. The extrudate is then further processed into a shaped body that is sintered at a temperature range of between 1300° C. and 1750° C.Type: GrantFiled: February 8, 2001Date of Patent: January 30, 2007Assignee: Treibacher Schleifmittel GmbHInventors: Paul Moeltgen, Wilhelm Pirmin, Frank J. Clemens
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Patent number: 7166552Abstract: The present invention provides a process for preparing a sintered body comprising as a basic component aluminum magnesium titanate represented by the composition formula: MgxAl2(1?x)Ti(1+x)O5 wherein the value of x is 0.1?x<1. The process comprises a step of sintering a formed product from a raw material mixture comprising 100 parts by weight, calculated on an oxide basis, of a mixture comprising a Mg-containing compound, an Al-containing compound and a Ti-containing compound at the same metal component ratio as the metal component ratio of Mg, Al and Ti in the above composition formula, and 1–10 parts by weight of an alkali feldspar represented by the composition formula: (NayK1?y)AlSi3O8 wherein the value of y is 0?y?1.Type: GrantFiled: October 9, 2003Date of Patent: January 23, 2007Assignee: Ohcera Co. Ltd.Inventors: Tsutomu Fukuda, Masahiro Fukuda, Masaaki Fukuda, Toshinobu Yoko, Masahide Takahashi
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Patent number: 7150849Abstract: In certain example embodiments, a coated article includes respective layers including diamond-like carbon (DLC) and zirconium nitride before heat treatment (HT). During HT, the hydrogenated DLC acts as a fuel which upon combustion with oxygen produces carbon dioxide and/or water. The high temperature developed during this combustion heats the zirconium nitride to a temperature(s) well above the heat treating temperature, thereby causing the zirconium nitride to be transformed into a new post-HT layer including zirconium oxide that is scratch resistant and durable.Type: GrantFiled: February 25, 2004Date of Patent: December 19, 2006Assignee: Guardian Industries Corp.Inventor: Vijayen S. Veerasamy
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Patent number: 7125600Abstract: A setter and a method for manufacturing a ceramic substrate are capable of suppressing deformation such as warpage occurring in a ceramic substrate after baking. A ceramic green sheet 4 is mounted and baked on a mount surface of a zirconia setter wherein an average particle size is 0.3 ?m, a porcelain density is not less than 6 kg/dm 3, a thermal conductivity is not more than 5 W/mK, and an arithmetic average roughness of the mount surface is 1 ?m–20 ?m, whereby it is feasible to suppress the deformation such as warpage occurring in a piezoelectric ceramic substrate after baked.Type: GrantFiled: May 10, 2005Date of Patent: October 24, 2006Assignee: TDK CorporationInventor: Satoshi Sasaki
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Patent number: 7067187Abstract: A spherical porous ceramic body and the production method thereof are provided. As to the porous ceramic body, the total volume of the pores having a pore radius of from 1.8 nm to 100 ?m is about 0.25 cm3/g or more, the mode of pore radius of the pores is from about 1 ?m to about 6 ?m and the packing density is from about 0.7 g/cm3 to about 1 g/cm3. The porous ceramic body is suitably used as a carrier for a catalyst and has high mechanical strength.Type: GrantFiled: March 14, 2002Date of Patent: June 27, 2006Assignee: Sumitomo Chemical Company, LimitedInventors: Hidekatsu Kawazu, Osamu Yamanishi
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Patent number: 7033537Abstract: A process for producing a continuous alumina fiber blanket by heat treating an alumina fiber precursor formed from a spinning solution containing an aluminum compound, by using a specific high-temperature furnace capable of high-temperature heat treatment. According to this process, a continuous sheet (W) of alumina fiber precursor formed from a spinning solution containing an aluminum compound is supplied continuously into a high-temperature furnace and subjected to heat treatment while being conveyed in one direction by plural conveying mechanisms (2, 3) disposed in said high-temperature furnace. In this operation, the speed of said conveying mechanisms is reduced progressively in the direction of conveyance in correspondence to the rate of heat shrinkage of the continuous sheet (W) of alumina fiber precursor, thereby to lessen fiber crush in the alumina fiber precursor and obtain a continuous alumina fiber blanket with uniform thickness and high bulk density as well as high strength.Type: GrantFiled: January 23, 2003Date of Patent: April 25, 2006Assignee: Mitsubishi Chemical Functional Products, Inc.Inventors: Mamoru Shoji, Norio Ikeda, Toshiaki Sasaki
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Patent number: 7014881Abstract: An inert anode 50, for use in an electrolytic cell 12 for producing metals such as aluminum, is made by providing chemical source materials 100 such as at least two of metal salts, metal particles, or metal oxides and dissolving them to form a solution or a slurry 110, followed by adding a base 120 and adjusting the pH so that a gel 130 is formed which is dried and calcined 150, 160, 190 to provide a blend of metal oxide powder 200 which can be pressed and sintered 220 to form an inert anode 50.Type: GrantFiled: November 13, 2002Date of Patent: March 21, 2006Assignee: Alcoa Inc.Inventors: Xinghua Liu, Siba P. Ray, Alfred F. LaCamera, Douglas A. Weirauch, Mark L. Weaver, Robert A. DiMilia, Kirk J. Malmquist, Frankie E. Phelps, Joseph M. Dynys
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Patent number: 7011788Abstract: The present invention provides a process for preparing an aluminum-titanate-based sintered body comprising the step of firing, at 1250 to 1700° C., a formed product prepared from a raw material mixture containing 100 parts by weight of a mixture of TiO2 and Al2O3 in a weight ratio of TiO2:Al2O3=40:60 to 60:40, and 1 to 15 parts by weight of an alkali feldspar represented by the formula:(NaxK1-x)AlSi3O8 wherein 0?x?1. According to the process of the present invention, it is possible to obtain an aluminum-titanate-based sintered body in which inherent properties of an aluminum titanate, i.e., a low coefficient of thermal expansion and high corrosion resistance are maintained, the mechanical strength thereof is improved, and which can be stably used even under high temperature conditions.Type: GrantFiled: November 6, 2001Date of Patent: March 14, 2006Assignee: Ohcera Co., Ltd.Inventors: Tsutomu Fukuda, Masahiro Fukuda, Masaaki Fukuda
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Patent number: 6998064Abstract: A thermochemically stable oxidic thermal insulating material presenting phase stability, which can be used advantageously as a thermal insulating layer on parts subjected to high thermal stress, such as turbine blades or such like. The thermal insulating material can be processed by plasma spraying and consists preferably of a magnetoplumbite phase whose preferred composition is MMeAl11O19, where M is La or Nd and where Me is chosen from among zinc, the alkaline earth metals, transition metals, and rare earths, preferably from magnesium, zinc, cobalt, manganese, iron, nickel and chromium.Type: GrantFiled: July 14, 2003Date of Patent: February 14, 2006Assignee: MTU Aero Engines GmbHInventors: Rainer Gadow, Guenter Schaefer
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Patent number: 6929772Abstract: A manufacturing method of ITO powder with tin dissolved in indium oxide, wherein the ITO powder is obtained by performing spray pyrolysis to a mixed solution or slurry of indium nitrate and tin chloride in which the concentration of indium and tin is 3.0 mol/L or more, thereby providing at low costs ITO powder superior in component dispersibility by dissolving tin in indium oxide as well as a precise target superior in uniformity. It is thereby possible to restrain the deterioration of quality or abnormal protrusions such as nodules in cases where the ITO sputtering target deposition is not uniform.Type: GrantFiled: December 19, 2001Date of Patent: August 16, 2005Assignee: Nikko Materials Co., Ltd.Inventors: Yoshiro Yanai, Atsushi Nakamura
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Patent number: 6924038Abstract: A mask suitable for protecting a portion of a substrate surface against diffusion coating of the substrate with a metal, which mask comprises a ceramic material comprising silica and an inert refractory diluent and a metal or metal alloy, wherein the metal or metal alloy is one which is reactive with silicon thereby minimising or preventing siliconisation of the substrate with silicon in the ceramic material under conditions of diffusion coating, and which is reactive with the metal being applied by diffusion coating thereby preventing diffusion coating of the portion of the substrate surface it is desired to protect.Type: GrantFiled: March 28, 2000Date of Patent: August 2, 2005Assignees: Chromalloy United Kingdom Limited, Wade Ceramics LimitedInventors: Bryan Anthony Hardy, David Arthur Goddard, Edward Hugh Shaw
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Patent number: 6843943Abstract: The present invention relates to a method of producing improved bioactive composite materials based on apatite, mainly for supporting functions in dental and orthopaedic applications, by adapting closure temperature and applying of pressure in closed systems using the production methods, according to reaction tendencies of the materials at their production, and by possibly further counteracting such reaction tendencies and tendencies for decomposition by additions of helping agents.Type: GrantFiled: September 29, 1999Date of Patent: January 18, 2005Assignee: Doxa AktiebolagInventors: Erik Adolfsson, Leif Hermansson
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Patent number: 6843956Abstract: A method of producing a ceramic object includes producing particles of a type A and a type B. Each particle has a dimension of at least 5 ?m and each type of particle includes a ceramic material that is based on a mixture of silver oxide, niobium oxide and tantalum oxide. The method includes producing a particle mixture by mixing the types of particles, producing a green compact by compressing the particle mixture, and sintering the green compact.Type: GrantFiled: August 14, 2001Date of Patent: January 18, 2005Assignee: Epcos AGInventors: Matjaz Valant, Danilo Suvorov, Christian Hoffmann, Helmut Sommariva
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Publication number: 20040239012Abstract: Round and spherical titanium dioxide scouring media and a method for producing the media are disclosed. The scouring media is effective in removing titanium dioxide buildup on the walls of a titanium dioxide reaction vessel. The method consists of forming green titanium dioxide pellets in a high intensity mixer by mixing commercially available titanium dioxide dust, water and a surfactant. The high intensity mixer produces substantially round, and spherical green pellets which are subsequently sized and sintered in a kiln to form round and spherical titanium dioxide sintered pellets that are suitable as a scouring media. The high intensity mixer allows the operator to closely control the size and shape of the pellets during the forming process to produce substantially round and spherical green pellets. Because the sintered titanium dioxide pellets are substantially round and spherical in shape, they are much less abrasive to the walls of the reaction vessel.Type: ApplicationFiled: April 30, 2004Publication date: December 2, 2004Applicant: CARBO Ceramics Inc.Inventors: Claude A. Krause, William Scott Woolfolk
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Patent number: 6825144Abstract: A high-purity rare earth metal oxide material powder of purity of 99.9% or over, of which Al content is 5-100 wtppm in metal weight and Si content is 10 wtppm or under in metal weight, and a binder are used to prepare a molding body of which molding density is 58% or over of the theoretical density. The binder is eliminated by thermal treatment, and then the molding body is sintered in an atmosphere of hydrogen or a rare gas or a mixture of them or in a vacuum at a temperature being not lower than 1450° C. and not higher than 1700° C. for 0.5 hour or over to prepare A transparent sintered rare earth metal oxide body represented by a general formula R2O3 (R being at least one element of a group comprising Y, Dy, Ho, Er, Tm, Yb and Lu).Type: GrantFiled: February 28, 2003Date of Patent: November 30, 2004Assignee: Konoshima Chemical Co., Ltd.Inventors: Yagi Hideki, Yanagitani Takagimi
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Patent number: 6821312Abstract: A method of making cermet inert anodes for the electrolytic production of metals such as aluminum is disclosed. The method includes the step of spray drying a slurry comprising ceramic phase particles and metal phase particles. The resultant spray dried powder, which comprises agglomerates of both the ceramic phase and metal phase particles, may then be consolidated by techniques such as pressing and sintering to produce a cermet inert anode material. The ceramic phase may comprise oxides of Ni, Fe and at least one additional metal selected from Zn, Co, Al, Li, Cu, Ti, V, Cr, Zr, Nb, Ta, W, Mo, Hf and rare earths. The metal phase may comprise Cu, Ag, Pd, Pt, Au, Rh, Ru, Ir and/or Os. The consolidated cermet inert anode material exhibits improved properties such as reduced porosity. The cermet inert anodes may be used in electrolytic reduction cells for the production of commercial purity aluminum as well as other metals.Type: GrantFiled: April 1, 2002Date of Patent: November 23, 2004Assignee: Alcoa Inc.Inventors: Siba P. Ray, Xinghua Liu, Frankie E. Phelps, Joseph M. Dynys, Douglas A. Weirauch, Jr.
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Patent number: 6814917Abstract: A process for producing a polycrystalline alumina sintered body which includes the steps of: subjecting alumina powder to ultrasonic irradiation, mechanical stirring not using a grinding medium, or ultrasonic irradiation and mechanical stirring not using a grinding medium, resulting in slurry dispersed in a solvent; drying and forming the slurry to produce a green body; and then sintering the green body in an air atmosphere at a temperature in the range of 1400° C. to 1800° C.; wherein the alumina powder has: a purity of 99.99 wt % or more and includes &agr; alumina particles having polyhedral shape, having substantially no red surface and a D/H ratio of from 0.5 or more to 3.0 or less; the number-average particle size of from 0.1 &mgr;m or more to 1.0 &mgr;m or less; and a D90/D10 ratio of 7 or less.Type: GrantFiled: July 27, 1999Date of Patent: November 9, 2004Assignee: Sumitomo Chemical Company, LimitedInventors: Hisashi Watanabe, Yoshio Uchida
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Publication number: 20040202823Abstract: Between dielectric ceramic sheets 11A-11C and magnetic ceramic sheets 13A-13C, metallic alkoxide solution films are formed so as not to interfere with wiring patterns 12A-12C and 14A-14C. Thereafter, the dielectric ceramic sheets 11A-11C and the magnetic ceramic sheets 13A-13C are stacked and heat-treated at the temperature of about 200-400° C. This heat treatment leads to a sol-gel reaction of the metallic alkoxide solution, thereby providing intermediate layers 15. Through the intermediate layers 15, the adjacent ceramic sheets are coupled with each other. Since the ceramic sheets are coupled with each other using the sol-gel reaction which proceeds at a low temperature of about 200-400° C., the ceramic laminate is prevented from being deformed due to a difference in the thermal shrinkage coefficient between the ceramic sheets, thereby providing a ceramic laminate with no warpage and peeling.Type: ApplicationFiled: January 28, 2003Publication date: October 14, 2004Inventors: Hideki Yoshikawa, Takashi Umemoto, Keiichi Kuramoto, Hitoshi Hirano
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Patent number: 6790806Abstract: The core/jacket catalyst molding with a core made from an inorganic support material and with a jacket made from a catalytically active material can be prepared by coextruding an aqueous molding composition which comprises the support material or a precursor thereof, with an aqueous molding composition which comprises the catalytically active material or a precursor thereof, then drying the coextrudate, and then calcining the dried coextrudate.Type: GrantFiled: January 17, 2002Date of Patent: September 14, 2004Assignee: BASF AktiengesellschaftInventors: Michael Hesse, Rainer Anderlik, Hans-Gerhard Fritz, Jochen Hammer
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Publication number: 20040168367Abstract: There is disclosed a metal particle-dispersed composite oxide comprising a matrix material containing a composite oxide comprising a non-reducible metal oxide and an easily reducible metal oxide, the composite oxide containing 0.01 to 0.25 mol % of at least one additive metal selected from Al, Sc, Cr, B, Fe, Ga, In, Lu, Nb and Si, surface metal particles precipitated on an outer surface of the matrix material containing the composite oxide, and inner metal particles precipitated on an inner surface of the matrix material containing the composite oxide.Type: ApplicationFiled: February 26, 2004Publication date: September 2, 2004Inventors: Seiichi Suenaga, Tomohiro Suetsuna, Takayuki Fukasawa, Yasuhiro Goto, Koichi Harada
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Patent number: 6777360Abstract: A ceramic material suitable for use in production of paving tiles, construction tiles, flooring in offices, flooring in machinery plants and so forth is obtained by a method comprising steps of mixing defatted bran derived from rice bran with a thermosetting resin before kneading, subjecting a kneaded mixture thus obtained to a primary firing in an inert gas at a temperature in a range of 700 to 1000° C., pulverizing the kneaded mixture after the primary firing into carbonized powders, kneading the carbonized powders with which ceramic powders, a solvent, and a binder as desired are mixed into a plastic workpiece (kneaded mass), pressure-forming the plastic workpiece at pressure in a range of 10 to 100 MPa, and subjecting a formed plastic workpiece thus obtained again to firing in an inert gas atmosphere at a temperature in a range of 100 to 1400° C.Type: GrantFiled: February 11, 2002Date of Patent: August 17, 2004Assignee: Minebea Co., Ltd.Inventors: Kazuo Hokkirigawa, Rikuro Obara, Motoharu Akiyama
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Patent number: 6764565Abstract: A method of producing lithium aluminosilicate (LAS) ceramics, which uses a mixing powder of lithium carbonate, aluminum oxide, and silicon oxide as a raw material powder. After being mixed by ball milling and baked dry, the raw material powder is processed with a calcinations process such that the raw material powder becomes a precursor. The precursor is then pressed into the green ceramic. Significantly, the high heat conducting metal sheets are tightly attached above and below the surfaces of the ceramic during sinter and heat-treatment processes. A solid-state sinter process is performed with the green ceramic. Next, the ceramic is treated with a proper heat-treatment process. Since the top and bottom surfaces of the ceramic are capped with the high heat conducting metal, the ceramics are uniformly heated during all the heating processes.Type: GrantFiled: December 17, 2002Date of Patent: July 20, 2004Assignee: National Central UniversityInventors: Jyh-Chen Chen, Gwo-Jiun Sheu