Abstract: The present disclosure is drawn to powder bed materials. The powder bed material can include from 20 wt % to 95 wt % of a large particulate metal and from 5 wt % to 80 wt % of a small particulate metal. The large particulate metal can have a D50 particle size distribution value ranging from 20 ?m to 100 ?m and an average aspect ratio from 1:1 to 1.1:1. The small particulate metal can have a D50 particle size distribution value ranging from 1 ?m to 15 ?m and an average aspect ratio from greater than 1.1 to 2.1.

Abstract: A method for preserving the shape of an object during sintering includes filling at least one volume defined by a surface of the object with a plurality of balls, sintering the object together with the balls and separating the object from the balls post sintering. The balls have a diameter of 0.5 mm-12 mm.

Abstract: A method of making an article includes depositing a plurality of layers to form a three-dimensional preform, sintering the preform to form a sintered preform, and infiltrating the preform with at least one metal to form the article. At least one layer of the plurality of layers is formed from a beryllium-containing composition including beryllium powder. The infiltrating metal can be selected from aluminum and magnesium.

Abstract: Systems, apparatus and methods of additively manufacturing objects are disclosed. Specifically, provided herein are methods of heating objects having a particle-based support at least partially surrounding the object during portions of stages of the heating. Additionally, systems, apparatus, and methods for removing the particle-based support during heating, such that the object can continue heating to form a final part. Systems, apparatus, and methods for distributing the particle-based support to shore the objects through heating are disclosed. Systems, apparatus, and methods for removing the particle-based support are also disclosed herein.

Abstract: 3D-printed parts may include binding agents to be removed following an additive manufacturing process. A debinding process removes the binding agents by immersing the part in a solvent bath causing chemical dissolution of the binding agents. The time of exposure of the 3D-printed part to the solvent is determined based on the geometry of the part, wherein the geometry is applied to predict the diffusion of the solvent through the 3D-printed part. The 3D-printed part is then immersed in the solvent bath to remove the binding agent, and is removed from the solvent bath after the time of exposure.

Abstract: A three-dimensional shaped article production method for producing a three-dimensional shaped article by stacking layers to form a stacked body includes a first layer formation step of forming a first layer on a support by supplying a first composition containing first particles and a binder, a second layer formation step of forming a second layer composed of one layer or a plurality of layers on the first layer by supplying a second composition containing second particles and a binder, and a separation step of separating the second layer from the support through the first layer, wherein after the separation step, a sintering step of sintering the second layer is performed.

Abstract: A particulate composite lubricant for powder metallurgy comprises: first discrete particles comprising at least about 90 wt % of a fatty primary monoamide wax, being substantially free of fatty bisamide wax, and being at least partially coated with metal oxide nanoparticles and second metal-stearate free discrete particles comprising a fatty bisamide wax. A particulate composite lubricant for powder metallurgy can comprise: a Montan acid ester wax and at least one fatty amide wax comprising at least one of a fatty monoamide wax and a fatty bisamide wax.

Abstract: A method of forming an article includes forming a layer of a mixture of at least two distinct metal powders selected such that when combined they are chemically in the proportions of a superalloy containing a gamma prime phase, and fusing the powders locally without diffusion to define the shape of a part of the article such that the materials of the distinct metal powders remain substantially chemically segregated forming regions of different chemical composition. The method further includes repeating the forming and fusing until the derived article is formed, and heat treating the finished article such that at least one of the distinct separate materials diffuses to form a gamma prime phase containing superalloy with the other.

Abstract: A nickel-free stainless steel stent using a stainless steel which does not substantially contain Ni in the stainless steel, has a metal allergy onset-preventing effect, and is excellent in terms of precision workability, strength, and ductility, is provided. The nickel-free stainless steel stent is characterized by using a stainless steel containing, as a chemical composition, from 15 to 30% by mass of Cr, from 0.97 to 2% by mass of Mo, and from 0.5 to 1% by mass of N, with the remainder being Fe, and optionally containing inevitable impurities.

Abstract: A first die is filled with a mixed powder including a lubricant. A first pressure is applied to the mixed powder to form a mixed powder intermediate compressed body having a density ratio of 85 to 96%, provided that the maximum density of the mixed powder intermediate compressed body that can be molded by applying the first pressure is 100%. The mixed powder intermediate compressed body is heated to the melting point of the lubricant powder. The mixed powder intermediate compressed body is placed in a second die that is pre-heated to the melting point. A second pressure is applied to the mixed powder intermediate compressed body in the second die to form a high-density mixed powder final compressed body.

Abstract: A method for preparing an implant having a porous metal component. A loose powder mixture including a biocompatible metal powder and a spacing agent is prepared and compressed onto a metal base. After being compressed, the spacing agent is removed, thereby forming a compact including a porous metal structure pressed on the metal base. The compact is sintered, forming a subassembly, which is aligned with a metal substrate portion of an implant. A metallurgical bonding process, such as diffusion bonding, is performed at the interface of the subassembly and the metal substrate to form an implant having a porous metal component.

Abstract: It is an objective of the present invention to provide an aluminum porous body which is formed of a pure aluminum and/or aluminum alloy base material and has excellent sinterability and high dimensional accuracy without employing metal stamping. There is provided an aluminum porous body having a relative density of from 5 to 80% with respect to the theoretical density of pure aluminum, in which the aluminum porous body contains 50 mass % or more of aluminum (Al) and from 0.001 to 5 mass % of at least one selected from chlorine (Cl), sodium (Na), potassium (K), fluorine (F), and barium (Ba). It is preferred that the aluminum porous body further contains from 0.1 to 20 mass % of at least one selected from carbon (C), silicon carbide (SiC), iron (II) oxide (FeO), iron (III) oxide (Fe2O3), and iron (II,III) oxide (Fe3O4).

Abstract: The present invention relates to ferromagnetic powders with an electrically insulating layer on iron particles intended for the manufacture of components having improved soft magnetic properties at low and medium frequencies. The invention comprises an iron powder coated with a dielectric insulating layer comprising boron bearing compounds to form an insulated ferromagnetic powder. The present invention also relates to a method of making these insulated ferromagnetic powders. The present invention further relates to a method of synthesizing a product made from insulated ferromagnetic powders via a post-heat treatment at a moderate temperature (300° C. to 700° C.), to form a glass-like coating which acts as an electrical insulator. A preferred embodiment of the present invention is obtained when small amounts of alkali bearing compounds are added to the precursors to modify the coating chemistry and significantly increase the electrical resistivity after heat treatment.

Abstract: Provided are methods for processing a green body that includes compacted metal powder, comprising impacting the green body with a particulate material for a time and under conditions effective to displace a portion of the metal powder from the green body. The present methods can be used to prepare green bodies that have “roughened” surfaces and that can be used to make orthopedic implants displaying low movement relative to bone when installed in situ, which corresponds to higher stability upon implantation and decreases the time required for biological fixation of the implant. Also provided are implants comprising a metallic matrix, and methods comprising surgically installing an implant prepared from a “surface roughened” green body in accordance with the present invention.

Abstract: A process for fabricating hollow metal shells such as Be or Al filled with a selected gas such as D or T. An organic preform is coated with a slurry of organic binder and metal powder of Be or Al. The coated preform is heated to remove the preform and any organics to form a hollow shell which is then fired at an elevated temperature in a gas so as to seal the shell and capture the gas inside the sealed shell.

Abstract: A sinter of stable quality is produced by molding a powder for powder metallurgy. This process includes successively conducting the following steps: charging a powder and a solid lubricant into a mold compact formation in which the powder charged into the mold is compacted; releasing the compact from the mold; and the powder for powder metallurgy is charged again into the mold after the release step. The temperature of the mold is set at a value in the range of from the boiling point of water to the melting point of the solid lubricant. The compact can be continuously formed without causing, e.g., a failure in the feeding of the powder for powder metallurgy. The sinter obtained by sintering the compact is almost even in strength and density.

Abstract: The invention relates to a method for fabricating an open-porous metal foam body with a nickel base alloy, to a metal foam body fabricated this way as well as advantageous applications for the separation of specific components and pollutants from fluid flows. On the occasion, according to the set object open-porous metal foam bodies which have improved mechanical properties, and in addition an enlarged specific surface and/or increased surface roughness are to be provided. During fabricating it is proceeded such that an open-porous base foam body made of nickel or a nickel base alloy is coated with a liquid binding agent. Subsequent to this, a mixture of a powdery nickel base alloy and an organic component the temperature of phase transformation of which is at least 30 degrees centigrade from its solid phase to the liquid phase is deposited. The temperature should then be below the respective temperature of phase transformation.

Abstract: A method for preparing a porous metal article using a powder metallurgy forming process is provided which eliminates the conventional steps associated with removing residual carbon. The method uses a feedstock that includes a ferrous metal powder and a polycarbonate binder. The polycarbonate binder can be removed by thermal decomposition after the metal article is formed without leaving a carbon residue.

Abstract: A valve sealant fitting includes a spring coupling unit having an internal screw thread for coupling unit assembly below the ball installation groove of the sealant body, the internal screw thread having a hexagonal groove for preventing a downward separation of the coil spring, allowing a fluid to flow and facilitating fastening and releasing of the screw, and having an external screw thread at an outer circumference of the spring coupling unit, and outer sealing O-rings disposed in O-ring installation grooves formed on respective upper and lower positions of the valve coupling taper screw part formed on the outer lower side of the sealant body.

Abstract: A method for providing a porous metal implant. A mixture of biocompatible metal, a spacing agent, and a binder is provided. The mixture is formed into a shape and the spacing agent is removed to form a plurality of pores in the implant. A shaped porous metal is also provided.

Abstract: A method for producing a soft magnetic powdered core includes preparing a mixture of a soft magnetic powder and a resin powder, compacting the mixture into a predetermined shape so as to obtain a compact, and heating the compact. The resin powder has a median size of not more than 30 ?m, a maximum particle size of not more than 100 ?m, and a specific surface area of not less than 1.0 m2/cm3, and the additive amount thereof is 0.005 to 2 vol %.

Abstract: The metallurgical composition includes a main particulate metallic material, for example iron or nickel, and at least one alloy element for hardening the main metallic material, which form a structural matrix; a particulate solid lubricant, such as graphite, hexagonal boron nitride or mixture thereof; and a particulate alloy element which is capable of forming, during the sintering of the composition conformed by compaction or by injection molding, a liquid phase, agglomerating the solid lubricant in discrete particles. The composition may include an alloy component to stabilize the alpha-iron matrix phase, during the sintering, in order to prevent the graphite solid lubricant from being solubilized in the iron. The invention further refers to a self-lubricating sintered product, obtained from the composition, and to the process for obtaining said product.

Abstract: A method for producing a sintered body includes: a) molding a composition containing a powder primarily made of an inorganic material and a binder including an aliphatic carbonic acid ester based resin in a predetermined shape so as to obtain a compact; b) exposing the compact to a first atmosphere containing an alkaline gas and thus decomposing and removing the aliphatic carbonic acid ester based resin from the compact so as to obtain a degreased body; and c) sintering the degreased body so as to obtain a sintered body.

Abstract: A sintering compound containing a sinterable powder and a binder removable in a debinding step is injected into a metal mold set provided with a sintering compound injecting mold, in a sintering compound molding step (S104). An add-on forming compound which becomes removable or separable from the sintering compound injection molded body in the debinding step or the sintering step is injected into the metal mold set provided with an add-on mold in an add-on forming step (S102). The sintering compound injection molded body and the add-on are formed integrally with each other in the metal mold set. The integral formation of the add-on and the sintering compound injection molded body enables to prevent damage during release from the mold and make easy to handle the injection molded body.

Abstract: A soft magnetic material includes a composite magnetic particle and an organic substance. The composite magnetic particle has a metallic magnetic particle and a coating layer coating the metallic magnetic particle and containing an oxide therein. The organic substance is formed by adding at least one of a thermoplastic resin and a higher fatty acid having an effect of increasing resistivity of the material, to a non-thermoplastic resin having an effect of improving durability such as material fatigue limit. The organic substance is contained in the soft magnetic material by not less than 0.001% by mass and not more than 0.2% by mass. The present invention provides a soft magnetic material having high magnetic property and mechanical strength and also having fatigue property and resistivity satisfying durability enough for use as a motor core or the like, and a method for manufacturing the same. Further, the invention provides a motor core and a transformer core made of the soft magnetic material.

Abstract: A method of reducing the oxygen content of a powder is provided. A canister is prepared with a getter, filled with the powder to be densified, sealed and evacuated. The canister is subjected to a hydrogen atmosphere at an elevated temperature whereby hydrogen diffuses into the canister through the walls thereof. The hydrogen forms moisture when reacted with the oxygen of the powder and the moisture in the reacted with the getter in order to remove oxygen from the powder to the getter. The atmosphere outside the canister is then altered to an inert atmosphere or vacuum, whereby hydrogen diffuses out of the canister. A dense body having a controlled amount of oxygen can thereafter be produced by conventional powder metallurgy techniques.

Abstract: The present invention provides powder metal compositions and methods of making and using the same. Powder metal compositions according to the invention include base metal particles, a lubricant that transforms from a solid phase material to a viscous, liquid phase material during pressing, and a micronized deformable solid material. The micronized deformable solid material fills at least a portion of the void space between the base metal particles during pressing, which allows at least a portion of the lubricant to migrate as a viscous liquid phase material to the interface between the surface of the green compact and the wall of the mold cavity to provide lubrication that reduces the ejection force necessary to remove the green compact from the mold cavity.

Abstract: A method for providing a porous metal implant. A mixture of a biocompatible metal, a spacing agent, and a binder is provided. The mixture is formed into a shaped the spacing agent is removed to form a plurality of pores in the implant. A shaped porous metal implant is also provided.

Abstract: The invention relates to a novel self-lubricating solid material; to a method of preparing such a material from a powder mixture; to said powder mixture; and to mechanical parts made of said novel material. Said powder mixture comprises a powder of a metal alloy that is a precursor for the matrix of said material, particles of a first solid lubricant such as CeF3 that are for insertion in said matrix without reacting with said metal alloy, and particles of a second solid lubricant such as WS2 or MoS2 for reacting with a component of said metal alloy during sintering of the powder to form a lubricating phase. Said material can be used for fabricating a bushing that is to receive a root of a variable-pitch vane of an airplane turbojet compressor.

Abstract: A method for producing a sintered body is provided. The method for producing the sintered body comprising: forming a green body by molding a composition for forming a green body into a specified shape to obtain the green body, the composition comprising powder constituted of a metallic material and a binder containing a first resin which is decomposable by ozone; first debinding the green body by exposing the green body to a high ozone content atmosphere to decompose the first resin and remove the decomposed first resin form the green body to obtain a brown body; exposing the thus obtained brown body at least once to a low ozone content atmosphere whose ozone concentration is lower than an ozone concentration of the high ozone content atmosphere to obtain an intermediate brown body; and sintering the intermediate brown body which has been exposed to the low ozone content atmosphere to obtain the sintered body.

Abstract: Hollow metal and/or metal alloy articles are fabricated by the reduction of metal containing compounds, particularly non-metallic metal compounds.

Abstract: A method for forming an article by metal injection moudling of aluminium or an aluminium alloy. The method comprises the steps of forming a mixture containing an aluminium powder or an aluminum alloy powder or both and optionally ceramic particles, a binder, and a sintering aid comprising a low melting point metal. The mixture is injection moulded and the binder is removed to form a green body. The green body is sintered. The sintering is conducted in an atmosphere containing nitrogen and in the presence of an oxygen getter.

Abstract: The invention provides a valve-acting metal sintered body for anode of a solid electrolytic capacitor, having a high capacitance, well impregnated with cathode material, and exhibiting excellent properties particularly when having a large volume, a capacitor having a low ESR, an excellent tan ? value and good long-term reliability such as moisture resistance and heat resistance by using the sintered body, and a production method therefor comprising the following steps: coating/printing/shaping a granulated product of a mixed dispersion containing a pore-forming agent, an organic binder and a primary powder or secondary aggregated powder of at least one member selected from valve-acting metal, a valve-acting metal compound and a valve-acting metal alloy or a granulated powder thereof, and a solvent, or compressing and shaping the granulated product of a mixture obtained by removing the solvent from the dispersion; sintering the shaped article containing a pore-forming agent; and removing the pore-forming agent

Abstract: Provided is iron-based metal powder for powder metallurgy including a metallic soap containing at least one or more types selected from a group of Ag, Au, Bi, Co, Cu, Mo, Ni, Pd, Pt, Sn, Te and W having a higher standard oxidization potential than iron, and an iron sintered body having a rust prevention function, wherein at least one or more types of metallic soap selected from a group of Ag, Au, Bi, Co, Cu, Mo, Ni, Pd, Pt, Sn, Te and W having a higher standard oxidization potential than iron is added to iron-based metal powder for powder metallurgy, and sintering is performed thereto. As a result, obtained is mixed powder for powder metallurgy capable of improving the rust prevention effect easily without having to hardly change the conventional processes.

Abstract: A metallurgical composition is provided for making compacted parts, comprising: (a) at least about 80 percent by weight of an iron or iron-based powder; (b) up to about 20 percent by weight of at least one alloying powder; (c) from about 0.05 to about 2 percent by weight of a binding agent comprising a C14-C30 fatty alcohol; and (d) from about 0.001 to about 0.2 percent by weight of a flow agent.

Abstract: A production method includes: preparing a metal powder composed of one of Mo and W, and a binder composed of a thermoplastic resin and a wax; mixing the metal powder and 40 to 60 volume % of the binder with respect to the metal powder into a mixed powder; and heating and kneading the mixed powder into a raw material. The production method further includes: supplying a predetermined of the raw material in a hole of a die; and compacting the raw material into a cup-shaped green compact by pressing the raw material by a punch, the cup-shaped green compact having a cylindrical portion, a bottom formed at one end portion thereof, and an opening formed at another end portion thereof. The production method further includes: ejecting the cup-shaped green compact from the hole of the die; removing the binder from the ejected cup-shaped green compact by heating; and sintering the cup-shaped green compact by heating the green compact and diffusion-bonding particles of the green compact.

Abstract: A sintering compound containing a sinterable powder and a binder removable in a debinding step is injected into a metal mold set provided with a sintering compound injecting mold, in a sintering compound molding step (S104). An add-on forming compound which becomes removable or separable from the sintering compound injection molded body in the debinding step or the sintering step is injected into the metal mold set provided with an add-on mold in an add-on forming step (S102). The sintering compound injection molded body and the add-on are formed integrally with each other in the metal mold set. The integral formation of the add-on and the sintering compound injection molded body enables to prevent damage during release from the mold and make easy to handle the injection molded body.

Abstract: Methods of forming cutter assemblies for use on earth-boring tools include sintering a cone structure to fuse one or more cutting elements thereto and having a hardened land area. In some embodiments, one or more green, brown, or fully sintered cutting elements may be positioned on a green or brown cone structure prior to sintering the cone structure to a final density. Cutter assemblies may be formed by such methods, and such cutter assemblies may be used in earth-boring tools such as, for example, earth-boring rotary drill bits and hole openers.

Abstract: The invention relates to the cost-effective manufacture of near-net shape titanium articles from sintered powders containing titanium and all required alloying elements. The cost-effective initial powder composition for subsequent room temperature consolidation and sintering contains: (a) 10-50 wt. % of underseparated titanium powder with ?500 ?m in particle size manufactured from underseparated titanium sponge comprising up to 2 wt. % of chlorine and up to 2 wt. % of magnesium. The underseparated titanium powder costs significantly less than that for fully separated powder of completely reduced sponge; (b) 10-90 wt. % of hydrogenated titanium powder, whereby this powder is a mixture of two hydrogenated powders A and B containing different amount of hydrogen: powder A contains amount of hydrogen in the range of 0.2-1 wt. % and powder B contains amount of hydrogen in the range of 2-3.9 wt. %.

Abstract: A hydroxy fatty acid salt having an average particle diameter of from 5 ?m to 100 ?m with a composition of from 0.3 wt % to 2 wt %, and more preferably, from 0.5 wt % to 2 wt % is added to a raw material powder in powder metallurgy, and worm molding is performed. In addition, a hydroxy fatty acid salt having an average particle diameter of 50 ?m or less is attached on a mold in advance, and after that, the warm molding is performed. As a hydroxy fatty acid salt, 12-hydroxy lithium stearate is suitably used.

Abstract: A prepreg material infused with a bulk resin, where the bulk resin has shape memory alloy (SMA) particles intermixed in the resin to toughen the material when the material is used in an application and is cured. The SMA particles may be of various shapes and sizes. The material may form a prepreg fabric having interwoven fibers or a prepreg unidirectional tape having fibers oriented unidirectionally. Opposing surfaces of the material may be infused with quantities of bulk resin having different concentrations of SMA particles. The SMA particles may be mixed in the bulk resin while in their austenitic or martensitic states to suit the needs of specific applications.

Abstract: The invention concerns a powder metal composition comprising an iron based powder and a lubricant and/or binder comprising at least one secondary amide of the general formula: R1—NH—CO—R2, wherein R1 and R2 are the same or different, straight or branched, saturated or unsaturated aliphatic hydrocarbon groups. The invention further concerns a method of making green bodies of the powder metal composition according to the invention, a method of producing a bonded iron-based powder composition, as well as the use of the at least one secondary amide as a lubricating and/or binding agent for iron based powders and the use as a die wall lubricant.

Abstract: A porous near-net-shape metallic parts with an open porosity of at least 10% by volume is made by first forming an injectable mass of a metallic powder of stainless steel, Ti, NiTi, or a titanium alloy, at least one thermoplastic binder, and at least one place holder. The mass then injection molded into the shape of the part to be produced, cooled, set in a capillary-active material, and subjected to a first-stage binder removal to produce an open porosity. The place holder is then removed at least partially from the part with a fluid, and the part is subjected to a thermal binder-removing process. Finally the part is sintered.

Abstract: Particulate lubricants are disclosed which comprise discrete particles of a fatty monoamide, especially oleamide and discrete particles of at least one other powder metallurgy lubricant, which provide a synergistic free-flowing composition; there are also provided novel compositions of matter for forming sintered metal components comprising a mixture of sinterable powdered metal and the particulate lubricants.

Abstract: A method of making tungsten carbide and a method of making a densified tungsten carbide-containing ceramic body with a transverse rupture strength greater than 300,000 psi are disclosed.

Abstract: The present invention provides a lubricant system in the pressing of powders to form a part. The lubricant system is a solid at ambient conditions. However, upon application of pressure during the pressing of the metal parts, the lubricant system forms a liquid phase along the walls of cavity in which the powder is being pressed. The lubricant system may also be used in connection with a polar powder thereby providing certain beneficial results.

Abstract: The present invention relates to a method of forming a part made of a molybdenum-copper composite material. The composite material is formed by forming a mixture of molybdenum, phenolic, and wax, laser sintering the mixture to form a green form, placing the green form and oxygen free copper into a furnace, and subjecting the green form and oxygen free copper to a furnace heating cycle.

Abstract: The invention relates to a method for producing highly porous, metallic molded bodies. The inventive method consists of the following steps: a metallic powder used as a starting material is mixed with a dummy; a green body is pressed out of the mixture; the green body is subjected to conventional mechanical machining, the dummy advantageously increasing the stability of the green body; the dummy material is thermally separated from the green body by means of air, a vacuum or an inert gas; and the green body is sintered to form the molded body and is then advantageously finished. Suitable materials for the dummy are, for example, ammonium bicarbonate or carbamide. The mechanical machining carried out before the sintering advantageously enables a simple production close to the desired final contours, even for complicated geometries of the molded body to be produced, without impairing the porosity, and without high wear of the tools.

Abstract: The porous material of the present invention is produced by heating a dry powder mixture, containing mainly an organic solid binder and inorganic particles. The mixture is foamed while the organic binder is melted. Foaming comes from a foaming agent in the powder mixture. The solid foamed structure comprising inorganic particles embedded in an organic binder is then heated to eliminate the organic binder and finally to sinter the remaining inorganic tri-dimensional network into a rigid structure having interconnected porosity.

Abstract: The present invention concerns a method of improving the properties of powder metallurgically produced SMC compacted body consisting of a soft magnetic material of insulated powder particles and a lubricant, to a stress relieving heat treatment in a furnace until the component has reached a temperature of at least 400° C. in an oxygen containing atmosphere having a CO content is less than 0.25% by volume.