Sintering Which Includes A Chemical Reaction Patents (Class 419/45)
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Patent number: 12068104Abstract: Systems and methods for forming a magnetically-enabled part via additive manufacturing. The method includes depositing a layer of additive manufacturing material on a build plate, melting or sintering the layer of additive manufacturing material, depositing additional layers of additive manufacturing material on previous layers of additive manufacturing material, the additive manufacturing material of at least some of the additional layers being magnetically permeable, and melting or sintering the additional layers of additive manufacturing material such that the magnetically-enabled part has a transition region including at least some of the magnetically permeable additive manufacturing material.Type: GrantFiled: May 11, 2023Date of Patent: August 20, 2024Assignee: Honeywell Federal Manufacturing & Technologies, LLCInventors: Jonathan Douglas Hatch, Bob Dearth, Ida Sanchez, Francisco Garcia-Moreno
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Patent number: 11998985Abstract: An assembly for densification under load along at least one direction of compression. The assembly includes: at least one volume to be densified having a powdery and/or porous composition and having variations in thickness along the direction of compression; and at least one counter-form of a powdery and/or porous composition, having at least one face facing at least one portion of the volume. The face and each of the portions are separated by at least one deformable interface layer.Type: GrantFiled: May 13, 2022Date of Patent: June 4, 2024Assignees: Universite Toulouse III—Paul Sabatier, Centre National De La Recherche ScientifiqueInventors: Claude Estournes, Charles Maniere, Lise Durand
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Patent number: 11986995Abstract: The disclosure provides methods of additive manufacture of components in layers in a powder bed by at least two laser beams that can be deflected two-dimensionally over the same powder bed region. Each laser focal spot is projected onto the power bed and is or is set to a diameter of less than or equal to 300 ?m. Components to be produced in the powder bed region are manufactured by each of the laser beams, and each individual surface contour of the component is manufactured solely by one of the laser beams.Type: GrantFiled: May 9, 2019Date of Patent: May 21, 2024Assignee: TRUMPF Laser- und Systemtechnik GmbHInventors: Uwe Huber, Johannes Bauer, Michael Thielmann, Joachim Wagner, Jürgen Ortmann, Matthias Allenberg-Rabe, Detlef Breitling, Damien Buchbinder, Florian Krist
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Patent number: 11939647Abstract: There is provided a tungsten sputtering target that can provide a film deposition rate with less fluctuation over the target life. A tungsten sputtering target, wherein an area ratio of crystal grains having any of {100}, {110} and {111} planes oriented to a sputtering surface is 30% or less for any of the orientation planes, and an area ratio in total of crystal grains having orientation planes oriented to the sputtering surface other than {100}, {110} and {111} planes is 46% or more, the area ratio being obtained by an analysis of a cross section perpendicular to the sputtering surface with an inverse pole figure mapping using electron backscatter diffraction.Type: GrantFiled: January 26, 2018Date of Patent: March 26, 2024Assignee: JX Metals CorporationInventors: Takafumi Dasai, Shinichiro Senda
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Patent number: 11890818Abstract: An apparatus for dispensing build powder and support powder, in a sequence of layers, and having a frame and a container. Also, a build powder pourer is at least partially filled with build powder and a support powder pourer at least partially filled with support powder, each of the pourers having a dispensing opening and a dispensing plug, controllably covering the dispensing opening. Further, a pourer-movement and dispensing plug-actuating assembly is supported by the frame over the container and includes a movement element that is selectively attachable to the build powder pourer and alternately to the support powder pourer and also capable to controllably move an attached pourer in three orthogonal dimensions and to control the dispensing plug. In addition, at least one docking station for holding a first one of the pourers; and a computing assembly controls the pourer-movement and dispensing plug-actuating assembly to create a target shape.Type: GrantFiled: April 29, 2023Date of Patent: February 6, 2024Inventor: Sergey Singov
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Patent number: 11772163Abstract: The present disclosure is drawn to a three-dimensional printing system can include a powder bed material, including from 80 wt % to 100 wt % metal particles having a D50 particle size distribution value ranging from 5 ?m to 75 ?m and a powder bed support substrate for receiving the powder bed material. The system can also include a fluid ejector operable to digitally deposit a thermally sensitive binder fluid onto a selected portion of the powder bed material on the powder bed support substrate. The thermally sensitive binder fluid can include water, a reducible metal compound, and a thermally activated reducing agent. A light source can also be present to generate a pulse energy sufficient to cause the thermally activated reducing agent to reduce the reducible metal compound and bind metal particles together to form a green three-dimensional part.Type: GrantFiled: February 9, 2018Date of Patent: October 3, 2023Assignee: Hewlett-Packard Development Company, L.P.Inventors: Krzysztof Nauka, Paul Olubummo
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Patent number: 11767271Abstract: A porous material including a composite oxide body containing calcium oxide, iron oxide, and silica, and a plurality of inter-connecting microchannel structures is provided. A preparing method of porous material is further provided. With the inter-connecting microchannel structures of the porous material and the advantages of high porosity and large specific surface area, the porous material has a bright prospect in the fields of catalysts, filters, adsorption materials, and fuel carriers.Type: GrantFiled: September 21, 2020Date of Patent: September 26, 2023Assignee: INDUSTRIAL TECHNOLOGY RESEARCH INSTITUTEInventors: Ming-Hui Chang, Sheng-Min Yu, Hsiu-Hsia Lee, Chien-Chung Hsu
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Patent number: 11759863Abstract: In an example of a three-dimensional (3D) printing method, a metallic build material is applied. A patterning fluid, including a metal salt, is selectively applied on at least a portion of the metallic build material. Prior to an application of additional build material, the metallic build material is exposed to light irradiation to cause the metal salt to reach a thermal decomposition temperature and thermally decompose to a metal. During the exposing, the metallic build material is maintained below a sintering temperature of the metallic build material.Type: GrantFiled: October 30, 2017Date of Patent: September 19, 2023Assignee: Hewlett-Packard Development Company, L.P.Inventors: Krzysztof Nauka, Thomas Anthony
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Patent number: 11688550Abstract: Systems and methods for forming a magnetically-enabled part via additive manufacturing. The method includes depositing a layer of additive manufacturing material on a build plate, melting or sintering the layer of additive manufacturing material, depositing additional layers of additive manufacturing material on previous layers of additive manufacturing material, the additive manufacturing material of at least some of the additional layers being magnetically permeable, and melting or sintering the additional layers of additive manufacturing material such that the magnetically-enabled part has a transition region including at least some of the magnetically permeable additive manufacturing material.Type: GrantFiled: October 20, 2020Date of Patent: June 27, 2023Assignee: Honeywell Federal Manufacturing & Technologies, LLCInventors: Jonathan Douglas Hatch, Bob Dearth, Ida Sanchez, Francisco Garcia-Moreno
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Patent number: 11121312Abstract: A method for fabricating semiconductor device includes the steps of: forming an inter-metal dielectric (IMD) layer on a substrate; forming a metal interconnection in the IMD layer; forming a magnetic tunneling junction (MTJ) on the metal interconnection; forming a top electrode on the MTJ; and forming a trapping layer on the top electrode for trapping hydrogen. Preferably, the trapping layer includes a concentration gradient, in which a concentration of hydrogen decreases from a top surface of the top electrode toward the MTJ.Type: GrantFiled: September 8, 2019Date of Patent: September 14, 2021Assignee: UNITED MICROELECTRONICS CORP.Inventors: Da-Jun Lin, Tai-Cheng Hou, Bin-Siang Tsai, Ting-An Chien
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Patent number: 11098207Abstract: A metallic nanoparticle dispersion includes metallic nanoparticles, a liquid carrier and an optional binder, and a silane compound according to Formula I: wherein R1, R2 and R3 are independently selected from the group consisting of a hydrogen, a substituted or unsubstituted alkyl group, a substituted or unsubstituted aryl group, an alkoxy group and an aryloxy group with the proviso that at least one of R1 to R3 represents an alkoxy group or an aryloxy group, L1 represents a divalent linking group including one to 20 carbon atoms, A represents a thiol, a disulfide or a functional moiety comprising at least one thiol or disulfide, having no more than 10 carbon atoms, and n represents 0 or 1.Type: GrantFiled: August 24, 2017Date of Patent: August 24, 2021Assignee: AGFA-GEVAERT NVInventor: Dirk Bollen
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Patent number: 10875127Abstract: The present disclosure provides a method for bonding an electronic component and a method for manufacturing a bonded body, which are capable of sintering a silver paste at a comparatively low temperature. Disclosed is a method for bonding an electronic component using a silver paste containing silver particles, the method including: applying a silver paste containing silver particles on a surface of a substrate and setting electronic components on the silver paste applied, heating in a reducing atmosphere at a temperature of lower than 300° C., and after heating in the reducing atmosphere, heating in an oxidizing atmosphere at a temperature of 300° C. or lower.Type: GrantFiled: September 20, 2018Date of Patent: December 29, 2020Assignee: NICHIA CORPORATIONInventor: Teppei Kunimune
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Patent number: 10537029Abstract: A method for producing an electrically conductive thin film on a substrate is disclosed. Initially, a reducible metal compound and a reducing agent are dispersed in a liquid. The dispersion is then deposited on a substrate as a thin film. The thin film along with the substrate is subsequently exposed to a pulsed electromagnetic emission to chemically react with the reducible metal compound and the reducing agent such that the thin film becomes electrically conductive.Type: GrantFiled: December 8, 2017Date of Patent: January 14, 2020Assignee: NCC NANO, LLCInventors: Dave S. Pope, Kurt A. Schroder, Ian M. Rawson
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Patent number: 10525688Abstract: The present invention disclosed a method of producing a three-dimensional porous tissue in-growth structure. The method includes the steps of depositing a first layer of metal powder and scanning the first layer of metal powder with a laser beam to form a portion of a plurality of predetermined unit cells. Depositing at least one additional layer of metal powder onto a previous layer and repeating the step of scanning a laser beam for at least one of the additional layers in order to continuing forming the predetermined unit cells. The method further includes continuing the depositing and scanning steps to form a medical implant.Type: GrantFiled: March 27, 2015Date of Patent: January 7, 2020Assignees: Howmedica Osteonics Corp., The University Of LiverpoolInventors: William O'Neill, Christopher J. Sutcliffe, Eric Jones, Robin Stamp
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Patent number: 9907183Abstract: This invention relates generally to uses of novel nanomaterial composition and the systems in which they are used, and more particularly to nanomaterial compositions generally comprising carbon and a metal, which composition can be exposed to pulsed emissions to react, activate, combine, or sinter the nanomaterial composition. The nanomaterial compositions can alternatively be utilized at ambient temperature or under other means to cause such reaction, activation, combination, or sintering to occur.Type: GrantFiled: October 5, 2016Date of Patent: February 27, 2018Assignee: NCC NANO, PLLCInventors: Kurt A. Schroder, Steve McCool, Denny Hamill, Dennis Wilson, Wayne Furlan, Kevin Walter, Darrin Willauer, Karl Martin
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Patent number: 9870862Abstract: A number of variations may include a method including providing a first powder comprising iron; compacting the first powder into a compacted powder product having a non-planar surface, wherein the compacting includes dynamic magnetic compaction or combustion driven compaction; and increasing the magnetic coercivity of at least one of the first powder or compact powder product.Type: GrantFiled: April 23, 2013Date of Patent: January 16, 2018Assignee: GM Global Technology Operations LLCInventors: Shekhar G. Wakade, Yucong Wang, Edward P. Becker
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Patent number: 8974719Abstract: A method of forming nano-structure composite materials that have a binder material and a nanostructure fiber material is described. A precursor material may be formed using a mixture of at least one metal powder and anchored nanostructure materials. The metal powder mixture may be (a) Ni powder and (b) NiAl powder. The anchored nanostructure materials may comprise (i) NiAl powder as a support material and (ii) carbon nanotubes attached to nanoparticles adjacent to a surface of the support material. The process of forming nano-structure composite materials typically involves sintering the mixture under vacuum in a die. When Ni and NiAl are used in the metal powder mixture Ni3Al may form as the binder material after sintering. The mixture is sintered until it consolidates to form the nano-structure composite material.Type: GrantFiled: February 12, 2010Date of Patent: March 10, 2015Assignee: Consolidated Nuclear Security, LLCInventors: Roland D. Seals, Paul A. Menchhofer, Jane Y. Howe, Wei Wang
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Patent number: 8955220Abstract: Methods of forming scroll compressor components are provided. The methods include forming at least one component of a scroll member from a powder metallurgy technique and joining the component with another distinct component via a sinter-brazing process. For example, a baseplate having a spiral scroll involute is joined to a hub via a joint interface having brazing material to form a braze joint with superior quality. At least one component is formed from a powder metal material including carbon and at least one species that reacts with or binds carbon to prevent migration during brazing of the sinter-brazing heat process. Optionally, during the powder metallurgy process, an alloy with a lower concentration of carbon is selected, which may be incorporated into a crystal structure with the species that prevents carbon migration.Type: GrantFiled: March 10, 2010Date of Patent: February 17, 2015Assignee: Emerson Climate Technologies, Inc.Inventors: Marc J. Scancarello, Roxana E. L. Ruxanda
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Publication number: 20150037197Abstract: An oxygen source-containing composite nanometal paste including at least composite nanometal particles, in which an organic coating layer is formed around a submicron or smaller silver core, and an oxygen source, which feeds oxygen contributing to pyrolysis at a pyrolysis temperature range in which the organic coating layer is pyrolyzed. The oxygen source comprises an oxygen-containing metal compound, and the oxygen content of the oxygen source is within a range of 0.01 mass % to 2 mass % per 100 mass % of the composite nanometal particles.Type: ApplicationFiled: February 20, 2013Publication date: February 5, 2015Inventor: Teruo Komatsu
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Publication number: 20150030494Abstract: Methods and apparatus for producing an object, the method comprising: performing an Additive Manufacturing process to produce an intermediate object from provided metal or alloy, whereby the intermediate object comprises regions having a contaminant concentration level above a threshold level; based upon one or more parameters, determining a temperature and a duration; and performing, on the intermediate object, a contaminant dispersion process by, for a duration that is greater than or equal to the determined duration, heating the intermediate object to a temperature that is greater than or equal to the determined temperature and less than the melting point of the metal or alloy, the contaminant dispersion process being performed so as to disperse, within the intermediate object, a contaminant from regions of high contaminant concentration to regions of low contaminant concentration until the intermediate object comprises no regions having a contaminant concentration level above the threshold level.Type: ApplicationFiled: February 20, 2013Publication date: January 29, 2015Inventor: Charles Malcolm WARD-CLOSE
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Publication number: 20140370323Abstract: A method for increasing the resolution when forming a three-dimensional article through successive fusion of parts of a powder bed, said method comprising providing a vacuum chamber, providing an electron gun, providing a first powder layer on a work table inside said vacuum chamber, directing an electron beam from said electron gun over said work table causing the powder layer to fuse in selected locations to form a first cross section of said three-dimensional article, providing a second powder layer on said work table, directing the electron beam over said work table causing said second powder layer to fuse in selected locations to form a second cross section of said three-dimensional article, reducing the pressure in the vacuum chamber from a first pressure level to a second pressure level between the providing of said first powder layer and said second powder layer.Type: ApplicationFiled: December 4, 2012Publication date: December 18, 2014Applicant: ARCAM ABInventor: Ulf Ackelid
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Patent number: 8802004Abstract: The invention relates to components which are produced or processed by powder metallurgy, and to processes for producing components of this type. The components produced by powder metallurgy are intended both to have porous regions and to provide fluid-tight properties, and it should also be possible to produce them at correspondingly low cost and suitably flexibly. For this purpose, a component of this type has at least one porous region, which is formed from an intermetallic phase or solid solutions. However, it may also have a corresponding surface coating. Moreover, in a component of this type there is at least one areal fluid-tight region which is formed from a meta or metal alloy of the corresponding intermetallic phase or solid solution.Type: GrantFiled: December 5, 2007Date of Patent: August 12, 2014Assignees: Alantum Corporation, Fraunhofer Gesellschaft zur Forderung der Angewandten Forschung E.V.Inventors: Dirk Naumann, Thomas Weissgarber, Alexander Bohm
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Patent number: 8636947Abstract: The present invention provides an improved metal separator for a fuel cell and a method for preparing same. More particularly, the invention provides a metal separator for a fuel cell, whereby the separator has a surface structure that imparts reduced contact resistance, improved corrosion resistance, and stable electrical conductivity. The invention further provides a surface treatment method for making the metal separator of the invention. The inventive method comprises sintering Fe—Cr—B—V-based powder on the surface of a metal foam to form an alloy layer; and forming a nitride layer of a (Cr—V—B)N-based material while supplying nitrogen gas on the surface of the alloy layer.Type: GrantFiled: November 22, 2010Date of Patent: January 28, 2014Assignee: Hyundai Motor CompanyInventors: Young Min Nam, Yoo Chang Yang, Suk Min Baeck, Seung Gyun Ahn
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Patent number: 8568117Abstract: Scrolls made from one or more near-net shaped powder metal processes either wholly or fabricated together from sections. Both “conventional” press and sinter methods and metal injection molding methods will be described.Type: GrantFiled: November 5, 2010Date of Patent: October 29, 2013Assignee: Emerson Climate Technologies, Inc.Inventor: Marc J. Scancarello
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Patent number: 8361381Abstract: A process for making a diffusion hardened medical implant having a porous surface is disclosed. The medical implant is made by a hot isostatic pressing process which simultaneously forms that porous surface and the diffusion hardened surface.Type: GrantFiled: July 21, 2009Date of Patent: January 29, 2013Assignee: Smith & Nephew, Inc.Inventors: Daniel A. Heuer, Vivek Pawar, Marcus Lee Scott, Shilesh C. Jani
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Patent number: 8309839Abstract: A method of improving the thermoelectric figure of merit (ZT) of a high-efficiency thermoelectric material is disclosed. The method includes the addition of fullerene (C60) clusters between the crystal grains of the material. It has been found that the lattice thermal conductivity (?L) of a thermoelectric material decreases with increasing fullerene concentration, due to enhanced phonon-large defect scattering. The resulting power factor (S2/?) decrease of the material is offset by the lattice thermal conductivity reduction, leading to enhanced ZT values at temperatures of between 350 degrees K and 700 degrees K.Type: GrantFiled: April 30, 2004Date of Patent: November 13, 2012Assignees: GM Global Technology Operations LLC, Shanghai Institute of Ceramics, Chinese Academy of SciencesInventors: Lidong Chen, Xun Shi, Jihui Yang, Gregory P. Meisner
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Publication number: 20120258008Abstract: The present invention relates to a method for controlling the carbon and/or oxygen content in a material by forming a feedstock composition comprising at least one powder, at least one platinum group metal and at least one binder; and forming the material by powder injection molding; wherein at least a proportion of the carbon and/or oxygen is catalytically removed by the at least one platinum group metal.Type: ApplicationFiled: October 13, 2010Publication date: October 11, 2012Applicant: JOHNSON MATTHEY PUBLIC LIMITED COMPANYInventor: Hugh Gavin Charles Hamilton
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Patent number: 8273291Abstract: A controlled combustion synthesis apparatus comprises an ignition system, a pressure sensor for detecting internal pressure, a nitrogen supply, a gas pressure control valve for feeding nitrogen and exhausting reaction gas, means for detecting the internal temperature of the reaction container, a water cooled jacket, and a cooling plate. A temperature control system controls the temperature of the reaction container by controlling the flow of cooling water supplied to the jacket and the cooling plate in response to the detected temperature. By combustion synthesizing, while controlling the internal pressure and temperature, the apparatus can synthesize a silicon alloy including 30-70 wt. % silicon, 10-45 wt. % nitrogen, 1-40 wt. % aluminum, and 1-40 wt % oxygen.Type: GrantFiled: March 19, 2009Date of Patent: September 25, 2012Assignee: Sumikin Bussan CorporationInventors: Toshiyuki Watanabe, Masafumi Matsushita, Toshitaka Sakurai, Kazuya Sato, Yoko Matsushita
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Publication number: 20110318216Abstract: Disclosed herein is a method and gas atmosphere for a metal component in a continuous furnace. In one embodiment, the method and gas atmosphere comprises the use of an effective amount, or about 1 to about 10 percent volume of endo-gas, into an atmosphere comprising nitrogen and hydrogen. In another embodiment, there is provided a method sintering metal components in a furnace at a one or more operating temperatures comprising: providing a furnace comprising a belt comprising a wire mesh material wherein the metal components are supported thereupon; and sintering the components in the furnace in an atmosphere comprising nitrogen, hydrogen, and effective amount of endothermic gas at the one or more operating temperatures ranging from about 1800° F. to about 2200° F. wherein the amount of endothermic gas in the atmosphere is such that it is oxidizing to the wire mesh material and reducing to the metal components.Type: ApplicationFiled: December 13, 2010Publication date: December 29, 2011Applicant: AIR PRODUCTS AND CHEMICALS, INC.Inventors: Donald James Bowe, Anna K. Wehr-Aukland, John Lewis Green
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Publication number: 20110176952Abstract: The aim of the invention is to devise a binder that is an alternative to prior art binders for producing sintered molded articles. Said aim is achieved by a binder comprising a first substance that has a first melting point and a first vapor pressure at 80° C. and a second substance that has a second melting point and a second vapor pressure at 80° C., the maximum melting point of the first and second substance amounting to about 150° C., and the minimum vapor pressure of the first and second substance amounting to about 5 torr (667 Pa) at 80° C.Type: ApplicationFiled: February 14, 2011Publication date: July 21, 2011Applicant: GKN SINTER METALS HOLDING GMBHInventors: Vladislav Kruzhanov, Lars Wimbert, Nicola De Cristofaro
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Publication number: 20110020164Abstract: The process for producing, processing, sintering, pressing or extruding thermoelectric materials with heat treatment under inert gas or under reduced pressure at temperatures in the range from 100 to 900° C. comprises producing, processing, sintering, pressing or extruding in the presence of oxygen scavengers which form thermodynamically stable oxides in the presence of free oxygen under the production, processing, sintering, pressing or extrusion conditions and hence keep free oxygen away from the thermoelectric material.Type: ApplicationFiled: July 26, 2010Publication date: January 27, 2011Applicant: BASF SEInventors: Madalina Andreea STEFAN, Frank Haass
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Patent number: 7845918Abstract: Scrolls made from one or more near-net shaped powder metal processes either wholly or fabricated together from sections. Both “conventional” press and sinter methods and metal injection molding methods will be described.Type: GrantFiled: February 28, 2006Date of Patent: December 7, 2010Assignee: Emerson Climate Technologies, Inc.Inventor: Marc J Scancarello
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Patent number: 7820097Abstract: This invention relates generally to uses of novel nanomaterial composition and the systems in which they are used, and more particularly to nanomaterial compositions generally comprising carbon and a metal, which composition can be exposed to pulsed emissions to react, activate, combine, or sinter the nanomaterial composition. The nanomaterial compositions can alternatively be utilized at ambient temperature or under other means to cause such reaction, activation, combination, or sintering to occur.Type: GrantFiled: November 23, 2005Date of Patent: October 26, 2010Assignee: NCC Nano, LLCInventors: Kurt A. Schroder, Steve McCool, Denny Hamill, Dennis Wilson, Wayne Furlan, Kevin Walter, Darrin Willauer, Karl Martin
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Patent number: 7718116Abstract: A method for obtaining a selectively non-carburized powdered metal part. The steps include compacting, sintering, removing, forging and cooling. A metal powder is compacted to form a preform having at least one first surface in which a forged part is required to have a case depth and at least one second surface in which a carburized portion is required to be removed prior to forging. The preform is then sintered and carburized. After carburizing the at least one second surface of the preform is removed and subsequently forged and cooled. The forged part has at least one second surface having improved post forging properties and at least one first surface having improved performance features. A part made from the present method is also provided.Type: GrantFiled: March 24, 2006Date of Patent: May 18, 2010Assignee: GKN Sinter Metals, Inc.Inventor: Timothy E. Geiman
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Patent number: 7635078Abstract: This invention relates to a method of brazing while the thickness of the opening between materials being brazed can not be maintained constant or can not be adjusted in the appropriate range. In order to solve this issue the porous material of metals or metal alloys consisting of Ni, Cu, Ti, Al, Ag or W should be utilized. The metallic porous material is inserted into the brazing opening mentioned above by using the softness of it, and is made to hold the brazing solder and to reinforce the bonding part after brazing.Type: GrantFiled: February 6, 2006Date of Patent: December 22, 2009Assignee: Kanto Yakin Kogyo Kabushiki KaishaInventors: Tadashi Ariga, Kiichi Kanda
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Patent number: 7615185Abstract: After an alloy powder including W, Cr, at least one of Ti, Zr, and Hf, and at least one of V, Nb, and Ta is produced, the alloy powder, a powdery carbon material, and a catalyst are heat-treated in the presence of a nitrogen gas. The alloy powder is carbonitrided into a multicomponent ceramics powder, and sintered into a sintered body. Alternatively, a powder of a first substance including at least two of Ti, Al, V, Nb, Zr, Hf, Mo, Ta, Cr, and W is molded into a molded body. Then, the surface of the molded body is surrounded by a second substance including a metal element which is not contained in the powder of the first substance, and the molded body is heat-treated in an atmosphere in which N is present. A porous sintered body thus produced is crushed into a multicomponent ceramics powder.Type: GrantFiled: December 12, 2007Date of Patent: November 10, 2009Assignee: Honda Giken Kogyo Kabushiki KaishaInventor: Mitsuo Kuwabara
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Patent number: 7601403Abstract: A method for preparing highly dense functional oxides with crystallite size in the range of 10-20 nm. Using a high pressure modification of a the Spark Plasma Sintering (SPS) technique, rapid thermal cycles (<10 min) coupled with very rapid pressure increase up to 1 GPa can be obtained allowing high degree of compaction and very limited grain growth. This combination of techniques was employed to produce the finest-grained ceramics ever prepared in bulk form in the case of fully stabilized zirconia and Sm-doped Ceria.Type: GrantFiled: April 15, 2005Date of Patent: October 13, 2009Assignee: The Regents of the University of CaliforniaInventors: Umberto Anselmi-Tamburini, Zuhair A. Munir, Javier E. Garay
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Patent number: 7524475Abstract: A cerium oxide powder for one-component CMP slurry, which has a specific surface area of 5 m2/g or more, and a ratio of volume fraction of pores with a diameter of 3 nm or more to that of pores with a diameter less than 3 nm of 8:2˜2:8, is disclosed. A method for preparing the same, a one-component CMP slurry comprising the same as an abrasive material, and a method of shallow trench isolation using the one-component CMP slurry are also disclosed. The CMP slurry causes no precipitation of the cerium oxide powder even if it is provided as a one-component CMP slurry, because the CMP slurry uses, as an abrasive material, cerium oxide powder that is obtained via a low-temperature calcination step, optionally a pulverization step, and a high-temperature calcination step and has a high pore fraction and low strength.Type: GrantFiled: September 1, 2006Date of Patent: April 28, 2009Assignee: LG Chem, Ltd.Inventors: Seung Beom Cho, Jun Seok Nho, Dong Mok Shin, Jong Pil Kim, Myoung Hwan Oh, Jang Yul Kim, Eun Mi Choi, Min Jin Ko
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Patent number: 7470393Abstract: Methods of fabricating cermet materials and methods of utilizing the same such as in filtering particulate and gaseous pollutants from internal combustion engines having intermetallic and ceramic phases. The cermet material may be made from a transition metal aluminide phase and an alumina phase. The mixture may be pressed to form a green compact body and then heated in a nitrogen-containing atmosphere so as to melt aluminum particles and form the cermet. Filler materials may be added to increase the porosity or tailor the catalytic properties of the cermet material. Additionally, the cermet material may be reinforced with fibers or screens. The cermet material may also be formed so as to pass an electrical current therethrough to heat the material during use.Type: GrantFiled: February 25, 2005Date of Patent: December 30, 2008Assignee: Battelle Energy Alliance, LLCInventor: Peter C. Kong
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Publication number: 20080170656Abstract: A method includes fabricating an energy detector using a sol-gel process.Type: ApplicationFiled: January 16, 2007Publication date: July 17, 2008Inventor: Haochuan Jiang
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Patent number: 7378053Abstract: The invention proposes a copper-based material with low thermal expansion and high thermal conductivity having good machinability and adaptability to nickel plating and also proposes a method for producing the same. The copper-based material is prepared through the steps of: adding 5 to 60% of iron-based alloy power having a certain value in thermal expansion coefficient into a matrix powder of pure copper phase powder and/or a precipitation hardening copper alloy powder; mixing the powders together; compacting the obtained powder mixture into a green compact and sintering it at temperatures of 400 to 600° C.Type: GrantFiled: April 27, 2004Date of Patent: May 27, 2008Assignee: Hitachi Powered Metals Co., Ltd.Inventor: Zenzo Ishijima
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Patent number: 7374717Abstract: The present invention provides a method for efficiently producing an intermetallic compound porous material. Specifically, the invention provides a porous material production method comprising molding a mixed powder of at least two inorganic powders and performing a combustion synthesis reaction of the resulting molded mixed powder; wherein (1) the porous material contains an intermetallic compound, (2) the intermetallic compound has a three-dimensional network skeletal structure, and (3) the porous material has a relative density of not more than about 80%.Type: GrantFiled: March 21, 2005Date of Patent: May 20, 2008Assignees: Osu CorporationInventor: Osamu Yamada
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Publication number: 20080075622Abstract: A composition for forming a green body is provided. The composition for forming the green body contains powder constituted of a metallic material and a binder containing a first resin which is decomposable by ozone and a second resin which is also decomposable by ozone but decomposed later than the first resin. The green body formed of the composition is used in producing a brown body, wherein the brown body is produced by first exposing the green body to a high ozone content atmosphere to decompose the first resin and remove the decomposed first resin and then decompose the second resin and remove the decomposed second resin, and then at least once exposing the thus obtained green body to a low ozone content atmosphere whose ozone concentration is lower than an ozone concentration of the high ozone content atmosphere.Type: ApplicationFiled: September 21, 2007Publication date: March 27, 2008Inventors: Masaaki Sakata, Junichi Hayashi
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Publication number: 20080075620Abstract: A method for producing a sintered body is provided. The method for producing the sintered body comprising: forming a green body by molding a composition for forming a green body into a specified shape to obtain the green body, the composition comprising powder constituted of a metallic material and a binder containing a first resin which is decomposable by ozone; first debinding the green body by exposing the green body to a high ozone content atmosphere to decompose the first resin and remove the decomposed first resin form the green body to obtain a brown body; exposing the thus obtained brown body at least once to a low ozone content atmosphere whose ozone concentration is lower than an ozone concentration of the high ozone content atmosphere to obtain an intermediate brown body; and sintering the intermediate brown body which has been exposed to the low ozone content atmosphere to obtain the sintered body.Type: ApplicationFiled: September 21, 2007Publication date: March 27, 2008Inventors: Masaaki Sakata, Junichi Hayashi
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Patent number: 7273581Abstract: The present invention relates to an improved process for in-situ preparation of alumina-(Ti,Zr) borides composite. The present invention particularly relates to fast and in-situ process for synthesis and consolidation of Al2O3—Zr/Ti B2 composites of approximate-95% density with controlled grain-growth in the range of less than or the order of 5 micrometer or less grain size using a dynamic Self propagating high temperature synthesis (SHS) process.Type: GrantFiled: September 7, 2004Date of Patent: September 25, 2007Assignee: Council of Scientific and Industrial ResearchInventors: Suman Kumari Mishra, Vladimir Andreevich Shcherbakov
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Patent number: 7112302Abstract: The manufacturing methods according to the present teachings provide shape memory alloy products having both a uniform composition and a precise shape memory recovery temperature. In this manufacturing method, raw material powders (e.g., Ti and Ni powders) may be precisely mixed. Next, a compound may be synthesized from the raw material powder mixture using a combustion synthesis method. The combustion synthesized compound may be melted and cast into a desired shape (e.g., a shape of the final product or a shape close to that of the final product).Type: GrantFiled: May 20, 2004Date of Patent: September 26, 2006Assignees: Yoshimi Inc., MIE TLO Co., Ltd.Inventors: Yoshiharu Yoshimi, Yasushi Okumura, Masataka Tokuda
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Patent number: 7086151Abstract: Scrolls made from one or more near-net shaped powder metal processes either wholly or fabricated together from sections. Both “conventional” press and sinter methods and metal injection molding methods will be described.Type: GrantFiled: January 20, 2004Date of Patent: August 8, 2006Assignee: Copeland CorporationInventor: Marc J Scancarello
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Patent number: 7052526Abstract: A magnesium base composite material is provided such that compound particles generated by a solid-phase reaction with magnesium are uniformly dispersed in a magnesium alloy body. The compound particles dispersed in the body comprise magnesium silicide (Mg2Si) and magnesium oxide (MgO) so that the magnesium base composite material may have excellent strength, hardness and abrasion resistance and tempered opponent aggression.Type: GrantFiled: February 14, 2003Date of Patent: May 30, 2006Assignee: Toudai TLO, Ltd.Inventor: Katsuyoshi Kondoh
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Patent number: 7048808Abstract: The present invention provides a rare-earth sintered magnet exhibiting desirable magnetic properties in which the amount of Nd and/or Pr forming a non-magnetic phase in a grain boundary phase is reduced. Specifically, the present invention provides a rare-earth sintered magnet having a composition of (R1x+R2y)T100-x-y-zQz where R1 is at least one element selected from the group consisting of all rare-earth elements excluding La (lanthanum), Y (yttrium) and Sc (scandium); R2 is at least one element selected from the group consisting of La, Y and Sc; T is at least one element selected from the group consisting of all transition elements; Q is at least one element selected from the group consisting of B and C, and including, as a main phase, a crystal grain of an Nd2Fe14B crystalline structure, wherein: molar fractions x, y and z satisfy 8?x?18 at %, 0.1?y?3.Type: GrantFiled: October 1, 2001Date of Patent: May 23, 2006Assignee: Neomax Co., Ltd.Inventors: Yuji Kaneko, Katsuya Taniguchi, Takao Sekino
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Patent number: 6926777Abstract: The invention relates to a method for producing rod-shaped permanent magnets according to which pressed parts (2) are produced that are then assembled to a rod-shaped green product. Said green product is subsequently sintered, whereby a rod-shaped single-piece permanent magnet (1) is produced.Type: GrantFiled: December 19, 2000Date of Patent: August 9, 2005Assignee: Vacuumschmelze GmbH & Co. KGInventors: Georg Werner Reppel, Volker Zellmann