Vacuum Patents (Class 419/60)
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Patent number: 5733427Abstract: A sputtering target formed of a refractory metallic silicide having a composition MSi.sub.x including a mixture composition of an MSi.sub.2 phase in the form of particles (M: at least one refractory metal selected from a group consisting of W, Mo, Ti, Zr, Hf, Ni and Ta), and an Si phase provided as a matrix phase. Interface layers having a predetermined thickness are formed at the interfaces between the MSi.sub.2 phase and the Si phase. The value X in the composition formula MSi.sub.x is set to a range of 2.0 to 4.0, and the thickness of the interface layers formed between the MSi.sub.2 phase and the Si phase, the dispersion of the composition, the density ratio of the target, the electrical resistivity of the Si phase and the surface roughness are set to predetermined values. An uniform high-quality thin film in which a composition distribution is uniform can be manufactured stably by using this target.Type: GrantFiled: March 30, 1995Date of Patent: March 31, 1998Assignee: Kabushiki Kaisha ToshibaInventors: Michio Satou, Takashi Yamanobe, Mitsuo Kawai, Tatsuzo Kawaguchi, Kazuhiko Mitsuhashi, Toshiaki Mizutani
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Patent number: 5722037Abstract: There is provided a process for producing titanium composite, comprising the steps of: molding titanium powder, titanium alloy powder, or powder comprising titanium into a certain shape by a cold isostatic press or cold press; reacting the shape with hydrocarbon gas at its decomposition temperature or higher, to form TiC therein; and providing the shape with high density by vacuum sintering, hot isostatic pressing, hot forging, hot rolling and/or the combinations thereof. TiC a reinforcing material, is in-situ formed by reacting a cold-pressed body of the powder with hydrocarbon gas and cleaner than the externally added one and distributed more uniformly and finely in the Ti matrix, leading to a significant improvement in wear resistance and high temperature property.Type: GrantFiled: May 9, 1996Date of Patent: February 24, 1998Assignee: Korea Institute of Machinery & MaterialsInventors: Hyung-Sik Chung, Yong-Jin Kim, Byung-Kee Kim, Jian-Qing Jiang
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Patent number: 5714700Abstract: This invention provides a self-lubricating composite material which has excellent strength and oxidation resistnce at a high temperature and can be used in air and in vacuum, and a production method thereof, the composite material is a Cu--Ni--Sn type composite sintered body containing 20 to 70 vol % of mixed particles of graphite and WS.sub.2 as the solid lubricant components and having a porosity of not greater than 25 vol %, and a matrix is a two-phase alloy comprising Cu--Ni alloy particles and an Sn single phase or an Sn--Ni intermetallic compound dispersed uniformly in the grain boundary of the alloy particles and firmly bonding them, and this matrix encompasses the solid lubricant particles. The matrix consists of 5 to 40 wt % of Ni, 4 to 15 wt % of Sn and the balance of Cu and unavoidable impurities as the alloy composition.Type: GrantFiled: December 18, 1996Date of Patent: February 3, 1998Assignee: Nippon Steel CorporationInventors: Tokuhiko Nishida, Shoichi Sekiguchi, Toru Ono, Yuko Tsuya
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Patent number: 5666636Abstract: The present invention provides a process for preparing titanium nitride sintered masses having no residual pores and consisting of TiN solid solution particles and Ni solid solution matrix, in which a granulated powder of the following composition:TiN-pMo.sub.2 C-qC-rNi-sMeCwherein:p is 5 to 20 wt %;q is 0 to 1.5 wt %;r is 15 to 30 wt %;s is 0 to 5 wt %;MeC is one or more carbides selected from VC, WC, TaC and NbC;with the proviso that q and s are not 0 wt % simultaneously;is compacted and sintered. The process according to the present invention can provide sintered TiN cermets of high density and a small grain size.Type: GrantFiled: March 22, 1996Date of Patent: September 9, 1997Assignee: Korea Institute of Science and TechnologyInventors: Jong Ku Park, Sung Tae Park
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Patent number: 5649279Abstract: There is disclosed a new process for binder phase enrichment. The process combines binder phase enrichment by dissolution of cubic phase with the requirements that cause formation of stratified layers, resulting in a unique structure. The new structure is characterized by, in comparison with the ones previously known, deeper stratified layers and less maximum binder phase enrichment. The possibility of combining dissolution of the cubic phase with formation of stratified layers offers new possibilities to optimize the properties of tungsten carbide based cemented carbides for cutting tools.The new process offers possibilities to combine the two types of gradients. The dissolution of cubic phase moves the zone with maximum mount of stratified binder phase from the surface to a zone close to and below the dissolution front.Type: GrantFiled: November 17, 1994Date of Patent: July 15, 1997Assignee: Sandvik ABInventors: Per Gustafson, Leif Akesson, Ake Ostlund
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Patent number: 5640666Abstract: A method of producing a composite powder by providing particles of (I) tungsten, niobium, zirconium, titanium or mixtures thereof, (II) silicon and (III) carbon in a proportion relative to each other so as to possess an overall chemical composition in that segment of the ternary diagram of FIGS. 2(a), 2(b), 2(c) and 2(d) designated A, and subjecting the particles to a mechanical alloying process under conditions and for a time sufficient to produce the composite powder. Also disclosed is a method of forming a substantially oxygen-free composition of matter comprising a matrix substance of WSi.sub.2, NbSi.sub.2, ZrSi.sub.2, TiSi.sub.2 or alloys thereof having SiC dispersed therein, the method comprising consolidating the above-described composite powder. Also disclosed is a method of forming oxidation- and wear-resistant coatings by subjecting the composite powder whose composition lies in segment A to a metallurgical process such as plasma spraying.Type: GrantFiled: October 2, 1995Date of Patent: June 17, 1997Assignee: University of FloridaInventors: S. Jayashankar, Michael J. Kaufman
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Patent number: 5637816Abstract: A metal matrix composite comprising an iron aluminide binder phase and a ceramic particulate phase such as titanium diboride, zirconium diboride, titanium carbide and tungsten carbide is made by heating a mixture of iron aluminide powder and particulates of one of the ceramics such as titanium diboride, zirconium diboride, titanium carbide and tungsten carbide in a alumina crucible at about 1450.degree. C. for about 15 minutes in an evacuated furnace and cooling the mixture to room temperature. The ceramic particulates comprise greater than 40 volume percent to about 99 volume percent of the metal matrix composite.Type: GrantFiled: August 22, 1995Date of Patent: June 10, 1997Assignee: Lockheed Martin Energy Systems, Inc.Inventor: Joachim H. Schneibel
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Patent number: 5623725Abstract: Process for producing very pure platinum materials dispersion-reinforced with Y.sub.2 O.sub.3 and having high strength and extensibility, even in the temperature range >800.degree. C., from platinum powder by mechanical alloying, which comprises the process stepspreparing platinum powder of high purity and low particle size of from 2 to 10 .mu.m,introducing and dispersing Y.sub.2 O.sub.3 particles >1 .mu.m in the platinum powder by milling in a platinum vessel using milling media of zirconium oxide,degassing the milled product under a vacuum of better than 10.sup.-3 mbar and with an increase in temperature to at least 1200.degree. C. in a platinum capsule for a period of up to 48 hours,gastight welding of the evacuated capsule and hot isostatic pressing at 1350.degree. C.Type: GrantFiled: May 16, 1995Date of Patent: April 22, 1997Assignee: Schott GlaswerkeInventors: Joachim Disam, Gerhard Jangg, Johannes Zbiral, Gerhard Schreier, Christian Edtmaier
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Patent number: 5607780Abstract: Disclosed are a target material for magneto-optical recording medium having a structure formed by sintering of an RE-TM phase (A) having a composition with an RE content higher than that of the composition of an intermetallic compound represented by the chemical formula TM.sub.2 RE, and a TM-RE phase (B) having a composition with an RE content equal to or lower than that of the composition of an intermetallic compound represented by the chemical formula TM.sub.2 E, wherein RE denotes at least one rare earth element selected from the group of elements consisting of Nd, Gd, Tb, Dy, Ho and Er, and TM denotes at least one element selected from the group of metals of the iron group which consists of Fe, Co and Ni; and a process for producing the same.Type: GrantFiled: May 20, 1994Date of Patent: March 4, 1997Assignee: Hitachi Metals, Ltd.Inventors: Kaoru Masuda, Takashi Meguro
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Patent number: 5580516Abstract: A powder of tantalum, niobium, or an alloy thereof, having an oxygen content less than about 300 ppm, and the production thereof without exposure to a temperature greater than about 0.7 T.sub.H. A powder metallurgy formed product of tantalum, niobium, or an alloy thereof, having an oxygen content less than about 300 ppm, and the production thereof without exposure to a temperature greater than about 0.7 T.sub.H.Type: GrantFiled: June 7, 1995Date of Patent: December 3, 1996Assignee: Cabot CorporationInventor: Prabhat Kumar
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Patent number: 5574954Abstract: A composite, a sintered product of the composite, and a process for producing products from this composite. The composite has a very high volummetric proportion of TiC, and its remainder of a matrix. The TiC constitutes at least 70% by volume and as much as 95% by volume of the ultimate product. The process includes making a green body which can be handled and is thereafter pre-sintered to form a pre-form. The pre-form is oversized relative to the ultimate product. It is sintered and machined, again oversize. Then it is again sintered and subjected to hot isostatic compression, to assume at least a close approximation to the pre-determined dimension of the product. It is characterized by its light weight, resistance to erosion, and resistance to chemical attack.Type: GrantFiled: June 4, 1992Date of Patent: November 12, 1996Assignee: Alloy Technology International, Inc.Inventor: Jayanti M. Panchal
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Patent number: 5552109Abstract: This invention relates to a process of forming a sintered article of powder metal comprising blending graphite and lubricant with a pre-alloyed iron based powder, pressing said blended mixture to shape in a single compaction stage sintering said article, and then high temperature sintering said article in a reducing atmosphere to produce a sintered article having a density greater than 7.4 g/cc.Type: GrantFiled: June 29, 1995Date of Patent: September 3, 1996Inventors: Rohith Shivanath, Peter Jones, Danny T. D. Thieu
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Patent number: 5523170Abstract: An article with a high temperature superalloy body having a directionally oriented microsuucture and a structural discontinuity, such as a crack, or surface erosion or wear portion, is repaired, to provide a repaired article, using a mixture of Ni base ahoy powders. One powder includes a careful balance of the temperature depressants Si and B. In the one powder, Si is included in the range of about 0.05-2.2 wt. % to provide about 0.02-1.3 wt. % Si in a repaired portion as bonded with the article. In that same powder, B is include in the range of about 0.2-1.2 wt. % to provide about 0.08-0.7 wt. % in that repaired portion. In the repair method, the repaired portion can be provided, when shorter brazing times are used, with improved mechanical properties by diffusing the brazed alloy and aging the repaired structure in the range of about 1600.degree.-1700.degree. F. for a time in the range of about 1-16 hours.Type: GrantFiled: December 28, 1994Date of Patent: June 4, 1996Assignee: General Electric CompanyInventors: David E. Budinger, Jim D. Reeves, Robert A. Anderson
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Patent number: 5516483Abstract: A process of forming a sintered article for powder metal comprising blending carbon and ferro alloys and lubricant with compressible elemental iron powder, pressing said blended mixture to form sintering said article, and then high temperature sintering said article in a reducing atmosphere to produce a sintered article having a high density from a single compression.Type: GrantFiled: February 8, 1994Date of Patent: May 14, 1996Assignee: Stackpole LimitedInventors: Rohith Shivanath, Peter Jones, Danny T. D. Thieu
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Patent number: 5512236Abstract: A process of coining sintered articles of powder metal comprising: blending carbon, ferro manganese, and lubricant with compressible elemental iron powder, pressing the blended mixture to form the articles, high temperature sintering of the articles in a reducing atmosphere and then coining the sintered articles to final shape so as to narrow the tolerance variability of coined articles and substantially eliminate secondary operations.Type: GrantFiled: August 25, 1994Date of Patent: April 30, 1996Assignee: Stackpole LimitedInventors: Peter Jones, Roger Lawcock
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Patent number: 5508000Abstract: According to the present invention, silicide grains are coupled with each other in a linked manner so as to provide a metal silicide phase, and grains forming a Si phase are dispersed in the gaps of the metal silicide phase discontinuously so as to provide a mixed structure of a sputtering target of high density and containing carbon at a rate less than 100 ppm. Because of the high density and high strength of the target, generation of particles at the time of sputtering can be reduced, and because of the reduced content of carbon, mixing of carbon in a thin film formed by the sputtering can be prevented.Type: GrantFiled: November 21, 1994Date of Patent: April 16, 1996Assignee: Kabushiki Kaisha ToshibaInventors: Michio Satou, Takasi Yamanobe, Mituo Kawai, Tooru Komatu, Hiromi Shizu, Noriaki Yagi
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Patent number: 5470527Abstract: A sputtering target that consists essentially of a continuous matrix of Ti-W phase, Ti phase having a particle diameter of 50 .mu.m or less distributed in the matrix, and a W phase having a particle diameter of 20 .mu.m or less also distributed in the matrix. Preferably the target contains aluminum in the range of 1 ppm or less. The target has high density and a low impurity content, which reduces the generation of particles from the target when it is used for sputtering. A method of manufacturing the sputtering target is also disclosed.Type: GrantFiled: September 12, 1994Date of Patent: November 28, 1995Assignee: Kabushiki Kaisha ToshibaInventors: Takashi Yamanobe, Michio Satou, Takashi Ishigami, Minoru Obata, Mituo Kawai, Noriaki Yagi, Toshihiro Maki, Shigeru Ando
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Patent number: 5456878Abstract: In a producing process of a sintered porous anode body of valve-metal for a solid-state electrolytic capacitor, molded pieces of the powder of valve-metal is sintered at a high temperature and at a lowered pressure in an atmosphere of an inert gas supplied at a fixed flow rate. Thanks to the usage of the inert gas, partial pressures of impurity elements can be suppressed and a gas emitted from the molded pieces in the sintering process can be washed out. Consequently, there is obtained a solid-state electrolytic capacitor in which the lead wire of the anode body is not easily bent down and which has a reduced leakage current and an increased withstand voltage.Type: GrantFiled: December 2, 1991Date of Patent: October 10, 1995Assignee: NEC CorporationInventors: Hirokazu Tadokoro, Arihiro Goto
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Patent number: 5455001Abstract: A method for manufacturing an intermetallic compound comprises (a) preparing a powder, (b) canning said powder in a tube, (c) executing a first heat treatment to said tube-canned powder, and (d) treating said tube-canned powder for obtaining an intermetallic compound. This invention offers a simple, efficient, and inexpensive method for producing an intermetallic compound possessing excellent mechanical properties.Type: GrantFiled: July 7, 1994Date of Patent: October 3, 1995Assignee: National Science CouncilInventor: Chen-Ti Hu
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Patent number: 5445789Abstract: A plunger charged as an electrode is received in a trough charged as a counter-electrode in order to heat material in the trough above the annealing temperature of metal material or the sintering temperature of ceramic-material. The trough and plunger are situated in a vacuum chamber separated from a condenser and pump stand by a valve. The plunger can be retracted into a cover of the chamber by a hydraulic drive on the cover. The cover, drive, and plunger are removable from the lower part of the chamber as a unit.Type: GrantFiled: March 16, 1994Date of Patent: August 29, 1995Assignee: Leybold Durferrit GmbHInventors: Erwin Wanetzky, Franz Hugo
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Patent number: 5441695Abstract: The invention relates to a process for the manufacture by sintering of a titanium part, characterized in that is consists of:(a) mixing a titanium hydride powder with a temporary binding agent,(b) injecting the mixture obtained into a mold to obtain a part in the desired shape,(c) removing the binding agent,(d) heating the part in a hydrogen atmosphere up to the desired sintering temperature,(e) replacing the hydrogen atmosphere by a vacuum or a non-reactive atmosphere once the sintering temperature has been reached, and(f) cooling the part in a non-reactive gas atmosphere.Type: GrantFiled: July 22, 1994Date of Patent: August 15, 1995Assignee: Asulab S.A.Inventor: Thomas Gladden
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Patent number: 5441694Abstract: In a method for preparing a high .alpha.-type silicon nitride powder by adding to and mixing with metallic silicon powder a copper catalyst and nitriding the mixture in a non-oxidizing gas atmosphere containing nitrogen or ammonia at 1,000.degree. to 1,500.degree. C., the amount of copper catalyst is limited to from 0.05 % to less than 0.5 % by weight of copper based on the weight of the metallic silicon. There is obtained silicon nitride powder of high purity at low cost and high efficiency since the copper catalyst can be efficiently removed from the silicon nitride powder through conventional acid treatment.Type: GrantFiled: June 10, 1994Date of Patent: August 15, 1995Assignee: Shin-Etsu Chemical Co., Ltd.Inventors: Masanori Fukuhira, Hirofumi Fukuoka, Yoshiharu Konya, Masaki Watanabe
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Patent number: 5437834Abstract: A porous living body repairing member obtained by compression-molding a metal fiber material into a desired shape, sintering the fiber mesh body or thereafter, and imparting a compressive stress of not more than 4.00 to 40.0 MPa to provide a porous living body repairing member having a compressive elasticity of not more than 2000 MPa and a permanent deformation of not more than 1% under a stress below a compressive yield stress.The compressive yield stress becomes approximately equal to the above compressive stress, and almost complete elasticity of a permanent deformation rate of not more than 0.1% is shown with respect to a compressive stress below this compressive yield stress. Accordingly, even when the porous living body repairing member is used at a high compressive load site such as man's lumbar body, permanent deformation hardly occurs.Type: GrantFiled: October 7, 1993Date of Patent: August 1, 1995Assignee: Kyocera CorporationInventors: Hideaki Okimatsu, Yasunori Tamura
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Patent number: 5429793Abstract: A process for producing metal oxide dispersion-strengthened anodes for use in fuel cells in which a metal alloy powder comprising at least one metal powder and at least one metal oxide forming phase is formed into a "green" cohesive structure. The "green" cohesive structure is heated in a sintering furnace resulting in simultaneous sintering and internal oxidizing of the oxide forming phase within the "green" cohesive structure, forming an oxide dispersion-strengthened structure. To promote simultaneous sintering of the "green" cohesive structure and internal oxidation of the oxide forming phase within the "green" cohesive structure, an oxidizing agent is disposed within the "green" cohesive structure or is applied to the exterior of the cohesive structure.Type: GrantFiled: May 17, 1994Date of Patent: July 4, 1995Assignee: Institute of Gas TechnologyInventors: Estela T. Ong, Nellie Burton-Gorman
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Patent number: 5418071Abstract: In the present invention, metal silicide grains form an interlinked structure of a metal silicide phase, and Si grains which form a Si phase are discontinuously dispersed between the metal silicide phase to provide a sputtering target having a high density two-phased structure and having an aluminum content of 1 ppm or less. Because of the high density and high strength of the target, the generation of particles from the target during sputtering is reduced, and due to the reduced carbon content of the target, the mixing of carbon into the thin film during sputtering can be prevented.Type: GrantFiled: February 4, 1993Date of Patent: May 23, 1995Assignee: Kabushiki Kaisha ToshibaInventors: Michio Satou, Takashi Yamanobe, Takashi Ishigami, Mituo Kawai, Noriaki Yagi, Toshihiro Maki, Minoru Obata, Shigeru Ando
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Patent number: 5409518Abstract: A sintered titanium alloy is composed of a titanium matrix or titanium alloy matrix and hard particles dispersed in the matrix, the sintered titanium alloy comprises: 4-8 mass % of aluminum (Al); 2-6 mass % of vanadium (V); 0.15-0.8 mass % of oxygen (O); at least one element selected from the group consisting of 0.2-9 mass % of boron (B), 0.5-3 mass % of at least one of molybdenum (Mo), tungsten (W), tantalum (Ta), zirconium (Zr), niobium (Nb), and hafnium (Hf), 0.05-2 mass % of at least one of Ia Group elements, IIa Group elements, and IIIa Group elements, 0.05-0.5 mass % of at least one of halogens; with the balance being titanium (Ti) and inevitable impurities.Type: GrantFiled: November 8, 1991Date of Patent: April 25, 1995Assignee: Kabushiki Kaisha Toyota Chuo KenkyushoInventors: Takashi Saito, Tadahiko Furuta
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Patent number: 5403542Abstract: Method of manufacturing a sintered carbonitride alloy comprising wet milling powders of forming binder phase containing Co, Ni and mixture thereof and powder forming hard constituents of nitrides and carbonitrides with Ti as the main component to a mixture with desired composition; compacting said mixture to form compact; heating the compact at 100-300 C. in oxygen or air and subjecting said compact in multiple heating steps to effect sintering.Type: GrantFiled: February 10, 1994Date of Patent: April 4, 1995Assignee: Sandvik ABInventors: Gerold Weinl, Rolf G. Oskarsson, Per Gustafsson
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Patent number: 5403374Abstract: A watch exterior part is formed of cemented carbide or stellite alloy, and has a three-dimensionally curved as-sintered surface or a small hole with an as-sintered interior peripheral surface, or has a three-dimensionally curved polished surface obtained by polishing an as-sintered surface. The watch exterior part is manufactured by a method in which organic binder is milled into a material powder, and a molded body obtained by injection molding is subjected to a binder removing process and then sintered. By the manufacturing method, a watch exterior part formed of cemented carbide or stellite alloy has a high strength and a complicated configuration such as a three-dimensional curved surface and a small hole, without applying secondary machining operations such as discharge operations.Type: GrantFiled: May 28, 1992Date of Patent: April 4, 1995Assignees: Sumitomo Electric Industries, Ltd., Namiki Precision Jewel Co., Ltd.Inventors: Nobuyuki Kitagawa, Toshio Nomura, Yoichi Yaguchi, Hidehiro Uchiumi, Naoko Iwashimizu
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Patent number: 5387272Abstract: The present invention provides an Al-Si based sintered alloy of high strength and high ductility, a method for production thereof and use thereof. The alloy comprises 1-45% of Si, 0.1-20% of an element of Group IIIa, 0.01-5% of at least one element of Groups IVa and Va, the balance of substantially Al. This alloy can further contain at least one of 0.01-5% of Cu, 0.01-5% of Mg, 2.0% or less of Fe, 1.5% or less of Mn and 1.5% or less of Co and the oxygen content is reduced to 0.15% or less by sintering under vacuum. The present invention is applied to automobile parts such as a piston and scroll compressors. The alloy has a tensile strength of about 40 kg/mm.sup.2 or higher and an elongation of 1.5% or more at 150.degree. C.Type: GrantFiled: April 8, 1992Date of Patent: February 7, 1995Assignees: Hitachi, Ltd., Hitachi Powdered Metals Company, LimitedInventors: Yasuo Kamitsuma, Yusaku Nakagawa, Mitsuo Chigasaki, Tadashi Iizuka, Kooichi Inaba, Keiichi Nakamura, Masaki Minabe, Tsuyoshi Kagaya
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Patent number: 5342573Abstract: A method of producing a tungsten heavy alloy product according to a powder metallurgical procedure utilizing the injection molding technique which enables production of tungsten heavy alloy products having high dimensional accuracy and complex configuration and yet having high physical strength and toughness in high productivity and at low cost. A powder mixture of tungsten powder and nickel powder, iron powder or copper powder is mixed with an organic binder and they are kneaded together. The kneaded mixture is injection molded into a predetermined shape, and thereafter the binder is removed from the molded product. Subsequently, the molded product is sintered in a temperature range of from the melting point of the bond phase of nickel, iron or copper to +50.degree. C. relative to the melting point.Type: GrantFiled: August 20, 1992Date of Patent: August 30, 1994Assignee: Sumitomo Electric Industries, Ltd.Inventors: Yoshinari Amano, Masahiro Omati, Junzo Matsumura
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Patent number: 5330704Abstract: Powder composed of particles of a rapidly solidified dispersion strengthened aluminum base alloy is compacted into billet form. The billet is vacuum autoclaved at a temperature ranging from 350.degree. C. to the alloy's incipient melting temperature and formed into a substantially fully dense wrought product. Gas content of the alloy is decreased and powder degassing steps are eliminated. The dispersion strengthened aluminum wrought product is produced in an economical and efficient manner.Type: GrantFiled: February 4, 1991Date of Patent: July 19, 1994Assignee: AlliedSignal Inc.Inventor: Paul S. Gilman
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Patent number: 5310520Abstract: Discrete powder particles of copper 14 and INVAR 12 are mixed together in a container 16 and packed into a powder metal article. This article is hot vacuum degassed and vacuum sealed and then heated to temperature well below the sintering temperature of copper or INVAR. Immediately after heating the article, it is subjected to a high pressure, high strain force such as extrusion through a die thereby yielding a fully dense, strong composite material 10 with excellent combined thermal expansion and conductivity properties.Type: GrantFiled: January 29, 1993Date of Patent: May 10, 1994Assignee: Texas Instruments IncorporatedInventors: Sunil C. Jha, James A. Forster, Henry F. Breit
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Patent number: 5277717Abstract: A rapidly solidified, low density aluminum base alloy consists essentially of the formula Al.sub.bal Li.sub.a Cu.sub.b Mg.sub.c Zr.sub.d wherein "a" ranges from about 2.2 to 2.5 wt %, "b" ranges from about 0.8 to 1.2 wt %, "c" ranges from about 0.4 to 0.6 wt % and "d" ranges from about 0.4 to 0.8 wt %, the balance being aluminum plus incidental impurities. The alloy is especially suited to be consolidated to produce a strong, tough, low density aircraft landing wheel.Type: GrantFiled: August 4, 1992Date of Patent: January 11, 1994Assignee: AlliedSignal Inc.Inventors: Jerry C. LaSalle, Santosh K. Das
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Patent number: 5275782Abstract: A housing for a semiconductor device is improved to avoid thermal distortions. The housing is formed of an Al-Si compound material and includes a housing member having a space for holding the semiconductor device. Occlusion gas contained in the Al-Si compound material is removed so that at least any nitrogen gas remaining in occlusion after degassing is 0.1 percent by weight or less. Since the housing member substantially does not contain occlusion gas, the housing is not subject to thermal distortion even though the housing is exposed to heat in operation.Type: GrantFiled: June 7, 1991Date of Patent: January 4, 1994Inventors: Mitsuo Osada, Yugaku Abe, Tetsuya Hayoshi
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Patent number: 5269830Abstract: A process for synthesizing intermetallic compounds from elemental powders. The elemental powders are initially combined in a ratio which approximates the stoichiometric composition of the intermetallic compound. The mixed powders are then formed into a compact which is heat treated at a controlled rate of heating such that an exothermic reaction between the elements is initiated. The heat treatment may be performed under controlled conditions ranging from a vacuum (pressureless sintering) to compression (hot pressing) to produce a desired densification of the intermetallic compound. In a preferred form of the invention, elemental powders of Fe and Al are combined to form aluminide compounds of Fe.sub.3 Al and FeAl.Type: GrantFiled: October 26, 1990Date of Patent: December 14, 1993Assignee: The United States of America as represented by the United States Department of EnergyInventors: Barry H. Rabin, Richard N. Wright
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Patent number: 5217541Abstract: A permanent magnet essentially consisting of in weight percent, 60% to 68% at least one transition element by weight, 30% to 38% at least one rare earth element by weight, 0.1% to 1.5% nitrogen by weight, and 0.8% to 1.5% boron by weight is disclosed. A method for producing the permanent magnet containing at least one rear element, at least one rare earth element, nitrogen and boron includes melting, cooling, milling, magnetizing, and compacting the transition element, the rare earth element and boron to form a green compact, and then sintering the green compact in nitrogen atmosphere having a constant partial pressure for 1 to several hours to form the permanent magnet.Type: GrantFiled: August 26, 1991Date of Patent: June 8, 1993Assignee: High End Metals Corp.Inventors: Tsung-Shune Chin, Shiang-Jiun Heh, Ken-Der Lin
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Patent number: 5207821Abstract: Disclosed is a sintered alloy composition and method of manufacturing the same, the sintered alloy composition having a multi-phase structure, comprising: a first phase composed of aluminum and copper; and a second phase being dispersed in the first phase and composed of molybdenum, chromium, silicon and cobalt. This alloy composition has excellent abrasion and corrosion resistance, preferably to be used for making machine parts such as valve seats for engines.Type: GrantFiled: July 9, 1991Date of Patent: May 4, 1993Assignees: Hitachi Powdered Metals Co., Ltd., Honda Giken Kogyo Kabushiki KaishaInventors: Yutaka Ikenoue, Keitaro Suzuki, Yoshimasa Aoki, Hideo Urata, Koji Koishikawa, Makoto Tsuji
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Patent number: 5174952Abstract: A process for the powder-metallurgical production of a workpiece by filling a binder-free and solvent-free, dry metal powder or ceramic powder into a mold, precompacting the powder by tapping and presintering it for 1/2 hour to 1 hour at 0.65 to 0.85 times the absolute melting temperature without significant shrinkage, adjacent powder particles being joined merely at their contact points by necking to give a skeletal formed body. The formed body is taken out of the mold and finish-sintered at at least 0.9 times the absolute melting temperature for at least 1 hour without additional support by a mold. Advantageously, the sintered body is additionally hot-isostatically pressed containerless in order to reach at least 98% of the theoretical density.Type: GrantFiled: September 6, 1990Date of Patent: December 29, 1992Assignee: Asea Brown Boveri Ltd.Inventors: Peter Jongenburger, Christoph Tonnes, Clemens Verpoort
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Patent number: 5156805Abstract: A ferritic alloy with a wear resistive oxide scale is obtained through the steps of pressing a ferritic alloy powder containing aluminum into a powder compact of a desired configuration, sintering the powder compact in a non-oxidizing atmosphere to provide a resulting sintered product, and heat-treating the sintered product in an oxidizing gas atmosphere in order to precipitate in the surface thereof alumina in the form of an alumina scale as the wear resistive oxide scale which is responsible for improved surface hardness or wear resistance. Due to the inherent porous nature of the sintered product, the oxidizing gas can readily penetrate deep into the surface of sintered product to facilitate the oxidization of the product surface into the alumina scale, in addition to that the oxidization depth can be controlled such as by the density of the product, which makes it possible to readily control the thickness of the alumina scale.Type: GrantFiled: July 25, 1991Date of Patent: October 20, 1992Assignee: Matsushita Electric Works, Ltd.Inventors: Junji Imai, Shuji Yamada, Tadashi Hamada, Hajime Kojima, Masao Tanahashi
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Patent number: 5152829Abstract: A rapidly solidified aluminum base alloy consists essentially of the formula Al.sub.bal Fe.sub.a Si.sub.b X.sub.c, wherein X is at least one element selected from the group consisting of W,Ta,Nb, "a" ranges from 3.0 to 7.1 at %, "b" ranges from 1.0 to 3.0 at %, "c" ranges from 0.25 to 1.25 at % and the balance is aluminum plus incidental impurities, with the provisos that the ratio [Fe+X]:Si ranges from about 2.33:1 to 3.33:1 and that the ratio Fe:X ranges from about 16:1 to 5:1. The alloy exhibits high strength, ductility and fracture toughness and is especially suited for use in high temperature structural applications such as gas turbine engines, missiles, airframes and landing wheels.Type: GrantFiled: June 3, 1991Date of Patent: October 6, 1992Assignee: Allied-Signal Inc.Inventors: David J. Skinner, Michael S. Zedalis
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Patent number: 5152828Abstract: The present invention relates to a method of producing a mold material used for obtaining a mold for casting metals such as Zn, Al and the like or molding resins. In the method, the short fibers having an aspect ratio of 30 to 300 and obtained by cutting ferritic stainless steel long fibers having a width of 100 .mu.m or less, ferritic stainless steel powder and at least one of Cu powder and Cu alloy powder are used as raw materials. The raw materials are blended to obtain a material mixture which is then compressed under pressure in a Cold Isostatic Press process. The thus obtained compressed product is sintered in a vacuum atmosphere. The sintered material is held in an atmosphere of nitrogen gas or decomposed ammonia gas so that 0.3 to 1.2 wt % of nitrogen is added to the stainless steel in the sintered material. The thus obtained mold material has a hardness of HMV 250 to 500.Type: GrantFiled: October 8, 1991Date of Patent: October 6, 1992Assignee: Sintokogio Ltd.Inventor: Tatsuhiko Katoh
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Patent number: 5151247Abstract: The present invention is a method for densifying powder metallurgical parts to 100% theoretical density. The method comprises applying a high pressure of 0.1-100 MPa during sintering in a high pressure furnace at a temperature before which the liquid phase is formed and maintaining this pressure during the rest of the sintering cycle until the furnace has cooled to almost room temperature. The method achieves rapid, complete closure of the porosity which results in parts with close dimensional tolerances and practically no warpage.Type: GrantFiled: November 1, 1991Date of Patent: September 29, 1992Assignee: Sandvik ABInventors: Bengt O. Haglund, Bengt N. During
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Patent number: 5149496Abstract: A magnesium based metal matrix composite is made from rapidly solidified magnesium alloy powder and SiC particulate using liquid suspension coprocessing or mechanical alloying. The composite is suitable for consolidation into bulk shapes having, in combination, high strength, high stiffness, low density, low coefficient of thermal expansion, and high hardness. The composite is suited for uses in such applications as space and missile guidance and navigation and control system precision components where low density, very high specific stiffness and long term dimensional and environmental stability are principal performance criteria.Type: GrantFiled: January 27, 1992Date of Patent: September 22, 1992Assignee: Allied-Signal Inc.Inventors: Santosh K. Das, Chin-Fong Chang, Derek Raybould
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Patent number: 5147601Abstract: A composition comprising a powder of iron and nickel and a binder (e.g. wax) is injection molded. The powder contains 0.5 to 10% by weight of nickel and has an average particle diameter not exceeding 45 microns. The binder is removed from the molded product. The molded product is sintered, and the sintered product is cooled to room temperature slowly at a rate of 2.degree. C. to 50.degree. C. per minute. The sintered product is of an iron-nickel alloy, has a high density and a high level of soft ferromagnetic properties, and may be complicated in shape.Type: GrantFiled: March 30, 1992Date of Patent: September 15, 1992Assignee: Sumitomo Metal Mining Co., Ltd.Inventors: Akihito Ohtsuka, Yoshio Kijima
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Patent number: 5145503Abstract: In a process for producing a high strength structural member by sintering a starting powder material, a powder mixture of a basic powder and an additional powder is used as the starting powder material. The basic powder is comprised of at least one of an amorphous single-phase alloy powder and at least one kind of a mixed-phase alloy powder which contains a crystalline phase and an amorphous phase and has a crystalline phase volume fraction C (Vf) less than 30%, and the additional powder is comprised of a mixed-phase alloy powder containing a crystalline phase and an amorphous phase and having a crystalline phase volume fraction C (Vf) of at least 30% to less than 80%. The relationship between the minimum volume fraction Pm (Vf) of the additional powder in the starting powder material and the crystalline phase volume fraction C (Vf) in the additional powder is established such that Pm (Vf)=-0.7 C (Vf)+61. This ensures that a structural member having a high strength and a high toughness can be produced.Type: GrantFiled: May 31, 1991Date of Patent: September 8, 1992Assignee: Honda Giken Kogyo Kabushiki KaishaInventor: Hiroyuki Horimura
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Patent number: 5122326Abstract: The present invention is a method of removing binder material which is non-sublimable at room temperature and pressures greater than 1 Torr from a binder and particulate mixture. The binder and particulate mixture is formed into a shaped article and placed in a closed furnace. The closed furnace is then adjusted to a pressure and temperature sufficient to effect transformation of the binder material from a solid to a vapor and diffusion of the binder material as a vapor through, and from, the binder and particulate mixture without formation of a liquid phase of binder material on the binder and particulate mixture surface. The shaped article is held under these processing conditions until substantially all of the binder material transforms to its vapor state and diffuses through, and from, the mixture into the closed furnace. The binder material vapor is then evacuated from the furnace through conventional means.Type: GrantFiled: March 2, 1987Date of Patent: June 16, 1992Assignee: Vacuum Industries Inc.Inventors: Martha L. Jackson, Elliot Thompson
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Patent number: 5098469Abstract: A powder metallurgy process for producing near-net shape, near-theoretical density structures of multiphase nickel, aluminum and/or titanium intermetallic alloys is provided by employing pressureless sintering techniques. The process consists of blending a brittle aluminide master alloy powder with ductile nickel powder, so as to achieve the desired composition. Then, after cold compaction of the powdered mixture, the compact is liquid phase sintered. The four step liquid phase sintering process is intended to ensure maximum degassing, eliminate surface nickel oxide, homogenize the alloy, and complete densification of the alloy by liquid phase sintering.Type: GrantFiled: September 12, 1991Date of Patent: March 24, 1992Assignee: General Motors CorporationInventor: Vadim Rezhets
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Patent number: 5098649Abstract: A rare earth metal-iron group metal target for a magneto-optical disk is produced by mixing power (a) produced by the rapid quenching treatment of an alloy composed of at least one rare earth metal and at least one iron group metal in a composition range which permits the formation of an eutectic structure, with powder (b) from at least one iron group metal in an amount necessary for meeting the composition requirements of the target; and subjecting the resulting mixture to pressure sintering in vacuum or in an inert gas atmosphere at a temperature lower than a liquid phase-appearing temperature of the mixture to produce a rare earth metal-iron group metal intermetallic bonding layer betwen the particles.Type: GrantFiled: June 26, 1990Date of Patent: March 24, 1992Assignee: Hitachi Metals, Ltd.Inventors: Shunichiro Matsumoto, Tsutomu Inui, Rokuo Ichiyasu, Yoshitaka Chiba
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Patent number: 5077002Abstract: Process for shaping any desired metallic and/or ceramic component, in which a dry powder is filled loosely into a ceramic mold, which elastically/plastically yields or cracks and breaks under the influence of shrinkage stresses during sintering, and is sintered. Variants for the mold: thin, resilient shells made of Al.sub.2 O.sub.3, SiO.sub.2 or MgO; special glass which cracks in a network-like manner; a mold having predetermined breaking points, ceramic shell disintegrating into fragments; flexible green ceramic sheeting; green ceramic composition with shrinkage during sintering.Type: GrantFiled: March 12, 1991Date of Patent: December 31, 1991Assignee: Asea Brown Boveri Ltd.Inventor: Reinhard Fried
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Patent number: RE34180Abstract: Cemented carbide substrates having substantially A or B type porosity and a binder enriched layer near its surface are described. A refractory oxide, nitride, boride, and/or carbide coating is deposited on the binder enriched surface of the substrate. Binder enrichment is achieved by incorporating Group IVB or VB transition elements. These elements can be added as the metal, the metal hydride, nitride or carbonitride.Type: GrantFiled: September 9, 1988Date of Patent: February 16, 1993Assignee: Kennametal Inc.Inventors: Bela J. Nemeth, deceased, George P. Grab